And Carbonaceous Material Patents (Class 501/90)
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Patent number: 11414354Abstract: A ceramic matrix composite article includes a melt infiltration ceramic matrix composite substrate comprising a ceramic fiber reinforcement material in a ceramic matrix material having a first free silicon proportion, and a melt infiltration ceramic matrix composite outer layer comprising a ceramic fiber reinforcement material in a ceramic matrix material having a second free silicon proportion disposed on an outer surface of at least a portion of the substrate, or a polymer impregnation and pyrolysis ceramic matrix composite outer layer comprising a ceramic fiber reinforcement material in a ceramic matrix material having a second free silicon proportion disposed on an outer surface of at least a portion of the substrate. The second free silicon proportion is less than the first free silicon proportion.Type: GrantFiled: May 22, 2018Date of Patent: August 16, 2022Assignee: General Electric CompanyInventor: James Dale Steibel
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Patent number: 11286209Abstract: A method of manufacturing a ceramic matrix composite component may include introducing a gaseous precursor into an inlet portion of a chamber that houses a porous preform and introducing a gaseous mitigation agent into an outlet portion of the chamber that is downstream of the inlet portion of the chamber. The gaseous precursor may include methyltrichlorosilane (MTS) and the gaseous mitigation agent may include hydrogen gas. The introduction of the gaseous precursor may result in densification of the porous preform(s) and the introduction of the gaseous mitigation agent may shift the reaction equilibrium to disfavor the formation of harmful and/or pyrophoric byproduct deposits, which can accumulate in an exhaust conduit 340 of the system.Type: GrantFiled: June 5, 2020Date of Patent: March 29, 2022Assignee: Goodrich CorporationInventors: Ying She, Naveen G. Menon, Zissis A. Dardas, Thomas P. Filburn
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Patent number: 11285242Abstract: Silicon carbide (SiC) is an inert material with excellent biocompatibility properties. The biocompatibility is associated with the chemical inertness of the material. Tissue response to inert material is the formation of thin fibrous capsule. In some embodiments described herein, the conversion of SiC from inert material to bioactive material capable of stimulating cell function and making direct bond with tissue is described and the body response to bioactive materials is direct binding without any fibrous capsule.Type: GrantFiled: December 17, 2020Date of Patent: March 29, 2022Assignee: THE UNIVERSITY OF NORTH CAROLINA AT CHARLOTTEInventor: Ahmed El-Ghannam
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Patent number: 11261133Abstract: This application describes a method of making a super-hard article that includes a super-hard structure bonded to a substrate. The super-hard structure generally includes a sintered plurality of super-hard grains made from cubic boron nitride. The method generally includes providing raw material powder suitable for sintering the super-hard structure; combining the raw material powder with an organic binder material in a liquid medium to form a paste; providing a substrate assembly having a formation surface area configured for forming a boundary of the super-hard structure, the substrate having a recess coterminous with the formation surface area; extruding the paste into contact with the formation surface area to provide a paste assembly; and heat treating and/or sintering the paste assembly to remove the binder material and provide a pre-sinter assembly.Type: GrantFiled: July 10, 2015Date of Patent: March 1, 2022Assignee: Element Six (UK) LimitedInventor: Santonu Ghosh
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Patent number: 11097985Abstract: A carbon composite composition and a carbon heater are provided. The carbon composite composition may include a phenolic resin as a binder, a lubricant, and a base material that determines a specific resistance of a resistance heating element at a high temperature. The carbon composite composition may prevent a dielectric breakdown, a spark and plasma from occurring in a carbon heater, and may improve radiation efficiency of the carbon heater.Type: GrantFiled: May 9, 2018Date of Patent: August 24, 2021Assignees: LG ELECTRONICS INC., INDUSTRY FOUNDATION OF CHONNAM NATIONAL UNIVERSITYInventors: Youngjun Lee, Kap Seung Yang, Sang Wan Kim
