Agglomerated Product Or Component, Or Process Of Preparing Patents (Class 510/444)
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Patent number: 7572760Abstract: The present invention relates to an auxiliary composition, for use in the laundering or treatment of fabrics, comprising an admix of (i) clay and (ii) a silicone in an emulsified form.Type: GrantFiled: October 31, 2007Date of Patent: August 11, 2009Assignee: The Procter & Gamble CompanyInventors: Kevin Graham Blyth, Andrew Russell Graydon, Colin Stephenson
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Publication number: 20090124532Abstract: [Problems] To provide detergent granules capable of suppressing paste formability and having low exothermic property; a process for producing the detergent granules; and a high-bulk density detergent composition containing the detergent granules. [Solving Means] Detergent granules containing a sodium linear alkylbenzenesulfonate (LAS-Na), sodium sulfate undetected by X-ray diffraction method and sodium sulfate detected by X-ray diffraction method, wherein a molar ratio of [sodium sulfate undetected by X-ray diffraction method]/[LAS-Na] is from 0.1 to 1.0, and a molar ratio of [sodium sulfate detected by X-ray diffraction method]/[chemically quantified sodium sulfate] is from 0.5 to 0.Type: ApplicationFiled: July 10, 2006Publication date: May 14, 2009Inventors: Yushi Sakata, Makoto Takahashi, Tsutomu Tokumoto
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Patent number: 7524807Abstract: Rinse-off personal care compositions comprising a perfume polymeric particle, which is useful as a delivery system for a perfume raw material (“PRM”), methods for making such personal care compositions and methods of treating substrates, such as skin and/or hair with such personal care compositions are provided.Type: GrantFiled: October 31, 2003Date of Patent: April 28, 2009Assignee: The Procter & Gamble CompanyInventors: Mannie Lee Clapp, Robert Richard Dykstra, Rebecca Ann Taylor
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Patent number: 7485615Abstract: The invention provides a process for producing a granular anionic surfactant, including the steps of carrying out drying and granulation simultaneously while adding an anionic surfactant paste to a powder raw material under reduced pressure in a granulator provided with a stirring blade and a cracking blade to obtain granules.Type: GrantFiled: August 5, 2004Date of Patent: February 3, 2009Assignee: Kao CorporationInventors: Masahiro Umehara, Hiroyuki Yamashita, Yasumitsu Sakuma, Kazuhito Miyoshi
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Patent number: 7470654Abstract: The present invention relates to a detergent auxiliary composition comprising: (i) a liquid or liquefiable active component; and (ii) a water-insoluble solid support component and (iii) a water-soluble and/or water dispersible encapsulating material; and (iv) optionally one or more adjunct components, characterised in that the composition further comprises (v) a surface deposition enhancing cationic polymer or oligomer having cationic groups such that fewer than 50% are de-activated when a 1% by weight solution of the polymer or oligomer (prepared in deionised water and then adjusted to pH 7.0 with sodium carbonate or citric acid) is stored at 25° C.Type: GrantFiled: September 6, 2005Date of Patent: December 30, 2008Assignee: The Procter & Gamble CompanyInventors: Fabrizio Meli, Andre Chieffi, Rebecca Louise Selway, Stefan Frenzel
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Patent number: 7459422Abstract: The present invention relates to a substrate composition comprising from about 20 wt % to about 60 wt % of a water-soluble and/or water-dispersible polymer and from about 20 wt % to about 80 wt % of a water-soluble inorganic salt. The substrate composition of the present invention has a median particle size of from about 1 micrometer to about 100 micrometers and comprises less than about 10 wt % of water-insoluble material.Type: GrantFiled: August 11, 2005Date of Patent: December 2, 2008Assignee: The Procter & Gamble CompanyInventors: Paul R Mort, III, Stewart Curtis Doty, Girish Jagannath
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Patent number: 7446085Abstract: Detergent particles obtained by a process comprising the step of dryneutralizing base particles comprising a water-soluble solid alkali inorganic substance (A) with a liquid acid precursor (B) of a non-soap anionic surfactant, wherein the base particles are obtained by a spray-drying method, and wherein the base particles contain the component (A) in an amount of equal to or greater than 4 times the amount equivalent for neutralizing the component (B) and have an average particle size of from 150 to 400 ?m; base particles having an average particle size of from 150 to 400 ?m, comprising 20 to 80% by weight of a water-soluble solid alkali inorganic substance; a process for preparing detergent particles comprising the steps of (a) preparing a slurry comprising a water-soluble solid alkali inorganic substance (A) in an amount equal to or greater than 4 times the amount equivalent for neutralizing a liquid acid precursor (B) of a non-soap anionic surfactant to be added in step (c); (b) spray-drying the slurry obtType: GrantFiled: September 2, 2003Date of Patent: November 4, 2008Assignee: Kao CorporationInventors: Yoshinobu Imaizumi, Hiroyuki Yamashita, Teruo Kubota
