Utilizing Isostatic Pressure (e.g., Hip, Etc.) Or Specified Pressure Patents (Class 505/491)
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Publication number: 20130252820Abstract: According to one embodiment, there is provided a method of manufacturing a high-frequency acceleration cavity component, the method including covering a mold with a conducting material, enclosing, in an outer shell, the mold covered with the conducting material, vacuum-airtight-welding the outer shell enclosing the mold, conducing hot isostatic pressing of the vacuum-airtight-welded outer shell, and taking the conducting material formed in the mold out of the outer shell which has undergone the hot isostatic pressing.Type: ApplicationFiled: September 14, 2012Publication date: September 26, 2013Inventors: Yujiro TAJIMA, Tomoko Ota, Junichi Shibuya, Koichi Nakayama, Takeshi Yoshiyuki, Yuji Nobusada
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Patent number: 8372784Abstract: A method for producing a superconductive wire, whereby an elongated intermediate element is formed out of an initial element in a deformation step and whereby the superconductive filaments are formed by a final reaction heat treatment, is characterized in that prior to the final reaction heat treatment the filaments in the intermediate element are densified in one or more high pressure densification steps following up the deformation step, said densification steps comprising a simultaneous action of at least four hard surfaces perpendicular to the axis of the elongated intermediate element, building up high pressure P?100 MPa on a part of the intermediate element having an axial length L. This leads to a substantial increase of the critical current density Jc, whereby the anisotropy factor ? is be almost not affected thus enabling production of almost isotropic wires or tapes.Type: GrantFiled: September 29, 2009Date of Patent: February 12, 2013Assignee: Bruker Biospin AGInventor: René Flükiger
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Patent number: 6605569Abstract: A Mg-doped high-temperature superconductor having low superconducting anisotropy includes a two-dimensional layered structure constituted by a charge reservoir layer and a superconducting layer, wherein some or all atoms constituting the charge reservoir layer are Cu and O atoms, metallizing or rendering the charge reservoir layer superconducting, a portion of the Ca of the CunCan+1O2n constituting the superconducting layer is replaced by Mg, increasing superconductive coupling between CuO2 layers, a thickness of the superconducting layer is increased, and therefore coherence length in a thickness direction is increased based on the uncertainty principle, lowering superconducting anisotropy.Type: GrantFiled: June 1, 2001Date of Patent: August 12, 2003Assignee: Agency of Industrial Science and Technology Ministry of International Trade and IndustryInventors: Hideo Ihara, Shyam Kishore Agarwal
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Publication number: 20010009888Abstract: A modified powder-in-tube process produces a superconductor wire having a significantly greater current density than will a superconductor wire of the same nominal superconductor composition produced using conventional draw-swage-extrude-roll deformation. In the process disclosed, a superconductor precursor is placed within a ductile tube, the tube with the powder therein is then deformed into a cross-section substantially corresponding to that of the end product, and the deformed tube is then subject to a plurality of heat treatments to convert the precursor into the desired superconducting ceramic oxide phase. Before the last of the heat treatments, the tube is isostatically pressed to densify and texture the superconductor precursor oxide in the tube.Type: ApplicationFiled: March 1, 2001Publication date: July 26, 2001Inventor: Gilbert N. Riley
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Patent number: 6258754Abstract: A process which relies on a joining technique between two individual strongly linked superconductors is disclosed. Specifically, this invention relates to fabrication of single domains of YBa2Cu3Ox or YBa2Cu3Ox with the addition of Y2BaCuO5 and/or other secondary phases such as Pt/PtO2, CeO2, SnO2, Ag, Y2O3 and other rare earth oxides, by using a top-seeded, melt processing technique. Beginning with a single crystal seed such as Nd1+xBa2−xCu3O3 or SmBa2Cu3Ox crystals, a melt-textured YBCO domain with crystallographic orientation nearly similar to that of the seed crystal can be fabricated. The samples are next machined to desired geometrical shapes. A bonding material is then applied to the ac plane. Low solidification or recrystalization point, similar crystal structure to that of YBa2Cu3Ox, and capability of growing epitaxially on YBCO domains are critical parameters of the bonding material.Type: GrantFiled: July 16, 1998Date of Patent: July 10, 2001Assignee: Superconductive Components, Inc.Inventor: Suvankar Sengupta
