Abstract: The invention describes stable colloidal polymeric particles of 0.2-5.0 microns size which are coated with a first aminodextran layer and a second metallic solid layer, The metal is coated by reduction of a metallic salt or complex by the aminodextran.

Abstract: The present invention relates to a method for producing a microgranulated particle having particle size of not more than 0.2 mm, wherein a fine powder with the average particle size of not more than 10 .mu.m, which is being agitated, tumbled or fluidized, is granulated, with a solution containing a binder alone or a binder and a surfactant being sprayed onto the surface thereof. The present invention allows to produce pharmaceutical preparations for poorly soluble and poorly absorbable drugs and preparations requiring a high content of the active ingredient. Also, it can provide an easy-to-handle powdery microgranulated particle in the field of food and fertilizers.

Abstract: A granular polymer composite comprising polymeric granules having coated on a surface thereof a calcium phosphate compound, at least a part of the particles of the calcium phosphate compound penetrates into the polymeric granules. The composite has a high bonding strength between the polymeric granules as a matrix and a coating of the calcium phosphate compound and also can fully exhibit the functions of a calcium phosphate compound. Using the granular polymer composite, a diagnostic agent which comprises of an antigen or antibody is adsorbed and immobilized on the composite and is therefore useful in diagnostic tests utilizing an antigen-antibody reaction for a number of infectious diseases.

Abstract: The invention is a method for making a metal containing article, comprising the steps of: providing a layer of a porous ground in a selected area; exposing selected regions of the layer of porous ground to light, thereby metallizing the selected regions; repeating the foregoing steps a selected number of times to produce a selected number of layers; and selectively modifying the metallized regions of the layers. The initial metallization can be by electroless or semiconductor photo deposition plating. The subsequent modification of the metallized regions can be by electroless plating, electroplating or sintering. It is also possible, in some instances, to forego the second phase modification, the initial phase having provided the desired parameters. In a third preferred embodiment, the invention is a method using an initial metallization phase effected by exposure of a metal salt, such as a metal halide, to light, thereby inducing activation of the halide.

Abstract: An improved dye composition for use in coating tablets and the like is constituted by a stable, aqueous suspension containing a water-soluble, nontoxic dye, an opacifying agent which may be titanium dioxide or iron oxide all immobilizing agent for immobilizing the dye and preventing it from migrating when applied to a tablet or the like, the immobilizing agent being constituted by a nontoxic metal salt present in an amount of from approximately 0.1 to 10 equivalents of metal per mole of dye, and water. The suspension may also contain a film-forming, water-soluble or water-dispersible edible polymer and a plasticizer. These compositions are used in lieu of lake compositions to produce tablets and the like with uniform, non-mottled coatings.

Abstract: A bone cement composition has adjustable rheological properties, high strength, and produces a uniform radiological image. The cement is characterized by controlled retention and release of additives incorporated in beads included in the dry component of the cement. The cement comprises beads containing a polymerization initiator in controllable concentrations from 0% to 5% or more by weight. These same beads or others may also contain an opacifier. The polymerization initiator and the opacifier may be selectively distributed throughout the beads or at specific radial locations in the beads. They may also be selectively placed in beads of a particular advantageous size range. Furthermore, in other embodiments of the invention, other advantageous additives can be incorporated in the beads such as dyes, antibiotics, bone growth factors, and other pharmacological or therapeutic agents.

Abstract: Methods of impregnating various polymer substrates with an impregnation additive, by simultaneously contacting the polymer substrate with an impregnation additive, carrier liquid, and supercritical fluid are provided. The impregnation additive is substantially insoluble in the supercritical fluid, and the carrier liquid is preferably substantially insoluble in the supercritical fluid.

Abstract: Pharmacologically inactive spherical seed cores comprising at least 50% by weight of microcrystalline cellulose having an average degree of polymerization of 60 to 375, wherein the spherical seed cores have an average particle size of 100 to 1000 .mu.m, a tapped bulk density of at least 0.65 g/ml, an aspect ratio of at least 0.7, a water absorption capacity of 0.5 to 1.5 ml/g, and a friability of no more than 1%; spherical granules comprising the spherical seed cores coated with a powdery layer comprising active ingredients and having an outer layer of coating provided on the powdery layer; and a process for the production of spherical granules, comprising the steps of coating the spherical seed cores with powder comprising active ingredients using an aqueous binding solution, spraying an aqueous solution or suspension of a coating agent thereon, and drying the resulting coated granules.

