Subjecting Mixture To Pressure, Vacuum, Or Steam Patents (Class 423/203)
  • Patent number: 9440872
    Abstract: A method is provided for treating brine recovered from a coal seam gas operation. The process entails directing brine recovered from a coal seam gas operation to a mixed reactor and mixing an alkaline earth reagent with the brine. This results in the precipitation of alkaline earth salts and silica, which form alkaline earth salt crystals having silica adsorbed thereto. Thereafter, the alkaline earth salt crystals and adsorbed silica are directed to an evaporator that produces a concentrate having the alkaline earth salt crystals and adsorbed silica.
    Type: Grant
    Filed: March 14, 2013
    Date of Patent: September 13, 2016
    Assignee: Veolia Water Technologies, Inc.
    Inventors: David E. Gamache, Timothy J. Rittof
  • Patent number: 8936710
    Abstract: The disclosure provides low-molecular-ratio cryolite for aluminum electrolytic industry, which consists of potassium cryolite and sodium cryolite with a mole ratio of 1:1˜1:3, wherein the molecular formula of the potassium cryolite is mKF.AlF3 and the molecular formula of the sodium cryolite is nNaF.AlF3, where m=1˜1.5 and n=1˜1.5. When the low-molecular-ratio cryolite provided by the disclosure is applied to the aluminum electrolytic industry, electrolytic temperature and power consumption can be reduced and electrolytic efficiency is improved.
    Type: Grant
    Filed: January 22, 2014
    Date of Patent: January 20, 2015
    Assignee: Shenzhen Sunxing Light Alloys Materials Co., Ltd.
    Inventors: Xuemin Chen, Jun Yang, Zhihong Li, Weiping Wu
  • Patent number: 8679318
    Abstract: The disclosure provides an electrolyte supplement system in an aluminum electrolysis process, which includes low-molecular-ratio cryolite, wherein the low-molecular-ratio cryolite is selected from mKF.AlF3, nNaF.AlF3 or mixture thereof, where m=1˜1.5 and n=1˜1.5. When the electrolyte supplement system provided by the disclosure is applied to the aluminum electrolytic industry, electrolytic temperature can be reduced obviously in the aluminum electrolysis process without changing the existing electrolytic process; thus, power consumption is reduced, volatilization loss of fluoride is reduced and the comprehensive cost of production is reduced.
    Type: Grant
    Filed: December 9, 2012
    Date of Patent: March 25, 2014
    Assignee: Shenzhen Sunxing Light Alloys Materials Co., Ltd.
    Inventors: Xuemin Chen, Jun Yang, Zhihong Li, Weiping Wu
  • Patent number: 7981388
    Abstract: The present invention relates to lithium secondary batteries comprising a negative electrode, a positive electrode, a separator and a lithium-based electrolyte carried in an aprotic solvent, and to the electrolyte compositions, and to methods for purifying battery active materials. The electrolyte comprises at least one solvent and a lithium salt of the formula: Li2B12FxH12-x-yZy where x+y is from 3 to 12, and x and y are independently from 0 to 12, and Z comprises at least one of Cl and Br.
    Type: Grant
    Filed: February 23, 2007
    Date of Patent: July 19, 2011
    Assignee: Air Products and Chemicals, Inc.
    Inventors: Sergei Vladimirovich Ivanov, William Jack Casteel, Jr., Wade H. Bailey, III
  • Publication number: 20100239477
    Abstract: A sodium sulfite liquor is formed by reacting sodium carbonate with sulfur dioxide. A CO2 byproduct may be removed from the formed liquor by injecting a stripping gas (e.g., steam and/or air) into the liquor, either into a transfer pipe or into a tank that is vented; by increasing the liquor temperature; and/or by reducing the liquor pressure. The decarbonated sodium sulfite liquor with a reduced carbon dioxide content is introduced into a crystallizer connected to a circulation loop comprising a heater and/or a filter. Additional decarbonation by heating, stripping and/or depressurization of the liquor may be carried out in a circulation loop connected to the crystallizer. The condensing side of the heater may be vented. The flow rate of the circulation loop and/or heater temperature differences may be monitored. Additional CO2 may be vented from a holding tank to maintain circulation loop flows and heater temperature differences.
    Type: Application
    Filed: November 12, 2008
    Publication date: September 23, 2010
    Applicant: Solvay Chemicals, Inc.
