Aluminum Compound Containing Patents (Class 501/153)
  • Patent number: 5641469
    Abstract: Dry milling an alpha alumina precursor produces direct conversion to alpha alumina at room temperature.
    Type: Grant
    Filed: May 28, 1991
    Date of Patent: June 24, 1997
    Assignee: Norton Company
    Inventors: Ajay K. Garg, Edward Lilley
  • Patent number: 5641718
    Abstract: Disclosed is a sintered aluminum nitride composition and a circuit substrate for use in semiconductor device. The sintered aluminum nitride composition comprises: aluminum nitride; a first component given by a compound containing an element which is selected from the group consisting of alkaline earth elements and group IIIa elements of the periodic table; a second component made of either a simple silicon or a silicon-containig compound; and a third component made of either a simple manganese or a manganese-containing compound. The circuit substrate has an insulating layer which is compoesd of the above-described sintered aluminum nitride composition, and an electrically conductive layer containing an electrically conductive material and the same components as those of the insulating layer.
    Type: Grant
    Filed: August 30, 1995
    Date of Patent: June 24, 1997
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Akihiro Horiguchi, Katsuyoshi Oh-Ishi, Mitsuo Kasori, Hiroyasu Sumino, Fumio Ueno, Jun Monma, Kazuo Kimura
  • Patent number: 5637543
    Abstract: A ceramic composition for thermistor exhibiting stable resistance values over a wide temperature range and capable of being used for a prolonged time. The composition is represented by (M.sup.1 M.sup.2 O.sub.3).sub.1-x .multidot.(M.sup.1 AlO.sub.3).sub.x, wherein M.sup.1 is an element selected from the elements of the group 3A excluding La and M.sup.2 is an element of the groups 4A, 5A, 6A, 7A and 8, and wherein the mixing ratio between an electrically conductive substance stable at elevated temperatures and an insulating substance stable at elevated temperatures, may be adjusted. A thermistor formed of the composition is superior in high-temperature stability and can be used over a broad temperature range because its resistance value can be selected to an optimum value.
    Type: Grant
    Filed: December 18, 1995
    Date of Patent: June 10, 1997
    Assignee: NGK Spark Plug Co., Ltd.
    Inventors: Masaki Iwaya, Kyohei Hayashi, Hiroshi Matsuzaki, Yoshirou Suematsu
  • Patent number: 5633084
    Abstract: Fused alumina particles are covered with a coating of aluminum titanate which is formed by applying a Ti-containing compound to the surface of the fused alumina particles and firing the same to cause a reaction between the Ti-containing compound and the alumina.
    Type: Grant
    Filed: April 28, 1994
    Date of Patent: May 27, 1997
    Assignee: Showa Denko K.K.
    Inventors: Tadashi Hiraiwa, Fumiyoshi Ono
  • Patent number: 5631201
    Abstract: An optically translucent polycrystalline alumina sintered body consists essentially of alumina, magnesia, terbia and, optionally, yttria. The magnesia is present in an amount of about 0.020 wgt. percent and the terbia is present in an amount of from about 0.005 to 0.060 wgt. percent. The yttria is present in an amount up to about 0.035 wgt. percent.
    Type: Grant
    Filed: July 29, 1996
    Date of Patent: May 20, 1997
    Assignee: Osram Sylvania Inc.
    Inventors: George Wei, Arlene Hecker, David Goodman
  • Patent number: 5627116
    Abstract: A sintered, translucent ceramic article comprises alpha alumina and up to 0.050 wgt. percent magnesia and between 0.001 to 0.100 wgt. percent lutetium oxide. In a preferred embodiment, the lutetium oxide is at 0.050 wgt. percent and in a second preferred embodiment half the lutetium oxide is replaced by yttrium oxide. A method of making a translucent ceramic article comprises the steps of: forming an aqueous slurry to yield one of the composition described above; adding nitric acid to adjust the pH to 4.6; adding an aqueous binder and plasticizer in the amount of 2.5 solids wgt. percent; spray-drying the slurry; forming an article by wet-bag isopressing; prefiring said article in air at about 1325.degree. C. for about 2 hours; and sintering said air-fired article in hydrogen for about 3 hours at 1800.degree. C.
    Type: Grant
    Filed: September 24, 1996
    Date of Patent: May 6, 1997
    Assignee: Osram Sylvania Inc.
    Inventor: Karlene J. Zuk
  • Patent number: 5625256
    Abstract: A ceramic discharge vessel (6) for a high-pressure discharge lamp (1) made from a sintered body of optically translucent polycrystalline alumina ceramic which is doped with only 100-800 ppm MgO, only 200-1200 ppm ZrO.sub.2 and only 10-300 ppm Y.sub.2 O.sub.3 (by weight). This improves the loading capacity and operating characteristics of the vessel and of the lamp.
    Type: Grant
    Filed: November 29, 1994
    Date of Patent: April 29, 1997
    Assignees: Patent-Treuhand-Gesellschaft F. Elektrische Gluehlampen mbH, NGK Insulators, Ltd.
