Pore-forming Patents (Class 501/39)
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Patent number: 11958981Abstract: Hydrophobized granular material comprising from 30 to 95% by weight of a pyrogenic mixed oxide based on silica and at least one oxide of metal M selected from of Al, Ti and Fe with the content of metal M oxide in the mixed oxide being from 01 to 10% by weight, and from 5 to 70% by weight of at least one IR-opacifier selected from the group consisting of silicon carbide, zirconium dioxide, ilmenites, iron titanates, zirconium silicates, manganese oxides, graphites, carbon blacks and mixtures thereof.Type: GrantFiled: July 9, 2019Date of Patent: April 16, 2024Assignee: Evonik Operations GmbHInventors: Uwe Numrich, Christian Moers, Bettina Gerharz-Kalte, Björn Lazar, Matthias Geisler
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Patent number: 11845685Abstract: A method of fining glass is disclosed that includes flowing a molten glass bath through a fining chamber. The molten glass bath has an undercurrent that flows beneath a skimmer that is partially submerged in the molten glass bath. One or more fining agents are introduced into the undercurrent of the molten glass bath directly beneath the skimmer from a dissolvable fining material component. In this way, the fining agent(s) may selectively target the gas bubbles drawn under the skimmer within the undercurrent of the molten glass for removal. The method may be employed to fine molten gas produced in a submerged combustion melter. A fining vessel for fining molten glass is also disclosed that includes a housing, a skimmer, and a dissolvable fining material component disposed directly beneath the skimmer.Type: GrantFiled: August 22, 2022Date of Patent: December 19, 2023Assignee: Owens-Brockway Glass Container Inc.Inventors: Scott Weil, Zhongming Wang, Roger P. Smith
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Patent number: 11691908Abstract: A vacuum insulated structure for use in an appliance includes an inner liner and an outer wrapper coupled to the inner liner. A vacuum insulated cavity is defined therebetween. An insulation material is disposed in the vacuum insulated cavity. The insulation material includes porous glass flakes.Type: GrantFiled: September 27, 2021Date of Patent: July 4, 2023Assignee: Whirlpool CorporationInventor: Devidas B. Raskar
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Patent number: 10865137Abstract: To provide a method for recycling a solar cell module glass, which enables development of other novel applications of a waste glass of a solar cell module while controlling an elution amount of Sb from the waste glass into water. Disclosed is a method for recycling a solar cell module glass, the method comprising: grinding a solar cell module glass into a glass powder; adding at least one foaming agent selected from SiC, CaCO3 and a seashell, and a particular inhibitor to the glass powder to produce a mixture; and heating the mixture to 700 to 1,100° C. to produce a foam glass.Type: GrantFiled: September 21, 2018Date of Patent: December 15, 2020Assignee: Tottori Resource Recycling Inc.Inventors: Shigenori Nakano, Hiroki Tanaka
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Patent number: 9598308Abstract: An embodiment of the present invention provides an environment-friendly functional material and a preparation method thereof, a display structure forming material, a color film substrate and a display device.Type: GrantFiled: October 15, 2014Date of Patent: March 21, 2017Assignees: BOE TECHNOLOGY GROUP CO., LTD., BEIJING BOE OPTOELECTRONICS TECHNOLOGY CO., LTD.Inventors: Jiuxia Yang, Feng Bai, Jiantao Liu
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Patent number: 9469885Abstract: An apparatus for recovering valuable metals and manufacturing multifunctional aggregate from slag. The apparatus includes a slag reforming processing pot 10 in which molten slag discharged from a converter or an electric furnace is stored, a reducing agent introducing part 20 which introduces a reducing agent into the slag reforming processing pot from above, the reducing agent recovering valuable metals from the molten slag, a reducing agent inflow part 25 which inputs a reducing agent into the slag reforming processing pot through a lower portion of a side of the slag reforming processing pot, the reducing agent recovering valuable metals from the molten slag, and cooling units 30 and 40 which create bubbles and perform controlled cooling in order to convert the molten slag, from which the valuable metals are recovered, into a light material having a porous structure.Type: GrantFiled: December 4, 2013Date of Patent: October 18, 2016Assignee: Hyundai Steel CompanyInventor: Joon-Seong Ki
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Patent number: 9302931Abstract: The invention relates to a method and to a device for ceramizing green glass in a continuous furnace, with the ceramization being carried out directly on rollers.Type: GrantFiled: March 20, 2010Date of Patent: April 5, 2016Assignee: SCHOTT AGInventors: Falk Gabel, Thoralf Johansson, Uwe Martens, Christian Roos, Friedrich Georg Schroder
