Metal Coating Patents (Class 427/319)
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Patent number: 4410564Abstract: A method for fabricating heat emitting plates permits such plates to be designed to have a wide variety of thermal emission characteristics. A metal plate is coated with dielectric material on both sides and then heated to 300.degree. to 400.degree. C. at which point it is sprayed by a molten conductive metal. The thickness of the molten conductive metal on the dielectric coating can be varied along the length of the plate by varying the speed of the mutual displacement between the spraying means and the plate during the spraying operation. A protective pattern is painted or otherwise deposited on the sprayed metal which is then subjected to a corrosive bath to eliminate all of the sprayed metal except that which is overlaid by the protective coating. The protective coating is then removed leaving a heating element of desired configuration to achieve the desired thermal emission characteristics of the plate.Type: GrantFiled: October 19, 1981Date of Patent: October 18, 1983Assignee: Raivi S.A.Inventor: Joaquin F. Cenefels
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Patent number: 4408561Abstract: A dual-purpose production plant for cold rolled steel sheets and hot-dip galvanized steel sheets having, successively disposed in series, a heating zone, a soaking zone, a primary cooling zone, an overaging zone equipped with a controlled cooling facility, a molten galvanizing zone, an intermediate cooling means, a secondary cooling zone, a temper rolling means, and a chemical treatment means, and a bypass for directly connecting the overaging zone and the secondary cooling zone with each other.Type: GrantFiled: August 24, 1981Date of Patent: October 11, 1983Assignee: Nippon Steel CorporationInventors: Hideo Yokoyama, Ichiro Shimbashi, Koichi Sakurai, Munetsugu Matsuo
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Patent number: 4397893Abstract: A system is described for coating a cylindrical surface of a long thin workpiece by a process which includes flame spray coating that heats the workpiece to a large portion of its melting temperature and which is followed by grinding of the coated cylindrical surface, which produces a final coated surface of more uniform coating thickness than heretofore. The workpiece is rotated about a vertical axis, to avoid slight bending deformation of it, the upper end of the workpiece is allowed to move slightly towards and away from its opposite end, and an upward bias is applied to the chuck device that engages the upper end of the rotating workpiece to avoid column-like buckling of it.Type: GrantFiled: September 8, 1981Date of Patent: August 9, 1983Inventor: Clifford C. Bottoms
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Patent number: 4380560Abstract: A process for treating food and beverage containers comprised of low-carbon steel sheet (black plate) to improve the adherence and to resist undercutting of organic can lacquers applied to the surfaces thereof when subjected to agressive environments without visually impairing the light-grey shiny steel appearance of the container surface and without loss of humidity resistance. The treatment can readily be integrated with conventional can body manufacturing procedures and includes contacting the cleaned black plate container body surface with an aqueous acidic solution containing a controlled amount of stannous ions at a controlled temperature for a period of time sufficient to deposit tin on the surfaces thereof in an amount up to about 5 mg/ft.sup.2 followed by rinsing, drying and lacquering.Type: GrantFiled: December 17, 1981Date of Patent: April 19, 1983Assignee: Occidental Chemical CorporationInventor: Peter F. King
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Patent number: 4357365Abstract: A continuous wire coating method is described which features a reaction chamber wherein a volatilized refractory metal compound is thermally decomposed to deposit said refractory metal as a coating on a refractory metal wire during passage through said reaction chamber. A substantially uniform thickness coating of the refractory metal is deposited in passing the refractory metal wire through said reaction chamber in a substantially vertical direction. The nature of said coating substantially precludes any subsequent thermal migration of the refractory metal in the wire core.Type: GrantFiled: March 26, 1981Date of Patent: November 2, 1982Assignee: General Electric CompanyInventor: Lewis V. McCarty