Abstract: A method for preparing deagglomerated fibres and/or particles and for providing the fibres and/or particles with a substantially uniform protective coating, the fibres and/or particles being of a material selected from the group consisting of carbides oxides, nitrides, silicides, borides, metals and graphite, including SiC, TiC, ZrC, WC, NbC, AlN, TiN, BN, Si.sub.3 N.sub.4, MgO, Al.sub.2 O.sub.3, SiO.sub.2, ZrO.sub.2, Fe.sub.2 O.sub.3, Y.sub.2 O.sub.3, steel, tungsten, molybdenum and carbon, the method comprising (a) preparing an inorganic colloid sol, and (b) mixing the fibres and/or particles are deagglomerated and substantially homogeneously distributed. The fibres and/or particles, e.g. SiC whiskers provided with an aluminum oxide coating by treatment with an aluminum hydroxide-based sol, are used for the preparation of metal matrix composite materials, e.g. based on aluminum or an aluminum alloy.

Abstract: A method for forming a coating on at least one part to be coated has the steps of agitating a mixture including (i) the at least one part to be coated, (ii) a material that forms an adhesive layer on the at least one part to be coated, (iii) impact media, and (iv) multiple compositions of powder material; and fusing at least one of the multiple compositions of powder material.

Abstract: An apparatus for dipping tablets into gelatin coating material and for spreading and setting the coating immediately after dipping is provided. Carrier plates having a plurality of tablet holders are transported from a tablet loading station to a dipping station along a transport guide. At the dipping station, a carrier plate is mounted to a vacuum chamber. A set of vacuum tubes in the vacuum chamber are extended through the tablet holders to contact and lift the tablets off of the holders and secure the tablets to the tubes. In a preferred embodiment, the vacuum chamber is rotated 180.degree. and a second carrier plate is mounted onto the housing and a second set of tubes secure the tablets to the plate. The carrier plates are alternately dipped and returned to the transport guide where new plates with uncoated tablets replace the plates with coated tablets. Immediately after dipping the carrier plates enter a rotating station where the plate is rotated 360.degree.

Abstract: A process for forming a medicament carrier for use in a dry powder inhalator device wherein the medicament carrier has at least one carrier screen portion. The carrier screen portion defines a plurality of interstices therein and carries a powdered medicament, applied in a suspension and the suspending agent then evaporated off, which is substantially loaded onto the screen portion surface such that the interstices of the carrier screen portion are at least partially open and free of the dry powdered medicament.

Abstract: Hollow microspheres produced by the present method each have a hollow interior evacuated of gases to a predetermined pressure. A reflective material layer coats the exterior of each microsphere and, optionally, an outer layer of a protective material is applied over the reflective material layer. Permeant gases are dissolved into glass or plastic frit particles prior to heating of the frit particles to form hollow microspheres having the permeant gases contained therein. The permeant gases are subsequently out-permeated in a non-permeant gas atmosphere to substantially evacuate the interior of each microsphere. The exterior layers of reflective material and protective material are then coated about each evacuated microsphere.

Abstract: The present invention relates to a novel process for forming metal matrix composite bodies. Particularly, an infiltration enhancer and/or an infiltration enhancer precursor and/or an infiltrating atmosphere are in communication with a rigidized filler material or a rigidized preform, at least at some point during the process, which permits molten matrix metal to spontaneously infiltrate the rigidized filler material or rigidized preform. Such spontaneous infiltration occurs without the requirement for the application of any pressure or vacuum. In one embodiment of the invention, a filler material or preform can be rigidized by firing and at least partially sintering the filler material so as to provide a three-dimensionally interconnected network of sintered filler material. In another embodiment of the invention, a refractory material mixture is contacted against an exterior surface of a preform or filler material and at least at some point during the process becomes structurally supportive.

Abstract: The present invention includes a first coating section, a second coating section and a device for transferring products from the first to the second sections. The first section includes a feeding and loading station for depositing products onto product holders retained in product carrier plates. The products are advanced to a first dipping station in the first section to coat a first portion of the product. The plates are then advanced to a first rotating station in the first station and rotated at least one revolution for spreading the coating over that first portion. The plates are then advanced to a dryer that extends over the first section of the coating apparatus and the coating is dried. The transfer device transfers the products to the second section of the coating apparatus in such a manner to expose the uncoated portion of the products. The plates are then advanced to identical dipping and rotating stations and dryer as in the first section.