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Patent number: 8936850Abstract: Foam glass may include natural glass, wherein the foam glass includes greater than 5% alumina by weight of the foam glass and has a coefficient of thermal expansion ranging between 4×10?6 ppm/° C. and 6×10?6 ppm/° C. A composition for making foam glass may include natural glass including at least 5% alumina by weight of the composition, soda ash including less than 10% by weight of the composition, and boric acid including at least 5% by weight of the composition. A method for making foam glass may include mixing natural glass with boron to form a mixture, milling the mixture, melting the mixture at a temperature of at least 900° C., and allowing the melted mixture to cool, such that the foam glass includes at least 5% alumina by weight of the foam glass and at least 5% boron oxide by weight of the foam glass.Type: GrantFiled: July 14, 2011Date of Patent: January 20, 2015Assignee: Imerys Filtration Minerals, Inc.Inventor: Bo Wang
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Patent number: 8916486Abstract: A method of making a foamed glass body, including preparing an admixture of powdered glass, at least one carbonate based foaming agent, and at least devitrification inhibitor, heating the admixture to a first temperature to soften the glass, heating the admixture to a second, higher temperature to foam the softened glass into a foamed glass body, and cooling the foamed glass body. The crystal silica content of the so-formed foamed glass body is less than 1 weight percent.Type: GrantFiled: June 4, 2008Date of Patent: December 23, 2014Inventors: Richard Lehman, Steven Haines, Andrew Ungerleider
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Patent number: 8865618Abstract: A carbon or ceramic monolithic materials with an M2 (macroporous/microporous) hierarchised porous structure is provided as well as method for preparing said materials using a macro/meso/microporous silica cavity. Such materials may be used, in particular for the production of hydrogen purifiers, supercapacitors or electrodes, or else for carrying out catalysed chemical reactions in a heterogeneous phase.Type: GrantFiled: October 28, 2009Date of Patent: October 21, 2014Assignee: Universite Pierre et Marie CurieInventors: Rénal Backov, Nicolas Brun, Clément Sanchez
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Patent number: 8846557Abstract: The present invention relates to a ceramic composition and a porous ceramic insulating material comprising the same, which is widely used as a core material in sandwich panels or fire doors. The ceramic composition comprises 44-60 wt % of glass powder, 8-15 wt % of fly ash, 4-8 wt % of surface treatment agent, and 23-29 wt % of water glass. The porous ceramic insulating material manufactured from the composition is lightweight and is an environmentally friendly material which generates no toxic gas when it catches fire. The ceramic insulating material can be produced at a low temperature of 800˜900° C., and thus has low production cost. In addition, it can be continuously manufactured in a sheet form.Type: GrantFiled: February 17, 2011Date of Patent: September 30, 2014Assignee: GMatex Co., Ltd.Inventors: Jae Young Rim, Jeong In Lim, Kil Sue Lhim
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Patent number: 8834983Abstract: The present invention provides a base material for disk rolls which is a platy molded article for obtaining ring-shaped disks for use in a disk roll comprising a rotating shaft and ring-shaped disks fitted thereon by insertion, whereby the peripheral surface of the disks serves as a conveying surface, the base material comprising inorganic fibers having a crystallization temperature of 800-900° C., a filler, and a clay. Also disclosed is a disk roll which comprises disks cut out of the base material.Type: GrantFiled: October 23, 2013Date of Patent: September 16, 2014Assignee: Nichias CorporationInventors: Masaaki Nakayama, Masatoshi Mitsuta
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Patent number: 8815758Abstract: The present application relates to a silica-based nonflammable material and to a method for preparing same. More particularly, the application relates to a silica-based nonflammable material which contains silica, limestone, and albite as main ingredients, which is obtained by a series of processes including grinding, melting, spraying, and molding, and which can replace asbestos, as well as to a method for preparing same. As functional building materials which are nonflammable even at high temperatures can be prepared using silica-based nonflammable materials consisting of silica-based minerals, and as only natural minerals may be used as main ingredients. The materials used as building materials may not be harmful to the human body and can replace asbestos that has been widely used as a conventional building material for thermal insulation, soundproofing, etc.Type: GrantFiled: May 10, 2010Date of Patent: August 26, 2014Inventors: Se-Lin Lee, Jang Seop Oh
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Patent number: 8722188Abstract: Disclosed is a process for producing ceramic particles, such as proppants, that have at least 10 percent total porosity. The process includes forming a particle precursor that includes 5 percent to 30 percent of a first ceramic material and at least 40 percent of a second ceramic material. The sintering temperature of the first ceramic material may be lower than the sintering temperature of a second ceramic material. Heating the precursor to a maximum temperature above the sintering temperature of the first material and below the sintering temperature of the second material. Also disclosed is a ceramic article that has a particular combination of chemistry and alumina crystalline phase.Type: GrantFiled: December 31, 2009Date of Patent: May 13, 2014Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventors: Tihana Fuss, Laurie San-Miguel, Kevin R. Dickson, Walter T. Stephens