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Patent number: 4350719Abstract: Ferrous metal or titanium or aluminum is coated with a mixture of phosphoric acid, chromic acid and magnesium salts of these acids, as well as with aluminum flakes, or coated with a mixture of aluminum flakes and magnesium chromate or dichromate, to provide after baking excellent resistance to attack. Aluminum-silicon alloys containing about 10 to about 15 weight percent silicon give better results than ordinary aluminum, particularly when the aluminum is in powder form; and when coated products are given a burnishing treatment. Very good masking for pack diffusion aluminizing or chromizing on any metal to keep portions from being diffusion coated is effected by localized coating, the lowest layer of which is depletion-reducing. The upper coating layer can be of non-contaminating particles like nickel or Cr.sub.2 O.sub.3 that upon aluminizing or chromizing become coherently held together to form a secure sheath. Such sheath can also be used for holding localized diffusion-coating layer in place.Type: GrantFiled: February 26, 1981Date of Patent: September 21, 1982Assignee: Alloy Surfaces Company, Inc.Inventor: Alfonso L. Baldi
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Patent number: 4348263Abstract: Substrates for use in electrical contacts are prepared prior to plating by rapid surface melting by means of a laser beam or an electron beam. Improved microscopic surface characteristics are obtained. In a preferred embodiment, improved macroscopic surface roughness characteristics are also obtained by shorter-duration melting, typically by means of a pulsed YAG laser. Gold which has been electroplated onto copper alloys prepared by this technique has shown improved resistance to sulfur and chlorine corrosive atmospheres. This allows, for example, a thinner layer of a protective metal to be used to obtain a given degree of protection.Type: GrantFiled: September 12, 1980Date of Patent: September 7, 1982Assignees: Western Electric Company, Inc., Bell Telephone Laboratories, IncorporatedInventors: Clifton W. Draper, Satya P. Sharma
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Patent number: 4343836Abstract: A problem addressed by this invention was how to obtain very long lengths of refractory metal-coated multifilamentary yarns having a uniform coating on the filaments which make up each yarn, the coating being uniform throughout the length of the yarn such that the coated yarns are suitable for being woven and are suitable for a variety of other uses. The solution is a continuous process which employs a chemical vapor deposition reaction at relatively low temperature and pressure and a separation of the gaseous reaction products from the coated yarn prior to allowing the coated yarn to cool.Type: GrantFiled: July 26, 1979Date of Patent: August 10, 1982Assignee: United States of America as represented by the United States Department of EnergyInventors: Lawrence R. Newkirk, Flavio Valencia, Robert E. Riley, Terry C. Wallace, Sr.
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Patent number: 4330574Abstract: A finishing method and apparatus for conventional continuous hot-dip coating of the type wherein a ferrous base metal strip is caused to pass beneath the surface of a coating bath of molten coating metal and is thereafter subjected to jet finishing, the ferrous base metal strip having been appropriately pretreated so as to be at the proper coating temperature and so as to have its surfaces oxide-free when passing through the bath of molten coating metal. The method comprises the steps of providing an enclosure for the two-side coated strip as it exits the coating bath, locating a finishing jet nozzle to either side of the coated strip within the enclosure, jet finishing the coated strip with a non-oxidizing or inert gas. The apparatus comprises the above mentioned enclosure with the jet finishing nozzles located therein and an appropriate system to provide a non-oxidizing or inert atmosphere within the enclosure.Type: GrantFiled: September 29, 1980Date of Patent: May 18, 1982Assignee: Armco Inc.Inventors: Marvin B. Pierson, Charles Flinchum
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Method of and apparatus for the cladding of steel sheet or strip with lower melting metals or alloys
Patent number: 4321289Abstract: A cladding process and apparatus in which steel strip or sheet is cladded with a metal of lower melting point, e.g. lead, by maintaining a bank of constant level of the molten cladding material between a belt and the strip or sheet substrate which passes along an inclined path and is cooled to harden the molten material thereon. During the cooling process the applied material is compressed against the substrate.Type: GrantFiled: August 22, 1980Date of Patent: March 23, 1982Assignee: Norddeutsche Affinerie AktiengesellschaftInventor: Adalbert Bartsch -