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Patent number: 7425526Abstract: The present disclosure relates to compositions useful for maintaining the clean impression of a carpet (that is, its scent and appearance) over an extended time despite occurrences that might damage the carpet surface. The composition, which includes an antimicrobial agent, an enzyme inhibitor, and an odor-reacting compound, can be used by a consumer to remove contaminants from the carpet and to prevent the odor associated with the decomposition of future contamination. Specifically, the composition has been shown effective in neutralizing odors associated with the decomposition of organic materials (such as urine or food spills) by absorbing and/or removing the odor-generating source. A manufacturing treatment composition and methods for using are also disclosed.Type: GrantFiled: November 8, 2006Date of Patent: September 16, 2008Assignee: Milliken & CompanyInventors: Shulong Li, Richard A. Mayernik
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Publication number: 20080188390Abstract: The invention refers to a solid compact cogranule suitable for use in solid detergent compositions and especially in tablet applications. These cogranules have a granule size from 300 ?m to 1400 ?m and a bulk density of at least 750 kg/m3, and they comprise alkali metal silicate, carbonate, citrate, and less than 25% water by weight of the cogranule. A method for producing the granule is described.Type: ApplicationFiled: February 1, 2008Publication date: August 7, 2008Inventors: Frank Schinkel, Cecilia Johansson, Ajse Sandqvist
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Patent number: 7354891Abstract: A process for preparing—a cleansing composition having pearlescence, which contains adding an ingredient (B) which has been molten beforehand, or an aqueous liquid in which the molten ingredient (B) is contained, to a suspension of an ingredient (A) and cooling the resultant mixture to cause the ingredient (B) to deposit; and the cleansing composition. The process makes it possible to economically produce cleansing compositions which have pearlescence, excellent in the stability of their pearlants, and superb long-term storage stability under acidic conditions and high-temperature conditions.Type: GrantFiled: August 8, 2003Date of Patent: April 8, 2008Assignee: Kao CorporationInventor: Kenji Arai
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Patent number: 7279453Abstract: A process of making particulate foam regulating granulates by spraying an aqueous foam regulating emulsion containing 16% to 70% by weight of a foam regulating active ingredient based on paraffin wax or silicone oil, 2% by weight to 15% by weight of a nonionic and/or anionic emulsifier, and not more than 80% by weight of water onto a solid carrier material, wherein the carrier material comprises an alkali metal carbonate and a Brønsted acid.Type: GrantFiled: August 22, 2003Date of Patent: October 9, 2007Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Volker Blank, Rene-Andres Artiga-Gonzalez, Ulrich Pegelow, Stefan Hammelstein, Adolf Wiche, Mario Sturm
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Patent number: 7271138Abstract: Through-the-wash automatic dishwashing detergent compositions, especially detergent compositions comprising zinc-containing materials, are provided for protecting glassware from surface corrosion during automatic dishwashing.Type: GrantFiled: October 12, 2004Date of Patent: September 18, 2007Assignee: The Procter & Gamble CompanyInventors: Brian Xiaoqing Song, Patricia Sara Berger, James Robert Schwartz, Robert William Corkery
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Patent number: 7256169Abstract: The invention relates to a pulverulent laundry and cleaning detergents ingredient, to a process for its preparation and to its use.Type: GrantFiled: January 30, 2001Date of Patent: August 14, 2007Assignee: Clariant Produkte (Deutschland) GmbHInventors: Günther Schimmel, Harald Bauer, Josef Holz, Volker Thewes, Richard Mertens, Peter Hardt, Matthias Berghahn, Thomas Müller
