Means Recirculating Solvent Patents (Class 422/281)
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Patent number: 5690821Abstract: A loading platform and chemical addition system are described for a machine that prepares a batch of dialysate. The loading platform is in fluid communication with a dialysate preparation tank, and receives chemical vessels that contain a batch quantity of dialysate chemicals. The chemicals are released from the vessels automatically and fall onto a shelf in the loading platform. Nozzles and spray equipment are provided for insuring the complete release of the chemicals from the vessels and their dispersion into the tank. Novel mixing techniques are implemented in the tank to insure complete mixing of the dialysate solution and prevention of settling of dialysate solution at the bottom of the tank.Type: GrantFiled: November 17, 1995Date of Patent: November 25, 1997Assignee: AKSYS, Ltd.Inventors: Rodney S. Kenley, Dennis M. Treu, Frederick H. Peter, Jr., Thomas M. Feldsein, Kenneth E. Pawlak
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Patent number: 5678593Abstract: A detergent mixing apparatus for use with a pressurized water source. The apparatus includes at least one mixing tank and a pair of liquid chemical supply containers each accommodating a liquid chemical composition. A water supply conduit connects a pressurized water source with the mixing tank. A pair of venturi chambers are disposed within the water supply conduit and are arranged for parallel flow. Each of the venturi chambers includes a suction port in fluid communication, respectively, with one of the liquid chemical supply containers so as to drawing the liquid chemical composition from each chemical supply container as pressurized water passes through the venturi chambers thus entraining the liquid chemical compositions in the water. A float-actuated control valve is operably connected to the water supply conduit for terminating the flow of water and entrained liquid chemical compositions through the water supply conduit when the liquid level in the mixing tank reaches a predetermined height.Type: GrantFiled: January 24, 1996Date of Patent: October 21, 1997Inventor: Barton Lockhart
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Patent number: 5547645Abstract: An apparatus for dissolving an adjusting agent of a dialytic solution according to the invention includes a vessel containing sealingly a constant quantity of a powdery or granular solid adjusting agent of a dialytic solution, a feeding means for supplying a fluid for dissolving the adjusting agent in said vessel, and a dissolving tank for mixing and dissolving the adjusting agent with the fluid and for storing the mixed solution.Type: GrantFiled: July 24, 1991Date of Patent: August 20, 1996Assignee: Nikkiso Co., Ltd.Inventors: Tomomichi Ego, Hiroshi Kinoshita
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Patent number: 5536479Abstract: A solubilizing apparatus includes a fluid permeable sleeve having opposed openings therein wherein a spray nozzle is in flow communication with one opening and a second opening is disposed to receive solids. The spray nozzle is designed to spray a fluid in a swirling spray sweeping the insides of the sleeve wall as it travels toward the opposite end. The solubilizing apparatus is specifically useful for dissolution of chemicals utilized in cleaning reverse osmosis membranes.Type: GrantFiled: October 17, 1994Date of Patent: July 16, 1996Assignee: International Purification Systems, Inc.Inventors: Steven L. Miller, Kerry L. Embry
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Patent number: 5527515Abstract: 35% to 45% by weight concentrated aqueous solutions of ferric chloride, directly useful as flocculating agents in a variety of water treatments, are prepared by (a) reacting chlorine with an aqueous solution of ferrous chloride, in the presence of a recycled aqueous solution of ferric chloride; (b) decompressing the step (a) reaction product solution to vaporize water therefrom, thereby concentrating same; and (c) recycling a fraction of the decompressed liquid phase to step (a) and recovering remaining fraction as final product aqueous solution of ferric chloride.Type: GrantFiled: June 5, 1995Date of Patent: June 18, 1996Assignee: AtochemInventors: Rene Clair, Alain Gallet
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Patent number: 5472674Abstract: An apparatus for preparing a stock wash liquor includes a stock liquor container with a stock liquor container comprising a tub-shaped bottom section and a top section which is hermetically mounted on the bottom section and is fitted with an integral suction fan designed to generate an underpressure or partial vacuum in the bottom section. A suction line leads out of the container and into a container of powder. The aim of the invention is to further develop a device of this kind so that stock liquor can be prepared from cleaning agent powder taken directly from its container without producing any dust, and the stock liquor thus prepared stored for feeding to industrial washing or cleaning machines. This is achieved by locating a secondary suction line end inside the stock liquor container at a point which is remote from the point of entry of a primary suction line into the bottom section.Type: GrantFiled: March 25, 1994Date of Patent: December 5, 1995Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Friedel Rings, Peter Holz
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Patent number: 5439020Abstract: A fluid handling apparatus and method for combining dissolved solid and liquid phase detergent constituents with water from an external source in predetermined proportions is disclosed. The apparatus includes a dissolution tank for dissolving powdered detergent constituents deposited therein and a number of other supply containers each filled with a discrete liquid chemical. A manifold, connecting the dissolution tank and at least one liquid chemical supply container, is in fluid communication with a venturi chamber. When pressurized water from the external source is directed or jetted through the venturi chamber, detergent constituents in the dissolution tank and the chemical supply container are drawn into the venturi chamber in proper proportion for mixing with pressurized water and discharged into a holding tank for subsequent use.Type: GrantFiled: May 27, 1994Date of Patent: August 8, 1995Inventor: Barton Lockhart