    Inventors: Jim Kisielewski, Donald M. Robertson, Robert N. Skogley
  • Patent number: 7323150
    Abstract: A method for recovering at least one metallic element from ore or other material is described and includes reacting ore or other material with a salt capable of recovering the metallic element from the ore or other material to form a reaction product that includes the metallic element. The method also includes recovering the metallic element from the reaction product. To remove the metallic element from the reaction product, the method can involve crushing the reaction product to form a crushed material and dissolving the crushed material in a solvent to remove the precipitates, thereby leaving a sulfate solution containing the metallic element.
    Type: Grant
    Filed: May 23, 2003
    Date of Patent: January 29, 2008
    Assignee: Cabot Corporation
    Inventors: Bart F. Bakke, David Madden
  • Patent number: 6241893
    Abstract: An amorphous potassium aluminosilicate filtration media which may be mixed with activated carbon filters water to remove oxygen, chlorines, hardness, alkalinity, ammonia, hydrogen, hydrogen sulfide, sodium sulfite and other contaminants. The particular sodium aluminosilicate is a porous amorphous material formed under ultraviolet light or sunlight to produce pore sizes of 60 Å to 250 Å at ambient temperatures (20° C.-35° C.) and low relative humidity (5%-20%). The media is initially formed as a microporous primarily amorphous gel containing Na2O, Al2O3, SiO2 and H2O. The sodium therein is displaced by potassium, whereby the filter removes impurities from water without introducing sodium. The potassium aluminosilicate may be a second stage filter to a first stage filter composed of a strong base anion media charged with potassium carbonate and/or bicarbonate.
    Type: Grant
    Filed: March 18, 1997
    Date of Patent: June 5, 2001
    Inventor: Ehud Levy
  • Patent number: 5900221
    Abstract: The process for preparing a cesium and rubidium salt-containing solution includes a hydrothermal digestion of an uncalcined pollucite and/or calcined lepidolite particulate having an average particle size up to 0.5 mm with an aqueous solution of Ca(OH).sub.2 in a suspension with a mole ratio of SiO.sub.2 to CaO of from 1:2.5 to 1:1.25 in a rotary tubular autoclave at a digestion temperature of 200 to 280.degree. C., under a pressure of from 15 to 65 bar and at a suspension density between 8 and 18% by weight for from 0.
    Type: Grant
    Filed: September 18, 1996
    Date of Patent: May 4, 1999
    Assignee: Metallgesellschaft Aktiengesellschaft
    Inventors: Hartmut Hofmann, Klaus Kobele, Horst Prinz, Klaus Schade
  • Patent number: 5770739
    Abstract: An apparatus and process for hydrogen peroxide vapor sterilization of medical instruments and similar devices make use of hydrogen peroxide vapor released from a substantially non-aqueous organic hydrogen peroxide complex, such as a urea-peroxide complex. Optionally, a plasma can be used in conjunction with the vapor. A method for preparing substantially non-aqueous hydrogen peroxide complexes is also provided. These complexes are useful as a source of peroxide vapor in hydrogen peroxide vapor sterilizers and as a component of self-sterilizing packaging materials.
    Type: Grant
    Filed: August 26, 1996
    Date of Patent: June 23, 1998
    Assignee: Johnson & Johnson Medical, Inc.
    Inventors: Szu-Min Lin, James Archie Swanzy, Paul Taylor Jacobs
  • Patent number: 5593650
    Abstract: The method of making a high density saline cesium and rubidium solution includes comminuting uncalcined pollucite and/or calcined lepidolite to a grain size of less than 0.1 mm; combining the comminuted material in the presence of water with Ca(OH).sub.2 at a mol ratio of SiO.sub.2 to CaO of not less than 1:2; hydro-thermally decomposing at a temperature of 200.degree. to 280.degree. C.
    Type: Grant
    Filed: July 17, 1995
    Date of Patent: January 14, 1997
    Assignee: Metallgesellschaft Aktiengesellschaft
    Inventors: Horst Prinz, Hartmut Hofmann, Klaus K obele, Marion Wegner
  • Patent number: 5173088
    Abstract: Disclosed is a process for preparing crystals of anhydrous sodium sulfide, the process being characterized in that the process comprises the steps of heating crystals of polyhydrate of sodium sulfide under a pressure of about 500 torr or less at a temperature varying not more than .+-.about 10.degree. C. from the phase transition point between polyhydrate crystals and monohydrate crystals of sodium sulfide for about 2 hours or longer and further heating the monohydrate under atmospheric or reduced pressure at about 90.degree. to about 200.degree. C. for about 2 hours or longer.