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Patent number: 6221813Abstract: The invention relates to a process for producing a shaped body, in which a mixture of oxidic starting powders or a superconducting material, which comprises at least 30% by volume of platelet-shaped primary particles and has such a composition that a high-temperature superconducting material is formed on later, suitable thermal treatment, is comminuted by milling, shearing and/or rolling in such a way that the comminuted powder has a powder particle size distribution having a d90 of ≦20 &mgr;m, and in which the powders which have been comminuted in this way are isostatically compacted by the dry bag method.Type: GrantFiled: November 30, 1999Date of Patent: April 24, 2001Assignee: Aventis Research & Technologies GmbH & Co. KGInventors: Günther Riedel, Jürgen Neumann, Joachim Bock, Stephan Gauss
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Patent number: 6191075Abstract: A method of preparing a high temperature superconductor. A method of preparing a superconductor includes providing a powdered high temperature superconductor and a nanophase paramagnetic material. These components are combined to form a solid compacted mass with the paramagnetic material disposed on the grain boundaries of the polycrystaline high temperature superconductor.Type: GrantFiled: December 21, 1993Date of Patent: February 20, 2001Assignee: University of ChicagoInventors: Uthamalingam Balachandran, Richard W. Siegel, Thomas R. Askew
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Patent number: 6143697Abstract: A method for producing a superconducting thick film involves the steps of forming a thick layer comprising a superconducting material on a substrate; firing the thick layer formed on the substrate; subjecting the fired thick layer to cold isostatic pressing; and refiring the thick layer subjected to cold isostatic pressing.Type: GrantFiled: August 10, 1999Date of Patent: November 7, 2000Assignee: Murata Manufacturing Co., Ltd.Inventors: Tsutomu Tatekawa, Yuji Kintaka, Akio Oota
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Patent number: 6121205Abstract: A bulk superconductor including a plurality of units each composed of a substrate and a superconductive layer of R--Ba--Cu--O, where R is selected from La, Nd, Sm, Eu, Gd, Y, Dy, Ho, Er, Tm, Yb and mixtures thereof, formed on the substrate. The units are arranged in a row or in a matrix such that the superconductive layers of respective units are superconductively joined with each other.Type: GrantFiled: May 13, 1997Date of Patent: September 19, 2000Assignees: International Superconductivity Technology Center, Railway Technical Research InstituteInventors: Masato Murakami, Kazuhiko Sawada, Naomichi Sakai, Takamitsu Higuchi
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Patent number: 6051534Abstract: A process for producing the 2223 phase of (Pb,Bi)SrCaCuO that is much faster than existing processes has the steps of: calcining a precursor powder mixture while maintaining intimate mixing of this precursor mixture by intermediate grindings during calcination; compressing the calcination product into a consolidated body; and heating the calcination product while maintaining intimate mixing of the calcination product, to form essentially phase pure 2223 (Pb,Bi)SrCaCu). A fast process for making a (Pb,Bi)SrCaCuO part with a high J.sub.c has the steps of: pressing calcined and reacted (Pb,Bi)SrCaCuO powder into a green body having the shaped of the part; and sintering the green body for a selected time, most preferably between 6 and 8 hours, that is long enough to establish superconducting electrical contact between grains of (Pb,Bi)SrCaCuO but short enough to prevent void formation or part shape distortion. The part made by this process has a high density, at least about 4 or 5 g/cm.sup.3.Type: GrantFiled: April 21, 1993Date of Patent: April 18, 2000Assignee: The United States of America as represented by the Secretary of the NavyInventors: Roy Rayne, Louis E. Toth, Barry A. Bender, Steven H. Lawrence
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Patent number: 5952272Abstract: Hg,Tl-based superconductors are produced by HIPping. A new superconducting phase, having a double (Hg,Tl)-layer and the nominal composition:(Hg.sub.1-x Tl.sub.x).sub.2 (Ba.sub.1-a Sr.sub.a).sub.2 (Ca.sub.1-b Y.sub.b).sub.2 Cu.sub.3 O.sub.zwhere 0.ltoreq.x.ltoreq.0.95, 0.ltoreq.a.ltoreq.1, 0.ltoreq.b.ltoreq.1, and z is sufficient to provide said phase with a resistive and magnetic superconducting transition of 100 K or above, can be produced. Either precursor oxides, or partially or fully reacted mixed oxides, can be used in the HIPping mixture.Type: GrantFiled: April 16, 1998Date of Patent: September 14, 1999Assignee: The United States of America as represented by the Secretary of the NavyInventors: Louis E. Toth, William Lechter, Earl F. Skelton, Michael Osofsky
