Vacuum Or Pressure Utilized Patents (Class 427/238)
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Patent number: 5378507Abstract: A continuous dry coating method and an apparatus therefor which are capable of removing cut chips and burrs from and smoothing inner walls of small-diameter holes in a substrate material and, then, successively performing a cold coating on these small holes in a short period of time. The continuous dry process coating method comprises the steps of: arranging electrodes on opposite sides of a substrate material; performing a plasma discharge to surface-treat small holes made in the substrate material; and then performing an electron cyclotron resonance plasma (ECR plasma) coating on the surfaces of these holes.Type: GrantFiled: June 4, 1993Date of Patent: January 3, 1995Assignees: Sakae Electronics Industrial Co., Ltd., Kazuo Ohba, Yoshinori Shima, Akira OhbaInventors: Kazuo Ohba, Yoshinori Shima, Akira Ohba
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Patent number: 5378510Abstract: A barrier coating is formed on a polymeric article, such as on the interior of a thermoplastic container. An oxidizing gas is converted to a plasma in a plasma chamber remote from the treatment chamber. The resulting plasma-activated oxidizing species are delivered to the interior of the container. An organosilicon reactant vapor is separately but simultaneously delivered to the interior of the container so that the organosilicon vapor and oxidizing active species mix within the container. An electric field is also applied to the container, so that the reaction products are deposited under the influence of the electrical field to form the barrier coating.Type: GrantFiled: February 15, 1994Date of Patent: January 3, 1995Assignee: Polar Materials Inc.Inventors: H. Ronald Thomas, Robert J. Babacz, Robert R. Newton
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Patent number: 5372862Abstract: A coating technique for beam tubes which employs a laser to ablate a target material and produce a plasma plume containing ions of the target material which adhere to the inner wall surface of the tube forming a thin film. The device employed in the coating process includes a pulse laser, a turning mirror used to direct the laser radiation, a window attached to tubing whose function is to evacuate the setup and to support a rail on which a carriage carrying the target material and optical elements for focusing the laser light onto the targets are mounted. During the coating process, the beam tube and the rail support tubes are evacuated to a lower pressure to remove ambient air. The apparatus is then filled with an inert gas. The laser is pulsed for a predetermined duration to ablate the target material for coating the vicinal surfaces of the beam tube.Type: GrantFiled: October 14, 1993Date of Patent: December 13, 1994Inventor: Jayaram Krishnaswamy
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Patent number: 5362526Abstract: A high pressure, high throughput, single wafer, semiconductor processing reactor is disclosed which is capable of thermal CVD, plasma-enhanced CVD, plasma-assisted etchback, plasma self-cleaning, and deposition topography modification by sputtering, either separately or as part of in-situ multiple step processing. The reactor includes cooperating arrays of interdigitated susceptor and wafer support fingers which collectively remove the wafer from a robot transfer blade and position the wafer with variable, controlled, close parallel spacing between the wafer and the chamber gas inlet manifold, then return the wafer to the blade. A combined RF/gas feed-through device protects against process gas leaks and applies RF energy to the gas inlet manifold without internal breakdown or deposition of the gas. The gas inlet manifold is adapted for providing uniform gas flow over the wafer.Type: GrantFiled: January 23, 1991Date of Patent: November 8, 1994Assignee: Applied Materials, Inc.Inventors: David N. Wang, John M. White, Kam S. Law, Cissy Leung, Salvador P. Umotoy, Kenneth S. Collins, John A. Adamik, Ilya Perlov, Dan Maydan
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Patent number: 5354586Abstract: A tubular liner for lining the inner wall of a pipe such as sewer pipe made up of a flexible tubular resin-absorbent fabric to be impregnated with a thermosetting liquid resin and a tubular plastic film welded on the external surface of the tubular resin-absorbent fabric; also disclosed are the methods for making such tubular liner and for impregnating such tubular liner with the thermosetting liquid resin, and in particular the impregnation method is characterized by using a plurality of vacuum suction hoses.Type: GrantFiled: December 7, 1992Date of Patent: October 11, 1994Assignees: Shonan Gosei-Jushi Seisakusho K.K., Yokoshima & Company, OAR Inc.Inventors: Yasuhiro Yokoshima, Hiroyuki Aoki
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Patent number: 5348764Abstract: An improved method for impregnating a tubular lining material with a hardenable liquid resin employed in a pipe repair operation by lining the pipe internally with the lining material; the method comprises (a) supplying about the same amounts of the same hardenable liquid resin to two mixing baths, (b) mixing the hardenable liquid resin with an agent to retard hardening and another agent selected from catalyst to facilitate hardening and hardener in one of the mixing baths, and, at the same time, mixing the hardenable liquid resin with a hardening accelerator in another one of the mixing baths, (c) supplying predetermined amounts of these mixtures to a static mixer from the respective mixing baths, (d) mixing these mixtures together in the static mixer to obtain a final mixture of hardenable resin, (e) supplying the final mixture to the tubular lining material, and (f) impregnating the tubular lining material with the final mixture.Type: GrantFiled: October 6, 1992Date of Patent: September 20, 1994Assignees: Yasuhiro Yokoshima, Minoru KamiyamaInventor: Yasuhiro Yokoshima