    Type: Grant
    Filed: May 26, 1989
    Date of Patent: December 22, 1992
    Assignee: Sankyo Kasei Co., Ltd.
    Inventors: Kannosuke Maeda, Yoshio Aoyama
  • Patent number: 4963515
    Abstract: Hydrogel-bound aggregate lightweight building materials, such as blocks for use in replacement of lightweight concrete or extruded clay blocks, prepared by expanding and drying a foamable composition containing precursors for an alkali metal aluminosilicate hydrogel, fine grain particulate aggregates, and a viscosity-reducing agent sufficient to result in a starting slurry composition viscosity of less than 40,000 cps at a solids content of 70% by weight or greater.
    Type: Grant
    Filed: November 18, 1988
    Date of Patent: October 16, 1990
    Assignee: The Duriron Company, Inc.
    Inventor: Richard L. Helferich
  • Patent number: 4913736
    Abstract: A process for recovering Platinum Group metals from material comprising one or more Platinum Group metals and one or more Group IA metals supported on carbon comprises heating at a temperature between 700.degree. C. and 1150.degree. C. in a stream of an inert gas or vacuum then in a stream of carbon dioxide.
    Type: Grant
    Filed: October 11, 1988
    Date of Patent: April 3, 1990
    Assignee: The British Petroleum Company p.l.c.
    Inventor: Edmund Gimzeski
  • Patent number: 4814300
    Abstract: Disclosed herein is a foamable, self-setting ceramic composition which can be poured into molds or injection-molded or extruded to achieve desired shapes, and thereafter fired to produce shaped, porous ceramic articles useful as filter elements, insulation, kiln furniture, molds furnace linings or other like articles, the composition containing agents capable of developing an aluminosilicate hydrogel and capable of generating gas to produce porosity within the hydrogel bound molded shape.
    Type: Grant
    Filed: December 2, 1987
    Date of Patent: March 21, 1989
    Assignee: The Duriron Company, Inc.
    Inventor: Richard L. Helferich
  • Patent number: 4812424
    Abstract: Low mass kiln furniture for supporting ceramic ware during the firing thereof is provided having excellent thermal shock resistance and high temperature stability, the kiln furniture being comprised of a porous refractory ceramic body of low density prepared by the firing of a porous aluminosilicate-bound aggregate of refractory ceramic compounds, and wherein the ceramic body has on one or more of its surfaces a smooth skin in the form of an integral thin porous ceramic membrane layer.
    Type: Grant
    Filed: December 2, 1987
    Date of Patent: March 14, 1989
    Assignee: The Duriron Company, Inc.
    Inventors: Richard L. Helferich, Robert C. Schenck
  • Patent number: 4169131
    Abstract: A process for recovering caustic alkali from spent alkali liquor, in which a spent alkali liquor and iron oxide are roasted to obtain a product containing alkali ferrate and the product of roasting is hydrolyzed at a temperature over 110.degree. C. and under pressurized conditions where liquid phase is retained, thereby recovering caustic alkali in the form of an aqueous solution of a concentration higher than approximately 15 wt% containing dissolved iron in an extremely small concentration.
    Type: Grant
    Filed: March 14, 1978
    Date of Patent: September 25, 1979
    Assignee: Nittetu Chemical Engineering Limited
    Inventors: Yoshiaki Kinoshita, Toshiaki Kurihara, Yoshiyuki Imagire
  • Patent number: 4140747
    Abstract: The present invention relates to a process for the production of potassium chloride and of magnesium chloride hexahydrate (bischoffite) from carnallite or from carnallite containing sodium chloride.The process comprises heating carnallite at a temperature of between above 70.degree. C. and above 167.5.degree. C. in the presence of added water at the above former temperature or without added water (but preventing evaporation of water) at the above latter temperature. Solid potassium chloride is then separated. In the residual brine, carnallite is precipitated by evaporation or by lowering the temperature, and it is recycled to the starting stage. The residual solution consists essentially of magnesium chloride which is recovered as bischoffite.
    Type: Grant
    Filed: October 20, 1977
    Date of Patent: February 20, 1979
    Assignee: Israel Chemicals Ltd.
    Inventor: Abraham Sadan