    Inventors: Rita Tiedt, Helmut Weske, Koichiro Maekawa, Junichi Doi
  • Patent number: 5622769
    Abstract: According to this invention, there is disclosed a thermal conductivity substrate which includes an aluminum nitride sintered body and a coating layer formed on the body of aluminum phosphate and having a surface roughness of 1 .mu.m or less, and which has excellent humidity resistance and chemical resistance.
    Type: Grant
    Filed: February 10, 1994
    Date of Patent: April 22, 1997
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Shoji Kozuka, Masaru Hayashi, Katsuyoshi Oh-Ishi, Takaaki Yasumoto, Nobuo Iwase, Hiroshi Endo, Koji Yamakawa, Kaoru Koiwa, Kiyoshi Iyogi
  • Patent number: 5614138
    Abstract: A mixture of calcinated metallic oxides are mixed with ZnO and SiO.sub.2, granulated, compacted and then sintered to form a nonlinear resistor. After sintering, the formed ZnO resistor elements are heat treated, preferably in a two-step heat treating process.
    Type: Grant
    Filed: February 7, 1995
    Date of Patent: March 25, 1997
    Assignee: Hitachi Ltd.
    Inventors: Seiichi Yamada, Shigeru Tanaka, Moritaka Shoji, Shigehisa Motowaki, Ken Takahashi, Shingo Shirakawa, Shinichi Oowada, Takeo Yamazaki
  • Patent number: 5612267
    Abstract: Ceramic preforms comprising monocrystalline hexagonal platelets of .alpha.-alumina, well adopted for conversion into refractory bricks or ceramic composites, are prepared by crystallizing a settled fine powder of amorphous alumina, transition alumina or alumina hydrate, advantageously in the presence of a fluoro-compound flux, into a coherent mass of such hexagonal platelets of .alpha.-alumina.
    Type: Grant
    Filed: June 5, 1995
    Date of Patent: March 18, 1997
    Assignee: Atochem
    Inventors: Roland Bachelard, Annick Faure
  • Patent number: 5612154
    Abstract: A beta-alumina solid electrolyte for use in a sodium-sulfur battery is composed of beta-alumina crystals having a degree of orientation toward the C axis thereof, of 0.2-0.4 and an aspect ratio of 4.0 or less. The beta-alumina solid electrolyte is composed of the beta-alumina crystals having a degree of orientation toward the C axis thereof, of 0.2-0.4 and has such a particle diameter distribution that the average particle diameter is 3 .mu.m or less, the proportion of the particles having a particle diameter of 5 .mu.m or less is 90% or more, and the maximum particle diameter is 300 .mu.m or less. A process for producing a beta-alumina solid electrolyte using an alumina source material, a magnesium source material and a sodium source material, uses a magnesium-aluminum spinel as the magnesium source material and subjects all materials to mixing, granulation, molding and firing to obtain a beta-alumina solid electrolyte without subjecting the materials to calcination.
    Type: Grant
    Filed: March 2, 1995
    Date of Patent: March 18, 1997
    Assignee: NGK Insulators, Ltd.
    Inventors: Masaharu Kajita, Takehiro Kajihara, Takao Totoki
  • Patent number: 5611829
    Abstract: An alpha alumina-based ceramic abrasive grain comprising, on a theoretical oxide basis, Al.sub.2 O.sub.3, Fe.sub.2 O.sub.3, and SiO.sub.2. The abrasive grain has a surface roughness height of greater than about 200 nanometers and a density of greater than about 3.50 g/cm.sup.3. Preferably, the alpha alumina-based ceramic abrasive grain has alpha alumina crystallites having an average crystallite size of less than about 0.5 micrometer (more preferably, less than about 0.3 micrometer). The presence of the SiO.sub.2 in combination with Fe.sub.2 O.sub.3 increases the amount of transgranular fracture of the abrasive grain, reduces the alpha alumina crystallite growth during sintering of the abrasive grain, dilates at least one of the unit cell dimensions of the abrasive grain, and generally improves the grinding performance of the abrasive grain.
    Type: Grant
    Filed: June 26, 1996
    Date of Patent: March 18, 1997
    Assignee: Minnesota Mining and Manufacturing Company
    Inventors: Larry D. Monroe, Thomas E. Wood
  • Patent number: 5609675
    Abstract: An inorganic composition comprises (A) 60 to 99% by weight of spherical inorganic oxide particles having a mean particle diameter greater than 0.1 .mu.m but not greater than 1 .mu.m, and (B) 40 to 1% by weight of inorganic oxide fine particles having a mean particle diameter not greater than 0.1 .mu.m, wherein a volume of micro pores due to strongly aggregated particles having pore diameters not smaller than 0.08 .mu.m is not greater than 0.1 cc per gram of the inorganic composition. The inorganic composition, when mixed with a polymerizable monomer and a catalyst, provides a composite useful for dental applications which has excellent surface smoothness, can be polished in a short time, exhibits improved bending strength, compressive strength, surface hardness and wear resistance and causes little wear on an antagonistic tooth.
    Type: Grant
    Filed: June 30, 1995
    Date of Patent: March 11, 1997
    Assignee: Tokuyama Corporation
    Inventors: Masaki Noritake, Shigeki Yuasa
  • Patent number: 5607885
    Abstract: A low thermal expansion cordierite aggregate, which consists mainly of cordierite crystals having a mean crystal diameter of at least 50 .mu.m and has little orientation in the crystal structure, shows hysteresis in its thermal expansion property accompanying a rise and fall of the temperature, and has a mean thermal expansion coefficient within a temperature range of from room temperature to 1000.degree. C. of at most 10.times.10.sup.-7 /.degree.C.
