Metal Base Patents (Class 427/216)
  • Patent number: 6982047
    Abstract: The present invention improves the oxidation resistance of an ultrafine metal powder for use in the internal electrode of a multilayer ceramic capacitance and suppresses an increase in the thickness of a metal internal electrode film resulting from the spheroidization of the molten metal under surface tension during the formation of the metal internal electrode film. The ultrafine metal powder has a sulfur-containing compound of not less than one element selected from the group consisting of Y, Zr, and La present on the surface of the particle thereof and is produced by performing an ultrafine metal powder purification step of dispersing the ultrafine metal powder in a slurry, a surface treatment step of adding an aqueous solution containing a sulfate of not less than one element selected from the group consisting of Y, Zr, and La to the slurry to form the compound on the surface of the metal particle, a filtering step, and a drying step.
    Type: Grant
    Filed: November 14, 2003
    Date of Patent: January 3, 2006
    Assignee: Kawatetsu Mining Co., Ltd.
    Inventor: Morishige Uchida
  • Patent number: 6977097
    Abstract: A particle forming method includes feeding a first set of precursors to a first energy application zone. Energy is applied to the first set of precursors in the first energy application zone effective to react and form solid particles from the first set of precursors. The application of any effective energy to the solid particles is ceased, and the solid particles and a second set of precursors are fed to a second energy application zone. Energy is applied to the second set of precursors in the second energy application zone effective to react and form solid material about the solid particles from the second set of precursors. At least one precursor is fed to at least one of the first and second energy application zones as a liquid. Other aspects are contemplated.
    Type: Grant
    Filed: July 23, 2003
    Date of Patent: December 20, 2005
    Assignee: Micron Technology, Inc.
    Inventor: Trung Tri Doan
  • Patent number: 6974601
    Abstract: Disclosed is a positive active material for a rechargeable lithium battery. The positive active material includes at least one compound represented by formulas 1 to 4: LixNi1-yMnyF2??(1) LixNi1-yMnyS2??(2) LixNi1-y-zMnyMzO2-aFa??(3) LixNi1-y-zMnyMzO2-aSa??(4) where M is selected from the group consisting of Co, Mg, Fe, Sr, Ti, B, Si, Ga, Al, Sc, Y, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Ac, Th, Pa, U, Np, Pu, Am, Cm, Bk, Cf, Es, Fm, Md, No and Lr, 0.95?x?1.1, 0<y?0.99, 0?z?0.5, and 0?a?0.5; and a metal oxide or composite metal oxide layer formed on the compound.
    Type: Grant
    Filed: March 23, 2004
    Date of Patent: December 13, 2005
    Assignee: Samsung SDI Co., Ltd.
    Inventors: Ho-Jin Kweon, Hyun-Sook Jung, Yong-Chul Park, Geun-Bae Kim
  • Patent number: 6958308
    Abstract: A method for producing dispersed metal particles on a substrate and the compositions produced is disclosed. A method for producing the particles comprises exposing an organometallic and a particulate substrate to supercritical or near supercritical fluid under conditions to form a mixture of the fluid and the organometallic, allowing the mixture to remain in contact with the substrate for a time sufficient to deposit dispersed organometallic onto the substrate, venting the mixture, thereby adsorbing the organometallic onto the substrate, and reducing the dispersed organometallic to dispersed metal particles with a reducing agent.
    Type: Grant
    Filed: March 16, 2004
    Date of Patent: October 25, 2005
    Assignee: Columbian Chemicals Company
    Inventor: Garth Desmond Brown
  • Patent number: 6926964
    Abstract: Disclosed is a fuel tank for a motor vehicle whose inner face is processed with an inorganic coating agent comprising (A) fine particles carrying silver and/or copper and (B) inorganic fine particles, and the tank inhibits oxidation of the fuel such as gasoline or light oil, and further decreases the cluster of gasoline or light oil to make finer the particle size of atomized fuel, thereby improving ignitionability and combustibility, which makes it possible to decrease imperfect combustion and to decrease substantially the consumption of the fuel.
    Type: Grant
    Filed: December 12, 2003
    Date of Patent: August 9, 2005
    Assignee: Kabushiki Kaisha Nippankenkyusho
    Inventor: Yoshio Ichikawa
  • Patent number: 6913825
    Abstract: Nanoparticles, nanocomposites, and methods for making the nanoparticles and nanocomposites are disclosed. Illustrated methods include preparing a nanocomposite particle by binding a silicate compound to the surface of a core particle in an aqueous suspension, adding a silicate source and an organic surfactant template, and stirring the aqueous suspension to obtain silicate growth.