Patent number: 4312894Abstract: Method for hard-facing substrates is disclosed using a hard facing material consisting essentially of at least one vanadium carbide. In a particular embodiment of the invention tungsten is present in the hard facing material in solid solution with vanadium carbide.Type: GrantFiled: June 13, 1980Date of Patent: January 26, 1982Assignee: Union Carbide CorporationInventors: Harry J. Brown, William D. Forgeng, Charles M. Brown
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Patent number: 4309460Abstract: A process is described for producing devices and articles with gold films made by gold evaporation in which certain fluoride compounds are used to insure good adhesion of the gold film to the substrate. The process is particularly applicable to the production of gold films on non-metallic surfaces such as ceramic and glass surfaces. This procedure not only insures better adhesion of the gold film to the surface, but also permits greater processing variations without adversely affecting film adhesion.Type: GrantFiled: October 14, 1980Date of Patent: January 5, 1982Assignee: Bell Telephone Laboratories, IncorporatedInventors: Shobha Singh, LeGrand G. Van Uitert, George J. Zydzik
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Patent number: 4299860Abstract: A method of impregnating the surface of a metal substrate with wear resist particles to impart wear resisting characteristics to the surface. The substrate surface is subjected to a relatively moving high-powered laser beam to cause localized surface melting in passes thereacross, and hard wear resistant particles are forcibly velocity injected into the melt. The particles are captured upon solidification of the melt pool and retained therein by metallurgical bond. A wear resistant layer is formed which is an integral part of the underlying material.Type: GrantFiled: September 8, 1980Date of Patent: November 10, 1981Assignee: The United States of America as represented by the Secretary of the NavyInventors: Robert J. Schaefer, Jack D. Ayers, Thomas R. Tucker
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Patent number: 4297398Abstract: Steel strip is dipped in a molten metal bath (e.g. Al-Zn) maintained at above 500.degree. C., cooled to solidify the metal coating, and then cooled to below 475.degree. C. by an intense and rapid cooling operation which does not impair the flatness of the strip, e.g. immersion in a hot aqueous bath or spraying a mist. Before hot-dipping, the steel strip is preferably recrystallisation annealed and cooled to a temperature not lower than that of the molten metal bath.Type: GrantFiled: March 3, 1980Date of Patent: October 27, 1981Assignee: Centre de Recherches Metallurgiques-Centrum voor Research in de MetallurgieInventor: Philippe Paulus
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Patent number: 4259365Abstract: Sodium nitrite in liquid form is deposited on a substrate and allowed to crystallize thereby forming a thin layer on the substrate. The substrate is either dipped into a solution containing sodium nitrite or into sodium nitrite in the molten state and then pulled out again. Subsequent drying or cooling of the wetted substrate top surface causes the crystalline film to form. Alternatively, sodium nitrite in a liquid state is applied to the top surface of the substrate and the substrate is rotated to assure an even distribution of the sodium nitrite. Again, drying or cooling causes the crystalline layer to form. The so manufactured unit is shown as part of a pyroelectric radiation detector, as image receiver in a television camera tube and as the storage element in a field effect transistor arrangement.Type: GrantFiled: March 2, 1978Date of Patent: March 31, 1981Inventors: Wolfgang Ruppel, Ullrich Hetzler, Horst Vogt, Peter Wurfel
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Patent number: 4254164Abstract: A method is disclosed for depositing a thick layer of copper upon a copper base wherein the base is heated and flame sprayed with molten copper until globules are observed. The globules are mechanically removed from the base and the flame spraying and globules removing steps repeated.Type: GrantFiled: July 6, 1979Date of Patent: March 3, 1981Assignee: Nassau Recycle CorporationInventors: Mieczyslaw Budzich, Forest G. Fitz, Jr.