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Publication number: 20140021419Abstract: Method for producing foam glass by recycling wasteglass mixture containing screen glass from television sets, computers, monitors and glass from fluorescent tubes, light bulbs and photovoltaic systems. Steps are: separately grinding individual fractions of wasteglass from various sources, forming glass powder; mixing a sintered glass composition including components of various glass powder fractions and an inorganic carbon carrier substance as activator in a dry process without adding water or liquids; and thermally treating the sintered glass composition. This composition is first subjected to a sintering process and later to a foaming process, at temperatures in a range of 855° C. to 890° C. The arising foam glass is subsequently cooled down. The sintered glass composition, which is thermally sintered glass powder and activator, is composed of at least 10 wt % of screen glass, with 85 to 90 wt % originating from screen glass and glass from fluorescent tubes, light bulbs and photovoltaic systems.Type: ApplicationFiled: April 2, 2012Publication date: January 23, 2014Applicant: TDC Trade Development and Construction Ltd.Inventors: Ralf Baier, Rainer Daniel
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Patent number: 8609244Abstract: A low density material and a method for preparing a low-density material and precursor for forming a low-density material are provided. An aqueous mixture of inorganic primary component and a blowing agent is formed, the mixture is dried and optionally ground to form an expandable precursor. Such a precursor is then fired with activation of the blowing agent being controlled such that it is activated within a predetermined optimal temperature range. The firing conditions are also controlled to provide a low density sphere containing a heterogeneous sphere wall structure comprising a combination of amorphous glass and a crystalline phase or gas phase or both.Type: GrantFiled: December 8, 2006Date of Patent: December 17, 2013Assignee: James Hardie Technology LimitedInventors: Huagang Zhang, Hamid Hojaji, Shannon Marie Labernik, David L. Melmeth, Thinh Pham, James A. McFarlane
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Patent number: 8453400Abstract: A prestressed, strong foam glass tile for use in construction. The prestressed, strong foam glass tiles of the present invention are capable of withstanding relatively large prestressing as a result of their relatively high compression strength. These prestressed, foam glass tiles will absorb and/or withstand more energy from an explosion, withstand higher heat and wind loading and other mechanical forces than traditional foam glass tiles. The foam glass tile of the present invention is strong enough that it can be prestressed over 1000 psi (lb./sq. in.), and more preferably over 2,000, 3,000, 4,000 and even more preferably over 5,000 psi. The prestressed, strong foam glass tiles of the present invention may be included as part of a prestressed assembly. Said prestressed assembly may be comprised of two metal members, one or more prestressed foam glass tiles, and a tension member such as a tension bolt and/or wires.Type: GrantFiled: July 22, 2003Date of Patent: June 4, 2013Inventor: Pedro M. Buarque de Macedo
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Patent number: 8453401Abstract: A prestressed, strong foam glass tile for use in construction. The prestressed, strong foam glass tiles of the present invention are capable of withstanding relatively large prestressing as a result of their relatively high compression strength. These prestressed, foam glass tiles will absorb and/or withstand more energy from an explosion, withstand higher heat and wind loading and other mechanical forces than traditional foam glass tiles. The foam glass tile of the present invention is strong enough that it can be prestressed over 1000 psi (lb./sq. in.), and more preferably over 2,000, 3,000, 4,000 and even more preferably over 5,000 psi. The prestressed, strong foam glass tiles of the present invention may be included as part of a prestressed assembly. Said prestressed assembly may be comprised of two metal members, one or more prestressed foam glass tiles, and a tension member such as a tension bolt and/or wires.Type: GrantFiled: December 1, 2006Date of Patent: June 4, 2013Inventor: Pedro M. Buarque de Macedo
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Publication number: 20130116107Abstract: Foam glass may include natural glass, wherein the foam glass includes greater than 5% alumina by weight of the foam glass and has a coefficient of thermal expansion ranging between 4×10?6 ppm/° C. and 6×10?6 ppm/° C. A composition for making foam glass may include natural glass including at least 5% alumina by weight of the composition, soda ash including less than 10% by weight of the composition, and boric acid including at least 5% by weight of the composition. A method for making foam glass may include mixing natural glass with boron to form a mixture, milling the mixture, melting the mixture at a temperature of at least 900° C., and allowing the melted mixture to cool, such that the foam glass includes at least 5% alumina by weight of the foam glass and at least 5% boron oxide by weight of the foam glass.Type: ApplicationFiled: July 14, 2011Publication date: May 9, 2013Applicant: Imerys Filtration Minerals, Inc.Inventor: Bo Wang