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Patent number: 7241433Abstract: The invention relates to a process for the preparation of coated granular sodium percarbonate having a low TAM value. The preparation is carried out by fluidized-bed spray granulation at a temperature TG in the range from 45 to 75° C., and the coating is effected by the spray application of an aqueous solution containing at least one coating component in a fluidized bed at a temperature TU in the range from 35 to 100° C. According to the invention, a) after the fluidized-bed spray granulation but before the coating, drying is carried out at TNT of greater than TG, or b) the fluidized-bed granulation is carried out in at least two steps at TG1, TG2 . . . TGn, TG2 or TGn being higher than TG1, and drying being unnecessary if ? of the granulate have been formed at TG1, or c) drying takes place not after the granulation but after the coating, at TUNT, TUNT being at least 20° C. higher than TG.Type: GrantFiled: August 20, 2002Date of Patent: July 10, 2007Assignee: Degussa GmbHInventors: Harald Jakob, Waldemar Hessberger, Juergen Lattich, Ralph Overdick
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Patent number: 7211555Abstract: A process for efficiently preparing fine zeolite particles comprising synthesizing zeolite in the presence of an alkaline earth metal-containing compound and/or with controlling the preparation process of zeolite, thereby giving fine zeolite particles being composed of crystalline aluminosilicate, the fine zeolite particles having a fine average primary particle size, being excellent in the cationic exchange properties and the oil-absorbing ability, having a fine average aggregate particle size, and being excellent in the dispersibility; fine zeolite particles obtainable by the above process; and a detergent composition comprising the fine zeolite particles, the detergent composition being excellent in the detergency.Type: GrantFiled: September 30, 2004Date of Patent: May 1, 2007Assignee: Kao CorporationInventors: Kazuo Oki, Hiroji Hosokawa, Mikio Sakaguchi, Hiroshi Kitagaito, Kazuo Taguchi, Hitoshi Takaya
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Patent number: 7208458Abstract: Surfactant compounds are claimed which consists essentially of a) fatty alcohol alkoxylates, b) amorphous silica, c) a carrier material and optionally d) an assistant.Type: GrantFiled: September 27, 2004Date of Patent: April 24, 2007Assignee: Clariant Produkte (Deutschland) GmbHInventors: Georg Borchers, Manfred Schreiber
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Patent number: 7199093Abstract: The present disclosure relates to compositions useful for maintaining the clean impression of a carpet (that is, its scent and appearance) over an extended time despite occurrences that might damage the carpet surface. The composition, which includes an antimicrobial agent, an enzyme inhibitor, and an odor-reacting compound, can be used by a consumer to remove contaminants from the carpet and to prevent the odor associated with the decomposition of future contamination. Specifically, the composition has been shown effective in neutralizing odors associated with the decomposition of organic materials (such as urine or food spills) by absorbing and/or removing the odor-generating source. A manufacturing treatment composition and methods for using are also disclosed.Type: GrantFiled: February 10, 2006Date of Patent: April 3, 2007Assignee: Milliken & CompanyInventors: Shulong Li, Richard A. Mayernik
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Patent number: 7186677Abstract: Provided is a method for producing surfactant granulates, comprising (a) providing a mixture of anionic surfactant acids and builder acids having a weight ratio of 1:100 to 1:20 of builder acid to surfactant acid; and (b) contacting the mixture with at least one solid neutralizing agent. The builder acid is selected from citric acid, tartaric acid, succinic acid, malonic acid, adipic acid, maleic acid, fumaric acid, oxalic acid, gluconic acid, nitrilotriacetic acid, aspartic acid, ethylenediaminetetraacetic acid, aminotrimethylenephosphonic acid, hydroxyethanediphosphonic acid, polyaspartic acids, polyacrylic acids, polymethacrylic acids, or copolymers thereof and has a particle size below 200 ?m.Type: GrantFiled: June 21, 2004Date of Patent: March 6, 2007Assignee: Henkel Kommanditgesellschaft Auf Aktien (Henkel KGAA)Inventors: Wilfried Rähse, Bernhard Orlich, Henriette Weber
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Patent number: 7135449Abstract: The present disclosure relates to compositions useful for maintaining the clean impression of a carpet (that is, its scent and appearance) over an extended time despite occurrences that might damage the carpet surface. The composition, which includes an antimicrobial agent, an enzyme inhibitor, and an odor-reacting compound, can be used by a consumer to remove contaminants from the carpet and to prevent the odor associated with the decomposition of future contamination. Specifically, the composition has been shown effective in neutralizing odors associated with the decomposition of organic materials (such as urine or food spills) by absorbing and/or removing the odor-generating source. A manufacturing treatment composition and methods for using are also disclosed.Type: GrantFiled: September 7, 2004Date of Patent: November 14, 2006Assignee: Milliken & CompanyInventors: Shulong Li, Richard A. Mayernik