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Patent number: 4242368Abstract: An improved method for manufacturing a composite metal wire including a core metal wire having extruded therearound a coating metal layer which is different in material from the core metal wire, includes feeding the coating metal into a narrow passageway which is defined between a circumferential groove formed on the outer edge of a rotary wheel and a close fitting surface of a fixed shoe block, carrying the coating metal towards an outlet end of the passageway by frictional drag with the surface of the passageway in accordance with the rotation of the wheel, and passing a core metal wire harder in material than the coating metal through a covering chamber of a larger cross sectional area which is provided with a die and a nipple at the front and rear portions, respectively, whereby the core metal wire is covered with the coating metal in the covering chamber so that a predetermined construction of a composite metal wire is extruded through the die.Type: GrantFiled: April 25, 1978Date of Patent: December 30, 1980Assignee: Hitachi Cable, Ltd.Inventors: Masahiro Nagai, Yasuhiko Miyake
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Patent number: 4230257Abstract: A method of and apparatus for applying beads of solder to a metallic plate as an integral part thereof for subsequent attachment to another component in an assembly operation.Type: GrantFiled: December 1, 1978Date of Patent: October 28, 1980Assignee: Libbey-Owens-Ford CompanyInventor: Charles W. Genson
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Patent number: 4221832Abstract: Metal strip, particularly steel strip, is heated above 300.degree. C. and immersed in a coating bath whose temperature is at least 80.degree. C. and which contains at least one metal salt, the strip being coated with a metal layer, e.g. Ni-based or Cr-based, by the coating bath.Type: GrantFiled: March 13, 1979Date of Patent: September 9, 1980Assignee: Centre de Recherches Metallurgiques-Centrum voor Research in de MetallurgieInventors: Paulus Philippe, Leroy Vincent, Henri Graas
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Patent number: 4214015Abstract: Method for coating metal substrates with alloys wherein the substrates are at a temperature above 500.degree. C. The coating process is interrupted temporarily at least once and the substrates are allowed to cool by at least 30.degree. C. Before the beginning of or during the resumed coating process, the substrate temperature is substantially restored.Type: GrantFiled: November 15, 1978Date of Patent: July 22, 1980Assignee: Leybold-Heraeus GmbHInventor: Herbert Stephan
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Patent number: 4210097Abstract: In a line for coating a ferrous base metal strip with a molten coating metal, the line being of the type having a preparation furnace for the strip comprising a direct fired furnace, a controlled atmosphere heating furnace, one or more cooling chambers and a snout leading beneath the surface of the molten coating metal bath, all in sealed relationship to each other, the improvement comprising a method and means for maintaining a non-oxidizing atmosphere at positive pressure within the entire preparation furnace during line stops. To this end, a retractable, refractory lined door means is provided in the conduit between the direct fired furnace and its exhaust fan to seal off the direct fired furnace from its exhaust fan and an air dilution opening in that conduit. Additionally, means are provided to add excess nitrogen flow to the preparation furnace to maintain a positive pressure therein.Type: GrantFiled: January 29, 1979Date of Patent: July 1, 1980Assignee: Armco Inc.Inventors: Fred Byrd, James A. Fisher
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Patent number: 4198449Abstract: Disclosed herein is the preparation of thin films of tungsten, molybdenum, rhenium or osmium on a high-temperature resistant substrate by thermal evaporation in a high vacuum, wherein the oxides of these high-temperature-resistant metals are evaporated simultaneously with a reduction metal in a manner such that the oxide molecules and the metal atoms or molecules impinge together on the surface of the substrate heated to a predetermined temperature and react with each other there chemically, so that the high-temperature-resistant metal oxides are reduced and the reduction metals are oxidized. In this process, the high-temperature-resistant metal is deposited on the surface of the substrate, and the oxides of the reduction metals evaporate, either completely or partially, and are pumped off.Type: GrantFiled: April 20, 1978Date of Patent: April 15, 1980Assignee: Siemens AktiengesellschaftInventors: Helmut Freller, Gunther Titze