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Publication number: 20130085056Abstract: A method for producing a quartz glass body from a get body is provided, wherein the gel body generated from a colloidal suspension is at least formed and compressed into the quartz glass body Displacement bodies are added to the colloidal suspension prior to gelating into the gel body, and are completely removed from the gel body after gelating, wherein hollow spaces are generated at the positions of the removed displacement bodies, so that a translucent or opaque quartz glass body is generated. Further, a gel body for producing a quartz glass body is provided, wherein displacement bodies are introduced into the gel body that can be completely removed from the gel body, so that hollow spaces arise at the positions of the displacement bodies. A quartz glass body is also provided that includes vacuoles or hollow spaces filled with gas.Type: ApplicationFiled: November 28, 2012Publication date: April 4, 2013Applicant: QSIL GMBH QUARZSCHMELZE ILMENAUInventor: QSIL GmbH Quarzschmelze Ilmenau
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Publication number: 20130045853Abstract: Provided is a method of producing a porous glass having a high strength by a safe, simple process that does not involve the use of any high-temperature heat treatment or acid treatment step. The method includes: mixing 4 wt % or more to 6.5 wt % or less of sodium oxide, 26 wt % or more to 36 wt % or less of boron oxide, and 60 wt % or more to 68 wt % or less of silicon oxide; heating the mixed materials to melt the materials and cooling the molten materials to obtain a glass body; and a step involving bringing the glass body into contact with water without reheating the glass body to obtain the porous glass.Type: ApplicationFiled: May 13, 2011Publication date: February 21, 2013Applicant: CANON KABUSHIKI KAISHAInventors: Yoshinori Kotani, Zuyi Zhang, Kenji Takashima
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Publication number: 20120028329Abstract: The present invention relates to an optically transparent glass foam or glass-ceramic foam as well as to a method for the production of an optically transparent glass foam or glass-ceramic foam. A method is described for the production of optically transparent foams, wherein the following steps are conducted: a) Mixing of pre-ceramic Si polymer, glass powder and glass converter; b) Heating of the mixture to a temperature below the decomposition temperature of the pre-ceramic Si polymer with the formation of a foam; c) Heating the obtained foam to a temperature above the decomposition temperature of the pre-ceramic Si polymer; d) Heating the obtained product to a temperature between 700° C. and 1400° C. with the formation of glass; and e) Cooling the thus-obtained product to ambient temperature.Type: ApplicationFiled: June 24, 2009Publication date: February 2, 2012Inventors: Michael Scheffler, Christiane Ohl, Christina Olschewski, Viola Wilker, Franziska Scheffler
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Patent number: 8025838Abstract: The invention provides a process of making porous structures or materials, including the colloidal processing (e.g. slip casting, pressure casting, tape casting or electrophoretic deposition) of solid particle emulsions to form a green body that can be directly sintered without a de-binding step.Type: GrantFiled: June 27, 2006Date of Patent: September 27, 2011Assignee: K.U. Leuven Research & DevelopmentInventors: Bram Neirinck, Jozef Vleugels, Jan Fransaer, Omer Van Der Biest
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Publication number: 20110152056Abstract: There is provided a method for making hollow microspheres including heating a feed under conditions sufficient to convert at least a portion of the feed into hollow microspheres, where the heating is conducted under a vacuum. There is also provided hollow microspheres made using this method.Type: ApplicationFiled: December 21, 2009Publication date: June 23, 2011Inventor: Gang Qi
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Publication number: 20110152057Abstract: There is provided hollow microspheres that are essentially free of blowing agent. There is also provided hollow microspheres comprising perlite and having a single cell structure.Type: ApplicationFiled: December 21, 2009Publication date: June 23, 2011Inventor: Gang Qi
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Patent number: 7932188Abstract: Low dielectric materials and films comprising same have been identified for improved performance when used as interlevel dielectrics in integrated circuits as well as methods for making same. In one aspect of the present invention, an organosilicate glass film is exposed to an ultraviolet light source wherein the film after exposure has an at least 10% or greater improvement in its mechanical properties (i.e., material hardness and elastic modulus) compared to the as-deposited film.Type: GrantFiled: October 31, 2008Date of Patent: April 26, 2011Assignee: Air Products and Chemicals, Inc.Inventors: Aaron Scott Lukas, Mark Leonard O'Neill, Jean Louise Vincent, Raymond Nicholas Vrtis, Mark Daniel Bitner, Eugene Joseph Karwacki, Jr.