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Patent number: 7132390Abstract: The invention provides an adsorbate which comprises a soluble zinc compound of a polycarboxylic acid adsorbed on crystalline alkali metal phyllosilicate, and the use thereof.Type: GrantFiled: July 21, 2004Date of Patent: November 7, 2006Assignee: Clariant GmbHInventors: Harald Bauer, Günther Schimmel
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Patent number: 7115548Abstract: A high-density detergent composition comprises 10 to 60% by weight of a surfactant composition having a weight ratio of an anionic surfactant to a nonionic surfactant of 4:10 or more and 10:0 or less, wherein the high-density detergent composition has a bulk density of from 600 to 1200 g/L, and has a total summation of a product of a mass base frequency Wi and a dissolving rate Vi of each group of classified granules obtained by classifying detergent granules by using a classifier, which satisfies the following formula: ?(Wi·Vi)?95(%), and wherein a mass base frequency of the classified granules having a size of less than 125 ?m is 0.1 or less, wherein the classifier comprises sieves each having a sieve-opening 2000 ?m, 1410 ?m, 1000 ?m, 710 ?m, 500 ?m, 355 ?m, 250 ?m, 180 ?m, and 125 ?m, and a receiver.Type: GrantFiled: January 14, 2000Date of Patent: October 3, 2006Assignee: Kao CorporationInventors: Shu Yamaguchi, Hideichi Nitta, Kyoko Okada, Kimihiro Mizusawa, Jun Kozuka, Toshiharu Noguchi, Hiroyuki Yamashita
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Patent number: 7098177Abstract: A process for preparing detergent particles containing step (I): mixing a base particle for supporting a surfactant ((a) component), and a surfactant composition ((b) component), under mixing conditions wherein the (a) component does not substantially undergo breakdown, to give a mixture; wherein the base particle is obtained by spray-drying an aqueous slurry, wherein the mixing operation is carried out by using a mixer containing agitation impellers, and where the mixer further contains disintegration impellers, the mixing operation step (I) is carried out without substantially rotating the disintegration impellers; and step (II): mixing the mixture obtained in step (I) with 5 to 100 parts by weight of fine powder, while substantially maintaining the shape of the (a) component containing (b) component, to give detergent particles, having a degree of particle growth of 1.3 or less, and a bulk density of 500 g/L or more.Type: GrantFiled: October 14, 1999Date of Patent: August 29, 2006Assignee: Kao CorporationInventors: Teruo Kubota, Hitoshi Takaya, Hiroyuki Yamashita
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Patent number: 7087568Abstract: The present invention provides a process for making a viscous reaction product and making this into a solid or suspendable component, so that it can be incorporated in solid and liquid compositions such as cleaning compositions or for example fabric care compositions. The process comprises the steps of: a) reacting at least two compounds with one another to form a first active material to form a viscous mixed product which has a viscosity of at least 500 cps or even at least 1000 cps at 20° C., thereby preferably mixing this with a second active material; b) mixing the product of step a) with a liquid carrier material, (which can then be suspended in a liquid composition); or if slid components are required, step b) being followed by: c) mixing the mixture of step b) with a solid granulation agent to form a solid component; d) optionally forming the solid component of step c) into granules.Type: GrantFiled: December 20, 2000Date of Patent: August 8, 2006Assignee: The Procter & Gamble CompanyInventor: Johan Smets
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Patent number: 7053038Abstract: A low shear mechanical granulation process for the production of detergent granules, the process comprising contacting an acid precursor of an anionic surfactant, a non-surfactant acid and a solid carbonated neutralising agent wherein the solid carbonated neutralizing agent has a d3,2 average particle size no more than 90 ?m, preferably no more than 80 ?m, more preferably no more than 70 ?m, still more preferably no more than 60 ?m, yet more preferably no more than 50 ?m and especially no more than 40 ?m.Type: GrantFiled: August 8, 2002Date of Patent: May 30, 2006Assignee: Unilever Home & Personal Care USA Division of Conopco, Inc.Inventors: Andreas Theodorus Groot, Cornelis Paulus Montanus