    Type: Grant
    Filed: April 24, 1996
    Date of Patent: March 4, 1997
    Assignee: AG Technology Co., Ltd.
    Inventors: Tomoko Ichii, Keiichiro Suzuki, Masataro Okumiya
  • Patent number: 5607887
    Abstract: The present invention provides a method for preparing a ceramic mixed-oxide of at least two metals including mixing an alloy with a ceramic oxide. The alloy including a metal selected from the group consisting of aluminum, calcium, lithium, magnesium, silicon, titanium, yttrium, and zirconium. The alloy also includes an element that is to be present in the ceramic mixed-oxide. The element is different from the metal and is selected from the group consisting of aluminum, calcium, lithium, magnesium, a combination of magnesium and silicon, silicon, titanium, yttrium, and zirconium. The ceramic oxide includes a metal that is to be present in the ceramic mixed oxide. The alloy and ceramic oxide are co-milled. The mixed and co-milled alloy and ceramic oxide are reaction-sintered, thereby oxidizing the metal and element of the alloy to produce the ceramic mixed-oxide.
    Type: Grant
    Filed: February 15, 1995
    Date of Patent: March 4, 1997
    Assignee: Volvo Aero Aktiebolag
    Inventors: Lars Pejryd, Robert Lundberg, Jesper Brandt
  • Patent number: 5593467
    Abstract: Crystalline ceramic, alpha alumina-based abrasive grain and a method of making the same. The abrasive grain can be incorporated into abrasive products such as coated abrasives, bonded wheels, and three dimensional, low density abrasives.
    Type: Grant
    Filed: November 2, 1994
    Date of Patent: January 14, 1997
    Assignee: Minnesota Mining and Manufacturing Company
    Inventor: Larry D. Monroe
  • Patent number: 5593781
    Abstract: In the method described, the degree of agglomeration of the nanometer-size particles can be readily checked, thus enabling dispersions of particles of this kind to be produced with high solids contents. The method calls for the unmodified powder to be dispersed in water and/or an organic solvent in the presence of a low-molecular organic compound including a functional group which can react and/or interact with groups present on the surface of the powder particles. The dispersant may subsequently be wholly or partly removed.
    Type: Grant
    Filed: November 3, 1994
    Date of Patent: January 14, 1997
    Assignee: Institut Fue Neue Materialien Gemeinnutzige GMBH
    Inventors: Rudiger Nass, Helmut Schmidt, Peter Schmitt
  • Patent number: 5593930
    Abstract: An object of the present invention is to shorten the working time for high pressure slip casting. There is provided a composition for high pressure casting slip including a first starting powder forming a frame of a mold body and second starting powder forming the frame of the mold body and acting as a plastic agent, wherein the first and second starting powders are uniformly mixed in a dry condition. "Slip" of a minimum water content is easily prepared by the composition to effect optimal fluidity of the slip so that the water is removed from the slip in a short time during a casting process.
    Type: Grant
    Filed: September 13, 1995
    Date of Patent: January 14, 1997
    Assignee: NGK Insulators, Ltd.
    Inventor: Ritsu Sato
  • Patent number: 5587346
    Abstract: A sintered, translucent ceramic article comprises alpha alumina and up to 0.050 wgt. percent magnesia and between 0.001 to 0.100 wgt. percent lutetium oxide. In a preferred embodiment, the lutetium oxide is at 0.050 wgt. percent and in a second preferred embodiment half the lutetium oxide is replaced by yttrium oxide. A method of making a translucent ceramic article comprises the steps of: forming an aqueous slurry to yield one of the composition described above; adding nitric acid to adjust the pH to 4.6; adding an aqueous binder and plasticizer in the amount of 2.5 solids wgt. percent; spray-drying the slurry; forming an article by wet-bag isopressing; prefiring said article in air at about 1325.degree. C. for about 2 hours; and sintering said air-fired article in hydrogen for about 3 hours at 1800.degree. C.
    Type: Grant
    Filed: June 16, 1995
    Date of Patent: December 24, 1996
    Assignee: Osram Sylvania, Inc.
    Inventor: Karlene J. Zuk
  • Patent number: 5587010
    Abstract: The present invention provides a process for producing fine flaky alumina particles suitable as a raw material for ceramics, a pigment for paint and etc., wherein aluminum hydroxide or alumina hydrate having a particle size regulated to the order of submicron is subjected to a hydrothermal treatment in water or an aqueous alkali solution at a temperature of 350.degree. C. or above under a pressure of 200 kg/cm.sup.2 or below. The present invention further provides an alumina-based plastic material which is produced by kneading the aforesaid fine flaky particles with an organic water holding material and water. Methylcellulose, polyvinyl alcohol, carboxymethylcellulose, polyethylene glycol, etc. are preferably used as the organic water holding agent. The alumina-based plastic material has a high plasticity, so that there is no need of using a large amount of a binder. Thus a dense molded article having stable properties can be prepared.