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Patent number: 5401476Abstract: To continuously produce and separate high purity p-xylene from a C.sub.8 aromatic hydrocarbon charge, successive use is made in combination of (1) a stage of separating low-purity p-xylene (75 to 98%) by simulated moving bed adsorption chromatography, with a ratio of the solvent to charge flow rates of 1.2 to 2.5; (2) a stage of purifying and washing the low-purity p-xylene by recrystallization (-25 to +10.degree. C.); (3) a stage of catalytic isomerization of the charge which has been p-xylene-depleted by the separating stage (1); and recovering an isomerate which is then recycled to the charge. The solvent for desorption in stage (1) and washing in stage (2) is advantageously toluene.Type: GrantFiled: October 27, 1993Date of Patent: March 28, 1995Assignee: Institut Francais du PetroleInventors: Gerard Hotier, Claude Roux Guerraz, Than Nguyen Thanh
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Patent number: 5393502Abstract: A solubilizing apparatus includes a fluid permeable sleeve having opposed openings therein wherein a spray nozzle is in flow communication with one opening and a second opening is disposed to receive solids. The spray nozzle is designed to spray a fluid in a swirling spray sweeping the insides of the sleeve wall as it travels toward the opposite end. The solubilizing apparatus is specifically useful for dissolution of chemicals utilized in cleaning reverse osmosis membranes.Type: GrantFiled: September 7, 1993Date of Patent: February 28, 1995Assignee: International Purification Systems, Inc.Inventors: Steven L. Miller, Kerry L. Embry
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Patent number: 5377426Abstract: The generation of volatiles from liquid or solid materials is enhanced and accelerated by exposure to microwave radiation. Normally the energy transfer is effected preferentially toward the liquid or solid materials over the generated gaseous volatiles. Sufficient energy is provided at a selected rate that enhances the generation of volatiles to produce headspace samples. Alternatively, the rate can be selected so as to disrupt the equilibrium normally present between the liquid or solid phase and the gaseous phase and produce purge and trap samples; the latter process resulting from the selective energy transfer toward the liquid or solid phase over the gaseous phase. The rate of energy transfer can be chosen so as to bring the medium being subjected to microwave radiation to its supercritical state. The material having reached that state can further be used in numerous applications such as supercritical fluid extraction.Type: GrantFiled: February 2, 1993Date of Patent: January 3, 1995Assignee: Her Majesty the Queen in right of Canada, as represented by the Minister of the EnvironmentInventor: J. R. Jocelyn Pare
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Patent number: 5308592Abstract: Equipment for mixed phase reaction distillation, particularly equipment for mixed phase reaction distillation to produce MTBE. The equipment comprises a rectifying section I at the upper part, a reaction section II at the middle part, and a stripping section III at the lower part. The reaction section II comprises a plurality of superposed catalyst beds which are connected by at least one catalyst flow pipe disposed between each pair of adjacent catalyst beds, and a sealed cover at the top above the uppermost catalyst bed of the plurality of catalyst beds. The reaction section II further comprises at least one vapor passageway disposed at one side of the reaction section II, and at least one liquid passageway disposed at the other side of the reaction section II.Type: GrantFiled: July 14, 1992Date of Patent: May 3, 1994Assignee: China Petrochemical Corporation (SINOPEC)Inventors: Zongren Yang, Xingren Hao, Jinshan Wang
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Patent number: 5294408Abstract: A compact lime slaker has an inner vessel forming an initial slaking chamber disposed in an outer vessel forming a final slaking chamber, with agitators provided In both chambers. Slaked lime from the final slaking chamber is pumped to a collection trough where slaked lime and grit are removed therefrom, while a major portion of slaked lime, with grit removed is returned to the final slaking chamber. The slaked lime in the final slaking chamber, at an elevated temperature due to the slaking exotherm, insulates the lime being slaked in the initial slaking chamber and provides heat thereto to aid in the initial slaking. Removal of grit from the portion of slaked lime recycled to the final slaking chamber prevents clogging or attrition of components of the slaker.Type: GrantFiled: April 16, 1993Date of Patent: March 15, 1994Assignee: Dravo Lime CompanyInventors: Charles J. Muzik, Kenneth L. Yoest
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Patent number: 5225074Abstract: An automatic swimming pool chlorinator having a submersible canister for receiving and containing chlorine tablets or sticks.Type: GrantFiled: August 28, 1992Date of Patent: July 6, 1993Assignee: Philip L. LeslieInventor: Siamak Moini