Abstract: Acicular cobalt-containing magnetic iron oxides having a high coercive force and a core/shell structure and hence low temperature dependence of the coercive force are prepared by a process in which, in a first stage, surface activation is effected by means of iron(II) and cobalt ions under alkaline conditions on the iron oxide core under an inert gas atmosphere and thereafter, in a second stage, an epitactic coating of cobalt ferrite is applied, which coating is formed oxidatively from iron (II) and cobalt (II) hydroxide, likewise under alkaline reaction conditions. The total amount of cobalt ions used for doping remains unchanged compared with the known doped iron oxides or is even smaller. In the second process stage, the achievable coercive force can be controlled by the proportion of air in the gas mixture during the formation of the epitactic coating.

Abstract: A prolonged release dosage form of drug made by coating a surface of an ungranulated medicinal particle with a water-insoluble material which is physiologically acceptable and does not dissolve in water and gastric juice; and then, granulating or tableting the coated medicinal particles.

Abstract: The object of the present invention is an improved hard coating process using a polyol in powder form, enabling easy, speedy creation of a hard coating on the surface of a product. This process consists essentially of the application of a syrup containing at least 90% of a polyol chosen from sorbitol, maltitol, mannitol, xylitol, erythritol, lactitol and isomalt to a product, followed by, the application, in powder form, of a quantity of powder which has a purity higher than 95% with respect to this same polyol; these applications being performed without carrying out a forced drying.

Abstract: Passivated metallic pigments obtainable by gas-phase decomposition of volatile phosphorus compounds and of volatile nitrogenous silicon compounds with steam and/or oxygen in the presence of the agitated pigment particles, and the production of these pigments and their use for coloring water-based printing inks, other inks and paints.

Abstract: The invention relates to color-stable tablets for the therapeutic drug oxcarbazepine, which tablets are provided with a hydrophilic, permeable layer containing white pigments and a hydrophilic, permeable outer layer containing white pigments in combination with iron(II) oxide pigments.

Abstract: Method of coating cores of pharmaceutical tablets with a dry powder, wherein the cores are fed onto a conveyor, the dry powder is supplied to a region through which the cores are to be conveyed, and the cores are conveyed on the conveyor through the region with the cores maintained at a different electric potential from the dry powder. In this way, the dry powder is attracted to the exposed surfaces of the cores to form powder coatings thereon. The dry powder on the surface of the cores is then melted to convert the powder into fused film coatings secured to the cores.

Abstract: Process for fixing wound items made from electrically conductive materials by impregnation with radically polymerisable compositions and thermal curing characterised in that the wound items are impregnated by immersion impregnation, flow coating, vacuum impregnation, vacuum pressure impregnation or trickle impregnation and that simultaneously with or after thermal curing the wound articles are cured by high-energy radiation. The process operates with low energy requirements and low emissions of volatile substances. Radically curable compositions are also described.

Abstract: The present invention is directed to an apparatus for coating a product such as a medicament in the shape of a tablet. The apparatus includes a plurality of plates for receiving and retaining the products and means for advancing the plates on a conveyor to various processing stations. At a dipping station, a dipping means lowers and raises at least one plate into a first coating tank for coating at least a portion of the product. At a rotating station, a rotation means rotates one of the plates containing the product for spreading the coating on the product. After rotation, a first elevator transfers the plates from the conveyor to a dryer disposed above the conveyor. A second elevator transfers the plates from the dryer back to the conveyor for further processing. The dryer includes complementary acting pusher bars for transporting a plurality of plates horizontally along a plurality of vertically spaced guides.

Abstract: The invention relates generally to colloidal particle having a core material and a gelatin/aminodextran coating with pendent functional groups attached thereto. Biological substances or molecules, especially monoclonal antibodies, may be attached to said particles. The monoclonal antibody containing particles are useful in a variety of positive and negative biological assays.