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Patent number: 7900474Abstract: Hollow glass microspheres are made using selenium oxide as the blowing agent. The use of selenium oxide provides two unique advantages: lower density and smaller hollow microspheres are obtained because loss of selenium oxide gas out of the liquid glass bubble during formation is slow, and the hollow microspheres will contain a vacuum due to the condensation of selenium oxide gas blowing agent upon cooling of the spheres below 315 deg. C.Type: GrantFiled: August 14, 2008Date of Patent: March 8, 2011Inventor: Warren R. Beck
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Patent number: 7871589Abstract: Provided is a pyrogenically prepared SiO2 powder in the form of aggregated primary particles having a statistical thickness surface area (STSA) of 10-500 m2/g, a thickening action based on the STSA of 4-8 mPas·g/m2, and a micropore volume of 0.03-0.Type: GrantFiled: May 21, 2008Date of Patent: January 18, 2011Assignee: Evonik Degussa GmbHInventors: Andreas Hille, Florian Felix Kneisel, Volker Hamm, Matthias Rochnia
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Patent number: 7829489Abstract: The present invention describes a composition, method and article for a photomachinable glass having a coefficient of thermal expansion from less than 6×10?6/° C. in the temperature range of 0° C. to 300° C. The photomachinable glass composition is a low expansion glass having an amorphous glass phase and crystalline phases selected from the group consisting of spudomene and lithium disilicate.Type: GrantFiled: August 31, 2007Date of Patent: November 9, 2010Assignee: Corning IncorporatedInventors: Nicholas Francis Borrelli, Kathryn L Goetschius, David Lathrop Morse, Charlene Marie Smith
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Publication number: 20100221540Abstract: The invention relates to a process for producing a porous glass and glass powder using a partial Vycor process on an alkali metal borosilicate glass material. The process is characterized in that an addition of metal oxides and/or rare earth metal oxides in variable proportions of from 0.05 to 15 percent by mass is carried out on the alkali metal borosilicate glass material during the course of the Vycor process, with a doping incorporation of the metal oxides and/or the rare earth metal oxides into the resulting SiO2 matrix with an increase in the optical index of refraction of the porous glass being brought about during the Vycor process, and an opposed jet milling process is employed in combination with a ceramic sifter wheel in a subsequent dry milling process, with classification of the porous glass particles produced which have a size range of less than 15 ?m being carried out.Type: ApplicationFiled: February 24, 2006Publication date: September 2, 2010Applicant: VitraBio GmbHInventor: Monika Hermann
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Patent number: 7700670Abstract: A molding composition formulation includes a thermoset cross-linkable polymeric resin. Glass microspheroids are present such that upon cure of the resin the resulting article has a linear shrinkage of less than ±0.06% and a density of less than 1.65. An article formed from such a composition is further strengthened by the addition of a surface activating agent bonded to the surface of the glass microspheroids. Conventional particulate fillers when added to an inventive formulation provide enhanced performance when the filler particle has a size sufficiently small to insert within adjacent microspheroid interstitial voids. An unsaturated polyester resin so formed is particularly well suited for the formation of sheet molding compound formulations.Type: GrantFiled: May 15, 2006Date of Patent: April 20, 2010Inventors: Brian A. Beach, Probir K. Guha, Brad Haskell, Michael J. Siwajek
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Patent number: 7658990Abstract: A super lightweight ceramic panel for a non-bearing wall utilizing an expandable clay mineral and a process for preparing the same are provided. The super lightweight ceramic panel is comprised of a clay composition containing 90 to 98% by weight of an expandable clay mineral, 1.5 to 5% by weight of a flux (glass), and 0.5 to 5% by weight of silicon carbide, and is prepared by mixing and pressing the clay composition, followed by firing at a temperature of 1100 to 1200° C. The super lightweight ceramic panel in accordance with the present invention is a material having a light weight and exhibiting improvement in physical properties such as water resistance, flame retardancy, heat insulation and rigidity, via formation of closed pores inside the ceramic material.Type: GrantFiled: November 4, 2005Date of Patent: February 9, 2010Assignee: LG Chem, Ltd.Inventor: Sang-Ho Shin