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Patent number: 5348774Abstract: Porous solid bodies, especially carbon bodies, are densified by chemical vapor deposition by establishing a thermal gradient within the body, thermally decomposing a gaseous precursor so deposit an electrically and thermally conductive deposit (e.g. carbon) within the body, and shifting the thermal gradient toward the lower temperature zone as deposition proceeds, by means of induction heating.Type: GrantFiled: August 11, 1993Date of Patent: September 20, 1994Assignee: AlliedSignal Inc.Inventors: Ilan Golecki, Robert C. Morris, Dave Narasimhan
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Patent number: 5344674Abstract: A composition is provided which, when applied to a metal surface, forms a corrosion-inhibiting film thereon. The composition comprises an epoxy resin, an effective amount of a curing agent for the epoxy resin, an alcohol, and a hydrocarbon diluent. The composition is applied by contacting the metal surface with the composition as one solution or as a hydrocarbon solution of the epoxy resin and a solution comprising the alcohol and the curing agent. The composition is particularly useful in the treatment of down-well metal surfaces in oil and gas wells to inhibit the corrosion of the metal.Type: GrantFiled: April 7, 1993Date of Patent: September 6, 1994Assignee: Phillips Petroleum CompanyInventor: Yulin Wu
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Patent number: 5336523Abstract: A method of applying a liquid coating material to the inside of a tank(10) and performing a hydrostatic pressure test on the tank at the same time. The method is useable for applying a liquid vitreous enamel coating material to a water heater tank, to be subsequently dried and furnace heated to form a glazed enamel internal coating. Preferably the hydrostatic pressure test is performed by displacing coating material from a portion(68) of an accumulator(51) by pumping liquid into a flexible bladder(66) housed in the accumulator. Pressure from pump(76) is transmitted to the tank(10 by the liquid coating material and held for a prescribed time interval to prove tank integrity. The method avoids excessive shear, hence viscosity changes in thixotropic coating materials.Type: GrantFiled: December 27, 1990Date of Patent: August 9, 1994Assignee: Rheem Australia LimitedInventors: Garry D. Chater, George Wilson
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Patent number: 5318805Abstract: A process has been developed for treating plastic and plastic composite materials wherein a protective epoxy coating is placed on said material by contacting with a composition comprising an epoxy resin, an effective amount of curing agent for the epoxy resin, an alcohol and a hydrocarbon solvent. In another embodiment, the protective epoxy coating is applied by a process comprising the sequential contacting of the plastic or plastic composite surface with a first hydrocarbon solution comprised of an epoxy resin and a hydrocarbon solvent, and a second hydrocarbon solution comprised of an alcohol, a curing agent, and a hydrocarbon solvent.Type: GrantFiled: December 10, 1992Date of Patent: June 7, 1994Assignee: Phillips Petroleum CompanyInventor: Yulin Wu
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Patent number: 5312489Abstract: Apparatus are disclosed for coating the inside surfaces of hollow objects with a coating material by vapor deposition wherein the objects are removably attached to a rotary fixture which is employed for holding the objects while the coating process is being conducted. The rotary fixture comprises a hollow chamber rotatably mounted about an axis of rotation wherein the chamber can have a plurality of connecting union assemblies which secure the objects and provide communication between the inside surfaces of the objects and the inside space of the hollow chamber. The coating material is introduced from the interior space of the hollow chamber to the interior space of the objects under vacuum conditions.Type: GrantFiled: September 30, 1993Date of Patent: May 17, 1994Assignee: Union Carbide Chemicals & Plastics Technology CorporationInventor: Roger A. Olson
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Patent number: 5306370Abstract: A method of fabricating thermal ink jet printheads comprises aligning and bonding a pair of silicon wafers together, which have, on opposing confronting surface thereof, a plurality of sets of linear arrays of heating elements and associated driver circuitry on one wafer surface and a plurality of sets of parallel grooves and a communicating reservoir for each set of grooves. The grooves and reservoirs are filled with a filler material which is solid or gels at room temperature and liquid at higher temperatures. The bonded pair of wafers are severed into a plurality of individual printhead sby dicing processes conducted at room temperature. One of the dicing processes cuts the grooves in a direction perpendicular thereto in order to form concurrently the nozzle face and nozzles. The solid filler material supports fragile edges of the wafers and prevents entry of dicing debris and other contaminants. The printheads are subjected to heat, spinning, and high pressure water spray to remove the filler material.Type: GrantFiled: November 2, 1992Date of Patent: April 26, 1994Assignee: Xerox CorporationInventors: Lawrence H. Herko, Robert P. Altavela, Joseph R. Weber, Robert M. White, Kathryn A. Wallace