    Type: Grant
    Filed: September 20, 2002
    Date of Patent: July 5, 2005
    Assignee: University of Notre Dame du Lac
    Inventors: Agnes E. Ostafin, Robert Nooney, Edward Maginn
  • Patent number: 6875465
    Abstract: A method for decorating a substrate using novel thiol-stabilised gold nanoparticles of the general formula HSR where R is a C3-C60 alkyl group, aryl, benzyl, alicyclic, or heterocyclic group which is substituted or unsubstituted, branched or unbranched. The thiol-stabilised gold nanoparticles exhibit a plasmon frequency of between 480 and 600 nm.
    Type: Grant
    Filed: March 12, 2001
    Date of Patent: April 5, 2005
    Assignee: Johnson Matthey Public Limited Company
    Inventors: Peter Trenton Bishop, Patricia Ann Marsh, Bénédiete Jeanne Suzanne Thiébaut, Alison Mary Wagland
  • Patent number: 6855426
    Abstract: Size-confined nanocomposite powders and methods for their manufacture are provided by coating fine powders with a nanoscale powder of a different composition. The nanocomposite plastics disclosed offer performance characteristics approaching those of metals and alloys. The nanocomposite powders are alternatively used for dispersion strengthening of metals, alloys, and ceramics. Novel materials based nanotechnology for energy devices and programmable drug delivery are disclosed.
    Type: Grant
    Filed: May 10, 2002
    Date of Patent: February 15, 2005
    Assignee: NanoProducts Corporation
    Inventor: Tapesh Yadav
  • Patent number: 6778062
    Abstract: In an organic PTC thermistor comprising an organic polymer matrix and conductive metal particles dispersed therein, the conductive metal particles are pretreated with an organic material which is different from the organic polymer matrix, does not covalently bond with the conductive metal particles, and is not compatible at a molecular level with the organic polymer matrix so that an organic material layer covers surfaces of conductive metal particles whereby the stability of thermistor performance is improved.
    Type: Grant
    Filed: November 15, 2002
    Date of Patent: August 17, 2004
    Assignee: TDK Corporation
    Inventors: Tokuhiko Handa, Yukie Yoshinari
  • Patent number: 6774052
    Abstract: A method of making a permeable base transistor (PBT) is disclosed. According to the method, a semiconductor substrate is provided, a base layer is provided on the substrate, and a semiconductor layer is grown over the base layer. The base layer includes metallic nanotubes, which may be grown or deposited on the semiconductor substrate. The nanotube base layer separates emitter and collector layers of semiconductor material.
    Type: Grant
    Filed: June 19, 2002
    Date of Patent: August 10, 2004
    Assignee: Nantero, Inc.
    Inventors: Bernhard Vögeli, Thomas Rueckes, Brent M. Segal
  • Patent number: 6773763
    Abstract: A method of manufacturing a permanent magnet by the steps of preparing an admixture of magnetic material and binder material, the admixture material having a particle size of less than 325 mesh. Then heating a carrier gas to a temperature substantially below the melting point of either component of the admixture. The admixture is introduced into the carrier gas and the admixture is sprayed atop a ductile carrier. The admixture adheres to the carrier and forms a solid permanent magnet. An electric field is applied to the sprayed admixture to create a permanent magnetic moment.
    Type: Grant
    Filed: July 29, 2002
    Date of Patent: August 10, 2004
    Assignee: Ford Global Technologies, LLC
    Inventors: Franco Leonardi, John Matthew Ginder, Robert Corbly McCune
  • Publication number: 20040146641
    Abstract: Embodiments of this invention comprise a pigment comprising one or more substantially spherical-shaped beads, wherein each substantially spherical-shaped bead comprises one or more high aspect ratio particles encapsulated within an encapsulating material. Embodiments also comprise a resinous composition comprising said pigment. Yet further embodiments comprise a method of preparing said pigment via suspension polymerization. The substantially spherical-shaped beads of this invention may be used to produce resinous compositions having a flowline-free colored, sparkling and/or metallescent appearance.
    Type: Application
    Filed: January 23, 2003
    Publication date: July 29, 2004
    Inventors: Stanley Young Hobbs, Fazila Seker, Daniel Steiger, Christopher Mark Hartshorn, Ali Ersin Acar, Robert Edgar Colborn, Eelco Michiel Sebastiaan van Hamersveld
  • Publication number: 20040139890
    Abstract: A composite pigment is provided with the composite pigment including a dense inorganic material and silica. The pigment composition is characterized by a CTAB surface area of greater than about 20 m2/g; a BET surface area of greater than about 15 m2/g; and a density of greater than about 2.5 g/cm3.