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Publication number: 20090298667Abstract: The present invention provides compositions and methods for producing porous ceramic articles. The compositions and methods comprise a ceramic precursor batch comprising an organic peroxide pore forming agent where the pore forming agent is an organo-adduct of hydrogen peroxide and an organic compound or an organic peroxide of the general formula R—O—O—R?. The organic peroxide pore forming agent is stable during extrusion and other methods for forming a green body and does not decompose until the green body is dried.Type: ApplicationFiled: May 30, 2008Publication date: December 3, 2009Inventors: William Peter Addiego, Christopher Raymond Glose
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Publication number: 20090133440Abstract: A method of making a foamed glass body, including preparing an admixture of powdered glass, at least one carbonate based foaming agent, and at least devitrification inhibitor, heating the admixture to a first temperature to soften the glass, heating the admixture to a second, higher temperature to foam the softened glass into a foamed glass body, and cooling the foamed glass body. The crystal silica content of the so-formed foamed glass body is less than 1 weight percent.Type: ApplicationFiled: June 4, 2008Publication date: May 28, 2009Applicant: Earthstone International LLCInventors: Richard Lehman, Steven Haines, Andrew Ungerleider
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Patent number: 7538068Abstract: A carbon dioxide gas absorbent includes a porous body containing a lithium complex oxide. The porous body includes pores having a pore diameter distribution such that main pores which consist of first pores with a diameter of 10 to 100 ?m and second pores with a diameter larger than 100 ?m and 500 ?m or smaller occupy 80 to 100%, third pores with a diameter smaller than 10 ?m occupy 0 to 10% and fourth pores with a diameter larger than 500 ?m occupy 0 to 10%, the main pores have a pore diameter distribution such that the first pores occupy 15 to 85% and second pores occupy 15 to 85%.Type: GrantFiled: March 16, 2006Date of Patent: May 26, 2009Assignee: Kabushiki Kaisha ToshibaInventors: Masahiro Kato, Toshihiro Imada, Kenji Essaki
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Patent number: 7479265Abstract: This invention relates to ?-SiC foam parts with a specific surface area preferably equal to at least 5 m2/g and with at least two zones A and B with a different cellular porosity distribution, wherein the parts were made by chemical transformation of a porous precursor medium comprising at least two blocks A? and B?, each having a different cellular porosity distribution, and in that the at least two zones A and B are derived from the chemical transformation of the two blocks A? and B?. This foam, optionally after deposition of an active layer, may be used as a filter medium in cartridges designed for the purification of exhaust gases. The invention also relates to manufacturing processes for preparing such a filter medium.Type: GrantFiled: October 14, 2004Date of Patent: January 20, 2009Assignees: SICAT, Entre National de la Recherche Scientifigue, Universite Louis Pasteur de StrasbourgInventors: Charlotte Pham, Laurie Pesant, Pierre Bernhardt, Michel Wolf, Cuong Pham-Huu, Marc-Jacques Ledoux, Michel Kartheuser, Estelle Vanhaecke
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Patent number: 7468290Abstract: Low dielectric materials and films comprising same have been identified for improved performance when used as interlevel dielectrics in integrated circuits as well as methods for making same. In one aspect of the present invention, an organosilicate glass film is exposed to an ultraviolet light source wherein the film after exposure has an at least 10% or greater improvement in its mechanical properties (i.e., material hardness and elastic modulus) compared to the as-deposited film.Type: GrantFiled: July 21, 2003Date of Patent: December 23, 2008Assignee: Air Products and Chemicals, Inc.Inventors: Aaron Scott Lukas, Mark Leonard O'Neill, Jean Louise Vincent, Raymond Nicholas Vrtis, Mark Daniel Bitner, Eugene Joseph Karwacki, Jr.