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Patent number: 5288521Abstract: A process for the impregnation of workpieces of porous material and an apparatus to carry out the process are disclosed. The impregnation of workpieces is carried out in that, initially, all gas is withdrawn from the workpiece by evacuation, whereupon the workpiece is saturated with impregnating agent. Impregnation can be carried out in a very short period of time, if the workpieces are subjected to vibration during impregnation.Type: GrantFiled: February 20, 1992Date of Patent: February 22, 1994Inventor: Hubert Maldaner
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Patent number: 5266248Abstract: A method of producing a hydroxylapatite base porous beads filler for an organism, including mixing hydroxylapatite powder having particle sizes not larger than 125 .mu.m, in an amount ranging from 40 to 90% by weight, synthetic resin powder having particle sizes not larger than 74 .mu.m, in an amount ranging from 5 to 55% by weight, and resinous binder in an amount ranging from 0.5 to 5% by weight to obtain a mixture, granulating the mixture to form beads each having a diameter ranging from 0.03 to 25 mm, firing the beads at a temperature ranging from 900.degree. C. to 1180.degree. C. to form hydroxylapatite base porous beads, dipping the porous beads in a colloidal solution, removing air from the porous beads under vacuum, and filling the colloidal solution into the pores in the porous beads under pressure.Type: GrantFiled: October 13, 1992Date of Patent: November 30, 1993Inventors: Torao Ohtsuka, Makoto Fukaya, Hideo Tagai, Takayuri Kato, Shinpei Hashimoto, Kazuhiko Sawai, Tomokazu Hattori, Shigeo Niwa
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Patent number: 5254374Abstract: A method for producing reinforced ceramic composite articles by means of chemical vapor infiltration and deposition in which an inverted temperature gradient is utilized. Microwave energy is the source of heat for the process.Type: GrantFiled: April 8, 1992Date of Patent: October 19, 1993Assignee: The United States of America as represented by the United States Department of EnergyInventors: David J. Devlin, Robert P. Currier, Joseph R. Laia, Jr., Robert S. Barbero
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Patent number: 5254366Abstract: A method for treating tubulars, e.g. a pipeline, wherein an ungelled gelatin solution is mixed with fluids flowing through the tubular to deposit a treatment layer onto the wall of the tubular. The ungelled gelatin is injected into the flowing fluids at a temperature which is at or above the temperature of the fluids in the pipeline. This keeps the gelatin solution liquid (i.e. ungelled) even after mixing with the fluids. Gelatin derived from collagen is mixed with a liquid (e.g water) and heated. A separate treating solution (e.g. anti-freeze, corrosion inhibitor, and/or a drag reducer) can be added into the ungelled gelatin solution as it is mixed. The concentration of gelatin in the solution concentration of gelatin in said ungelled solution is the maximum amount which will allow the solution to remain ungelled at said the temperature of the flowing fluids.Type: GrantFiled: April 6, 1992Date of Patent: October 19, 1993Assignee: Atlantic Richfield CompanyInventor: Frank E. Lowther
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Patent number: 5254372Abstract: A method for plasma treatment of a predetermined portion of a substrate. The impedance of the coil and an established normal plasma is matched with the impedance of a power source, thereby maximizing the efficiency of the transfer of energy from the power source to the coil and producing a resonant plasma. The predetermined portion of the substrate is exposed to the resonant plasma for treatment. Additionally, a method for plasma treatment of a predetermined portion of the outside surface of a filament. The filament is trained through an inlet and exit of a plasma treatment chamber, through an inlet side tubular mask within the chamber, and through an exit side tubular mask within the chamber, each mask being adjustable within the chamber axially of the filament to expose a predetermined segment of the filament to plasma in the chamber while masking the remainder of the filament within the chamber from exposure to plasma.Type: GrantFiled: February 27, 1991Date of Patent: October 19, 1993Assignee: Nichols Technologies, Inc.Inventor: Michael F. Nichols