    Type: Grant
    Filed: June 16, 1995
    Date of Patent: December 24, 1996
    Assignees: Agency Of Industrial Science And Technology, Ministry Of International Trade And Industry, YKK Corporation
    Inventors: Yasuo Shibasaki, Kiichi Oda, Takeshi Fukuda
  • Patent number: 5572091
    Abstract: Ultraviolet (UV) radiation in the UV-C and UV-B bands, which is particularly dangerous, is absorbed and filtered by quartz glass doped with between 0.065% and 3.25%, and preferably between 0.065% and 1.3% by weight, of cerium metal, or cerium as such. Preferably, the cerium is added to quartz sand and/or rock crystal, in form of a fine-grained powder of up to 2 0 .mu.m grain size, in form of cerium aluminate (CeAlO.sub.3), present in up to about 5% by weight, and preferably up to about 2%, and melted together in a single step. The quartz glass so obtained is particularly suitable for a metal halide discharge lamp, e.g. as an outer envelope (1), or as the discharge vessel (27) itself, or for halogen incandescent lamps, to form the quartz-glass light bulb or an envelope therefor. A small quantity of titanium oxide, up to about 0.05%, may be added as a further doping agent to the melt to further improve the UV absorption in the B and C bands.
    Type: Grant
    Filed: May 17, 1995
    Date of Patent: November 5, 1996
    Assignee: Patent-Treuhand-Gesellschaft f ur elektrische Gl uhlampen mbH
    Inventors: Alfred Langer, Andreas Genz, Manfred Deisenhofer, Walter Keile, Bernd Lewandowski, J urgen Reichardt
  • Patent number: 5567663
    Abstract: Cordierite honeycomb ceramics comprises a cordierite phase as a main ingredient. A value of [Fe.sub.2 O.sub.3 wt %/(MgO wt %+Fe.sub.2 O.sub.3 wt %)].times.100 is 2-10, where a ferric component is calculated as Fe.sub.2 O.sub.3. A thermal expansion coefficient of the cordierite honeycomb ceramics is less than 0.5.times.10.sup.-6 /.degree. C. within a temperature range of 40.degree.-800.degree. C. in a direction parallel to a flow passage of a honeycomb body. In the cordierite honeycomb ceramics including a ferric component, a ferric component is added from a talc as raw materials. The cordierite honeycomb ceramics having a low thermal expansion coefficient is obtained by mixing raw materials for cordierite generation to obtain a batch, extruding the batch into a honeycomb formed body, drying the honeycomb formed body, and firing the dried honeycomb formed body at a temperature range of 1350.degree.-1450.degree. C. After that, the sintered honeycomb body is immersed in an acid solution if necessary.
    Type: Grant
    Filed: March 2, 1995
    Date of Patent: October 22, 1996
    Assignee: NGK Insulators, Ltd.
    Inventors: Wataru Kotani, Yoshiro Ono, Kazuhiko Kumazawa
  • Patent number: 5556817
    Abstract: A barrier comprising:a) between about 75 w/o and about 95 w/o alumina-silica refractory grain, andb) between about 2 w/o and about 10 w/o of a sealant selected from the group consisting of zinc borate; sulfur; R1 Al.sub.x/2 Si.sub.y/2 O.sub.z/2 and R2 Si.sub.b/2 S.sub.c/2 C.sub.d/2 O.sub.e/2 H.sub.f/2 wherein:i) R1 is selected from the group consisting of Na, K, and Li, and mixtures thereof,ii) x,y and z are integers between 0 and 16,iii) R2 is selected from the group consisting of Ca, Sr and Mg, and mixtures thereof, andiv) b,c,d,e and f are integers between about 0 and 16.
    Type: Grant
    Filed: November 9, 1995
    Date of Patent: September 17, 1996
    Assignee: Saint Gobain/Norton Industrial Ceramics Corp.
    Inventor: Edmund A. Cortellini
  • Patent number: 5552356
    Abstract: The present invention relates to boron subphosphide/aluminum oxide composite materials, to processes for the production of these materials and to the use thereof.
    Type: Grant
    Filed: June 29, 1995
    Date of Patent: September 3, 1996
    Assignee: Bayer AG
    Inventor: Nils Perchenek
  • Patent number: 5552349
    Abstract: A low thermal expansion cordierite aggregate, which consists mainly of cordierite crystals having a mean crystal diameter of at least 50 .mu.m and has little orientation in the crystal structure, shows hysteresis in its thermal expansion property accompanying a rise and fall of the temperature, and has a mean thermal expansion coefficient within a temperature range of from room temperature to 1000.degree. C. of at most 10.times.10.sup.-7 /.degree.C.
    Type: Grant
    Filed: August 11, 1994
    Date of Patent: September 3, 1996
    Assignee: AG Technology Co., Ltd.
    Inventors: Tomoko Ichii, Keiichiro Suzuki, Masataro Okumiya
  • Patent number: 5547479
    Abstract: Alpha alumina-based abrasive grain having an as sintered outer surface. The abrasive grain can be incorporated into abrasive articles such as bonded abrasives (e.g., grinding wheels), coated abrasives, and nonwoven abrasives.