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Patent number: 5929001Abstract: A method of preparing a high temperature superconductor. A method of preparing a superconductor includes providing a powdered high temperature superconductor and a nanophase material. These components are combined to form a solid compacted mass with the material disposed in the polycrystalline high temperature superconductor. This combined mixture is rapidly heated, forming a dispersion of nanophase size particles without a eutectic reaction. These nanophase particles can have a flat plate or columnar type morphology.Type: GrantFiled: October 11, 1995Date of Patent: July 27, 1999Assignee: University of ChicagoInventors: Kenneth C. Goretta, Michael T. Lanagan, Dean J. Miller, Suvankar Sengupta, John C. Parker, Jieguang Hu, Uthamalingam Balachandran, Richard W. Siegel, Donglu Shi
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Patent number: 5786304Abstract: A joining product of oxide superconducting materials having a high current density and process for producing the same. A joining product comprising a plurality of oxide superconducting materials having an identical crystal orientation joined with each other through a superconducting phase of the same type as described above which has the same crystal orientation as the oxide superconducting materials and a lower peritectic temperature than the oxide superconducting materials.Type: GrantFiled: September 30, 1994Date of Patent: July 28, 1998Assignee: Nippon Steel CorporationInventors: Keiichi Kimura, Katuyoshi Miyamoto, Misao Hashimoto
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Patent number: 5674814Abstract: The present invention is directed to a process for producing high temperature superconducting ceramic materials. More particularly, the present invention is directed to a process that enhances the densification of Bi.sub.1.8 Pb.sub.0.4 Sr.sub.2 Ca.sub.2 Cu.sub.3 O.sub.10 "BSCCO" ceramics.Type: GrantFiled: November 14, 1994Date of Patent: October 7, 1997Assignee: University of ChicagoInventors: Michael T. Lanagan, John J. Picciolo, Stephen E. Dorris
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Patent number: 5646097Abstract: A method is disclosed for fabricating a polycrystalline <223> thallium-containing superconductor having high critical current at elevated temperatures and in the presence of a magnetic field. A powder precursor containing compounds other than thallium is compressed on a substrate. Thallium is incorporated in the densified powder precursor at a high temperature in the presence of a partial pressure of a thallium-containing vapor.Type: GrantFiled: December 15, 1995Date of Patent: July 8, 1997Assignee: General Electric CompanyInventors: John Eric Tkaczyk, Kenneth Wilbur Lay, Qing He
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Patent number: 5627140Abstract: Enhanced flux pinning in superconductors is achieved by embedding carbon nanotubes into a superconducting matrix. The carbon nanotubes simulate the structure, size and shape of heavy ion induced columnar defects in a superconductor such as Bi.sub.2 Sr.sub.2 CaCu.sub.2 O.sub.8+x. The nanotubes survive at treatment temperatures of up to approximately 800.degree. C. both in oxygen containing and in inert atmospheres. The superconducting matrix with nanotubes is heat treated at a lower temperature than the temperature used to treat the best case pure superconductor material.Type: GrantFiled: May 19, 1995Date of Patent: May 6, 1997Assignees: NEC Research Institute, Inc., Florida State UniversityInventors: Kristian Fossheim, Thomas W. Ebbesen
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Patent number: 5545613Abstract: A method of preparing a superconducting oxide by combining the metallic elements of the oxide to form an alloy, followed by oxidation of the alloy to form the oxide. Superconducting oxide-metal composites are prepared in which a noble metal phase intimately mixed with the oxide phase results in improved mechanical properties. The superconducting oxides and oxide-metal composites are provided in a variety of useful forms.Type: GrantFiled: July 11, 1994Date of Patent: August 13, 1996Assignee: Massachusetts Institute of TechnologyInventors: Gregory J. Yurek, John B. VanderSande