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Patent number: 5244654Abstract: Internal polymeric surfaces of medical devices are provided that have enhanced biocompatibility properties. The internal polymeric surface presents an anti-thrombogenic, fibrinolytic or thrombolytic interface with body fluids such as blood flowing through medical device tubing during implantation for medical procedures. The biocompatibility enhancing agent is secured to the polymeric substrate by a spacer molecule which is covalently bound to the internal polymeric surface which had been subjected to radiofrequency plasma treatment with a low pressure plasma medium of water vapor, oxygen or combination of water vapor and oxygen gas.Type: GrantFiled: June 25, 1991Date of Patent: September 14, 1993Assignee: Cordis CorporationInventor: Pallassana V. Narayanan
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Patent number: 5238710Abstract: A method for the production of ceramic matrix composites by chemical vapor infiltration. The method includes exposing an infiltrated preform to microwave energy, with pressure variation of the reactant gases in the processing chamber and/or temperature variation of the preform during processing, to produce substantially improved composites. The process provides higher deposition rates within the core of the ceramic matrix composite, higher densification which advantageously initiates within the interior of the ceramic matrix composite and proceeds radially outward, and a thick wall ceramic matrix composite with an overall reduced density gradient.Type: GrantFiled: March 30, 1992Date of Patent: August 24, 1993Assignee: Technology Assessment & Transfer, Inc.Inventors: Iftikhar Ahmad, Edward L. Paquette, Richard Silberglitt
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Patent number: 5232741Abstract: A composition is provided which, when applied to a metal surface, forms a corrosion-inhibiting film thereon. The composition comprises an epoxy resin, an effective amount of a curing agent for the epoxy resin, an alcohol, and a hydrocarbon diluent. The composition is applied by contacting the metal surface with the composition as one solution or as a hydrocarbon solution of the epoxy resin and a solution comprising the alcohol and the curing agent. The composition is particularly useful in the treatment of down-well metal surface in oil and gas wells to inhibit the corrosion of the metal.Type: GrantFiled: September 26, 1991Date of Patent: August 3, 1993Assignee: Phillips Petroleum CompanyInventor: Yulin Wu
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Patent number: 5230842Abstract: To rehabilitate an internally corroded underground pipeline, excavations are made at its opposite ends to which launching and receiving pipe structures are then secured. Various pig member sets, with appropriate treatment fluids carried thereby, are air-driven through the entire length of the pipeline to successively acid clean, etch, and neutralize its interior surface. The interior pipeline surface is then thoroughly dried by flowing dehydrated air through the pipeline. Specially designed leading and trailing extruder pigs, with 100% solid, high viscosity, solvent-free epoxy coating material therebetween, are then air-driven through the pipeline to extrude a first protective coating layer onto its interior surface. The first layer is then dried with dehydrated air.Type: GrantFiled: October 4, 1991Date of Patent: July 27, 1993Inventor: Bruce A. Munde
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Patent number: 5225252Abstract: A glass vacuum flask coating method comprising a step to put a metal material in the gap between an inner flask and an outer flask before said inner and outer flasks being formed into a blank for a glass vacuum flask, after the process of exhausting and tipping-off said metal material being heated by a magnetic field generated from an inductance coil into a metal vapor inside said gap, permitting said metal vapor to be adhered to the glass surface inside said gap, forming into a metal reflecting film thereon.Type: GrantFiled: January 23, 1992Date of Patent: July 6, 1993Inventors: Ming-Wen Chang, Yu-Cheng Chuang
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Patent number: 5223308Abstract: A method for the low temperature, microwave enhanced, chemical vacuum deposition of thin film material onto a surface of a hollow member by creating a sub-atmospheric pressure condition adjacent the surface to be coated while maintaining the applicator through which microwave energy is introduced at substantially atmospheric pressure.Type: GrantFiled: October 18, 1991Date of Patent: June 29, 1993Assignee: Energy Conversion Devices, Inc.Inventor: Joachim Doehler
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Patent number: 5221355Abstract: An apparatus for forming a high purity silicon carbide film on the inner surface of a cylindrical member by a chemical vapor phase deposition process is provided. The member to be coated is received in a reaction vessel and heated by a heating means. The apparatus includes a gas feed conduit having a distal end disposed for axial motion within the member, for feeding a source gas containing a carbon source and a silicon source into the interior of the member, and a gas discharge conduit having a distal end disposed for axial motion within the member, for discharging used reaction gases from within the member. The gas feed and discharge conduits are moved so that their distal ends move through the member in unison to continuously move the reaction region.Type: GrantFiled: October 16, 1992Date of Patent: June 22, 1993Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Toshiyasu Ohashi, Yoshihiro Kubota, Kesazi Harada, Takesi Satoh