Abstract: A process for preparing a biodegradable water-resistant film. The process includes the steps of dispersing zein in an aqueous solution comprising acetone in an amount of from 65 to 75% by volume to form a zein dispersion, forming the resulting zein dispersion into a film, and drying the film in an atmosphere having a relative humidity of 85% or less at an initial temperature of 55.degree. C. or less. The present invention also relates to a method for imparting water resistance to an article with poor water resistance by coating the article with the zein dispersion prepared as above, and drying the coated zein dispersion under the above conditions. The film or coating film according of the present invention neither dissolves upon contact with water, nor becomes weak due to water absorption or swelling on contact with water.

Abstract: A directly compressed cholestyramine tablet with a solvent-free coating is disclosed. The inner core of the tablet is made up of cholestyramine agglomerates consisting of numerous small, irregularly-shaped, jagged-edged fragments having relatively few smooth or flat surfaces with a moisture content ranging from about 8 to 14 percent by weight. A process is also disclosed for preparing cholestyramine agglomerates of the invention. The solvent-free coating comprises from about 60 percent to about 95 percent by weight of stearic acid and from about 5 percent to about 40 percent of polyethylene glycol.

Abstract: Particles including a first material and having a first value of an intrinsic property such as thermal conductivity or coefficient of thermal expansion are coated, by a method such as electroless plating, electrolytic plating, sputtering, or spraying, with a second material having a second value of the intrinsic property in approximately the ratio of volume of coating to volume of each of the particles which makes the value of the intrinsic property of each of the coated particles equal to a desired value. The first and second materials can be metal or non-metal. A plurality of particles, including the coated particles, can be consolidated to form an article, or the particles and a matrix material can be co-deposited on a surface as a coating by a method such as electrolytic plating.

Abstract: A method for reducing abrasion during film coating of susceptible solid dosage forms by applying to an uncoated dosage form, a subcoat containing a pharmaceutically acceptable polyalkylene glycol and the resulting solid pharmaceutical dosage form.

Abstract: Apparatus and method for coating products with two colors including a first coating section, a second coating section and a side to side transfer device for transferring products from the first to the second sections. The transfer device includes a pair of plate grippers each having a movable upper jaw and a movable lower jaw. The upper and lower jaws are each adapted to receive and retain a product carrier plate. The transfer device includes a cam follower that precisely closes the upper and lower jaws so that carrier plates located in the jaws are positioned in registration with each other in order to clamp product between the plates and to maintain the product clamped in the plates while the grippers are transferred between the first and second conveyor guides. An unloading station includes breaker pins for breaking a seal that may be formed between the coating material applied in the first coating section and the carrier plates.

Abstract: A high strength particle comprised of a particulate substrate, a substantially cured inner resin coating, an outer resin coating, and a reinforcing agent interspersed at the inner coating/outer coating boundary.

Abstract: An improved dye composition for use in coating tablets and the like is constituted by a stable, aqueous suspension containing a water-soluble, nontoxic dye, an opacifying agent which may be titanium dioxide or iron oxide an immobilizing agent for immobilizing the dye and preventing it from migrating when applied to a tablet or the like, the immobilizing agent being constituted by a nontoxic metal salt present in an amount of from approximately 0.1 to 10 equivalents of metal per mole of dye, and water. The suspension may also contain a film-forming, water-soluble or water-dispersible edible polymer and a plasticizer. These compositions are used in lieu of lake compositions to produce tablets and the like with uniform, non-mottled coatings.

Abstract: Solid particles are coated with a polymer coating, by a process that includes, dispersing the uncoated particles in water, containing a wetting agent, adding a liquid polymer coupling agent, so that the dispersed solid particles have a film of the coupling agent, and agitating the mixture while adding a prepolymer. The coupling agent is reacted with the polymer to form polymer coatings on the dispersed particles. Relatively thin polymer coatings can be achieved by this process. As an extension of the process, the core particles can be materials used for abrasive blast cleaning, filtration, separation catalysis, animal feed, drug dispensing, contacting, tumble cleaning, and slow release of active ingredients.

Abstract: The invention pertains to a process for preparing a phenylalanine-free dietetic product comprising L-amino acids, and optionally comprising carbohydrates, minerals, trace elements and/or vitamins, for persons afflicted with phenylketonuria particularly adults, juveniles and pregnant women. The process comprises preparing a wet batch by dispersing in water the L-amino acids, some or all of the optional components, and at least one fatty material as an emulsifier, after which the wet batch is spray-dried. The spray-dried wet batch is then mixed with additional vitamins and/or carbohydrates and at least one fatty material as a separation agent to produce a mass. The mass thus produced is processed into cores for dragees or tablets, and the dragee or tablet cores are provided with coatings or dragee covers. The dietetic product is used as a nutrition supplement.