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Patent number: 11033863Abstract: A filter for the filtration of a fluid, such as a liquid, includes or composed of a support element made of a porous ceramic material, the element having a tubular or parallelepipedal shape delimited by an external surface and including, in its internal portion, a set of adjacent channels with axes parallel to one another and separated from one another by walls of the porous inorganic material, wherein at least a portion of the channels and/or at least a portion of the external surface are covered with a porous separating membrane layer, wherein the layer is made of a material essentially composed of sintered grains of silicon carbide (SiC), and the weight content of elemental oxygen of the layer is less than 0.5%.Type: GrantFiled: December 18, 2015Date of Patent: June 15, 2021Assignees: SAINT-GOBAIN CENTRE DE RECHERCHES ET D'ETUDES EUROPEAN, CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE, UNIVERSITE DE MONTPELLIER, ECOLE NATIONALE SUPERIEURE DE CHIMIE DE MONTPELLIERInventors: Daniel Urffer, Christian Guizard
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Patent number: 10961161Abstract: A production method of a ceramic matrix composite is consisted of: forming a ceramic compact including one or more of a reinforcement fiber and a powder, each including SiC; attaching an ingot of a ternary or more multicomponent Si alloy including Y onto the ceramic compact; and infiltrating the alloy into the ceramic compact by heating up to a temperature at which the alloy melts.Type: GrantFiled: January 8, 2019Date of Patent: March 30, 2021Assignee: IHI CorporationInventors: Shingo Kanazawa, Akihiro Sato, Yousuke Mizokami, Takeshi Nakamura, Ryoji Kakiuchi, Yuuya Nagami
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Patent number: 10800709Abstract: A ceramic composite can include a first ceramic phase and a second ceramic phase. The first ceramic phase can include a silicon carbide. The second phase can include a boron carbide. In an embodiment, the silicon carbide in the first ceramic phase can have a grain size in a range of 0.8 to 200 microns. The first phase, the second phase, or both can further include a carbon. In another embodiment, at least one of the first ceramic phase and the second ceramic phase can have a median minimum width of at least 5 microns.Type: GrantFiled: December 13, 2018Date of Patent: October 13, 2020Assignee: SAINT-GOBAIN CERAMICS AND PLASTICS, INC.Inventors: Diana R. Tierney, Matthew Creedon, Tom J. Trunzo, Kenneth R. Delahunty
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Patent number: 10508056Abstract: Disclosed herein are methods of forming substantially crystalline, dense silicon carbide fibers from infusible polysilazane fibers by utilizing a single stage pyrolysis. The pyrolysis is performed using a continuous process in a single furnace with a constant atmospheric condition. Also disclosed are substantially crystalline, dense silicon carbide fibers formed by these methods.Type: GrantFiled: April 12, 2016Date of Patent: December 17, 2019Assignee: GENERAL ELECTRIC COMPANYInventors: Anthony Yu-Chung Ku, Gary C. Buczkowski, Ryan Christopher Mills, Peter Kennedy Davis
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Patent number: 9751807Abstract: Systems, methods and devices adapted to ease manufacture of composite articles (e.g., ceramic composite articles), particularly composite articles which include a hollow feature are disclosed. In one embodiment, a system includes: a consumable core formed to be disposed within an inner portion of a composite precursor, the consumable core adapted to convert into an infiltrant during a manufacturing process and infiltrate the composite precursor.Type: GrantFiled: August 16, 2012Date of Patent: September 5, 2017Assignee: General Electric CompanyInventors: Glenn Curtis Taxacher, Peter de Diego, Paul Edward Gray, Philip Harold Monaghan
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Patent number: 9362576Abstract: In one embodiment, an electrical power storage system using hydrogen includes a power generation unit generating power using hydrogen and oxidant gas and an electrolysis unit electrolyzing steam. The electrical power storage system includes a hydrogen storage unit storing hydrogen generated by the electrolysis and supplying the hydrogen to the power generation unit during power generation, a high-temperature heat storage unit storing high temperature heat generated accompanying the power generation and supplying the heat to the electrolysis unit during the electrolysis, and a low-temperature heat storage unit storing low-temperature heat, which is exchanged in the high-temperature heat storage unit and generating with this heat the steam supplied to the electrolysis unit.Type: GrantFiled: December 3, 2012Date of Patent: June 7, 2016Assignee: KABUSHIKI KAISHA TOSHIBAInventors: Shoko Suyama, Yoshiyasu Ito, Shigeo Kasai, Yasuo Takagi, Tsuneji Kameda, Kentaro Matsunaga, Masato Yoshino, Daisuke Horikawa, Kazuya Yamada
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Patent number: 9353013Abstract: A SiC ceramic material includes a bundle of SiC continuous fibers in a porous SiC ceramic matrix, has thermal insulation properties, a high level of strength and a high degree of toughness. A SiC ceramic structure is made of the SiC ceramic material. It is produced by preparing a pressure-sintered compact using a slurry prepared by mixing SiC powder and carbon powder in a liquid and by gasifying and releasing the carbon powder. The SiC ceramic structure can be produced by heating a reaction preparation containing a bundle of SiC continuous fibers and Si powder to a temperature equal to or higher than the melting point of silicon causing a reaction of the carbon component and Si powder and thereby obtaining a reaction-sintered compact, and by gasifying and releasing the carbon component from the reaction-sintered compact. The SiC ceramic can be produced by a chemical vapor deposition method.Type: GrantFiled: November 10, 2011Date of Patent: May 31, 2016Assignee: KYOTO UNIVERSITYInventors: Tatsuya Hinoki, Yi-Hyun Park