    Type: Grant
    Filed: May 26, 1995
    Date of Patent: August 20, 1996
    Assignee: Minnesota Mining and Manufacturing Company
    Inventors: Stanley L. Conwell, William P. Wood
  • Patent number: 5541145
    Abstract: An aluminum nitride ceramic having desired properties suitable for electronic packaging applications can be prepared from a novel aluminum nitride powder/sintering aid mixture. The sintering aid comprises a glassy component formed from alumina, calcia and boria, and a non-vitreous component comprising an element or compound of a metal of Group IIa, IIIa, or the lanthanides, preferably crystalline oxides, reactibis with the crystallized glass component and the alumina from the Al N grains. Alternatively, the sintering aid comprises a multi-component glass composition capable of forming the above components upon melting and thereafter crystallizing upon reaction.
    Type: Grant
    Filed: June 12, 1995
    Date of Patent: July 30, 1996
    Assignee: The Carborundum Company/IBM Corporation
    Inventors: Jonathan H. Harris, Subhash L. Shinde, Takeshi Takamori, Robert A. Youngman, Lester W. Herron, Benjamin V. Fasano
  • Patent number: 5527370
    Abstract: A lapping composition which contains abrasive grains which are commercially available and which consists of plate alumina-powder prepared by milling and class:trying a sintered body of plate alumina obtained by calcinating aluminum hydroxide, and other plate alumina powder classified and prepared separately from but similarly to the first-mentioned plate alumina powder having average grain size which is in a range of from 1.3 times to 2.3 times as large as the average grain size of the first-mentioned plate alumina powder. Further provided is a lapping method with such a lapping composition by which the removal rate is improved and a lapped surface excellent in quality can be obtained.
    Type: Grant
    Filed: June 17, 1994
    Date of Patent: June 18, 1996
    Assignee: Fujimi Incorporated
    Inventors: Masaaki Kubo, Koji Nishikawa, Shinji Maruyama
  • Patent number: 5525561
    Abstract: The invention provides a method of making a magnesium/aluminium spinel compound having the formula Mg.sub.(1+x) Al.sub.(2+y) O.sub.4 in which 0.ltoreq.x.ltoreq.0.2 and 0.ltoreq.y.ltoreq.0.35. Particulate aluminium metal and a magnesium-containing component selected from magnesium oxide and precursors thereof are mixed together and heated to 800.degree.-1150.degree. C. in an oxidising environment to cause oxidation of at least part of the aluminium. Further heating then takes place to a temperature of 1150.degree.-1350.degree. C. in the oxidizing environment to cause aluminium oxide and magnesium oxide in the admixture to react together.
    Type: Grant
    Filed: October 28, 1994
    Date of Patent: June 11, 1996
    Assignee: Programme 3 Patent Holdings
    Inventor: Arnold Van Zyl
  • Patent number: 5520716
    Abstract: An Al.sub.2 O.sub.3 -TiC sintered product comprising Al.sub.2 O.sub.3 as a main component and containing TiC in an amount of from 20 to 40% by weight, wherein the average particle diameter of Al.sub.2 O.sub.3 particles in the sintered product is larger by 5 to 50% than the average particle diameter of TiC particles, the average particle diameter of the sintered product as a whole is not larger than 1 .mu.m, the average particle diameter of TiC particles is not larger than 0.9 .mu.m, and the total amount of the grain boundary phases other than Al.sub.2 O.sub.3 and TiC is not larger than 1.0% by weight. The Al.sub.2 O.sub.3 -TiC sintered product can be used as a substrate 1 for a magnetic head, and has portions such as grooves 4 and stepped portions formed in the surface of the air bearing surface 2 of the slider by being irradiated with ions. The sintered product exhibits excellent surface quality after machined by being irradiated with ions and can be machined at an increased rate.
    Type: Grant
    Filed: March 2, 1995
    Date of Patent: May 28, 1996
    Assignee: Kyocera Corporation
    Inventors: Nobuoki Takagi, Hiroki Tokunaga, Shinichiro Masuyama
  • Patent number: 5518975
    Abstract: A method of making a .beta.-alumina compound which is a polyaluminate of the general formula M.sub.y O.multidot.xAl.sub.2 O.sub.3 in which M is a metal selected from monovalent metals and divalent metals, y=2 when M is a monovalent metal, y=1 when M is a divalent metal and x=4-12 comprises forming a green precursor of the 62 -alumina compound by mixing together particulate aluminium metal and a reagent compound comprising an oxide of the metal M or a precursor thereof. The mixture is heated to 800.degree.-1150.degree. C. in an oxidizing environment to cause oxidation of at least part of the aluminium. Further heating then takes place to 1150.degree.-1350.degree. C. in said environment to cause the oxidized aluminium and oxide of the metal M to react to form the .beta.-alumina compound.
    Type: Grant
    Filed: October 28, 1994
    Date of Patent: May 21, 1996
    Assignee: Programme 3 Patent Holdings
    Inventors: Arnold Van Zyl, Sikha Ray
  • Patent number: 5518974
    Abstract: The invention relates to a densely sintered tabular ceramic part of aluminum oxide having improved thermal shock resistance, which possesses a fine porosity of at most 10% by volume, does not contain inclusions having a diameter of .gtoreq.70 .mu.m within the ceramic microstructure and is not destroyed on immersion in a molten metal bath having a temperature of at least 350.degree. C. The invention also relates to a process for producing such a shaped part.