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Patent number: 5219614Abstract: The present invention provides a method capable of lining a multibranch piping with a coating material within the pot life of the coating material without leaving an area uncoated or having to apply excessive repeated coatings. Lining of a main pipe is performed by pouring the coating material into the main pipe from an end portion of the pipe, and the lining of branch pipes is effected by the feed of the coating material and air for each of the branch pipes. A completed time point of lining in each branch pipe is detected by any one of the following methods:(A) A method wherein the time required for lining a branch pipe is estimated in advance and upon lapse of the estimated time it is determined that the lining of the branch pipe was completed.Type: GrantFiled: April 22, 1992Date of Patent: June 15, 1993Assignee: Mitsui Petrochemical Industries, Ltd.Inventors: Masato Kawazoe, Takaharu Tomoyasu
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Patent number: 5215781Abstract: An ablating gelatin pig for use in tubulars which can easily negotiate the bends, etc in a tubular. Due to the properties of gelatin, the pig will ablate thereby depositing a protective layer onto the wall of the tubular. The pig can be molded outside the tubular or it can be formed in situ. The pig is formed by mixing common gelatin with a heated liquid and then allowing the mixture to cool to ambient temperature. Preferably, the liquid includes a treating solution (e.g. corrosion inhibitor, drag reducer, etc ) which is to be used to treat the pipeline. In some applications, a slug of the treating solution is also passed through the pipeline between two ablating gelatin pigs. For high temperatures applications, a hardener may be added to the pig to increase the melting temperature of the pig and/or a slug of the hardener can also be passed through the pipeline between two ablating gelatin pigs if necessary.Type: GrantFiled: March 16, 1992Date of Patent: June 1, 1993Assignee: Atlantic Richfield CompanyInventor: Frank E. Lowther
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Patent number: 5212000Abstract: This invention provides a method for providing a functionalized inner skin on the lumen-defining surface of a hollow tube using either a Newtonian coating fluid used in combination with a relatively non-Newtonian plug fluid, or a non-Newtonian coating fluid (optionally in combination with a more non-Newtonian plug fluid). This invention enables the facile provision of a functionalized inner skin on the lumen-defining surface of tubes previously deemed difficult to coat, e.g., tubes wherein the inner diameter varies along the length of the tubes, tubes having elliptical or irregular cross-sectional configurations, branched tubes, and tubes having lumens of small diameter, e.g. tubes useful in membrane applications. Preferably, the coating will be dried or crosslinked to promote sustained adhesion and/or to increase the functionality of the coating.Type: GrantFiled: March 11, 1991Date of Patent: May 18, 1993Assignee: The Dow Chemical CompanyInventors: Gene D. Rose, Donald L. Schmidt, William J. Settineri
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Patent number: 5207292Abstract: A process for simultaneously lubricating the interior wall of a underground conduit, while by use of compressed air, placing in the conduit a cable along the entire length of the conduit. The cable is drawn through the conduit by a puller, or comparable device, which is connected to the head of the cable, and rests in the conduit in a substantially air tight relation. This puller transmits a traction force to draw the cable through the conduit. The internal surface of the conduit is lubricated substantially uniformly over the entire length as the puller travels along the conduit by means of a reservoir of lubricant of a variable volume. This reservoir is at the rear of the puller, but in front of the cable. The lubrication and placement of the cable is along the entire length of the conduit. The invention also concerns an apparatus for carrying this process.Type: GrantFiled: January 28, 1992Date of Patent: May 4, 1993Assignee: France Telecom Etablissement autonome de droit publicInventors: Alain Pecot, Yvon Beaumanoir
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Patent number: 5205886Abstract: An improved method of inserting a liner into a metallic pipeline is disclosed. The liner is formed from a plurality of concentric tubes that are enveloped in a flexible, expansible, tear resistant material. When the concentric tubes are pulled into the pipeline, the tear resistant material provides protection against tearing of the tubes by burrs, snags or other imperfections on the inside of the metallic pipeline. The tear resistant material may be a fabric, woven material or mesh. Materials having a structure that permits escape of fluid entrapped during subsequent expansion of the concentric tubes on formation of the liner are preferred. The method permits the lining of pipeline sections that have bends, loops or the like, while protecting the liner from tearing during insertion into the pipeline.Type: GrantFiled: June 12, 1992Date of Patent: April 27, 1993Assignee: Du Pont Canada Inc.Inventor: George White
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Patent number: 5205903Abstract: A process for producing a honeycomb structure-extruding die by etching a surface of a base material for a honeycomb structure-extruding die with a gas, and coating the etched base material by CVD before an oxidized film is formed after the etching.Type: GrantFiled: January 9, 1992Date of Patent: April 27, 1993Assignee: NGK Insulators, Ltd.Inventors: Kazuo Suzuki, Kenji Arai, Masayuki Matsuzaki