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Patent number: 9085493Abstract: Produced is a silicon carbide-coated carbon base material in which a silicon carbide coating is densely and uniformly formed on the surface of a carbon base material, such as graphite. A production process includes the steps of: preparing a carbon base material the surface of which has basal plane sites of an SP2 carbon structure with no dangling bond and edge plane sites of an SP2 carbon structure with a dangling bond; and reacting the surface of the carbon base material with SiO gas in an atmosphere at a temperature of 1400° C. to 1600° C. and a pressure of 1 to 150 Pa to form silicon carbide, whereby the carbon base material coated with silicon carbide is produced.Type: GrantFiled: September 1, 2010Date of Patent: July 21, 2015Assignee: Toyo Tanso Co., Ltd.Inventors: Masaharu Nakamura, Yoshinari Miyamoto, Tetsuro Tojo
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Publication number: 20150141235Abstract: A method of fabricating a carbon fiber-reinforced article includes providing carbon fibers that have surfaces that include an initial interfacial bonding strength capacity with respect to bonding with boron nitride. The surfaces are then modified to reduce the initial interfacial bonding strength capacity. A layer of boron nitride is then deposited on the modified surfaces and the carbon fibers are then embedded in a ceramic matrix. A carbon fiber-reinforced article includes the carbon fibers, the layer of boron nitride on the surfaces of the carbon fibers, and the ceramic matrix. The article exhibits non-brittle fracture.Type: ApplicationFiled: December 28, 2012Publication date: May 21, 2015Applicant: UNITED TECHNOLOGIES CORPORATIONInventors: Michael A. Kmetz, Sam Frueh
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Patent number: 9006121Abstract: A pipe choke for use in drilling and mining operations comprising a body including a first end and a second end configured to couple to a pipe, an opening extending through the body from the first end to the second end, and wherein the body includes a first phase comprising recrystallized silicon carbide and a second phase comprising silicon.Type: GrantFiled: December 31, 2012Date of Patent: April 14, 2015Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventors: Christopher J. Reilly, Edmund A. Cortellini, Robin M. Harrington
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Patent number: 8962504Abstract: The disclosure provides novel graphene-reinforced ceramic composites and methods for making such composite materials.Type: GrantFiled: July 27, 2012Date of Patent: February 24, 2015Assignee: Arizona Board of Regents on Behalf of The University of ArizonaInventors: Erica L. Corral, Luke S. Walker, Victoria R. Marotto, Mohammad A. Rafiee, Nikhil Koratkar
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Patent number: 8951638Abstract: A silicon carbide powder for the production of a silicon carbide single crystal has an average particle diameter of 100 ?m or more and 700 ?m or less and a specific surface area of 0.05 m2/g or more and 0.30 m2/g or less. A method for producing a silicon carbide powder for the production of the silicon carbide single crystal including sintering a silicon carbide powder having an average particle diameter of 20 ?m or less under pressure of 70 MPa or less at a temperature of 1900° C. or more and 2400° C. or less and in a non-oxidizing atmosphere, thereby obtaining a sintered body having a density of 1.29 g/cm3 or more; adjusting particle size by means of pulverization of the sintered body; and removing impurities by means of an acid treatment.Type: GrantFiled: May 15, 2013Date of Patent: February 10, 2015Assignees: Denki Kagaku Kogyo Kabushiki Kaisha, National Institute of Advanced Industrial Science and TechnologyInventors: Tomohisa Katou, Yusuke Takeda, Hiroshi Murata
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Publication number: 20150005151Abstract: There are provided a carbon fiber composite material having higher strength than conventional carbon fiber composite materials, and a brake member, a structural member for semiconductor, a heat resistant panel and a heat sink, all of which use this carbon fiber composite material. The carbon fiber composite material is obtained by mixing carbon fiber with a resin, subsequently molding the mixture and carbonizing the molded product, and subjecting the resultant carbonized product to melt impregnation with silicon, in which the lattice spacing d002 of the carbon (002) plane of the carbon fiber as measured by an X-ray diffraction method is 3.36 to 3.43. A brake member, a structural member for semiconductor, a heat resistant panel and a heat sink, all of which use this carbon fiber composite material, are provided. The carbon fiber is preferably a carbon fiber obtained by calcining a pitch-derived precursor.Type: ApplicationFiled: February 18, 2011Publication date: January 1, 2015Inventors: Kazuya BABA, Kazuyuki Akasaka