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Patent number: 4177326Abstract: The invention relates to a process and installation for making stainless els coated with a lead-based alloy and having undergone annealing. The surface of the product is first prepared by mechanical treatment, then the product is pre-coated by known techniques such as hot tin-plating, after which the annealing treatment is effected, followed by the final coating. Such products may be used, inter alia, in the manufacture of car radiators.Type: GrantFiled: December 16, 1977Date of Patent: December 4, 1979Assignee: VALLOUREC Usines a Tubes de Lorraine-Escaut et Vallourec ReuniesInventors: Bernard A. M. Windal, Edmond Lobry
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Patent number: 4162345Abstract: A method for producing a hard deposit on a substrate is described wherein a volatile halide of tungsten or molybdenum is reacted with a gas or gases containing hydrogen, oxygen and carbon to effect the deposition on a substrate of a compound of the metal in a liquid phase. The liquid phase deposited on the substrate is then reacted to remove oxygen and halogen and produce a hard deposit containing the metal and carbon. Also described are products which may be produced by the above method.Type: GrantFiled: November 7, 1977Date of Patent: July 24, 1979Assignee: Chemetal CorporationInventor: Robert A. Holzl
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Patent number: 4160048Abstract: The invention contemplates a method and means for making a dryer or the like roll having a ferrous metal surface provided with a surface coating of a hardfacing alloy, the ferrous metal surface having a thermal conductivity relative to silver taken as 1 cal/cm.sup.2 /cm/.degree.C./sec of at least about 0.06 the hardfacing alloy being a hardfacing heat, corrosion and wear resistant iron-group metal-base alloy mechanically and metallurgically bonded to said ferrous metal surface which is preferably made of cast iron, the hardfacing alloy coating having a thickness ranging from about 0.01 to 0.15 inch, the thermal conductivity of said coating being at least 0.05.Type: GrantFiled: May 24, 1978Date of Patent: July 3, 1979Assignee: Eutectic CorporationInventor: Frederick T. Jaeger
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Patent number: 4152471Abstract: Method and means for continuously contact-coating one side only of a ferrous base metal strip with a molten coating metal. One or more roll means are provided to conduct the strip surface to be coated above the surface of a bath of the molten coating metal. The strip surface to be coated is caused to travel sufficiently close to the molten coating metal bath surface that the surface tension and wetting characteristics of the coating metal will permit the formation of a meniscus which will continuously contact and coat the strip surface. The coating is subjected to jet finishing. The strip is maintained in a protective non-oxidizing atmosphere at least until the one side thereof is coated. Alternatively, at least that side of the strip to be coated with the molten coating metal is coated with a flux which remains on the strip until contacted by the coating metal meniscus.Type: GrantFiled: September 19, 1977Date of Patent: May 1, 1979Assignee: Armco Steel CorporationInventors: Paul E. Schnedler, Marvin B. Pierson, Hart F. Graff, Thomas A. Compton, William R. Leasure
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Patent number: 4150180Abstract: According to the proposed method, the upper layer of the working solution is heated and components restoring its concentration are added thereto, while the lower layer of the solution is simultaneously cooled and a reagent restoring the pH of the solution is added thereto. The installation for realizing said method comprises a bath composed of two communicating vessels mounted one atop the other. The lower vessel is provided with an arrangement for cooling the solution therein and with a device for feeding thereinto the reagent restoring the pH of the solution, whereas the upper vessl is provided with an arrangement for heating the solution therein and with a device for feeding thereinto the components restoring the concentration of the solution.Type: GrantFiled: September 12, 1977Date of Patent: April 17, 1979Inventors: Fedor P. Potapov, Alexei K. Zorin, Jury N. Sulie, Anatoly I. Artemov, Alexandr K. Kolchevsky, Tamara P. Lavrischeva, Naum G. Lyandres, Lilia A. Toltinova, Mikhail J. Murylev