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Patent number: 7049280Abstract: Free-flowing cyclodextrin is made by combining water soluble, substantially perfume-free cyclodextrin with inorganic compounds, especially zeolites. The cyclodextrin is used in a laundry detergent product capable of removing malodor from laundered items during an automatic laundry washing process.Type: GrantFiled: February 28, 2005Date of Patent: May 23, 2006Assignee: The Procter & Gamble companyInventors: Adrian John Wayneforth Angell, Paul Amaat France
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Patent number: 7049279Abstract: A process for making surfactant granules involving: (a) providing a surfactant component selected from the group consisting of a surface-active protein, a surface-active protein derivative, and mixtures thereof; (b) providing a disintegrator component; (c) combining the surfactant component and the disintegrator component to form a surfactant mixture; and (d) granulating and compacting the surfactant mixture to form the surfactant granules.Type: GrantFiled: November 16, 2000Date of Patent: May 23, 2006Assignee: Cognis Deutschland GmbH & Co. KGInventors: Manfred Weuthen, Ditmar Kischkel
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Patent number: 7018971Abstract: A process for the preparation of detergent granules, the process comprising: (i) a first step of admixing in a mechanical granulator, an aluminosilicate and a first liquid binder comprising at least one surfactant, to produce a powder; and (ii) a second step of admixing in a low shear granulator, the powder produced in step (i), a water soluble salt and a second liquid binder, to produce the said detergent granules; wherein in step (ii), no more than 2%, preferably 0% by weight of the aluminosilicate based on the weight of the detergent granules is introduced into the low shear granulator of step (ii).Type: GrantFiled: October 23, 2002Date of Patent: March 28, 2006Assignee: Unilever Home and Personal Care USA division of Conopco, Inc.Inventors: Johannes Hendrikus Akkermans, Remy Antal Verburgh
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Patent number: 7018972Abstract: A process for the preparation of detergent granules, the process comprising: (i) a first step of admixing in a mechanical granulator, a solid component and a first liquid binder, to produce a powder; and (ii) a second step of admixing in a low shear granulator, the powder produced in step (i), and a second liquid binder, to produce the detergent granules; the second liquid binder having a different composition from the first liquid binder and the weight ratio of the first liquid binder to the second liquid binder being from 15:1 to 1:1, preferably from 10:1 to 1:1, more preferably from 5:1 to 1:1, most preferably from 3:1 to 2:1.Type: GrantFiled: October 23, 2002Date of Patent: March 28, 2006Assignee: Unilever Home and Personal Care USA a division of Conopco, Inc.Inventors: Johannes Hendrikus Maria Akkermans, Roland Wilhemus Johannes van Pomeren, Remy Antal Verburgh
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Patent number: 6992055Abstract: A method for producing detergent granules, includes the step of dry-neutralizing a liquid acid precursor of a non-soap, anionic surfactant with a water-soluble, solid, alkali inorganic substance. In this method, a dry-neutralizing step is carried out in the presence of 0.1 to 1.0 mol of an inorganic acid per mol of the liquid acid precursor of a non-soap, anionic surfactant. The above detergent granules have the features of extremely low tackiness of the granules and containing larger number of micropores. By using the detergent granules, a high-bulk density detergent composition having a small particle size can be obtained at high yields.Type: GrantFiled: September 3, 1997Date of Patent: January 31, 2006Assignee: Kao CorporationInventors: Hideichi Nitta, Hiroyuki Yamashita, Jun Saito
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Patent number: 6964945Abstract: The invention relates to solid detergent compositions comprising an aluminosilicate builder and an anionic surfactant and comprising (n) components (i), n being at least 2, whereby the level of aluminosilicate builder in said components together is at least 5% by weight of the composition and the level of the anionic surfactant in said components together is at least 5% by weight of the composition, and whereby the degree of mixture (M) of the anionic surfactant and the aluminosilicate builder is from 0 to 0.7, as defined in the description.Type: GrantFiled: September 25, 1998Date of Patent: November 15, 2005Assignee: The Procter & Gamble CompanyInventors: Richard Timothy Hartshorn, Zayeed Alam, Kevin Norwood