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Patent number: 5204141Abstract: Process for depositing films of silicon dioxide by a low pressure CVD method, utilizing 1,4 disilabutane as the silicon precursor and molecular oxygen as the oxygen source. The deposition process permits films to be put down on a substrate at temperatures as low as 100.degree. C. with essentially no carbon in the film. The 1,4 disilabutane can be used as a substitute for silane, a toxic, pyrophoric compressed gas.Type: GrantFiled: September 18, 1991Date of Patent: April 20, 1993Assignee: Air Products and Chemicals, Inc.Inventors: David A. Roberts, Arthur K. Hochberg
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Patent number: 5202157Abstract: The present invention relates to an improvement in a lining method for internal surfaces of pipes in multi-branched pipings such as water pipes, gas pipes, etc. in which a plurality of branched pipelines are branched from a main pipeline, and particularly to a shaping method for a lining surface.In a multi-branched piping in which a plurality of branched pipelines are branched from a main pipeline, a coating is poured into a pipeline from one end of a main pipeline or each of the branched pipelines, gas is then fed to thereby line the internal surface of the pipeline, a sponge consisting of an elastic foam body having a larger diameter than the inside diameter of the pipe constituting the pipeline, said foam body being made of synthetic resin and having a continuous foam, is inserted from an end of each branched pipeline, and the sponge is then pushed with the aid of air pressure whereby the lining surface can be shaped to have substantially uniform film thickness.Type: GrantFiled: August 23, 1991Date of Patent: April 13, 1993Assignee: Mitsui Petrochemical Industries, Ltd.Inventors: Takaharu Tomoyasu, Kanji Miyamoto
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Patent number: 5178724Abstract: A method of making a double-walled vacuum container includes the steps of forming a double-walled container from gas-impermeable, radiation transmissive material with spaced-apart inner and outer walls that enclose an interior volume with a lacuna between the inner and outer walls; coating surfaces of the container walls that face the lacuna with a reflective coating; positioning the container in proximity to a source of coherent radiant energy; and removing selected portions of the reflective coating by impinging coherent radiant energy on portions of the reflective coating selected for removal.Type: GrantFiled: September 12, 1991Date of Patent: January 12, 1993Assignee: Eagle Flask, Inc.Inventor: Riaz A. Padamsee
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Patent number: 5175017Abstract: In forming a metal or metal silicide film by CVD, a fluorosilane is used as a reaction gas, or a fluoro-silane is added to a source gas. Examples of the metal halide used in the present invention include fluorides and chlorides of tungsten, molybdenum, titanium, tantalum and niobium. Among them, fluorides of tungsten and molybdenum are more desirable particularly from the viewpoint of the availability of the deposited metal or metal silicide. It is preferred that the source gases, i.e. silane series gas and metal halide, be diluted with a carrier gas such as nitrogen, hydrogen, helium or argon, and this is also true of the fluoro-silane. The total pressure is preferably 0.01 to 10 Torr. The reaction temperature is desirably 200.degree. to 800.degree. C., more desirably 300.degree. to 500.degree. C. Plasma CVD instead of thermal CVD may be employed for the purpose of lowering the reaction temperature.Type: GrantFiled: January 28, 1991Date of Patent: December 29, 1992Assignee: Hitachi, Ltd.Inventors: Nobuyoshi Kobayashi, Hidekazu Goto, Masayuki Suzuki, Yoshio Homma, Natsuki Yokoyama
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Patent number: 5173325Abstract: A method and apparatus for spraying a solid particulate powder onto the interior surface of tubular articles by intermittently pumping the powder from a fluidized bed of powder through a powder supply line containing an intermittently operated venturi pump and air amplifier, as well as a pair of constantly operated air diffusers and an electrostatic charging apparatus. A powder collection shroud adjacent at least one open end of the tubular article has a carefully regulated vacuum applied thereto in order to collect oversprayed powders.Type: GrantFiled: October 4, 1990Date of Patent: December 22, 1992Assignee: Nordson CorporationInventors: Alan J. Knobbe, Joseph A. E. Pintelon, Daniel Pinault
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Patent number: 5167901Abstract: In a tube eversion apparatus a first chamber in which the eversion pressure is developed is controllably sealed by a sphincter-type valve, the valve being in turn actuated by pressure developed in a preferably separately controllable and adjustable second chamber, another chamber preferably being provided above the sphincter-type valve for containing a supply of liquid and limiting turbulence from any escape of fluid past the sphincter-type valve, the other chamber also providing apparatus for supplying heated fluid to a lay-flat hose adapted to be pulled through the sphincter-type valve by the tube being exerted. Use of the improved apparatus involves appropriate modifications of the usual eversion process involving applying and controlling the everting pressure and the pressure exerted against the sphincter-type valve by the fluid in the second chamber.Type: GrantFiled: February 25, 1992Date of Patent: December 1, 1992Inventors: F. Thomas Driver, Joseph A. Alexander, Lloyd G. Buchanan