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Patent number: 5209905Abstract: A wet-type exhaust gas desulfurization system comprises a reservoir for trapping an absorbing solution which has absorbed SO.sub.2 from exhaust gas; an absorbing solution circulating tank disposed directly under the reservoir; a plurality of bottom pipes which are installed at the bottom of reservoir and extend downward into the absorbing solution in the circulating tank and whose lower end is open, or drop pipes which depend into the absorbing solution and whose lower ends are open; and air supply pipe at least one end of which is open to the atmosphere; a pipe for discharging the air above the surface of absorbing solution onto the surface of solution in the reservoir; and a pipe for supplying the absorbing solution in the circulating tank to a spray nozzle at the upper part of the absorbing tower.Type: GrantFiled: December 5, 1991Date of Patent: May 11, 1993Assignee: Mitsubishi Jukogyo Kabushiki KaishaInventors: Masakazu Onizuka, Kenji Inoue, Naohiko Ukawa, Susumu Okino, Toru Takashina
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Patent number: 5205995Abstract: Sodium sesquisulfate produced in crystalline form in a high acidity methanol-based highly efficient chlorine dioxide generating process is converted by metathesis to crystalline anhydrous neutral sodium sulfate and the acid recovered as a result is recycled to the chlorine dioxide generating step. The metathesis is effected by contacting the crystalline sodium sesquisulfate with aqueous sodium chlorate solution, aqueous sodium chloride solution, aqueous methanol or water alone. The metathesis is effected in such manner as to minimize the additional evaporative load imposed on the chlorine dioxide generating process by the metathesis medium.Type: GrantFiled: March 2, 1992Date of Patent: April 27, 1993Assignee: Sterling Canada Inc.Inventors: Herbert C. Scribner, Maurice C. J. Fredette, Edward J. Bechberger
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Patent number: 5137694Abstract: A cleaning system and dispenser are disclosed which feature a reservoir for retaining a liquid detergent solution; a chamber for retaining a mass of solid, dissolvable detergent; a measurement device for measuring the concentration of detergent in the liquid detergent solution; and a flow control device for circulating the liquid detergent solution from the reservoir into contact with the solid detergent so as to dissolve a portion of the solid detergent and increase the concentration of detergent in the liquid detergent solution. The circulation of the liquid detergent solution is in response to a signal from the concentration measuring device that the concentration of detergent in the liquid detergent solution has fallen below a predetermined minimum. The dispenser also includes a measurement device for measuring the volume of solution in the reservoir and for adding fresh water to the reservoir when the volume of solution is below a predetermined minimum.Type: GrantFiled: November 30, 1988Date of Patent: August 11, 1992Assignee: Ecolab Inc.Inventors: James L. Copeland, Henry A. Snyder, Sherwood A. Bergseid, Thomas H. Indieke
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Patent number: 5082574Abstract: An apparatus for treating material with liquid has defined therein a cylindrical chamber, suspended above the bottom of which is a receptacle for holding the material to be tested, the bottom of which receptacle is permeable to the treatment liquid. Above the receptacle there is arranged a duct with inlets at its end and outlets disposed above the receptacle. In use, a magnetic stirrer drives a vortex of liquid up the side wall of the chamber and liquid from the vortex enters the duct from which liquid pours down onto the material to be treated in the receptacle and is then recycled. The apparatus includes one or more of the improvements that suspension of the receptacle and duct is by means which does not interfere with the vortex, that the area of the inlets is maximized by forming them with an arcuate profile, and that the bore in the duct is formed such that the wall above the bore is relatively thick and a suspending rod can be screwed thereinto.Type: GrantFiled: July 12, 1989Date of Patent: January 21, 1992Assignee: Trenchbond LimitedInventor: Alan Carrol
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Patent number: 5043280Abstract: A sterile product containing a substance embedded in a carrier is produced by use of a supercritical gas. In one embodiment, a mixture is formed of a substance, carrier and supercritical gas such as nitrous oxide or carbon dioxide, and the supercritical gas is separated from the substance and carrier to obtain the product. In another embodiment, the supercritical gas contains the substance, and is mixed with an atomized organic solvent containing the carrier to form a mixture. The supercritical gas extracts the solvent, and is separated from the substance and carrier to produce the product. Alternatively, the carrier can be in the supercritical gas and the substance in the solvent, or both the substance and carrier can be in the solvent. Atomization and formation of the mixture can be carried out by feeding the supercritical gas and solvent through a nozzle into a spray tower or column.Type: GrantFiled: December 21, 1988Date of Patent: August 27, 1991Assignee: Schwarz Pharma AGInventors: Wilfried Fischer, Bernd W. Muller
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Patent number: 4963329Abstract: Gas reacting apparatus and method are described for wet mass transfer of solute gases from a gas stream with a liquid or slurry reacting medium capable of chemisorption of solute gases in the gas stream. The apparatus comprises an elongated conduit defining a primary reaction zone in fluid-flow communication with a fan defining both a secondary reaction zone and a spray coalescence zone, and a plurality of dual-fluid spray nozzles coaxially spaced in series within the conduit and countercurrently or cocurrently directed to the gas stream for spraying the liquid or slurry reacting medium into said conduit to form a plurality of spray contact zones of uniformly-distributed fine droplets wherein intimate contact of high interfacial surface area between the sprayed liquid or slurry and the gas stream is effected to remove solute gases from the gas stream.Type: GrantFiled: September 13, 1988Date of Patent: October 16, 1990Assignee: Turbotak Inc.Inventors: J. Stuart Burgess, Donald R. Spink, Jerry Y. Stein