    Type: Application
    Filed: January 17, 2003
    Publication date: July 22, 2004
    Inventors: Fitzgerald Alphanso Sinclair, Mark Edward Wozniak, Louis Frank Gatti, William C. Fultz
  • Patent number: 6756118
    Abstract: In order to state a powdered metal composite material having a high specific electrical resistance and having good mechanical strength, very good resistance to temperature and to fuel, and a starting material and a method for the economical production of such a composite material, a powdered metal composite material having a high specific electrical resistance, which contains at least two oxides encapsulating the powdered metal particles, the oxides forming at least one common phase, and a starting material containing a powdered metal, which contains at least two antitack agents having oxidic pyrolysis residue and oxidic fine powder, and a method for producing such a composite material are made available, which relate to a starting material of the kind named, in which the starting material is pressed to form molded articles, in which the antitack agents are pyrolyzed in a nonreducing atmosphere to form oxides, and the oxides then present are made to react with one another to form at least one common phase.
    Type: Grant
    Filed: February 28, 2002
    Date of Patent: June 29, 2004
    Assignee: Robert Bosch GmbH
    Inventors: Wilfried Aichele, Hans-Peter Koch, Andreas Harzer
  • Patent number: 6739928
    Abstract: A mercury-containing material, a method for producing the same and a fluorescent lamp using the same that can enclose a minimal amount of mercury in a glass bulb precisely, prevent flaws in a fluorescent coating while suppressing a noise during a lamp transportation, and prevent deterioration in appearance are provided. A surface of liquid mercury is coated with a continuous film made of metal oxide or metal complex oxide by dipping the mercury in a metal alkoxide solution and then heating the mercury on which the metal alkoxide solution adheres. Accordingly, the minimal amount of the mercury can be enclosed in the fluorescent lamp precisely, thus achieving friendliness to the environment. It also is possible to prevent flaws in the fluorescent coating while suppressing a noise during the lamp transportation and further to prevent deterioration in appearance.
    Type: Grant
    Filed: February 24, 2003
    Date of Patent: May 25, 2004
    Assignee: Matsushita Electric Industrial Co., Ltd.
    Inventor: Kouji Honda
  • Patent number: 6720074
    Abstract: A series of bulk-size magnetic/insulating nanostructured composite soft magnetic materials with significantly reduced core loss and its manufacturing technology. This insulator coated magnetic nanostructured composite is comprises a magnetic constituent, which contains one or more magnetic components, and an insulating constituent. The magnetic constituent is nanometer scale particles (1-100 nm) coated by a thin-layered insulating phase (continuous phase). While the intergrain interaction between the immediate neighboring magnetic nanoparticles separated by the insulating phase (or coupled nanoparticles) provide the desired soft magnetic properties, the insulating material provides the much demanded high resistivity which significantly reduces the eddy current loss. The resulting material is a high performance magnetic nanostructured composite with reduced core loss.
    Type: Grant
    Filed: October 26, 2001
    Date of Patent: April 13, 2004
    Assignee: Inframat Corporation
    Inventors: Yide Zhang, Shihe Wang, Danny Xiao
  • Patent number: 6706394
    Abstract: The subject invention related to methods and apparatuses for the manufacture of magnetizable carrier particles. In addition the subject invention pertains to particles having one or more of a variety of particle configurations and/or functional features. These geometric particle configurations and/or functional features such as delivering or removing a pay load can be tailored to achieve one or more desired missions. The subject invention also pertains to a method and apparatus for the delivery of particles to target materials, in order to accomplish one or more of a variety of missions. In a specific embodiment of the subject invention, acicular and other particles with a lengthwise dimension that are substantially uniform and homogenous in their geometry are manufactured and provided with magnetizations. In this way, predictable mechanical force responsivity can be achieved when these particles are subjected to an external magnetic field gradient.
    Type: Grant
    Filed: May 2, 2001
    Date of Patent: March 16, 2004
    Inventors: Manfred R. Kuehnle, Adelheid Kuehnle
  • Patent number: 6706324
    Abstract: A product in which at least a portion of the product has a nanocrystalline microstructure, and a method of forming the product. The method generally entails machining a body in a manner that produces chips consisting entirely of nano-crystals as a result of the machining operation imposing a sufficiently large strain deformation. The body can be formed of a variety of materials, including metal, metal alloy and ceramic materials. Furthermore, the body may have a microstructure that is essentially free of nano-crystals, and may even have a single-crystal microstructure. The chips produced by the machining operation may be in the form of particulates, ribbons, wires, filaments and/or platelets. The chips are then used to form the product. According to one aspect of the invention, the chips are consolidated to form the product, such that the product is a monolithic material that may contain nano-crystals.
    Type: Grant
    Filed: October 27, 2001
    Date of Patent: March 16, 2004
    Assignee: Purdue Research Foundation
    Inventors: Srinivasan Chandrasekar, Walter D. Compton, Thomas N. Farris, Kevin P. Trumble
  • Patent number: 6685986
    Abstract: The present invention is for particulate compositions and methods for producing them that can absorb or scatter electromagnetic radiation. The particles are homogeneous in size and are comprised of a nonconducting inner layer that is surrounded by an electrically conducting material. The ratio of the thickness of the nonconducting layer to the thickness of the outer conducting shell is determinative of the wavelength of maximum absorbance or scattering of the particle. Unique solution phase methods for synthesizing the particles involve linking clusters of the conducting atoms, ions, or molecules to the nonconducting inner layer by linear molecules. This step can be followed by growth of the metal onto the clusters to form a coherent conducting shell that encapsulates the core.