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Publication number: 20080307760Abstract: Disclosed are plugging mixtures for forming a ceramic honeycomb wall flow filter. The plugging mixtures exhibit a reduced percentage of volumetric shrinkage during the drying process and generally comprise an inorganic ceramic powder batch composition; an organic binder; a liquid vehicle; and a non-foaming volume transformation agent. Also disclosed are methods for forming plugged ceramic wall flow filters from such plugging mixtures and honeycomb articles produced therefrom.Type: ApplicationFiled: March 19, 2008Publication date: December 18, 2008Inventors: Shyam Lekhraj Chatlani, Isabelle Marie Chauvel-Melscoet, Luiz Eduardo Ferri
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Patent number: 7459208Abstract: Improved foam glass products prepared from natural glasses, such as unexpanded fine perlite ore and expanded fine perlite, methods of producing the improved foam glass products, and methods of use thereof are provided. The improved foam glass product made from natural glasses has, for example, a thermal conductivity less than 0.70 Btu·in/hr·F·ft2 (0.101 W/m° K) at 73° F.(296° K), a compressive strength greater than 100 PSI (689 kPa) and a density less than 20 lb/ft3 (320 kg/m3). The improved foam glass product made from natural glasses may be used in a variety of applications including thermal and acoustic insulation applications.Type: GrantFiled: August 20, 2001Date of Patent: December 2, 2008Assignee: Advanced Minerals CorporationInventor: Bo Wang
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Publication number: 20080191834Abstract: A low-capacitance multilayer chip varistor has capacitance lower than 0.5 pF at 1 MHz and has a characteristic of resisting more than thousands of times of 8 KV electrostatic shock, which comprises a ceramic main body, outer electrodes disposed at two ends of the ceramic main body and inner electrodes disposed therein; the ceramic main body comprises inorganic glass of 3˜50 wt % and semi-conductive or conductive particles of 50˜97 wt % with particle size of more than 0.1 ?m, and a layer of inorganic glass film covers the surface of semi-conductive or conductive particles, wherein the inorganic glass film contains semi-conductive or conductive particles of submicron or nanometer which is smaller than 1 micron, and the quantity contained of semi-conductive or conductive particles is less than 20 wt % of that of inorganic glass.Type: ApplicationFiled: February 12, 2007Publication date: August 14, 2008Applicant: SFI Electronics Technology Inc.Inventors: Ching-Hohn Lien, Cheng-Tsung Kuo, Jun-Nun Lin, Jie-An Zhu, Li-Yun Zhang, Xing-Guang Huang, Wei-Cheng Lien
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Patent number: 7252713Abstract: A method of facilitating the crystallisation of a macromolecule comprising the step of adding a mesoporous glass to a crystallisation sample wherein the mesoporous glass comprises pores having diameters between 4 nm and 100 nm and has a surface area of at least 50 m2/g. A method of facilitating the crystallisation of a macromolecule comprising the step of adding to a crystallisation sample a mesoporous glass of the composition Si02; CaO—P205-SiO2 or Na20-CaO—P205-SiO2, wherein each of the Ca, P, Si or Na atoms within the compositions may be substituted with a suitable atom chosen from B, Al, Ti, Mg, or K, and, optionally, the composition may also include heavy elements to enhance X-ray diffraction contrast such as Ag, Au, Cr, Co, Sr, Ba, Pt, Ta or other atom with an atomic number over 20.Type: GrantFiled: November 7, 2003Date of Patent: August 7, 2007Assignee: Imperial Collage Innovations LimitedInventors: Naomi Chayen, Larry Hench
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Patent number: 7169721Abstract: Disclosed herein are a self-foamed porous ceramic composition and a method for making a porous ceramic using the self-foamed porous ceramic composition. The self-foamed porous ceramic is obtained by fabricating a glass consisting of 41˜47 mole % of calcium oxide (CaO), 41˜47 mole % of silica (SiO2) and 6˜18 mole % of borate (B2O3), pulverizing the glass into a finely-divided glass powder having an average particle size of 1˜10 ?m, molding the glass powder, and sintering the molded glass powder.Type: GrantFiled: August 27, 2003Date of Patent: January 30, 2007Assignee: Seoul National University Industry FoundationInventors: Hyun Seung Yu, Kug Sun Hong, Hwan Kim, Dong Ho Lee, Choon Ki Lee, Bong Soon Chang, Deug Joong Kim, Jun Hyuk Seo, Jae Hyup Lee, Ki Soo Park