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Patent number: 4929348Abstract: The present invention relates generally to improvements in processes and apparatus for effecting solvent extractions using liquefied gas or gases in the supercritical state as the solvents and specifically to continuous processes for carrying out such extractions at high pressures. Further, the present invention relates to an apparatus which is a long vertical cylinder of relatively small diameter, wherein the solvent gas and the material to be extracted are continuously circulated through the long vertical reactor.Type: GrantFiled: March 6, 1989Date of Patent: May 29, 1990Assignee: Wayne K. RiceInventor: Wayne K. Rice
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Patent number: 4911897Abstract: An automated device for deconcentration and potentiation of homeopathic remedies, comprising a preparations flask held by a support fastened to a horizontal shaft driven in rotation. The mouth of the flask describes a circle and can be moved among several positions, particularly an original position for introduction of the dose to be diluted or rediluted and for introduction of the solvent, and a position for pouring the dilution into a wide-mouth bottle containing granules to be impregnated and put into rotation. Between each deconcentration, the flask is cleaned by washing means and drying means located on its path in other positions.Type: GrantFiled: December 7, 1988Date of Patent: March 27, 1990Assignee: Co ArtzInventor: Jean Alphonse
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Patent number: 4898673Abstract: Soluble materials are continuously extracted from solids using extracting solvents such as carbon dioxide by circulating a mixture of the solids in carbon dioxide at elevated pressure through a closed loop pipeline. A mixture of extracts dissolved in carbon dioxide is continuously removed from the system and material to be extracted is continually added. Multiple extraction stages are also disclosed.Type: GrantFiled: July 11, 1987Date of Patent: February 6, 1990Assignee: Vitamins, Inc.Inventors: Wayne K. Rice, Laxman Singh
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Patent number: 4885098Abstract: An elastic bar member is coupled to an orbiting mass oscillator and the entire assembly is suspended from a cable or the like such that the bar member has freedom of lateral motion and is nakedly immersed in a slurry having particulate material contained therein such as a mineral ore reject from which metal has been extracted. The rotor of the orbiting mass oscillator is driven at a speed such as to generate cycloidal sonic energy in the bar preferably at a frequency such as to set up resonant standing wave vibration of the bar in a cycloidal quadrature pattern. The cycloidal vibrational energy tends to set the surrounding fluid material into a whirling rotation or rotary traveling wave which facilitates the agglomeration or coagulation of the particles in the material and enhances the settling operation to make for more complete separation of the particles from the liquid.Type: GrantFiled: October 21, 1988Date of Patent: December 5, 1989Inventor: Albert G. Bodine
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Patent number: 4883532Abstract: An elastic bar member is clamped to an orbiting mass oscillator and the entire assembly is suspended from a cable or the like such that the bar member has freedom of lateral motion and is nakedly immersed in a leachant having a material contained therein such as a mineral ore from which metal is to be extracted. The rotor of the orbiting mass oscillator is driven at a speed such as to generate cycloidal sonic energy in the bar preferably at a frequency such as to set up resonant standing wave vibration of the bar in a cycloidal nutating pattern. The cycloidal vibrational energy tends to set the surrounding fluid material into a whirling rotation or rotary traveling wave which facilitates the mixing of the ore and leachant and enhances the leaching operation to make for more complete separation of the mineral from the ore.Type: GrantFiled: July 22, 1988Date of Patent: November 28, 1989Inventor: Albert G. Bodine
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Patent number: 4865817Abstract: Gas reacting apparatus and method are described for wet mass transfer of solute gases from a gas stream with a liquid or slurry reacting medium capable of chemisorption of solute gases in the gas stream. The apparatus comprises an elongated conduit means defining a primary reaction zone in fluid-flow communication with a fan means defining both a secondary reaction zone and a spray coalescence zone, and plurality of dual fluid spray means coaxially spaced in series within the conduit means and countercurrently or cocurrently directed to the gas stream for spraying the liquid or slurry reacting medium into said conduit means to form a plurality of spray contact zones of uniformly-distributed fine droplets wherein intimate contact of high interfacial surface area between the sprayed liquid or slurry and the gas stream is effected to remove solute gases from the gas stream.Type: GrantFiled: March 2, 1987Date of Patent: September 12, 1989Assignee: University of WaterlooInventors: J. Stuart Burgess, Donald R. Spink, Jerry Y. Stein