Abstract: Method of making an ingestible composition useful as a contrast enhancing agent in ultrasonic imaging of the digestive tract of humans and animals, wherein the composition has microballoons as contrast enhancing particles bound to an organic carrier phase, which when hydrated has an adhesive affinity for the gastrointestinal mucosa.Method includes grafting a silane coupler having at least two reactive functions to the microballoons through one of the reactive functions and binding the grafted microballoons to the carrier phase through another reactive function.

Abstract: A method of inhibiting algae growth on an asphalt shingle surface exposed to varying humidity using a blend of copper-containing algae-resistant granules and non-algae-resistant granules. The copper-containing algae-resistant granules comprise a substrate granule having at least one inner ceramic coating layer comprising cuprous oxide and a seal coating having a thickness covering the inner layer and which is at time t.sub.o devoid of copper.

Abstract: A method for preparing a self-propelling, powder dispersing aerosol composition comprising at least 0.0001% by weight of a finely-divided solid medicament coated with a non-perfluorinated surface active dispersing agent which constitutes at least 0.0001% by weight of the coated solid material, and suspended in an aerosol propellant in which the non-perfluorinated surface-active dispersing agent is substantially insoluble. Propellant-insoluble non-perfluorinated surfactants are used to prepare stable dispersions of powdered medicament by way of pre-coating the medicament with the surfactant prior to admixture with propellant.

Abstract: What is disclosed is a method for preparing carrier systems, adaptable to the covalent bonding thereto of biologically active materials, consisting of a known solid support material having a surface coated with a polymer containing functional groups suitable for covalent bonding, by coating the support material with a film-forming polymer dispersion and a non-film-forming polymer dispersion, suitably in admixture, at least one of the two polymer dispersions containing a polymer having functional groups suitable for covalent bonding with a biologically active material.

Abstract: A bone cement composition has adjustable rheological properties, high strength, and produces a uniform radiological image. The cement comprises beads containing a polymerization initiator in controllable concentrations from 0% to 5% or more by weight. These same beads or others may also contain an opacifier. The polymerization initiator and the opacifier may be selectively distributed throughout the beads or at specific radial locations in the beads or within the beads in specific strata. They may also be selectively placed in beads of a particular advantageous size range. Furthermore, in other embodiments of the invention, other advantageous additives can be incorporated in the beads such as dyes, antibiotics, bone growth factors, and other pharmacological or therapeutic agents.

Abstract: In producing an additive for a building material, lightweight granules (e.g., polystyrene beads) are first coated with a waterproof adhesive by mixing in a suitable mixer. When the granules are satisfactorily coated, they are further coated with a wet cementitious material, for example aggregate and wet cement, or with wet plaster, which is added to the mixture. Only sufficient moisture is added to allow the cement or plaster to initiate the chemical reaction which results in the curing of the coating material on the granules. The wet material acts to separate the granules while forming a coating thereon. The granules are then removed from the mixture and allowed to dry and set. The dry granules may then be added to a conventional concrete or plaster mix.

Abstract: The invention relates to a soybean seed, lucerne seed or clover seed coated with an inoculant composition comprising a carrier medium, a beneficial microorganism and an adhesive polymeric material. A high average loading of viable organisms per seed is maintained in storage.

Abstract: The present invention relates to a novel process for forming metal matrix composite bodies. Particularly, an infiltration enhancer and/or an infiltration enhancer precursor and/or an infiltrating atmosphere are in communication with a rigidized filler material or a rigidized preform, at least at some point during the process, which permits molten matrix metal to spontaneously infiltrate the rigidized filler material or rigidized preform. Such spontaneous infiltration occurs without the requirement for the application of any pressure or vacuum.

Abstract: Composite electroluminescent phosphor particles may be made by forming, on a substrate, a composite layer comprising at least one layer of a dielectric or conductive material and at least one layer of an electroluminescent phosphor, physically removing the composite layer from the substrate, and pulverizing the composite layer to obtain composite electroluminescent phosphor particles.