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Patent number: 4148946Abstract: In a line for coating a ferrous base metal strip with a molten coating metal, the line being of the type having a preparation furnace for the strip comprising a direct fired furnace, a controlled atmosphere heating furnace, one or more cooling chambers and a snout leading beneath the surface of the molten coating metal bath, all in sealed relationship to each other, the improvement comprising a method and means for maintaining a non-oxidizing atmosphere at positive pressure within the entire preparation furnace during line stop. To this end, a retractable, refractory lined door means is provided in the conduit between the direct fired furnace and its exhaust fan to seal off the direct fired furnace from its exhaust fan and an air dilution opening in that conduit. Additionally, means are provided to add excess nitrogen flow to the preparation furnace to maintain a positive pressure therein.Type: GrantFiled: February 14, 1977Date of Patent: April 10, 1979Assignee: Armco Steel CorporationInventors: Fred Byrd, James A. Fisher
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Patent number: 4126489Abstract: A method of improving the thermal emmissivity of a cathode heater wire to allow lower temperature operation of the heater without an attendant lowering in the cathode operating temperature, in which method the surface of a tungsten or molybdenum wire is oxidized, then coated with a salt of a refractory metal, and finally heated to reduce the salt and oxide to their metallic forms thereby causing the heater wire to be roughened and darkened.Type: GrantFiled: July 21, 1975Date of Patent: November 21, 1978Assignee: Varian Associates, Inc.Inventor: Paul D. Williams
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Patent number: 4097624Abstract: A method for decontaminating and subsequently metallizing a filament comprises:Passing the filament through the inner tube of a first chamber for decontamination which comprises two concentric tubes having an annular space therebetween, the inner tube of which has a series of fine holes therein; wherein said inner tube is heated and said annular space contains an inert gas such that said gas flows through said holes in heated jet streams which impinge upon said filament, thereby heating and decontaminating said filament;Passing said heated and decontaminated filament into a second chamber for metallization also comprising two concentric tubes having an annular space therebetween, the inner tube of which has a series of fine holes therein; wherein said inner tube of said second chamber is heated and said annular space of said second chamber contains a gaseous, thermally decomposable metal compound such that said gaseous metal compound flows through said holes in heated jet streams and impinges upon said heatedType: GrantFiled: September 30, 1977Date of Patent: June 27, 1978Assignee: University of VirginiaInventor: Hermann J. Schladitz
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Patent number: 4081296Abstract: The heat treatment of a continuous band or sheet of metal as the same travels through a plurality of stages in a protective atmosphere, between conveying rollers, by applying direct-current electricity to the rollers for inclusion of the travelling sheet in the circuit therebetween. The charged rollers in the initial stage are spaced more widely from one another than those in the later stage, to compensate for the lower resistivity of the metal in the former, so that the Joule effect of I.sup.2 R factor in the stages are substantially equalized. The protective atmosphere of oxidizing, reducing or inert gases which encompasses the sheet, is confined in chambers of galvanized iron sheeting and the like, the walls of which are in close proximity to the travelling sheet, so that lesser amounts of reacting gases are necessary.Type: GrantFiled: July 3, 1975Date of Patent: March 28, 1978Assignee: ValJim CorporationInventors: Vladimir Janatka, James J. Dolan
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Patent number: 4075376Abstract: A boiler tube coating and method are disclosed in which industrial steel tubes or pipes, for example, steel boiler tubes and/or integrated panels of steel boiler tubes, are provided with a fused overlay of a corrosion and erosion resistant coating comprised of a refractory hard component, e.g. tungsten carbide, dispersed through a corrosion resistant matrix alloy.Type: GrantFiled: April 1, 1976Date of Patent: February 21, 1978Assignee: Eutectic CorporationInventor: Frederick T. Jaeger