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Patent number: 4857279Abstract: Edible fats and oils are extracted from oil-bearing materials by loading the raw materials onto an inlet end of a flat and fixed conveying surface having elongate slits therein. The materials are conveyed from the inlet end to the outlet end of the conveying surface by scrapers moved by endless chains. Oil extracting solvent is sprayed onto the material on the conveying surface, to produce miscella, which flows through the slits in the surface and into hoppers beneath the surface. The miscella is circulated back to additional sprayers located upstream of the solvent sprayers for spraying the miscella onto the upstream end of the conveying surface. The resulting concentrated miscella is collected in hoppers beneath the surface and delivered to a further use.Type: GrantFiled: December 24, 1986Date of Patent: August 15, 1989Assignee: Showa Sangyo Co., Ltd.Inventors: Yoshio Kawamata, Kiyoshi Iwai
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Patent number: 4780138Abstract: An elastic bar member is clamped to an orbiting mass oscillator and the entire assembly is suspended from a cable or the like such that the bar member has freedom of lateral motion and is nakedly immersed in a leachant having a material contained therein such as a mineral ore from which metal is to be extracted. The rotor of the orbiting mass oscillator is driven at a speed such as to generate cycloidal sonic energy in the bar preferably at a frequency such as to set up resonant standing wave vibration of the bar in a cycloidal nutating pattern. The cycloidal vibrational energy tends to set the surrounding fluid material into a whirling rotation or rotary traveling wave which facilitates the mixing of the ore and leachant and enhances the leaching operation to make for more complete separation of the mineral from the ore.Type: GrantFiled: December 3, 1987Date of Patent: October 25, 1988Inventor: Albert G. Bodine
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Patent number: 4741806Abstract: Supercritical extraction of diatomaceous earth results in a much more significant improvement in hydrocarbon recovery over Fischer retorting than achievable with tar sands. Process and apparatus for supercritical extraction of diatomaceous earth are disclosed.Type: GrantFiled: March 21, 1984Date of Patent: May 3, 1988Assignee: Phillips Petroleum CompanyInventor: James Scinta
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Patent number: 4741807Abstract: In a reactor, granular feedstock having particle sizes in the range from about 0.5 to 15 mm is subjected in a moving bed to a countercurrent extraction at a temperature in the range from 20.degree. to 150.degree. C. and under a pressure in the range from 50 to 400 bars by a continuously supplied solvent which is in a liquid or supercritical state. A mixture of valuable substances and solvent is withdrawn from the upper portion of the reactor. The solvent is separated from the valuable substances by a pressure relief and/or temperature rise and is recycled to the reactor. The extraction residue is withdrawn from the lower end of the reactor. Respective locks are used to charge the feedstock into the reactor and to discharge the extraction residue from the reactor. Solvent and an entrainer are supplied to the reactor at different locations. Outlet ducts having a length of 0.1 to 1 m are preferably used to deliver the feedstock onto a moving bed in the reactor so that a free space is provided over the bed.Type: GrantFiled: September 15, 1986Date of Patent: May 3, 1988Assignee: Metallgesellschaft AktiengesellschaftInventors: Joachim Wilhelm, Rainer Reimert, Georg Penk
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Patent number: 4710360Abstract: Apparatus for endothermic dissolutions in water, including: a mixing tank 40, wherein solute is slurried with water; pump 59 and spray pipe 63, for spraying slurry into spray box 70; and fan 75 for drawing ambient air upwardly, in direct heat exchange relationship with descending slurry droplets. Dissolution is promoted, as the droplets extract heat from the countercurrent flow of air.Type: GrantFiled: June 11, 1986Date of Patent: December 1, 1987Assignee: Union Oil Company of CaliforniaInventors: Bruce Harbolt, Perry L. Murata, Neal C. Burmaster
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Patent number: 4664891Abstract: A system and process for preparation of dialysis concentrate solution from dry chemicals and water. The source of hemodialysis chemicals for a batch is a drum selectively filled with dry chemicals such that an inner core region therewithin is loaded with chemicals which slurry and dissolve the least readily. The required amount of water is metered into a mix tank. Water is pumped from the tank into a spray head fitted over the selectively filled drum. Water is injected onto the chemicals within the inner core region by the use of a nozzle having a narrow spray angle. The chemicals within the inner core region are preferentially dissolved or slurried before the other chemicals within the drum. The slurried and dissolved chemicals are removed from the drum by a suction wand and are entirely solubilized in the tank. Cycling of fluid continues from the drum to the tank and vice versa until all of the chemicals in the drum have been removed. Circulation of the fluid is continued until a uniform solution results.Type: GrantFiled: April 11, 1986Date of Patent: May 12, 1987Assignee: Renal Systems, Inc.Inventors: Louis C. Cosentino, Wayne I. Nelson
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Patent number: 4617177Abstract: A system for the solid/liquid extraction of in particular vegetable raw materials, such as oilseeds and oil-yielding plants, with low-boiling solvents, such as gasoline and the like, in continuous co-current manner.The equipment, which is also to be regarded as the actual extraction unit, is formed by the combination of a conveyor screw (1) having a screw flight pitch (3) which widens in the direction of the transport of material, and a screen-like or perforated bottom portion (4) provided at a short distance upstream of the discharge of the extracted material (6). The equipment is closed on all sides.Several individual sets of equipment of this type are combined in the installation and interconnected by a logical circulation system for the miscella in such a way that the extraction time is shortened, the extraction yield is improved and the residual solvent content in the fully extracted material (groats) is reduced.Type: GrantFiled: October 4, 1982Date of Patent: October 14, 1986Inventor: Heinz O. Schumacher