    Type: Grant
    Filed: January 31, 1994
    Date of Patent: May 21, 1996
    Assignee: Hoechst Aktiengesellschaft
    Inventors: Wolfgang Krahn, Johannes Ernst, Claudia Drabent
  • Patent number: 5516347
    Abstract: Seeded sol-gel alumina abrasive grits with improved grinding performance incorporating alkali metal oxides selected from rubidium and cesium oxides.
    Type: Grant
    Filed: April 5, 1995
    Date of Patent: May 14, 1996
    Assignee: Saint-Gobain/Norton Industrial Ceramics Corp.
    Inventor: Ajay K. Garg
  • Patent number: 5516348
    Abstract: Alpha alumina-based abrasive grain including aluminate platelets. The abrasive grain can be incorporated into abrasive articles such as bonded abrasives (e.g., grinding wheels), coated abrasives, and nonwoven abrasives.
    Type: Grant
    Filed: May 26, 1995
    Date of Patent: May 14, 1996
    Assignee: Minnesota Mining and Manufacturing Company
    Inventors: Stanley L. Conwell, William P. Wood
  • Patent number: 5510210
    Abstract: The present invention is directed to a solid electrolyte and a process for making the same for a sodium-sulfur secondary cell including a composition of 7.0 to 10.0 weight percent of Na.sub.2 O, 0.5 to 3.5 weight percent of MgO or 0.7 to 1.0 weight percent of Li.sub.2 O, 0.01 to 0.6 weight percent of WO.sub.3, and the balance of Al.sub.2 O.sub.3. The solid electrolyte is prepared by mixing Na.sub.2 O, MgO, Li.sub.2 O, WO.sub.3, and Al.sub.2 O.sub.3, calcining the resulting mixture, pulverizing the calcined body, and subjecting the resulting powders to sintering. Alternatively, the solid electrolyte is prepared by mixing Na.sub.2 O, MgO, or Li.sub.2 O, and Al.sub.2 O.sub.3 with one another, calcining the mixture, adding WO.sub.3 to the calcined body, pulverizing the resulting material, and subjecting the resulting powders to sintering.
    Type: Grant
    Filed: October 31, 1994
    Date of Patent: April 23, 1996
    Assignee: Yukong Limited
    Inventor: Young-shol Kim
  • Patent number: 5502013
    Abstract: A method of forming a ceramic having a smooth ceramic surface and an assembly for forming ceramics having a flat and smooth ceramic surface are disclosed. A greenware precursor is disposed between a greenware base and a greenware cover. A frame is disposed between the greenware base and greenware cover for limiting compression of the greenware article to an amount which allows formation of a smooth ceramic surface during densification of the greenware precursor. The greenware base, greenware cover and greenware precursor are densified to cause the greenware precursor to form a ceramic having a smooth ceramic surface.
    Type: Grant
    Filed: May 27, 1994
    Date of Patent: March 26, 1996
    Inventor: Gilbert James
  • Patent number: 5496529
    Abstract: Novel aluminum phosphates, in particular amorphous aluminum phosphate powders having a BET specific surface no greater than 25 m.sup.2 /g, well suited as binders/hardeners or for the production of ceramic shaped articles, are prepared by reacting at least one aluminum compound, e.g., an aluminum oxide, hydroxide or oxyhydroxide, with phosphoric acid or an aluminum phosphate, e.g., an acid aluminum orthophosphate, in a liquid reaction medium devoid of inorganic acid anions other than of phosphoric acid, and then spray- or freeze-drying the suspension thus obtained.
    Type: Grant
    Filed: March 17, 1994
    Date of Patent: March 5, 1996
    Assignee: Rhone-Poulenc Chimie
    Inventors: William Fogel, Laurent Frouin
  • Patent number: 5484750
    Abstract: Transparent, polycrystalline garnet bodies having desirable properties for use as laser material, luminescent x-ray scintillator materials and other uses are produced by mixing a chloride source solution of the desired cations with a basic ammonium solution to produce a precipitate having a substantially uniform composition which can be further processed to provide the desired transparent body. This precipitate is separated from the solution, dried, thermally decomposed at a temperature in the range from 700.degree. to 1,000.degree. C., pressed to form a compact, isostatically pressed at up to 60,000 psi to provide a green, unsintered compact having a density in the vicinity of 55% of theoretic density. That green compact is then sintered in oxygen at a temperature between 1,400.degree. and 1,700.degree. C. to produce the desired transparent body. Alternatively, the compact may be sintered in oxygen at temperatures in the range from about 1,400.degree. to about 1,600.degree. C.
    Type: Grant
    Filed: August 10, 1994
    Date of Patent: January 16, 1996
    Assignee: General Electric Company
    Inventors: Charles D. Greskovich, William P. Minnear, Chester R. O'Clair, Erdogan O. Gurmen, Robert J. Riedner
  • Patent number: 5484752
    Abstract: A novel ceramic composite material consisting of single crystal .alpha.-Al.sub.2 O.sub.3 and polycrystal Y.sub.3 Al.sub.5 O.sub.12 and a ceramic composite material consisting of polycrystal .alpha.-Al.sub.2 O.sub.3 and polycrystal Y.sub.3 Al.sub.5 O.sub.12, each having a high mechanical strength and creep behavior particularly at high temperature are provided.