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Patent number: 4069358Abstract: A method of cladding metal plate with a protective layer of copper or copper base alloy is disclosed. The metal plate is contacted with a standing waveform of molten copper or copper base alloy in order to provide the cladding layer. This clad composite material is used to provide corrosion resistance for the metal plate substrate and an inexpensive alternative to solid thick sheets of copper or copper base alloy to deter corrosion.Type: GrantFiled: January 28, 1976Date of Patent: January 17, 1978Assignee: Olin CorporationInventors: Joseph Winter, Derek E. Tyler
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Patent number: 4051275Abstract: The process described herein involves a method of compacting and increasing the amount of particles, such as polytetrafluoroethylene, etc., deposited in fissures in a surface which involves heating the surface to expand the size of the fissures or pores in the surface, then depositing in the expanded fissures finely divided particles at a temperature at least 100.degree. F, preferably at least 300.degree. F below the temperature of the surface, and subsequently permitting the temperature of the surface and of the particles to come to equilibrium whereby the particles are locked into the fissures by interference fit. The surface is then subjected to a blasting fluid stream carrying finely divided particles applied at a pressure of 30-120 psi, preferably 40-80 psi, to compact the particles in the fissures, after which the original treatment is repeated by heating the surface, depositing additional finely divided particles at a temperature at least 100.degree.Type: GrantFiled: March 3, 1976Date of Patent: September 27, 1977Inventor: Clarence W. Forestek
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Patent number: 4045591Abstract: A method of treating sucker rod comprising shot peening the rod to clean and harden the exterior surface thereof, preheating the rod, and coating the rod with a metal alloy by using an electric arc spray gun to provide a layer of alloy on the exterior surface thereof. The rod is subsequently cooled and then coated with a baked-on, plastic-like surface.In one embodiment of the invention, used rod is first degreased, and following the shot peening operation the rod is subjected to an electronic test to determine the symmetry of compositon of the metal, as well as to ascertain if any flaws are present therein. The rod is then coated with metal and subsequently sprayed with plastic as in the above recited example.Type: GrantFiled: May 3, 1976Date of Patent: August 30, 1977Assignee: Rodco, Inc.Inventor: Bobby L. Payne
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Patent number: 3996398Abstract: A metal coating is deposited on a metal substrate by means of a method which consists in sand-blasting the metal substrate, in heating the substrate to a temperature between 100.degree. and 650.degree. C, then in spraying a powder of nickel or cobalt alloy having a high value of hardness and containing reducing agents as well as agents for reducing the melting point, the spraying operation being performed at a distance of 50 to 200 mm from the nozzle of a spray-gun and at a velocity within the range of 100 to 250 meters per second.Type: GrantFiled: July 25, 1975Date of Patent: December 7, 1976Assignee: Societe de Fabrication d'Elements CatalytiquesInventor: Pierre Manfredi
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Patent number: 3987217Abstract: A metallization system for metallurgically bonding a semiconductor die to metallic conducting slugs as terminals at the same time, and at the same temperature, that a surrounding glass sleeve is hermetically sealed to the conducting slugs for forming a zener diode, for example, is disclosed. The metallization system comprises a combination of aluminum, tin and palladium, for bonding to molybdenum, the aluminum being vapor deposited followed by a vapor co-deposition of aluminum and tin and further followed by a vapor deposited layer of palladium.Type: GrantFiled: October 16, 1974Date of Patent: October 19, 1976Assignee: Motorola, Inc.Inventors: Richard L. Greeson, Elliott M. Philofsky