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Patent number: 8916488Abstract: A sliding member having a sliding surface comprising a silicon carbide sintered body having a primary phase comprising mainly silicon carbide, and a subphase having a different composition from the primary phase and containing at least boron, silicon and carbon. The ratio of pores having a roundness of 6 ?m or less and a pore diameter of 10 to 60 ?m with respect to all pores having a pore diameter of 10 ?m or more in the sliding surface is 60% or more. This enables retention of good seal properties even in a long-term continuous use. The subphase in the silicon carbide sintered body is preferably granular crystal phases dotted among a plurality of the primary phases. This provides excellent lubricating liquid holding performance as well as excellent thermal conductivity and excellent thermal shock resistance properties.Type: GrantFiled: October 30, 2007Date of Patent: December 23, 2014Assignee: Kyocera CorporationInventors: Yuusaku Ishimine, Kazuaki Takigawa
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Publication number: 20140339718Abstract: Silicon carbide composite materials contain CSiC with a density of 2.95 to 3.05 g/cm?3 and a fiber bundle content of 2 to 10 wt. %. The fiber bundles have a length of 6 to 20 mm, a width of 0.2 to 3 mm, and a thickness of 0.1 to 0.8 mm. The fiber bundles are filled with a cured phenolic resin content of up to 45 wt. %, and the protected fiber bundles are integrated into an SiC matrix. A method produces the silicon carbide composite materials.Type: ApplicationFiled: August 4, 2014Publication date: November 20, 2014Inventors: TANJA DAMJANOVIC, ANDREAS KIENZLE, INGRID KRAETSCHMER
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Publication number: 20140329663Abstract: A composition having nanoparticles of silicon carbide and a carbonaceous matrix or silicon matrix. The composition is not in the form of a powder. A composition having silicon and an organic compound having a char yield of at least 60% by weight or a thermoset made from the organic compound. A method of combining silicon and the organic compound and heating to form silicon carbide or silicon nitride nanoparticles.Type: ApplicationFiled: May 19, 2014Publication date: November 6, 2014Applicant: The Govenment of the United States of America, as represented by the Secretary of the NavyInventors: Teddy M. Keller, Andrew Saab, Matthew Laskoski
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Patent number: 8828540Abstract: A process for manufacturing an article includes the steps of applying a quantity of a refractory metal sufficient to produce a coating on a carbon based felt; processing thermally a refractory metal coated carbon based felt at a temperature and for a period of time sufficient to form a ceramic based felt; and cooling the ceramic based felt under a controlled atmosphere.Type: GrantFiled: June 16, 2006Date of Patent: September 9, 2014Assignee: United Technologies CorporationInventors: Wayde R. Schmidt, Robert A. Barth
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Patent number: 8748009Abstract: The present invention relates to a material including a matrix and at least one reinforcing element introduced therein, wherein the matrix is selected from the group consisting of plastic, carbon, ceramic, glass, clay, metal, and combinations thereof, and the reinforcing element is spherical to ellipsoidal in shape and has an onionskin-like structure. The present invention further relates to a method for producing a material including steps preparing at least one spherical to ellipsoidal reinforcing element having an onionskin-type structure, and introducing the reinforcing element into a matrix, wherein the matrix is selected from the group consisting of plastic, carbon, ceramic, glass, clay, metal, and combinations thereof. The present invention further relates to use of the material in a friction application, as abrasion protection, an injection molding part, a support plate, catalyst substrate or as bone replacement material.Type: GrantFiled: October 5, 2010Date of Patent: June 10, 2014Assignee: SGL Carbon SEInventors: Wilhelm Frohs, Andreas Kienzle, Ingrid Krätschmer
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Patent number: 8741797Abstract: A composite article having a body including a first phase that includes a nitride material, a second phase that includes a carbide material, and a third phase having one of an amorphous phase material with a nitrogen content of at least about 1.6 wt % or an amorphous phase material comprising carbon.Type: GrantFiled: September 27, 2012Date of Patent: June 3, 2014Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventors: Christopher J. Reilly, Vimal K. Pujari, Edmund A. Cortellini, David M. McElwee