Abstract: Roofing granules having surfaces treated with an oil and an elastomeric rubber. The elastomeric rubber can be an organic block copolymer having elastomeric and nonelastomeric repeating units. The oil and rubber are applied to the roofing granules' surfaces as a thin film. The thin film of oil and rubber impedes granule staining from oils in asphalt roofing materials, and reduces dust formation during granule handling. Also disclosed is a roofing shingle and a process for making the roofing granule composition.

Abstract: This invention provides a novel process of producing magnetically responsive fluorescent polymer particles comprising polymeric core particles coated evenly with a layer of polymer containing magnetically responsive metal oxide. A wide variety of polymeric particles with sizes ranging from 1 to 100 microns can be used a core particles and transformed into magnetically responsive polymer particles. The surface of these magnetically responsive polymer particles can be coated further with another layer of functionalized polymer. These magnetically responsive fluorescent polymer particles can be used for passive or covalent coupling of biological material such as antigens, antibodies, enzymes or DNA/RNA hybridization and used as solid phase for various types of immunoassays, DNA/RNA hybridization probes assays, affinity purification, cell separation and other medical, diagnostic, and industrial applications.

Abstract: Inorganic hydrated metal oxide and metal silicate gels are supported on the surface of particles of porous material by precipitation therein without significant deposit within pores of the support material and without encapsulating the particles of porous material. Especially preferred hydrated oxides and silicate gels are those of titanium. Preferred porous particles are composed of carbon.These novel composite materials are prepared by spraying an aqueous basic material onto the porous particles and then spraying a concentrated aqueous acidic solution of a source of suitable metallic ions so as to rapidly form a gelatinous precipitate on the surface of the porous particles which remain porous.

Abstract: A metastable crystal layer is deposited by chemical plasma deposition on diamonds at subatmospheric pressure (10.sup.-3 Torr) at 850.degree.-1050.degree. C. The metastable layer enables the diamond to be metallurgically bonded to a suitable substrate.

Abstract: The soil composition of this invention is comprised of a mixture of sand, clay, a plasticizer material, water, and a coloring pigment, if desired. The components of the soil composition are preferably present in the following proportions by weight: sand 50-70%; clay 10-40%; plasticizer 0.5-5.0%; water 5-20%; and coloring pigment 1-5%. The method of making the invention involves continuously mixing a portion of the sand and the plasticizer in an agitation mixer. The same becomes coated with the plasticizer, whereupon a quantity of clay is then added, followed by an additional portion of the plasticizer material It is particularly important that the sand particles become coated with the plastizing compound and clay. The coloring pigments are added and mixed thereafter. As soon as complete mixing takes place, material can be immediately transferred from the mixer to suitable packaging.

Abstract: A method of making a soil composition involves continuously mixing sand and plasticizer in an agitation mixer. The sand becomes coated with the plasticizer, whereupon a quantity of clay is then added, followed by an additional portion of the plasticizer. The sand particles coated with the plasticizer become coated with the clay. Coloring pigments are added and mixed thereafter. As soon as complete mixing takes place, the coated sand particles can be immediately transferred from the mixer to suitable packaging. The ingredients are added in the following proportions by weight: sand 50-70%; clay 10-40%; plasticizer 0.5-5.0%; water 5-20%; and coloring pigment 1-5%.

Abstract: Purple pigments based on glass frits having an average particle diameter (D.sub.50 value) of 0.5 to 50 .mu.m, of which the surface has a coating of essentially 0.05 to 5% by weight, based on the pigment, of colloidal gold and, if desired, color-modifying metals from the group consisting of Ag, Cu, Co, Ni, Sn, Ru, Rh, Pd, Os, Ir and Pt in a total quantity below that of the gold. The purple pigments do not require the hitherto necessary calcination step and can be used for pigmenting glazes, enamels, glass colors, decorative colors, plastics, printing inks and lacquers.

Abstract: The invention concerns the production of a decorative high-pressure laminate with a surface layer (3) on the surface of which an adhesive primer layer (4) of polyvinyl butyral is applied. The adhesive primer layer (4) enables a lacquer coating to be applied subsequently, so that a lacquer layer optimally suited to the particular application for which the laminate is eventually used can be chosen. The adhesive primer layer (4) can be applied by impregnating a web of paper with melamine resin, dusting the impregnated web with polyvinyl butyral powder while the resin is still wet and then drying. Another way of producing the coat is to apply polyvinyl butyral in alcoholic solution to a web of paper which has been impregnated with melamine resin and dried, and subsequently drying.