    Type: Grant
    Filed: November 8, 1994
    Date of Patent: January 16, 1996
    Assignee: Ube Industries, Ltd.
    Inventors: Yoshiharu Waku, Hideki Ohtsubo, Yasuhiko Kohtoku
  • Patent number: 5482907
    Abstract: A ceramic composite contains one spinel phase and one or more than one oxides phases. The composite is derived from the mixtures of two oxides, A.sub.2 O.sub.3 and BO, with different molar ratio, in which A and B are metallic ions of three and two valences respectively. The oxides are heated at a high temperature to form a composite containing a spinel and residual oxides. The formed spinel and residual oxides also undergo densification under high temperature. After the treatment at high temperature, not only the spinel is formed but also the composite is densified. The performance of the composite is superior in its strength, toughness and high-temperature stability.
    Type: Grant
    Filed: May 26, 1994
    Date of Patent: January 9, 1996
    Assignee: National Science Council
    Inventors: Wei-Hsing Tuan, Ming-Cherng Lin
  • Patent number: 5482903
    Abstract: An unsintered aluminum nitride body including:(a) 1 to 5 weight percent of a vitreous solid of boria, alumina, and calcia in the proportions of (1) boria between 3 and 25 weight percent, (2) alumina between 10 and 50 weight percent, and (3) calcia between 40 and 80 weight percent; and(b) aluminum nitride powder as the balance of the aluminum nitride body.
    Type: Grant
    Filed: December 22, 1993
    Date of Patent: January 9, 1996
    Assignee: International Business Machines Corporation
    Inventors: Peter R. Duncombe, Subhash L. Shinde, Takeshi Takamori
  • Patent number: 5476822
    Abstract: A ceramic composition for thermistor exhibiting stable resistance values over a wide temperature range and capable of being used for a prolonged time. The composition is represented by (M.sup.1 M.sup.2 O.sub.3).sub.1-x .multidot.(M.sup.1 AlO.sub.3).sub.x, wherein M.sup.1 is an element selected from the elements of the group 3A of the International Periodic Table excluding La and M.sup.2 is an element of the groups 4A, 5A, 6A, 7A and 8 of the International Periodic Table, and wherein the mixing ratio between an electrically conductive substance stable at elevated temperatures and an insulating substance stable at elevated temperatures, may be adjusted. A thermistor formed of the composition is superior in high-temperature stability and can be used over a broad temperature range because its resistance value can be selected to an optimum value.
    Type: Grant
    Filed: May 9, 1994
    Date of Patent: December 19, 1995
    Assignee: NGK Spark Plug Co., Ltd.
    Inventors: Masaki Iwaya, Kyohei Hayashi, Hiroshi Matsuzaki, Yoshirou Suematsu
  • Patent number: 5474959
    Abstract: The present invention provides a process for the production of a K- or Rb-.beta."- or -.beta.-aluminum oxide powder preparation, wherein a cubic densely packed aluminum oxide (.gamma.-aluminum oxide) or a precursor thereof is subjected to attrition together with a doping material or a precursor thereof, the so obtained mixture is calcined in an oxygen-containing atmosphere, potassium oxide or rubidium oxide or a precursor of these compounds is added to the calcination product obtained, the mixture is subjected to attrition and then calcined in an oxygen-containing atmosphere at a temperature greater than 900.degree. C. The present invention also provides a process for the production of a ceramic formed body in which a powder obtained by the above process is converted by attrition, isostatic pressing and sintering into a ceramic formed body. Such a ceramic formed body can be used as an ion conductor.
    Type: Grant
    Filed: March 28, 1994
    Date of Patent: December 12, 1995
    Assignee: Max-Planck-Gesellschaft zur Forderung der Wissenschafter e.V.
    Inventors: Gunter Schafer, Arnold van Zyl, Werner Weppner
  • Patent number: 5468690
    Abstract: A slurry for joining metallic or ceramic surfaces or for coating metallic or ceramic and refractory surfaces, comprising a liquid suspending medium and at least two constituents in particulate form suspended in the medium, the constituents being so selected and proportioned as to undergo combustion synthesis when ignited. A method for coating or joining metallic or ceramic surfaces comprises applying such a slurry to a surface to be coated or to surfaces to be joined, and igniting the slurry to cause combustion synthesis.
    Type: Grant
    Filed: February 15, 1994
    Date of Patent: November 21, 1995
    Assignee: University of Cincinnati
    Inventors: Jainagesh A. Sekhar, V. Subramanian, Necip S. Canarslan
  • Patent number: 5464462
    Abstract: Ultraviolet (UV) radiation in the UV-C and UV-B bands, which is particularly dangerous, is absorbed and filtered by quartz glass doped with between 0.065% and 3.25%, and preferably between 0.065% and 1.3%, by weight, of cerium metal, or cerium as such. Preferably, the cerium is added to quartz sand and/or rock crystal, in form of a fine-grained powder of up to 20 .mu.m grain size, in form of cerium aluminate (CeAlO.sub.3), present in up to about 5% by weight, and preferably up to about 2%, by weight, and melted together in a single step. The quartz glass so obtained is particularly suitable for a metal halide discharge lamp, e.g. as an outer envelope (1), or as the discharge vessel (27) itself, or for halogen incandescent lamps, to form the quartz-glass light bulb or an envelope therefor. A small quantity of titanium oxide, up to about 0.05%, may be added as a further doping agent to the melt to further improve the UV absorption in the B and C bands.