    Type: Grant
    Filed: January 5, 2001
    Date of Patent: February 3, 2004
    Assignee: William Marsh Rice University
    Inventors: Steven J. Oldenburg, Richard D. Averitt, Nancy J. Halas
  • Patent number: 6682776
    Abstract: Herein disclosed is surface-modified nickel fine powder in which a precursor of barium titanate having a perovskite structure and consisting of a reaction product of a soluble titanium-containing compound and a soluble barium-containing compound is adhered to the surface of individual nickel fine particles, wherein the fine powder shows X-ray diffraction peaks of nickel and is free of any peak of barium titanate having a perovskite structure in the X-ray diffraction pattern determined by the X-ray diffraction method, but the fine powder shows X-ray diffraction peaks of both nickel and barium titanate having a perovskite structure in the X-ray diffraction pattern after the fine powder is subjected to a heat-treatment at a temperature of not less than 400° C. The nickel fine powder has a small heat shrinkage factor upon firing and improved resistance to oxidation.
    Type: Grant
    Filed: December 13, 2002
    Date of Patent: January 27, 2004
    Assignee: Mitsui Mining and Smelting Co., Ltd.
    Inventors: Takayuki Araki, Takashi Mukuno
  • Patent number: 6680081
    Abstract: A conductive powder having an organic silicon polymer layer on the surface of each particle and a metal layer enclosing the silicon polymer layer possesses a stronger bond between the particle base and the metal even at elevated temperature and exhibits a high and stable conductivity and heat resistance.
    Type: Grant
    Filed: March 22, 2002
    Date of Patent: January 20, 2004
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Motoo Fukushima, Kunio Itoh, Shigeru Mori, Masaki Kasashima, Yoshitaka Hamada, Mikio Aramata
  • Patent number: 6680128
    Abstract: Solder compositions, solder pastes and methods of manufacturing thereof having a solder material coated with a coating material by an immersion coating process or an electroless plating process. The solder composition and solder pastes are substantially lead-free and have melting temperatures approaching those of traditional tin-lead solders.
    Type: Grant
    Filed: September 27, 2001
    Date of Patent: January 20, 2004
    Assignee: Agilent Technologies, Inc.
    Inventor: Zequn Mei
  • Patent number: 6656524
    Abstract: A continuous process for gas phase coating of polymerization catalyst. The polymerization catalyst is introduced in a gas phase plug flow type reactor wherein it is submitted to polymerization conditions in the presence of at least one monomer such that at least 95% by weight of the produced coated catalysts have a coating yield comprised between 0.5 to 2 times the average coating yield.
    Type: Grant
    Filed: February 1, 2001
    Date of Patent: December 2, 2003
    Assignee: BP Chemicals Limited
    Inventors: Daniel Claude Durand, Estelle Marie Joelle Meurice, Frederic Robert Marie Michel Morterol
  • Patent number: 6649222
    Abstract: A method for treating substrates including the steps of: providing a substrate; exposing said substrate to a plasma glow discharge in the presence of a fluorocarbon gas; maintaining said gas at a pressure between about 50 mTorr and about 400 mTorr; generating said plasma as a modulated glow discharge; pulsing said discharge at an on time of 1-500 milliseconds; pulsing said glow at an off time of 1-1000 milliseconds; maintaining said plasma glow discharge at a power density of 0.02-10 watts/cm2; and applying a hydrophobic coating to said substrate.
    Type: Grant
    Filed: February 28, 2001
    Date of Patent: November 18, 2003
    Assignee: The Procter & Gamble Company
    Inventors: Riccardo D'Agostino, Italo Corzani, Pietro Favia, Ritalba Lamendola, Gianfranco Palumbo
  • Patent number: 6645625
    Abstract: The invention relates to a stabilized, pulverulent red phosphorus material composed of phosphorus particles whose particle size is not more than 2 mm, and whose surface has been covered with a thin layer of an oxidation stabilizer, wherein the oxidation stabilizer is silver, and also to the use of the same, and to a process for its preparation.
    Type: Grant
    Filed: November 28, 2001
    Date of Patent: November 11, 2003
    Assignee: Clariant GmbH
    Inventors: Sebastian Hörold, Jürgen Laubner
  • Patent number: 6641918
    Abstract: Geldhart class C tungsten carbide particles are provided with a discontinuous coating of grain growth inhibitor. Further, the fine tungsten carbide coatings are preferably provided with a continuous coating of another discreet phase material, such as, for example, a continuous coating of cobalt. Compacts produced using such materials are particularly useful as WC—Co hardmetals wherein the compacts are extremely fine grained.