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Publication number: 20140100104Abstract: The present invention provides a method of preparing a carbon fiber-reinforced silicon carbide composite material, wherein carbon nanotubes are formed in the composite material, and then metal silicon is melted and infiltrated into the composite material, so the amount of unreacted metal is reduced and the strength of the composite material is improved, and provides a carbon fiber-reinforced silicon carbide composite material prepared by the method.Type: ApplicationFiled: October 3, 2013Publication date: April 10, 2014Applicant: KOREA INSTITUTE OF ENERGY RESEARCHInventors: Se-Young KIM, Nam-Jo JEONG, In-Sub HAN, Sang-Kuk WOO, Doo-Won SEO, Kang BAI, Ji-Haeng YU, Sun-Dong KIM
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Publication number: 20140094355Abstract: Provided is a novel method for producing a silicon carbide-carbon composite. A green body containing a carbonaceous material 2 having silicon nitride attached to a surface thereof is fired to obtain a silicon carbide-carbon composite 1.Type: ApplicationFiled: May 24, 2012Publication date: April 3, 2014Applicant: TOYO TANSO CO., LTD.Inventors: Weiwu Chen, Yoshinari Miyamoto, Tetsuro Tojo
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Publication number: 20140038808Abstract: A process for the fabrication of a SiC-based article that includes preparing an aqueous suspension with SiC powder, a titanium source, a carbon source and boron carbide powder, spray drying the mixture to obtain a powder, preparing a green body from the powder, applying heat treatment to the green body in a pyrolysis/thermolysis step, pressureless sintering the green body, optimally followed by HIPing for further densification.Type: ApplicationFiled: July 31, 2013Publication date: February 6, 2014Inventors: Charles Schenck WILEY, Robert F. SPEYER
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Patent number: 8618006Abstract: A cement free refractory mixture contains aluminum oxide, silicon carbide, fumed silica, aluminum metal, an anti-oxidant, reactive alumina, and a carbon-bearing material. The mixture can be formed by conventional techniques to create refractory articles to contain or direct the flow of liquid metals. Refractory articles formed by the mixture do not require firing to achieve an initial cure.Type: GrantFiled: January 31, 2012Date of Patent: December 31, 2013Assignee: Vesuvius Crucible CompanyInventors: Robert A. Pattillo, Samuel B. Bonsall
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Publication number: 20130323152Abstract: Provided are: a readily sinterable silicon carbide powder substantially having a stoichiometric composition and from which a dense sintered body can be obtained; a silicon carbide ceramic sintered body having a low specific resistance; and a production method thereof. This readily sinterable silicon carbide powder has a carbon/silicon elemental ratio of 0.96 to 1.04, an average particle diameter of 1.0 to 100 ?m, and a ratio of 20% or less of an integrated value of an absorption intensity in a chemical shift range of 0 to 30 ppm to an integrated value of an absorption intensity in a chemical shift range of 0 to 170 ppm, in a 13C-NMR spectrum. By sintering this silicon carbide powder under pressure, there can be produced a dense sintered body having a low specific resistance and a high purity.Type: ApplicationFiled: February 28, 2012Publication date: December 5, 2013Applicant: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Yoshitaka Aoki, Kazuhide Yanaizumi
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Patent number: 8598057Abstract: A monolithic, unitary, seamless and physically continuous ceramic armor plate having first regions of one mechanical property and one chemical composition and one microstructural composition isolated from one another by a network of second regions of another mechanical property different from the one mechanical property and another chemical composition different from the one chemical composition and another microstructural composition different from the one microstructural composition, the one mechanical property and the another mechanical property being the propensity to crack.Type: GrantFiled: May 4, 2010Date of Patent: December 3, 2013Assignee: Verco Materials, LLCInventor: Robert F. Speyer
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Publication number: 20130301151Abstract: Substrates suitable for mirrors used at wavelengths in the EUV wavelength range have substrates (1) including a base body (2) made of a precipitation-hardened alloy, of an intermetallic phase of an alloy system, of a particulate composite or of an alloy having a composition which, in the phase diagram of the corresponding alloy system, lies in a region which is bounded by phase stability lines. Preferably, the base body (2) is made of a precipitation-hardened copper or aluminum alloy. A highly reflective layer (6) is preferably provided on a polishing layer (3) of the substrate (1) of the EUV mirror (5).Type: ApplicationFiled: July 19, 2013Publication date: November 14, 2013Inventors: Claudia EKSTEIN, Holger MALTOR