    Type: Grant
    Filed: September 13, 1993
    Date of Patent: November 7, 1995
    Assignee: Patent-Treuhand-Gesellschaft fur elektrische Gluhlampen mbH
    Inventors: Alfred Langer, Andreas Genz, Manfred Deisenhofer, Walter Kiele, Bernd Lewandowski, Jurgen Reichardt
  • Patent number: 5462903
    Abstract: The invention relates to nano-composite powders of alumina and metal constituted of grains of micronic size. Each grain comprises a compact matrix of alumina of a specific surface area less than 5 m.sup.2 /g, in which are dispersed crystallites of transition metals of alloys of these metals, of sizes less than 50 nm. The powder according to the invention may be produced starting with a precursor comprised of a mixed carboxylic salt of aluminum and one or more transition metals. The powders according to the invention permit producing by sintering cermets of alumina/metal benefitting from greatly improved mechanical and thermo-mechanical properties.
    Type: Grant
    Filed: May 24, 1994
    Date of Patent: October 31, 1995
    Assignee: Centre National De La Recherche Scientifique (C.N.R.S.)
    Inventors: Abel Rousset, Xavier Devaux
  • Patent number: 5461015
    Abstract: A porcelain having 9 to 55% by weight of SiO.sub.2, 36 to 87% by weight of Al.sub.2 O.sub.3, 0 to 2.0% by weight of Fe.sub.2 O.sub.3, 0 to 1.0% by weight of TiO.sub.2, 0 to 0.5% by weight of CaO, 0 to 0.5% by weight of MgO, 1.0 to 4.0% by weight of K.sub.2 O and Na.sub.2 O combined, and 0.25 to 25.0% by weight of bismuth oxide is disclosed. The porcelain has unexpectedly high unglazed bending strength and may be used for dielectric and structural applications.
    Type: Grant
    Filed: August 29, 1994
    Date of Patent: October 24, 1995
    Assignee: Raychem Corporation
    Inventors: Karin M. Kinsman, Ryan W. Dupon, Martha L. McCrum, Linas Mazeika, Amy S. Chu
  • Patent number: 5459113
    Abstract: A sinterable aluminum nitride powder composition is prepared by adding about 0.05-10.0 parts by weight of at least one compound selected from the group consisting of calcium tungstate and calcium molybdate and optionally about 1.0-7.0 parts by weight of at least one compound selected from the group consisting of yttria, calcium oxide, and calcium carbonate to 100 parts by weight of an aluminum nitride powder prepared by the alumina reduction method without decarbonization and having a residual carbon content of about 2%-10% by weight. The resulting powdery composition is subjected to mixing and deagglomeration in a dry process so as to form a powder mixture having a bulk density of about 0.3-0.5 g/cm.sup.3, and then to decarbonization by heating in an oxidizing atmosphere. The aluminum nitride powder composition has a pressurized bulk density of about 1.50-1.75 g/cm.sup.3 as measured at a pressure of 500 kg/cm.sup.2 and an average particle diameter of about 1.0-3.0 .mu.
    Type: Grant
    Filed: February 1, 1994
    Date of Patent: October 17, 1995
    Assignee: Sumitomo Metal Ceramics Inc.
    Inventors: Toshio Nozaki, Seigo Ohiwa, Hiroshi Iwase, Masanori Oguni
  • Patent number: RE35090
    Abstract: The present invention relates to a ceramic cutting insert containing whiskers for chip forming machining of steel and having improved mechanical, thermal and wear properties. The insert comprises besides the oxide-based matrix 5-50% by volume, preferably 10-40% by volume, of homogeneously dispersed whiskers of carbides, nitrides and/or borides of titanium and/or zirconium and, where applicable, solid solutions thereof. A part of the whiskers may be replaced by whiskers of silicon carbide. The properties of the composite material can be further modified by coating the whisker material with thin layers. The whiskers reinforced cutting material shows an improved toughness behaviour and resistance to thermal crack formation without having a negative influence on the wear resistance to any appreciable extent.
    Type: Grant
    Filed: April 8, 1994
    Date of Patent: November 21, 1995
    Assignee: Sandvik AB
    Inventors: Nils G. L. Brandt, Zeljka D. Senesan
  • Patent number: H1567
    Abstract: A transparent composite armor providing complete protection for small arms rojectiles up to and including caliber .50 AP M2 projectiles consisting of two or more layers of transparent material having a hard frangible face plate backed by one or more tough resilient plates to absorb the excess impact force after contact with the face plate, the several plates being bonded together with a suitable transparent adhesive.
    Type: Grant
    Filed: September 7, 1967
    Date of Patent: August 6, 1996
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Gordon R. Parsons, Fred E. Mooney