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Patent number: 5165970Abstract: A method for the uniform coating of honeycomb bodies with finely divided solid matter from a dispersion in an amount which is below that which arises during customary immersion. To this end, the honeycomb is flooded from below with dispersion, emptied after a dwell time and blown out. Filling time, filling amount, dwell time emptying time as well as the time between emptying and blowing out are measured in such a manner that in order to increase the separated amount of solid matter, filling time, dwell time, pumping-out time and the time between emptying and blowing out are increased but the filling amount is reduced.Type: GrantFiled: February 27, 1991Date of Patent: November 24, 1992Assignee: Degussa AktiengesellschaftInventors: Felix Schmidt, Wilfried Baumgartner, Reinhard Manner, Gerhard Birtigh, Ewald Dittrich
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Patent number: 5132057Abstract: In a blood gas sensing probe, a cylindrical sleeve contains an optical fiber. The end of the optical fiber is withdrawn into the sleeve thereby creating a receptacle at the end of the sleeve. A sensitive dye, HOPSA for example, is encapsulated in a gel and deposited in the receptacle to form the probe. In making the probe, the end of the optical fiber is in the same plane as the end of the sleeve in which it is placed. The dye and gel contact the combined ends of optical fiber and sleeve. The fiber is withdrawn into the sleeve thereby creating a vacuum which is filled by the dye and gel.Type: GrantFiled: April 22, 1991Date of Patent: July 21, 1992Assignee: Medex, Inc.Inventors: Dennis M. Tomisaka, John C. Toomey
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Patent number: 5124014Abstract: A method of forming silicon dioxide layers by bias ECR is described. The layers are formed by reacting oxygen with TEOS or TMCTS. High-quality, void-free layerc can be formed over conductor patterns having high-aspect-ratio intermetallic spacings.Type: GrantFiled: April 11, 1991Date of Patent: June 23, 1992Assignee: AT&T Bell LaboratoriesInventors: Pang-Dow Foo, Ajit S. Manocha, John F. Miner, Chien-Shing Pai
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Patent number: 5116451Abstract: According to the invention, a method and system of injecting material into a wound filament items such as a fiber optic canister is provided. The method is useful with a canister which, when dry wound, has at least one channel formed therein.In one aspect, the method includes the step of injecting adhesive into the channel to impregnate the canister with adhesive. In another aspect, the method includes the additional step of discharging adhesive from a second channel to remove excess adhesive from the canister. The method may also include the step of circulating air through the two channels to purge excess adhesive and solvent.Type: GrantFiled: August 29, 1990Date of Patent: May 26, 1992Assignee: Hughes Aircraft CompanyInventor: George W. LeCompte
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Patent number: 5091218Abstract: A method of producing a metallized pattern on a substrate includes the steps of providing a substrate having a high aspect ratio groove defining a desired metallization pattern and applying metallization to the substrate. The high aspect ratio groove is utilized to prevent metallization across the groove boundary thereby producing electrically isolated areas. The substrate can be a circuit board, hybrid module or other component carrying structure. Also the substrate can be a resonator or a stripline device in which the groove is used to electrially isolate a lead or wire extending from the substrate in the ground plane portion of the structure.Type: GrantFiled: August 16, 1990Date of Patent: February 25, 1992Assignee: Motorola, Inc.Inventors: Leonard F. Altman, Dale W. Dorinski
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Patent number: 5089297Abstract: Liquefied resin is supplied into a pipeline having a branch pipe from an end. Mass of the resin is moved by compressed air passing through the pipeline at constant speed, thereby lining inner walls of the pipeline and branch pipe with the resin.Type: GrantFiled: November 2, 1990Date of Patent: February 18, 1992Assignee: Hakko Co., Ltd.Inventors: Motoyuki Koga, Nobukatsu Ike, Kenji Ohshima
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Patent number: 5073405Abstract: An electrode is deposited on a support by providing a porous ceramic support tube (10) having an open end (14) and closed end (16); masking at least one circumferential interior band (18 and 18') inside the tube; evacuating air from the tube by an evacuation system (30), to provide a permeability gradient between the masked part (18 and 18') and unmasked part (20) of the tube; applying a liquid dispersion of solid electrode particles to the outside surface of the support tube, where liquid flows through the wall, forming a uniform coating (42) over the unmasked support part (20) and a tapered coating over the masked part (18 and 18').Type: GrantFiled: January 15, 1991Date of Patent: December 17, 1991Assignee: Westinghouse Electric Corp.Inventors: Theodore R. Vasilow, Gregory E. Zymboly