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Patent number: 8575051Abstract: The invention relates to a heat sink comprising a diamond-containing composite material. In addition to a diamond content of 40-90% by volume, the composite material further comprises from 0.005 to 12% by volume of a silicon-carbon compound, from 7 to 49% by volume of an Ag-, Au- or Al-rich phase and less than 5% by volume of a further phase, with the volume ratio of the Ag-, Au or Al-rich phase to silicon carbide being greater than 4 and at least 60% of the diamond surface being covered by the silicon-carbon compound. Preferred production processes include atmospheric pressure and pressure-aided infiltration techniques. The component is suitable, in particular, as heat sink for semiconductor components.Type: GrantFiled: January 20, 2004Date of Patent: November 5, 2013Assignee: Plansee SEInventor: Arndt Lüdtke
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Publication number: 20130224479Abstract: A carbon-fiber-reinforced silicon-carbide-based composite material which has better strength and toughness, and a braking material, such as a brake disc using the composite material, are provided. By using the carbon-fiber-reinforced silicon-carbide-based composite material including a bundle of fibers having chopped carbon fibers arranged in parallel and the other carbon component, carbon, silicon, and silicon carbide, in which the fiber bundle is flat, its cross-section perpendicular to its longitudinal direction has a larger diameter of 1 mm or more, a ratio of the larger diameter to a smaller diameter is from 1.5 to 5, and a plurality of the fiber bundles are randomly oriented substantially along a two-dimensional plane, and a two-dimensional side serves as a braking side to thereby constitute the braking material.Type: ApplicationFiled: February 21, 2013Publication date: August 29, 2013Applicant: Covalent Materials CorporationInventor: Covalent Materials Corporation
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Publication number: 20130196844Abstract: A composition having nanoparticles of silicon carbide and a carbonaceous matrix or silicon matrix. The composition is not in the form of a powder. A composition having silicon and an organic compound having a char yield of at least 60% by weight or a thermoset made from the organic compound. A method of combining silicon and the organic compound and heating to form silicon carbide or silicon nitride nanoparticles.Type: ApplicationFiled: March 11, 2013Publication date: August 1, 2013Applicant: The Government of the United States of America, as represented by the Secretary of the NavyInventors: Teddy M. Keller, Andrew Saab, Matthew Laskoski, Syed B. Qadri
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Patent number: 8480993Abstract: A diamond reference standard contains a diamond composite of 60-90% diamond crystals and 10-40% silicon carbide binding agent doped with a plurality of elements. The standard is prepared by doping a diamond composite containing a silicon carbide binder with a plurality of elements, the presence of which can readily be detected using a variety of instruments, e.g. a mass spectrometer.Type: GrantFiled: December 16, 2009Date of Patent: July 9, 2013Assignee: Her Majesty the Queen in right of Canada as represented by the Solicitor General acting through the Commissoner of the Royal Canadian Mounted PoliceInventors: David Ballantyne, Claude Dalpe
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Publication number: 20130090228Abstract: A composite article having a body including a first phase that includes a nitride material, a second phase that includes a carbide material, and a third phase having one of an amorphous phase material with a nitrogen content of at least about 1.6 wt % or an amorphous phase material comprising carbon.Type: ApplicationFiled: September 27, 2012Publication date: April 11, 2013Inventors: Christopher J. Reilly, Vimal K. Pujari, Edmund A. Cortellini, David M. McElwee
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Patent number: 8357623Abstract: Methods of forming composite materials include coating particles of titanium dioxide with a substance including boron (e.g., boron carbide) and a substance including carbon, and reacting the titanium dioxide with the substance including boron and the substance including carbon to form titanium diboride. The methods may be used to form ceramic composite bodies and materials, such as, for example, a ceramic composite body or material including silicon carbide and titanium diboride. Such bodies and materials may be used as armor bodies and armor materials. Such methods may include forming a green body and sintering the green body to a desirable final density. Green bodies formed in accordance with such methods may include particles comprising titanium dioxide and a coating at least partially covering exterior surfaces thereof, the coating comprising a substance including boron (e.g., boron carbide) and a substance including carbon.Type: GrantFiled: March 30, 2009Date of Patent: January 22, 2013Assignee: U.S. Department of EnergyInventors: Thomas M. Lillo, Henry S. Chu, William M. Harrison