    Type: Grant
    Filed: May 30, 2000
    Date of Patent: November 4, 2003
    Assignee: Powdermet, Inc.
    Inventors: Andrew J. Sherman, Animesh Bose
  • Patent number: 6635122
    Abstract: Methods of making and using annealable insulated metal-based powder particles are provided. The insulated metal-based powder particles are formed from metal-based core particles that are coated with an annealable insulating material. The annealable insulating material has at least one inorganic compound and at least one organic polymeric resin. The inorganic compound in the insulating material forms a nonporous insulating layer surrounding the metal-based core particles upon heating. The organic polymeric resin preferably aids in dispersing or binding the inorganic compound to the metal-based core particles prior to annealing. The insulated metal-based powder particles produced can be formed into core components that can be annealed to improve the magnetic performance of the core component. The core components produced are particularly useful under AC operating conditions of 500 Hz or lower.
    Type: Grant
    Filed: October 3, 2001
    Date of Patent: October 21, 2003
    Assignee: Hoeganaes Corporation
    Inventors: Francis G. Hanejko, George Ellis
  • Patent number: 6613383
    Abstract: Particles have an ultrathin, conformal coating are made using atomic layer deposition methods. The base particles include ceramic and metallic materials. The coatings can also be ceramic or metal materials that can be deposited in a binary reaction sequence. The coated particles are useful as fillers for electronic packaging applications, for making ceramic or cermet parts, as supported catalysts, as well as other applications.
    Type: Grant
    Filed: June 21, 2000
    Date of Patent: September 2, 2003
    Assignee: Regents of the University of Colorado
    Inventors: Steven M. George, John D. Ferguson, Alan W. Weimer
  • Patent number: 6596342
    Abstract: A method of coating of mass-produced bulk goods (5) including loading the bulk goods (5) into a rotatable drum (1) through an opening (4) formed in a side surface of the drum (1), heating a coating material in coating apparatus (8), having a spray gun (6) and provided outside of the rotatable drum (1); and thereafter, applying the heated coating material to the bulk goods (5) with the spray gun (6) through the drum opening (4).
    Type: Grant
    Filed: December 21, 2001
    Date of Patent: July 22, 2003
    Assignee: Hilti Aktiengesellschaft
    Inventors: Rainer Batliner, Gerald Felder, Werner Schörghofer
  • Patent number: 6592935
    Abstract: A method of manufacturing electric machines comprised of geometrically patterned arrays of permanent magnets, soft magnetic materials, and electrical conductors deposited by kinetic spraying methods directly atop a carrier. The magnets and planar coils of the present invention may be integrally formed atop carriers to form electrical machines such as motors, generators, alternators, solenoids, and actuators. The manufacturing techniques used in this invention may produce highly defined articles that do not require additional shaping or attaching steps. Very high-purity permanent and soft magnetic materials, and conductors with low oxidation are produced.
    Type: Grant
    Filed: May 30, 2001
    Date of Patent: July 15, 2003
    Assignee: Ford Motor Company
    Inventors: Franco Leonardi, John Matthew Ginder, Robert Corbly McCune
  • Patent number: 6586046
    Abstract: Apparatus and method for producing metallic flake having an environmental coating for use in oxidative and corrosive atmospheres. Fluidized bed techniques are utilized to perform a controlled oxidation of metallic particles that include aluminum. The fluidized techniques permit the formation of a thin, outer shell of alumina over the outer surface of the flake. Because the oxidation is controlled so that the selective oxidation produces a thin outer shell, the particle has good reflectance and the metallic core of the particle is unaffected by the oxidizing treatment. Although the techniques of the present invention are effective for producing a reflective surface on aluminum-containing iron alloys while the core particles can be either magnetically soft or hard, the techniques can be used to produce a reflective surface that is corrosion and oxidation resistant on any aluminum containing alloy. Apparatus that facilitates the controlled oxidation is also set forth.
    Type: Grant
    Filed: January 26, 2000
    Date of Patent: July 1, 2003
    Assignee: General Electric Company
    Inventors: John F. Ackerman, Andrew J. Skoog, Matthew B. Buczek, Jane A. Murphy
  • Publication number: 20030116228
    Abstract: A process and apparatus prepares and collects metal nanoparticles by forming a vapor of a metal that is solid at room temperature, the vapor of the metal being provided in an inert gaseous carrying medium. At least some of the metal is solidified within the gaseous stream. The gaseous stream and metal material is moved in a gaseous carrying environment into or through a dry mechanical pumping system. While the particles are within the dry mechanical pumping system or after the nanoparticles have moved through the dry pumping system, the vaporized metal material and nanoparticles are contacted with an inert liquid collecting medium.