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Patent number: 4603115Abstract: There is described an automated process for the solvent separation of organic/inorganic substances that operates continuously and unattended and eliminates potential errors resulting from subjectivity and the aging of the sample during analysis. In the process, metered amounts of one or more solvents are passed sequentially through a filter containing the sample under the direction of a microprocessor control apparatus. The mixture in the filter is agitated by ultrasonic cavitation for a timed period and the filtrate is collected. The filtrate of each solvent extraction is collected individually and the residue on the filter element is collected to complete the extraction process.Type: GrantFiled: October 19, 1984Date of Patent: July 29, 1986Assignee: International Coal Refining CompanyInventor: Frank K. Schweighardt
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Patent number: 4588476Abstract: A process for replacing a solution obtained for instance by exposing oil shale particles to the action of a solvent under supercritical conditions, by a solvent is provided for. The solid/solution mixture is extracted in a multitude of cross flow extractions such as to gradually replace the solution e.g. a bitumen solution, by the solvent, e.g. toluene. An apparatus for carrying out this process is also disclosed.Type: GrantFiled: September 20, 1982Date of Patent: May 13, 1986Assignee: Phillips Petroleum CompanyInventor: F. Morgan Warzel
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Patent number: 4555385Abstract: An introduction process and apparatus is described concerning the continuous elution of a value, i.e. a metal value such as gold, from a particulate carrier by a counterflow of stripping liquid through the pressurized vessel in which the loaded particulate carrier is introduced to the vessel as a low velocity plug in a liquid carrier. The extraction process is also used with the continuous elution process in which the particulate material is extracted from the bottom part of a pressure vessel through a discharge pipe extending therefrom and in which a discharge liquid is introduced into the discharge pipe upstream of the discharge end under such pressure as to maintain a head of the discharge liquid upstream of that location and a flow of the liquid downstream from the location to transport the particulate material through the discharge pipe.Type: GrantFiled: August 19, 1983Date of Patent: November 26, 1985Assignee: Ok Tedi Mining LimitedInventor: Alan M. Stone
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Patent number: 4548228Abstract: A device for controlled feeding of a water-soluble chemical into a water line having a pressure varying between a minimum and a maximum in the line. Water flows from the water line into an air impervious chemical mixing tank through a first one-way check valve. When the pressure in the line is less than the air pressure in the tank, an air reservoir in the mixing tank forces the mixture of water and chemical back into the water line through a control valve which is set at a restricted flow value with respect to the first check valve. A second one-way check valve located in the water line between the one-way check valve and the control valve prevents the contents of the mixing tank fed through the control valve from backing up toward the first one-way check valve.Type: GrantFiled: September 30, 1983Date of Patent: October 22, 1985Inventors: Stephen D. Moore, Murrill Maglio
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Patent number: 4521400Abstract: Apparatus for agitating and circulating a liquid 20 comprising a vessel having two upright chambers 10, 12 and two vertically displaced ducts 14, 18 connecting the chambers 10, 12. In use of the apparatus, a steady flow of gas into the top of one chamber 10 provides both an oscillation and a circulation of the liquid 20 in the apparatus, as the gas is periodically vented through the upper duct 18.The apparatus has one application in the dissolution of material from nuclear fuel pins during reprocessing.Type: GrantFiled: September 27, 1982Date of Patent: June 4, 1985Assignee: United Kingdom Atomic Energy AuthorityInventors: Thomas D. Hodgson, William R. Foot
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Patent number: 4473532Abstract: Ore leaching structure including a base portion, a shelter portion, a transfer portion and a treatment portion; the base portion including a peripheral concrete foundation, concrete wall sections extending upwardly therefrom, a concrete floor section extending between the wall sections, the floor section including at least one drain opening adjacent one wall section, the floor section being sloped from the other of the wall sections toward the drain opening; the shelter portion including vertical sections extending upwardly from the wall sections, the vertical sections and the wall sections together forming the sidewalls of the structure, a roof section extending between and joining the upper edges of the sidewalls; the transfer portion including a first group of doorways in a sidewall adjoining the sidewall along which the drain opening is located, the doorways being spaced along the length of the sidewall, a second group of doorways along a sidewall opposite to the first group of doorways, the doorways of tType: GrantFiled: November 30, 1981Date of Patent: September 25, 1984Inventors: Shirley M. Rose, William R. Rector