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Patent number: 8349231Abstract: This invention relates to a process for the production of a shaped composite material and the material obtained through that process. In particular it relates to a process for obtaining a disk of composite ceramic material for disc brakes in which the friction coefficient is varied by varying the composition of the surface layer.Type: GrantFiled: December 30, 2004Date of Patent: January 8, 2013Assignee: Brembo Ceramic Brake Systems S.p.A.Inventors: Ralf Siegfried Goller, Marco Orlandi, Riccardo Piavani
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Patent number: 8293667Abstract: It is an object of the invention to provide a ceramic sintered body that has a dense structure and minimal cracking and that exhibits excellent sliding properties even in a non-lubricated state, as well as a process for its production and sliding parts that employ the same. According to a preferred mode, the sintered body of the invention comprises silicon carbide as the parent material and further contains a solid lubricant A with a mean particle size of no greater than 5 ?m and a solid lubricant B with a mean particle size of 10-70 ?m.Type: GrantFiled: February 22, 2007Date of Patent: October 23, 2012Assignee: Hitachi Chemical Company, Ltd.Inventors: Kazuyuki Akasaka, Kiyoshi Kawai
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Patent number: 8282878Abstract: Embodiments of the present invention disclosed herein include a sintering aid composition that has a material useful for sintering, an amine, and optionally a carboxylic acid.Type: GrantFiled: January 27, 2011Date of Patent: October 9, 2012Assignee: Huntsman Petrochemical LLCInventors: Alan P. Croft, David C. Lewis
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Patent number: 8222171Abstract: A method for the production of a ceramic substrate for a semiconductor component, includes the steps of producing paper containing at least cellulose fibers, as well as a filler to be carbonized and/or SiC, pyrolizing the produced paper, and siliconizing the pyrolyzed paper.Type: GrantFiled: July 13, 2007Date of Patent: July 17, 2012Assignee: Schunk Kohlenstofftechnik GmbHInventors: Marco Ebert, Martin Henrich, Andreas Lauer, Gotthard Nauditt, Thorsten Scheibel, Roland Weiss
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Patent number: 8097546Abstract: A composition for ceramic extrusion-molded bodies includes a ceramic material, a water-soluble cellulose ether, a styrenesulfonate and water. A method for manufacturing a ceramic extrusion-molded body using the composition is also provided.Type: GrantFiled: July 29, 2009Date of Patent: January 17, 2012Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Shingo Niinobe, Kazuhisa Hayakawa
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Patent number: 7985354Abstract: Carbon nanomaterials are stabilized and uniformly dispersed in a liquid such as water using a simple procedure. Methylcellulose is added to hot water where it separates and expands with a temperature of about 80-90 degree Celsius. Methylcellulose swiftly dissolves when the water cools down. Carbon nanomaterials are dispersed in a solvent and sonicated. This nanomaterial dispersed solvent is then added to the methylcellulose dispersed water and mechanically stirred. The resulting uniform mixture is up to 90% by weight nanomaterials and is stable for months.Type: GrantFiled: March 19, 2010Date of Patent: July 26, 2011Assignee: Oceanit Laboratories, Inc.Inventor: Vinod P. Veedu
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Publication number: 20110175264Abstract: A method of forming a sintered silicon carbide body includes mixing silicon carbide powder having an oxygen content of less than about 3 wt % and having a surface area in a range of between about 8 m2/g and about 15 m2/g, with boron carbide powder and carbon sintering aid to form a green silicon carbide body. Alternatively, a method of producing a sintered silicon carbide body includes mixing the silicon carbide powder with titanium carbide powder having an average particle diameter in a range of between about 5 nm and about 100 nm and with carbon sintering aid to form a green silicon carbide body. In another alternative, a method of forming a sintered silicon carbide body includes mixing silicon carbide powder with boron carbide powder, the titanium carbide powder, and carbon sintering aid to form a green silicon carbide body. After sintering, the silicon carbide bodies have a density at least 98% of the theoretical density of silicon carbide.Type: ApplicationFiled: July 22, 2010Publication date: July 21, 2011Inventors: Vimal K. Pujari, Eric Jorge, Christopher J. Reilly