    Type: Application
    Filed: December 20, 2001
    Publication date: June 26, 2003
    Applicant: Aveka, Inc.
    Inventor: Gary A. Pozarnsky
  • Publication number: 20030118723
    Abstract: Herein disclosed is surface-modified nickel fine powder in which a precursor of barium titanate having a perovskite structure and consisting of a reaction product of a soluble titanium-containing compound and a soluble barium-containing compound is adhered to the surface of individual nickel fine particles, wherein the fine powder shows X-ray diffraction peaks of nickel and is free of any peak of barium titanate having a perovskite structure in the X-ray diffraction pattern determined by the X-ray diffraction method, but the fine powder shows X-ray diffraction peaks of both nickel and barium titanate having a perovskite structure in the X-ray diffraction pattern after the fine powder is subjected to a heat-treatment at a temperature of not less than 400° C.
    Type: Application
    Filed: December 13, 2002
    Publication date: June 26, 2003
    Applicant: MITSUI MINING & SMELTING CO., LTD.
    Inventors: Takayuki Araki, Takashi Mukuno
  • Patent number: 6582506
    Abstract: Pigment flakes having cores preferably composed of resins, polymers, thermoplastics, and/or thermosets with colorant (pigment and/or dyes) deposited thereon, coating applications thereof, and a method for making pigment flakes which includes providing a core material, compounding the core material, processing the core material into uniform forms such as films, wires, thread with rectangular cross sections and bead strings, providing colorant material, vaporizing the colorant material, exposing a surface of core material to the vaporized colorant material to form a layer of colorant on thereon, and fracturing the resultant colorant layered core material into flakes.
    Type: Grant
    Filed: May 25, 2001
    Date of Patent: June 24, 2003
    Assignee: Hampden Papers, Inc.
    Inventor: Michael E. Archambeault
  • Patent number: 6582763
    Abstract: The oxide coated fine metal particles include fine core metal particles that are covered with a coating layer including an oxygen-containing compound of a dissimilar element that do not contain as a main component a metal element which is the main component of the fine core metal particles, or a complex oxide or a complex salt of the oxide, the complex oxide or the oxy-acid salt and an oxide of the metal element. A metal powder material is mixed with an oxide powder material of the oxygen-containing compound to obtain a powder material mixture. The powder material mixture is supplied into a thermal plasma to make a vapor-phase mixture and then the vapor-phase mixture is quenched to form the oxide coated fine metal particles comprising the fine core metal particles that are finer than the metal powder material and which are covered with the coating layer including the oxygen-containing compound.
    Type: Grant
    Filed: January 31, 2000
    Date of Patent: June 24, 2003
    Assignees: Nisshin Seifun Group Inc., Nisshin Engineering Inc.
    Inventors: Keiichi Nishimura, Takashi Fujii, Kazuhiro Yubuta, Sadao Shinozaki
  • Patent number: 6582765
    Abstract: Chain parts and other steel articles are provided with hard, wear-resistant carbide coatings by tumbling them in a heated retort with a particulate mix which includes a source of vanadium and/or niobium. The steel substrate comprises a steel having at least 0.2% carbon, preferably 0.7-1.2%. Where the chromium content of the steel is 4-12%, preferably 4-8%, the chemical deposition process includes drawing a small amount of chromium from the steel substrate into the vanadium or niobium carbide coating, where it is distributed substantially homogeneously, helping to provide adhesion strength to the coating.
    Type: Grant
    Filed: June 26, 2001
    Date of Patent: June 24, 2003
    Assignee: BorgWarner, Inc.
    Inventors: Yumin Wang, Yoshito Hanayama, Doug Fornell, Naosumi Tada, Kunihiko Mishima
  • Patent number: 6562403
    Abstract: A method of forming ligated nanoparticles of the formula Y(Z)x where Y is a nanoparticle selected from the group consisting of elemental metals having atomic numbers ranging from 21-34, 39-52, 57-83 and 89-102, all inclusive, the halides, oxides and sulfides of such metals, and the alkali metal and alkaline earth metal halides, and Z represents ligand moieties such as the alkyl thiols. In the method, a first colloidal dispersion is formed made up of nanoparticles solvated in a molar excess of a first solvent (preferably a ketone such as acetone), a second solvent different than the first solvent (preferably an organic aryl solvent such as toluene) and a quantity of ligand moieties; the first solvent is then removed under vacuum and the ligand moieties ligate to the nanoparticles to give a second colloidal dispersion of the ligated nanoparticles solvated in the second solvent. If substantially monodispersed nanoparticles are desired, the second dispersion is subjected to a digestive ripening process.