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Patent number: 5462917Abstract: A superconductor material having a current density, J, of from about 30,000 to about 85,000 amps/cm.sup.2 at zero magnetic field and 77.degree. K is disclosed. The 123 superconductor, of the formula L.sub.1 Ba.sub.2 Cu.sub.3 O.sub.6 +.delta. wherein L is preferably yttrium, is capable of entrapping sufficiently high magnetic fields and exhibits a low microwave surface resistance. The process of preparing the superconductor comprises compacting the bulk product, L.sub.1 Ba.sub.2 Cu.sub.3 O, and then sintering the reaction product at a temperature between about 40.degree. C. to about 90.degree. C. below its melting point, i.e., for Y.sub.1 Ba.sub.2 Cu.sub.3 O.sub.6 +.delta. at a temperature of approximately 940.degree. C. The composition is then heated in a preheated chamber maintained at approximately 1090.degree. C. to about 1,200.degree. C. (approximately 1,100.degree. C. for Y.sub.1 Ba.sub.2 Cu.sub.3 O.sub.6 +.delta.Type: GrantFiled: February 14, 1994Date of Patent: October 31, 1995Assignee: University of Houston-University ParkInventors: Kamel Salama, Venkatakrishnan Selvamanickam
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Patent number: 5439878Abstract: A process for preparing a copper oxide superconductor of (Ba,Sr)-Cu-C-O containing carbonate radicals is disclosed, which comprises the steps of: mixing alkaline earth metal compounds and a copper compound with a molar ratio of 1.1 to 2.25 to obtain a mixture; pressing said mixture to form a pellet; and sintering said pellet in an oxygen atmosphere, wherein the alkaline earth metal compounds including a barium compound selected from the group consisting of barium carbonate and barium oxalate, and a strontium compound selected from the group consisting of strontium carbonate and strontium oxalate and the copper compound selected from the group consisting of copper carbonate, copper nitrate, copper oxalate and copper oxide.Type: GrantFiled: July 7, 1994Date of Patent: August 8, 1995Assignee: Nippon Telegraph and Telephone CorporationInventors: Kyoichi Kinoshita, Tomoaki Yamada
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Patent number: 5439880Abstract: A method of preparing a superconducting oxide by combining the metallic elements of the oxide to form an alloy, followed by oxidation of the alloy to form the oxide. Superconducting oxide-metal composites are prepared in which a noble metal phase intimately mixed with the oxide phase results in improved mechanical properties. The superconducting oxides and oxide-metal composites are provided in a variety of useful forms.Type: GrantFiled: May 3, 1993Date of Patent: August 8, 1995Assignee: Massachusetts Institute of TechnologyInventors: Gregory J. Yurek, John B. Vander Sande
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Patent number: 5382405Abstract: A method of manufacturing a shaped article from a powdered precursor, wherein the components of the powdered precursor are subjected to a self-propagating high-temperature synthesis (SHS) reaction and are consolidated essentially simultaneously. The shaped article requires essentially no machining after manufacture.Type: GrantFiled: September 3, 1993Date of Patent: January 17, 1995Assignee: Inland Steel CompanyInventors: Kenneth F. Lowrance, II, Eric C. Knorr, William M. Goldberger, Daniel Boss, Doreen Edwards
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Patent number: 5344816Abstract: High temperature superconducting oxide materials can be taken to a higher, but stable, state of oxidation by removing H-impurities, such as OH.sup.-, using I.sub.2 /O.sub.2 mixtures in a reactive atmosphere process. A higher T.sub.c and a narrower .DELTA.T-transition result.Type: GrantFiled: February 24, 1993Date of Patent: September 6, 1994Assignee: Hughes Aircraft CompanyInventors: Ricardo C. Pastor, Antonio C. Pastor, deceased, Luisa E. Gorre, deceased, Keith C. Fuller
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Patent number: 5318745Abstract: A method of manufacturing an oxide superconductor having a composition expressed by formula La.sub.2-X Sr.sub.X CaCu.sub.2 O.sub.6 (0<X.ltoreq.0.6), comprising the steps of: preliminarily burning a raw powder having a predetermined composition, and sintering the powder to obtain a sintered body; and subjecting the sintered body to hot isostatic pressing at a temperature falling within a range of from 940.degree.-1600.degree. C. under total pressure of 10 MPa or more and oxygen partial pressure of 2 MPa or more. By virtue of the step of subjecting the sintered body to hot isostatic pressing, a superconductor can be manufactured at a temperature and under a pressure within respective wide ranges. Further, the composition of the superconductor can be selected within a wide range of 0<X.ltoreq.0.6. Moreover, the superconductor can be manufactured by performing quenching after the hot isostatic pressing.Type: GrantFiled: July 8, 1992Date of Patent: June 7, 1994Assignees: International Superconductivity Technology Center, Mitsubishi Materials Corporation, Hitachi, Ltd.Inventors: Takeshi Sakurai, Toru Yamashita, Hisao Yamauchi, Shoji Tanaka