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Patent number: 5063178Abstract: A blood chemical sensor has a blood gas sensitive dye contained in a hydrogel matrix, the combination of dye and gel being mounted on the end of an optical fiber. The hydrogel is freeze-dried to facilitate packaging and handling.Type: GrantFiled: March 19, 1990Date of Patent: November 5, 1991Assignee: Medex, Inc.Inventor: John C. Toomey
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Patent number: 5059231Abstract: For producing a fiberoptic waveguide preforms by plasma pulse-induced chemical vapor deposition (PICVD), blank glass tubes are prepared having a continuously increasing internal diameter in the direction of gas flow. This type of blank compensates for the otherwise occurring decrease in the density of the layer-forming molecules due to pressure drop, thereby permitting the formation of a uniform masswise deposition of layer-forming molecules along the length of the tube. This permits the production of collapsed preforms having a series of coating layers of substantially uniform thickness.Type: GrantFiled: September 12, 1989Date of Patent: October 22, 1991Assignee: Schott GlaswerkeInventors: Ulrich Ackermann, Hartmut Bauch, Volker Paquet
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Patent number: 5045352Abstract: A method of cleaning and coating water conducting pipes is provided wherein a mixture of water and compressed air is forced through the emptied pipe system to rough clean such system, a pressurized acid is introduced into the pipe system and allowed to react with the interior surface of the pipes for a predetermined period of time. The acid is then drained from the pipes, and the interior of the pipes is dried by compressed air. A pressurized liquid plastic is then introduced into the pipes to coat the pipes with the excess plastic being subsequently drained from the pipe system.Type: GrantFiled: February 3, 1989Date of Patent: September 3, 1991Inventor: Karl Mueller
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Patent number: 5043182Abstract: A method for the production of ceramic-metal composite materials, in which ceramic materials are infiltrated with molten metal, includes building up a porous ceramic material of several layers by spraying on a base body, the thickness of the layers being between 10 and 150 microns with an average pore radius of between 100 and 1,000 nm, an open porosity of 5-14% and an overall porosity of 5-30%; and filling molten metal into the pore volume up to a residual pore volume of 0.1 to 10%, based on the initial porosity. In an alternate embodiment, a gradient structure of the ceramic is created by increasing or decreasing the particle size of the ceramic material while spraying layers. In the gradient structure, infiltration of molten metal is greatest in the layers sprayed with particles having the largest diameter.Type: GrantFiled: April 25, 1990Date of Patent: August 27, 1991Assignee: Vereinigte Aluminum-Werke AktiengesellschaftInventors: Werner Schultze, Stefan Schindler, Friedrich-Ulf Deisenroth
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Patent number: 5021270Abstract: The moisture or water vapor barrier protection of a composite pressure vessel suitable for use as a composite cased solid propellant rocket motor is improved by immersing the pressure vessel, during pressure testing thereof, in a curable liquid polymer solution, optionally containing electrically conductive material such as metallic flakes or powder, so that the solution may flow into open voids, cracks or fractures in the pressure vessel and subsequently curing the curable liquid polymer in said voids, cracks or fractures.Type: GrantFiled: December 11, 1989Date of Patent: June 4, 1991Assignee: Thiokol CorporationInventors: Robert E. Black, Jr., Don C. Carson, Frederick W. Van Name
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Patent number: 5009930Abstract: A method whereby the thickness distribution of a vapor deposited layer, such as an interference filter deposited on a skirted substrate such as a glass faceplate for a projection television tube, is improved by shielding the substrate from indirect flux of vapor so as to reduce the shadowing effect of the skirt upon the thickness distribution of the deposited layer, thereby improving the white field uniformity of the resultant projection image.Type: GrantFiled: December 8, 1989Date of Patent: April 23, 1991Assignee: North American Philips CorporationInventor: Matthew S. Brennesholtz
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Patent number: 4987001Abstract: A method and apparatus for spraying a solid particulate powder onto the interior surface of tubular articles by intermittently pumping the powder from a fluidized bed of powder through a powder supply line containing an intermittently operated venturi pump and air amplifier, as well as a pair of constantly operated air diffusers and an electrostatic charging apparatus. A powder collection shroud adjacent at least one open end of the tubular article has a carefully regulated vacuum applied thereto in order to collect oversprayed powders.Type: GrantFiled: February 9, 1989Date of Patent: January 22, 1991Assignee: Nordson CorporationInventors: Alan J. Knobbe, Joseph A. E. Pintelon, Daniel Pinault