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Publication number: 20110172080Abstract: A porous sintered silicon carbide body that includes silicon carbide and graphite and methods of making thereof are described. The porous silicon carbide body can be a seal. The porous sintered silicon carbide body defines pores with an average pore size in a range of between about 20 ?m and about 40 ?m, comprising a porosity in a range of between about 1% and about 5% by volume.Type: ApplicationFiled: July 22, 2010Publication date: July 14, 2011Inventors: Vimal K. Pujari, Nikolas J. Ninos
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Publication number: 20110160035Abstract: In a method of preparing a boron carbide material, boron carbide powder is washed with essentially pure water at an elevated temperature to generate washed boron carbide powder. The washed boron carbide powder is combined with a sintering aid. The mixture of the boron carbide powder and the sintering aid is pressed to form a shaped material, and the shaped material is sintered. A sintered boron carbide material comprises a boron carbide component that includes boron carbide, elemental carbon, and not more than about 0.6 wt % of oxygen on the basis of the total weight of the boron carbide component. The sintered boron carbide material has a density of at least about 99% of the theoretical density. Another sintered boron carbide material comprises a boron carbide component that includes boron carbide, silicon carbide, elemental carbon, and not more than about 0.3 wt % oxygen on the basis of the total weight of the boron carbide component, and has a density of at least about 97% of the theoretical density.Type: ApplicationFiled: March 10, 2011Publication date: June 30, 2011Applicant: Saint-Gobain Ceramics & Platics, Inc.Inventors: Vimal K. Pujari, James T. Hennessey, William T. Collins
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Patent number: 7959841Abstract: Uniformly dense, diamond-silicon carbide composites having high hardness, high fracture toughness, and high thermal stability are prepared by consolidating a powder mixture of diamond and amorphous silicon. A composite made at 5 GPa/1673K had a measured fracture toughness of 12 MPa·m1/2. By contrast, liquid infiltration of silicon into diamond powder at 5 GPa/1673K produces a composite with higher hardness but lower fracture toughness.Type: GrantFiled: May 31, 2006Date of Patent: June 14, 2011Assignee: Los Alamos National Security, LLCInventor: Yusheng Zhao
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Publication number: 20110124483Abstract: In various embodiments, composite materials containing a ceramic matrix and a carbon nanotube-infused fiber material are described herein. Illustrative ceramic matrices include, for example, binary, ternary and quaternary metal or non-metal borides, oxides, nitrides and carbides. The ceramic matrix can also be a cement. The fiber materials can be continuous or chopped fibers and include, for example, glass fibers, carbon fibers, metal fibers, ceramic fibers, organic fibers, silicon carbide fibers, boron carbide fibers, silicon nitride fibers and aluminum oxide fibers. The composite materials can further include a passivation layer overcoating at least the carbon nanotube-infused fiber material and, optionally, the plurality of carbon nanotubes. The fiber material can be distributed uniformly, non-uniformly or in a gradient manner in the ceramic matrix. Non-uniform distributions may be used to form impart different mechanical, electrical or thermal properties to different regions of the ceramic matrix.Type: ApplicationFiled: November 23, 2010Publication date: May 26, 2011Applicant: APPLIED NANOSTRUCTURED SOLUTIONS, LLCInventors: Tushar K. SHAH, Harry C. Malecki, Murray N. Carson
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Publication number: 20110082033Abstract: The present invention relates to a material including a matrix and at least one reinforcing element introduced therein, wherein the matrix is selected from the group consisting of plastic, carbon, ceramic, glass, clay, metal, and combinations thereof, and the reinforcing element is spherical to ellipsoidal in shape and has an onionskin-like structure. The present invention further relates to a method for producing a material including steps preparing at least one spherical to ellipsoidal reinforcing element having an onionskin-type structure, and introducing the reinforcing element into a matrix, wherein the matrix is selected from the group consisting of plastic, carbon, ceramic, glass, clay, metal, and combinations thereof. The present invention further relates to use of the material in a friction application, as abrasion protection, an injection moulding part, a support plate, catalyst substrate or as bone replacement material.Type: ApplicationFiled: October 5, 2010Publication date: April 7, 2011Inventors: Wilhelm Frohs, Andreas Kienzle, Ingrid Krätschmer
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Publication number: 20110028301Abstract: Disclosed is a method for the synthesis of silicon carbide (SiC) bodies having a relative density of 99% or higher and a SiC body synthesized according to the method.Type: ApplicationFiled: December 2, 2009Publication date: February 3, 2011Inventors: Lionel VARGAS-GONZALEZ, Robert SPEYER