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Patent number: 4416764Abstract: Method and apparatus for separating coarse sand particles from fine sand particles in a slurry of sand and a solution such as results from the solvent extraction of tar sand, such method comprising causing flow of such slurry in a generally horizontal direction and then causing upward flow at a rate such that coarse particles settle out and fine particles move upwardly to a slurry outlet. The apparatus preferably comprises a tubular duct for downward flow, bottom openings in the duct for outward flow, a lower receptacle for coarse particles and an annular space surrounding the duct for upward flow of slurry of solution and fine sand particles.Type: GrantFiled: November 28, 1980Date of Patent: November 22, 1983Assignee: Natomas Energy CompanyInventors: Benjamin J. Gikis, Abner Y. Jones, Rudolf Elbrecht
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Patent number: 4407322Abstract: A device for controlled feeding of a water-soluble chemical into a water line having a pressure varying between a minimum and a maximum in the line. Water flows from the water line into an air impervious chemical mixing tank through a first one-way check valve. When the pressure in the line is less than the air pressure in the tank, an air reservoir in the mixing tank forces the mixture of water and chemical back into the water line through a control valve which is set at a restricted flow value with respect to the first check valve. A second one-way check valve located in the water line between the one-way check valve and the control valve prevents the contents of the mixing tank fed through the control valve from backing up toward the first one-way check valve.Type: GrantFiled: December 2, 1980Date of Patent: October 4, 1983Inventors: Stephen D. Moore, Murrill Maglio
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Patent number: 4390506Abstract: The apparatus serves particularly for the continuous charging of extractors for oil-containing vegetable raw materials, wherein highly flammable, low-boiling solvents, such as benzene, hexane, heptane etc. are used as extractants or solvents for the glyceride constituents to be extracted. The apparatus, which is provided between the preparation (comminution) of the raw material and the extraction plant proper, comprises an equalizing vessel having a mixing zone and a double screw disposed at an inclination with respect to the horizontal wherein the spacing of the screw turns, in the area of the vessel, increases continuously in the direction towards the discharge outlet.The inclination of the screw is such that the space defined by the base of the screw and an imaginary line is constantly filled.Equalizing vessel, mixing zone and screw are interconnected to form a tightly sealed unit.Type: GrantFiled: October 22, 1981Date of Patent: June 28, 1983Inventor: Heinz O. Schumacher
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Patent number: 4375451Abstract: A device and method for measuring the antifouling coating leach rates on ps' hulls uses a spherical segment shaped shell that circulates water over a coated area. A pump connected in closed circuit with the shell assures proper flow rate. A second pump creates a partial vacuum and holds the shell on the coated surface. A combination of nozzles and outlet fittings assures that the coating is exposed to a circulating flow of water. A portion of the circulated water is passed through a cupric ion electrode sensor which provides signals representative of the dissolved copper in water over time and, hence, the leach rate of the coating.Type: GrantFiled: August 13, 1981Date of Patent: March 1, 1983Assignee: The United States of America as represented by the Secretary of the NavyInventors: Peter F. Seligman, John W. Neumeister
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Patent number: 4329319Abstract: An apparatus for extracting pulverous or granular material from a mixture means of a solvent brought into contact with the mixtue. A receptacle is provided for receiving the material to be extracted as well as the solvent. A conduit system is connected with the lower portion of the receptacle and empties into the upper portion of the receptacle. Within the conduit system is arranged a device for conveying the solvent to be withdrawn from the receptacle as well as the mixture containing the material to be extracted. The device also serves to mechanically form a dispersion of the material to be extracted in the solvent. The device includes a rotatable body operated at a speed of 10,000 to 30,000 rpm.Type: GrantFiled: May 27, 1980Date of Patent: May 11, 1982Assignee: Kernforschungsanlage Julich Gesellschaft mit beschrankter HaftungInventors: Hans-Gunter Sittardt, Matthias Radke
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Patent number: 4313912Abstract: A cylindrical housing encloses a plurality of vertically stacked extractor sections each containing a plurality of baskets in vertical registry with baskets of the other sections, with the baskets all being stationary so that material to be processed passes in a vertical path down through each successive extractor section. Rotating screens and miscella collection pans are disposed beneath the baskets in each extractor section and form the bottom thereof, with the screens and pans having aligned openings which during rotation permit the material being processed to be passed from an upper basket to a lower basket in vertical registry therewith. A countercurrent flow miscella and solvent distribution and collection system supplies miscella or fresh solvent to the upper portion of each of the extractor sections above the baskets and rotates with the screen and collection pan to progressively apply the proper strength of miscella or solvent to each of the baskets in each of the extractor sections.Type: GrantFiled: October 8, 1980Date of Patent: February 2, 1982Assignee: The French Oil Mill Machinery CompanyInventor: William M. Barger