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Patent number: 7041366Abstract: The invention provides porous silicon nitride ceramics that having uniform, fine closed pores and a manufacturing method thereof. Metal Si powder is mixed with a sintering additive, followed by thermal treatment, which is a pre-process for forming a specific grain boundary phase. Two-stage thermal treatment is thereafter performed by microwave heating at a temperature of 1000° C. or more. The metal Si powder is thereafter subjected to a nitriding reaction from its surface, the metal Si is thereafter diffused to nitride formed on the outer shell thereof such that porous silicon nitride ceramics having uniform, fine closed pores can be produced. Having a high ratio of closed pores and being superior in electrical/mechanical characteristics, the porous silicon nitride ceramics can display excellent characteristics if used, for example, for an electronic circuit board that requires an anti-hygroscopicity, a low dielectric constant, a low dielectric loss, and mechanical strength.Type: GrantFiled: March 22, 2002Date of Patent: May 9, 2006Assignee: Sumitomo Electric Industries, Ltd.Inventors: Michimasa Miyanaga, Osamu Komura
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Patent number: 6927185Abstract: As-prepared AlPO4—B2O3—Na2O-based glasses were placed in an autoclave together with distilled water and were treated at 150° C. for two hours. Although the specific surface area of the as-prepared glass prior to autoclave treatment was negligibly small, the autoclave treatment dissolved most of the borate component and the sodium component to obtain a mesoporous material having a specific surface area of 236 m2/g and a pore size distribution of 5 to 10 nm. This mesoporous material is hydrophobic and has weak solid acidity and small polarity.Type: GrantFiled: January 11, 2002Date of Patent: August 9, 2005Assignee: Japan Science and Technology CorporationInventors: Shoji Yamanaka, Toshiyuki Sasaki
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Patent number: 6890873Abstract: Pyrogenically prepared silicon dioxide with the following physicochemical properties: 1. Average particle size (D50 value) D50?150 nm (dynamic light scattering, 30 wt %) 2. Viscosity (5 rpm, 30 wt %) ??100 m·Pas 3. Thixotropy of Ti (?(5 rpm))/(?(50 rpm))?2 4. BET surface area 30-60 m2/g 5. Compacted bulk=100-160 g/L 6. Original pH?4.5 that can be used for the preparation of dispersions and glass bodies.Type: GrantFiled: December 8, 2003Date of Patent: May 10, 2005Assignee: Degussa AGInventors: Monika Oswald, Gerrit Schneider, Klaus Deller
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Patent number: 6770111Abstract: A ceramic structure which is pollucite-based and has high refractoriness and high resistance to thermal shock. The inventive structure is suitable in high temperature applications such as a filtering particulates from diesel engine exhaust.Type: GrantFiled: October 25, 2001Date of Patent: August 3, 2004Assignee: Corning IncorporatedInventors: Robert Morena, Dell J. St. Julien, Bryan R. Wheaton, John F. Wight, Jr.
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Patent number: 6710001Abstract: A porous sintered body in which the leaching amounts of heavy metals are small and having high availability contains 0.5-15 weight % of B2O3, preferably contains 20-60 weight % of Al2O3, 18-60 weight % of SiO2, 1-12 weight % of the sum of Na2O, K2O, Li2O, and P2O5, 1-30 weight % of the sum of CaO, SrO, BaO, and MgO, and 0.5-15 weight % of B2O3.Type: GrantFiled: July 31, 2001Date of Patent: March 23, 2004Assignee: Inax CorporationInventors: Osamu Watanabe, Shuji Kawai
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Publication number: 20040053766Abstract: Disclosed herein are a self-foamed porous ceramic composition and a method for making a porous ceramic using the self-foamed porous ceramic composition. The self-foamed porous ceramic is obtained by fabricating a glass consisting of 41˜47 mole % of calcium oxide (CaO), 41˜47 mole % of silica (SiO2) and 6˜18 mole % of borate (B2O3), pulverizing the glass into a finely-divided glass powder having an average particle size of 1˜10 &mgr;m, molding the glass powder, and sintering the molded glass powder.Type: ApplicationFiled: August 27, 2003Publication date: March 18, 2004Inventors: Hyun Seung Yu, Kug Sun Hong, Hwan Kim, Dong Ho Lee, Choon Ki Lee, Bong Soon Chang, Deug Joong Kim, Jun Hyuk Seo, Jae Hyup Lee, Ki Soo Park
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Patent number: 6596834Abstract: Silicone resins having the general formula (R1SiO3/2)x(HSiO3/2)y where R1 is an alkyl group having 8 to 24 carbon atoms; x has a value of 0.05 to 0.7; y has a value of 0.3 to 0.95 and x+y =1. The resins are used to form porous ceramic materials and porous thin films on semiconductor devices.Type: GrantFiled: September 12, 2001Date of Patent: July 22, 2003Assignee: Dow Corning CorporationInventor: Bianxiao Zhong
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Patent number: 6562744Abstract: Inorganic porous materials contained in a confined space with at least one dimension of less than 1 mm, which are in liquid tight contact with the walls of said confined space. Preferred as the confined space are capillaries. Articles contained such materials and methods for making them in the confined space are described.Type: GrantFiled: July 21, 2000Date of Patent: May 13, 2003Assignee: Merck Patent GmbHInventors: Kazuki Nakanishi, Naohiro Soga, Tokiyo Minakuchi