    Type: Grant
    Filed: October 15, 2001
    Date of Patent: May 13, 2003
    Assignee: Kansas State University Research Foundation
    Inventors: Kenneth J. Klabunde, Savka Stoeva, Christopher Sorensen
  • Patent number: 6555160
    Abstract: Processes for coating three dimensional inorganic substrates, with shielded surfaces, with metal oxide-containing coatings are disclosed. Such processes comprise contacting a substrate with a powder metal oxide precursor formed reactant mixture at fast reaction and elevated temperature reaction conditions to form a substrate containing metal oxide on at least a portion of the three dimensions and shielded surfaces of the substrate. Also disclosed are substrates coated with metal oxide-containing coatings for use in various applications including catalysis, shielding, electrostatic dissipation and battery applications.
    Type: Grant
    Filed: May 18, 2001
    Date of Patent: April 29, 2003
    Assignee: Ensci Inc
    Inventor: Thomas J. Clough
  • Patent number: 6555161
    Abstract: Processes for coating three dimensional inorganic substrates, with shielded surfaces, with metal oxide-containing coatings are disclosed. Such processes comprise contacting a substrate with a metal oxide precursor reactant mixture at fast reaction and elevated temperature reaction conditions to form a substrate containing metal oxide on at least a portion of the three dimensions and shielded surfaces of the substrate. Also disclosed are substrates coated with metal oxide-containing coatings for use in various applications including catalysis, shielding, electrostatic dissipation and battery applications.
    Type: Grant
    Filed: May 18, 2001
    Date of Patent: April 29, 2003
    Assignee: Ensci Inc.
    Inventor: Thomas J. Clough
  • Publication number: 20030077448
    Abstract: An iron-based powder including a heat-resistant insulate coating and a powder core are suggested. A paint containing silicone resin and pigment is added to a raw material powder primarily containing a ferromagnetic metal, especially, iron, agitation and mixing are performed and, thereafter, a drying treatment is performed so as to form a coating containing silicone resin and pigment on the surface of the iron-based powder. The ratio of the silicone resin content to the pigment content in the coating is preferably 0.01 or more, but less than 4.0 on a mass basis. The pigment is preferably at least one selected from the group consisting of metal oxides, metal nitrides, metal carbides, minerals, and glass. The paint may be sprayed to the iron-based powder in a fluidized state. A coating containing at least one of Si compounds, Ti compounds, Zr compounds, P compounds, and Cr compounds may be formed as a lower layer of the aforementioned coating.
    Type: Application
    Filed: March 21, 2002
    Publication date: April 24, 2003
    Applicant: KAWASAKI STEEL CORPORATION
    Inventors: Masateru Ueta, Naomichi Nakamura, Satoshi Uenosono
  • Patent number: 6551657
    Abstract: Processes for coating three dimensional inorganic substrates, with shielded surfaces, with metal oxide-containing coatings are disclosed. Such processes comprise contacting a substrate with a liquid soluble metal oxide precursor formed reactant mixture at fast reaction and elevated temperature reaction conditions to form a substrate containing metal oxide on at least a portion of the three dimensions and shielded surfaces of the substrate. Also disclosed are substrates coated with metal oxide-containing coatings for use in various applications including catalysis, shielding, electrostatic dissipation and battery applications.
    Type: Grant
    Filed: May 18, 2001
    Date of Patent: April 22, 2003
    Assignee: Ensci Inc.
    Inventor: Thomas J. Clough
  • Patent number: 6551658
    Abstract: Processes for coating three dimensional inorganic substrates, with shielded surfaces, with metal oxide-containing coatings are disclosed. Such processes comprise contacting a substrate with a precipated metal oxide precursor formed liquid slurry reactant mixture at fast reaction and elevated temperature reaction conditions to form a substrate containing metal oxide on at least a portion of the three dimensions and shielded surfaces of the substrate. Also disclosed are substrates coated with metal oxide-containing coatings for use in various applications including catalysis, shielding, electrostatic dissipation and battery applications.
    Type: Grant
    Filed: May 18, 2001
    Date of Patent: April 22, 2003
    Assignee: Ensci Inc.
    Inventor: Thomas J. Clough
  • Patent number: 6551659
    Abstract: Processes for coating three dimensional inorganic substrates, with shielded surfaces, with metal oxide-containing coatings are disclosed. Such processes comprise contacting a substrate with a metal oxide precursor reactant mixture at fast reaction and elevated temperature reaction conditions maintained by a flame combustion source to form a substrate containing metal oxide on at least a portion of the three dimensions and shielded surfaces of the substrate. Also disclosed are substrates coated with metal oxide-containing coatings for use in various applications including catalysis, shielding, electrostatic dissipation and battery applications.