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Patent number: 4311561Abstract: A method and apparatus for extracting bitumen from tar sand utilizes a plurality of individually sealed pressure adjusted interconnected extraction chambers in which the tar sand flows countercurrent to the flow of solvent with mixing in each extraction chamber of solvent and tar sand. Tar sand is provided to the first of the extraction chambers and after removal of a portion of the bitumen is carried by a conveyor and disposed into the next chamber where further bitumen is extracted and so on through the plurality of chambers until all the bitumen is extracted and the sand and remaining solvent then conveyed into a last chamber where the sand and solvent is treated with hot water to remove solvent and pure sand is discharged.Type: GrantFiled: April 2, 1980Date of Patent: January 19, 1982Assignee: Tarco IncorporatedInventor: Larry W. Hastings
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Patent number: 4307064Abstract: A continuous solvent extracting apparatus with a generally cylindrical stationary housing containing a plurality of stationary bottomless baskets disposed laterally adjacent one another in a circular pattern in a single stage with a screen forming the bottom of the baskets. The screen is mounted for rotation beneath the baskets with a single opening through which material being processed can be emptied from each of the baskets in sequence after the miscella has been removed from the material being treated by drainage through the screen. The miscella is collected in a pan which also rotates with the screen and includes a hopper in registry with the opening in the screen through which the processed material can pass from each of the baskets to a discharge opening from the extracting apparatus.Type: GrantFiled: October 9, 1980Date of Patent: December 22, 1981Assignee: The French Oil Mill Machinery CompanyInventors: William M. Barger, Raymond L. Upchurch
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Patent number: 4299798Abstract: In an apparatus including a column through which the liquid and the divided solids to be treated thereby circulate in counter-current, the treated solids which tend to collect at one of the column being conveyed hydraulically by a fraction of the liquid introduced into the column towards separating means from which the said fraction is re-cycled into the column, the circuit of the liquid intended to circulate through the column and the circuit of the liquid intended to convey the treated solids are wholly separated from each other, the first one comprising a first inlet nozzle directed towards the other end of the column and the second one a second inlet nozzle directed towards the inlet of the conduit through which the treated solids are hydraulically conveyed, this second nozzle being located between the first one and the adjacent end of the column. In the case of solids heavier than the treating liquid, both inlet nozzles are disposed axially in a chamber provided at the lower end of the column.Type: GrantFiled: January 16, 1980Date of Patent: November 10, 1981Assignee: Commissariat a l'Energie AtomiqueInventors: Pierre Faugeras, Pierre Fremeaux, Edouard Henry, Roger Malaterre, Pierre Ros
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Patent number: 4290998Abstract: Washing apparatus for the washing of by-product salts from chlorine dioxide generating processes comprising a multi-stage decantation washer.Type: GrantFiled: December 17, 1979Date of Patent: September 22, 1981Assignee: Erco Industries LimitedInventors: Peter D. Dick, Gerald Cowley
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Patent number: 4255386Abstract: The apparatus of the present invention includes a quartz flask for containing 71% nitric acid and the organic matrix to be destroyed, a Soxhlet extractor disposed above the flask, and a Friedrich coldfinger reflux condenser disposed above the extractor. A Meeker or Fisher burner is employed to provide heat to the flask and distill the acid, and the vapors are condensed within the condenser and transmitted to the extractor. An adjustable volume displacement cylinder is disposed within the extractor so as to control siphoning of the acid condensate from the extractor back into the flask. The distillation-condensation-siphoning procedure of the present invention is automatically operative once the displacement cylinder is adjusted. The organic matrix is completely destroyed so as to produce a clear, colorless acid solution within which the trace inorganic salts are disposed. The acid solution may be subsequently qualitatively and quantitatively analyzed in accordance with known techniques.Type: GrantFiled: November 30, 1978Date of Patent: March 10, 1981Assignee: The United States of America as represented by the Deptartment of Health, Education and WelfareInventors: Myron M. Schachter, Kenneth W. Boyer
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Patent number: RE31913Abstract: A cylindrical housing encloses a plurality of vertically stacked extractor sections each containing a plurality of baskets in vertical registry with baskets of the other sections, with the baskets all being stationary so that material to be processed passes in a vertical path down through each successive extractor section. Rotating screens and miscella collection pans are disposed beneath the baskets in each extractor section and form the bottom thereof, with the screens and pans having aligned openings which during rotation permit the material being processed to be passed from an upper basket to a lower basket in vertical registry therewith. A countercurrent flow miscella and solvent distribution and collection system supplies miscella or fresh solvent to the upper portion of each of the extractor sections above the baskets and rotates with the screen and collection pan to progressively apply the proper strength of miscella or solvent to each of the baskets in each of the extractor sections.Type: GrantFiled: January 30, 1984Date of Patent: June 11, 1985Assignee: The French Oil Mill Machinery CompanyInventor: William M. Barger