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Patent number: 3982047Abstract: An automatic soldering machine and method for soldering the ends of pretinned components such as ceramic chip capacitors, transistors and the like, while leaving one side of the component flat, is disclosed. The components are supplied by a vibratory feeder to a pick-up station where they are sequentially picked up by a vacuum probe and are transferred to a print station where a retaining mechanism comprising a spring biased finger and a metal plate retains the component. A plurality of these retaining mechanisms are secured to an indexing table which passes in succession a printing station, a preheating station, a soldering station and a take-off station. At the soldering station a predetermined amount of solder is fed to the ends of the components and a heat lamp is flashed to melt the solder.Type: GrantFiled: May 22, 1975Date of Patent: September 21, 1976Assignee: Illinois Tool Works Inc.Inventor: Denver Braden
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Patent number: 3973061Abstract: A composition of matter comprising a mass of ferrous scrap pieces compressed together in random orientation forming a network of interlocking pieces has been prepared. The ferrous metal network has a density of 1.2 to 4.0 g/cc, a porosity of 50% to 85% and a short transverse tensile strength (S.T.T.S.) of at least 2 psi, preferably at least 2.5 psi.This ferrous metal network may be impregnated with magnesium in amount from 18 to 55% by weight of the impregnated body. The magnesium impregnated body is useful for treating high melting metals such as ferrous metal to reduce the sulphur content or to produce nodular iron.Type: GrantFiled: March 25, 1975Date of Patent: August 3, 1976Assignee: NL Industries, Inc.Inventors: Jairaj Easwaran, George S. Foerster
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Patent number: 3969544Abstract: This invention discloses the plating of a metallic workpiece, particularly aluminum with a layer of tin. The plating is accomplished in the presence of sonic or ultrasonic vibrations at a temperature determined by the phase diagram for a binary alloy to provide for the presence of an alloy interface encompassing both metals. This contrasts with the heretofore achieved adhesive bond.Type: GrantFiled: February 14, 1975Date of Patent: July 13, 1976Assignee: Branson Ultrasonics CorporationInventor: Edward G. Obeda
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Patent number: 3949118Abstract: Difficultly solderable material having an oxide surface such as glass, ceramics or such metals as Si, Ge, Al, Ti, Zr or Ta is soldered using a solder alloy composed of 2-98.5% by wt. of Pb, 1-97.5% by wt. of Sn and 0.1-15% by wt. of rare earth metals, while applying vibration, preferably of the ultrasonic type.Type: GrantFiled: August 9, 1974Date of Patent: April 6, 1976Assignee: Asahi Glass Company, Ltd.Inventors: Kentaro Nagano, Kohji Nomaki, Yoshihito Saoyama
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Patent number: 3936543Abstract: A method of preparing carbon steel strip and sheet for hot dip metallic coating in a Selas-type direct-fired furnace, wherein the atmosphere in the furnace is controlled to contain from about 3% oxygen to about 2% excess combustibles by volume, thereby forming a thin iron oxide film on the carbon steel surfaces. The strip and sheet is then heated in a subsequent furnace containing at least 5% hydrogen by volume at a temperature sufficient to reduce the oxide film, viz., at least about 675.degree.C. The direct-fired furnace is preferably operated at stoichiometrically equivalent fuel:air ratios.Type: GrantFiled: August 22, 1974Date of Patent: February 3, 1976Assignee: Armco Steel CorporationInventors: Fred Byrd, Marvin B. Pierson, Thomas A. Compton, Frank C. Dunbar
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Patent number: RE29726Abstract: A method of preparing carbon steel strip and sheet for hot dip metallic coating in a Selas-type direct-fired furnace, wherein the atmosphere in the furnace is controlled to contain from about 3% oxygen to about 2% excess combustibles by volume, thereby forming a thin iron oxide film on the carbon steel surfaces. The strip and sheet is then heated in a subsequent furnace containing at least 5% hydrogen by volume at a temperature sufficient to reduce the oxide film, viz., at least about 675.degree. C. The direct-fired furnace is preferably operated at stoichiometrically equivalent fuel:air ratios.Type: GrantFiled: February 14, 1977Date of Patent: August 8, 1978Assignee: Armco Steel CorporationInventors: Fred Byrd, Marvin B. Pierson, Thomas A. Compton, Frank C. Dunbar