    Type: Grant
    Filed: May 18, 2001
    Date of Patent: April 22, 2003
    Assignee: Ensci Inc
    Inventor: Thomas J. Clough
  • Publication number: 20030072874
    Abstract: A method of forming ligated nanoparticles of the formula Y(Z)x, where Y is a nanoparticle selected from the group consisting of elemental metals having atomic numbers ranging from 21-34, 39-52, 57-83 and 89-102, all inclusive, the halides, oxides and sulfides of such metals, and the alkali metal and alkaline earth metal halides, and Z represents ligand moieties such as the alkyl thiols. In the method, a first colloidal dispersion is formed made up of nanoparticles solvated in a molar excess of a first solvent (preferably a ketone such as acetone), a second solvent different than the first solvent (preferably an organic aryl solvent such as toluene) and a quantity of ligand moieties; the first solvent is then removed under vacuum and the ligand moieties ligate to the nanoparticles to give a second colloidal dispersion of the ligated nanoparticles solvated in the second solvent. If substantially monodispersed nanoparticles are desired, the second dispersion is subjected to a digestive ripening process.
    Type: Application
    Filed: October 15, 2001
    Publication date: April 17, 2003
    Applicant: KANSAS STATE UNIVERSITY RESEARCH FOUNDATION
    Inventors: Kenneth J. Klabunde, Savka Stoeva, Christopher Sorensen
  • Publication number: 20030059526
    Abstract: The present invention relates to patterned thin film electrochemical devices such as batteries on fibrous or ribbon-like substrates, as well as the design and manufacture of the same, for utilization in electrochemical cells, electronic devices, optical devices, synthetic multi-functional materials, and superconducting materials, as well as fiber reinforced composite material applications.
    Type: Application
    Filed: April 1, 2002
    Publication date: March 27, 2003
    Inventors: Martin H. Benson, Bernd J. Neudecker
  • Publication number: 20030059642
    Abstract: Solder compositions, solder pastes and methods of manufacturing thereof having a solder material coated with a coating material by an immersion coating process or an electroless plating process. The solder composition and solder pastes are substantially lead-free and have melting temperatures approaching those of traditional tin-lead solders.
    Type: Application
    Filed: September 27, 2001
    Publication date: March 27, 2003
    Inventor: Zequn Mei
  • Patent number: 6531304
    Abstract: The present invention relates to a process for modifying the dispersing properties of organometallic-prestabilized or organometallic-pretreated nanometal colloids by reacting reactive metal-carbon bonds in the protective shell to prepare nanometal colloids having a wide range of solubilities in hydrophilic and hydrophobic media including water, to the colloids thus prepared and their use.
    Type: Grant
    Filed: November 15, 2000
    Date of Patent: March 11, 2003
    Assignee: Studiengesellschaft Kohle mbH
    Inventors: Helmut Bönnemann, Werner Brijoux, Rainer Brinkmann
  • Patent number: 6528166
    Abstract: Nickel composite particles having a layer of a nickel-containing spinel on at least a part of the surface of nickel particles, or nickel composite particles having an oxide layer of metals other than nickel on at least a part of the surface of nickel particles and a layer of a nickel-containing spinel at an interface between the nickel particles and the metal oxide layer. The nickel composite particles are produced by forming fine liquid droplets from a solution containing (a) at least one thermally decomposable nickel compound and (b) at least one thermally decomposable metal compound capable of forming a spinel together with nickel; and heating the liquid droplets at a temperature higher than the decomposition temperatures of the compound (a) and (b) to nickel particles and simultaneously deposit a nickel-containing spinel layer, or further a metal oxide layer on the spinel layer.
    Type: Grant
    Filed: November 15, 2001
    Date of Patent: March 4, 2003
    Assignee: Shoei Chemical Inc.
    Inventors: Yuji Akimoto, Kazuro Nagashima, Hiroshi Yoshida, Yiyi Ma
  • Patent number: 6527843
    Abstract: Fine colored particles include a dye adsorbed on metal oxide fine particles having a nanometer size, and stabilized with an organic compound having an ionic group. Thus, fine colored particle having a nanometer size having good color properties, transparency and storage stability can be produced with high reproducibility.
    Type: Grant
    Filed: November 2, 2000
    Date of Patent: March 4, 2003
    Assignee: Kansai Research Institute, Inc.
    Inventors: Hiroaki Zaima, Hideo Matsui
  • Patent number: 6514575
    Abstract: Magnetic composites exhibit distinct flux properties due to gradient interfaces. The composites can be used to improve fuel cells and effect transport and separation of different species of materials. A variety of devices can be made utilizing the composites including a separator, a cell, an electrode for channeling flux of magnetic species, an electrode for effecting electrolysis of magnetic species, a system for channeling electrolyte species, a system for separating particles with different magnetic susceptibilities. Some composites can be used to make a dual sensor for distinguishing between two species of materials and a flux switch to regulate the flow of a redox species and a flux switch to regulate the flow of a chemical species. Some composites can control chemical species transport and distribution.
    Type: Grant
    Filed: June 8, 2001
    Date of Patent: February 4, 2003
    Assignee: University of Iowa Research Foundation
    Inventors: Johna Leddy, Sudath Amarasinghe