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Patent number: 6951837Abstract: A process for detergent composition which has improved solubility or dissolution in laundering solutions, especially in solutions kept at cold temperatures (i.e., less than about 30° C.), is disclosed. The process includes mixing in at least one high-speed, low-speed, or a moderate-speed mixer, and various combinations of such mixers, at least two materials selected from the group consisting of dry agglomerates, wet agglomerates, spray dried granules, and detergent adjunct ingredients to form particles. Optionally a conditioning apparatus may also be used. The granular detergent composition made from this process is aesthetically pleasing to consumers and has improved flowability.Type: GrantFiled: June 20, 2000Date of Patent: October 4, 2005Assignee: The Procter & Gamble CompanyInventors: Scott William Capeci, Girish Jagannath, Noe Ongcoy Hidalgo, Manivannan Kandasamy, Takashi Kazuta, Yuji Nakamura
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Patent number: 6936577Abstract: A particulate laundry detergent composition which comprises a detergent base powder comprising surfactant and builder and, as separate particulate components: (a) an alkali metal carbonate salt selected from carbonate, bicarbonate, sesquicarbonate and combinations thereof; and (b) a water-soluble organic acid which, when reacted with (a) in the presence of water, generates carbon dioxide gas; wherein the alkali metal carbonate salt, when taken separately, has a 90% dissolution time of less than 15 seconds, preferably less than 10 seconds, more preferably less than 7 seconds; and the water-soluble organic acid has a d50 particle size which is in the range of from 150 to 1500 microns. The alkali metal carbonate salt preferably has an average bulk density of at most 1000 g/l, preferably at most 800 g/l, more preferably at most 600 g/l. The alkali metal carbonate salt preferably has a d50 particle size of at most 250 microns, preferably from 1 to 200 microns, more preferably from 10 to 150 microns.Type: GrantFiled: October 17, 2002Date of Patent: August 30, 2005Assignee: Unilever Home Products and Care USA, division of Conopco, Inc.Inventors: Prasanna Rao Dontula, Alyn James Parry, Catherine Maria Powell, Karen Robinson, Wiebe Schokker, Gilbert Martin Verschelling, Pieter Broer van der Weg
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Patent number: 6936581Abstract: Processes are described for preparing anhydrous detergent granules, wherein the processes comprise: (a) providing an alk(en)yl oligoglycoside composition having a residual fatty alcohol content; (b) reducing the fatty alcohol content of the composition to 30% by weight or less to provide a reduced alcohol content alk(en)yl oligoglycoside; and (c) combining the reduced alcohol content alk(en)yl oligoglycoside with one or more detergent additives.Type: GrantFiled: April 10, 2001Date of Patent: August 30, 2005Assignee: Cognis Deutschland GmbH & Co. KGInventors: Rainer Eskuchen, Manfred Weuthen, Ditmar Kischkel, Tycho Michel, Bernhard Gutsche
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Patent number: 6911423Abstract: In order to improve the dispersion of nonionic surfactant into wash water from a granule in which the nonionic surfactant is carried on a water-insoluble granular material, the nonionic surfactant is intimately mixed with a structurant which is a non-soap ionic surfactant in finely divided particulate form. A preferred structurant is an anionic surfactant, for example, primary alcohol sulphate.Type: GrantFiled: May 14, 2002Date of Patent: June 28, 2005Assignee: Unilever Home & Personal Care USA, division of Conopco, Inc.Inventors: Peter Robert Garrett, John Edley Wilson
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Patent number: 6908895Abstract: A particulate zeolite-built laundry detergent composition having a bulk density of at least 550 g/l comprising at least two different granular components containing both surfactant and builder, preferably one prepared by non-tower granulation and another spray-dried, also contains from 1 to 10 wt % citric acid admixed as a separate particulate component. The admixed citric acid improves dispensing and dissolution properties, whether or not separately admixed sodium carbonate is present.Type: GrantFiled: May 14, 2002Date of Patent: June 21, 2005Assignee: Unilever Home & Personal Care USA, division of Conopco, Inc.Inventors: Vera Johanna Bakker, Arie Krijgsman, Edwin Leo Lempers, Jasper Mol
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Patent number: 6906022Abstract: A detergent composition which has improved solubility or dissolution in laundering solutions, especially in solutions kept at cold temperatures (i.e., less than about 30° C.), is provided. The granular detergent composition is aesthetically pleasing to consumers and has improved flowability. The granular detergent composition has a homogeneity number of greater than 1 wherein the homogeneity number is defined by the equation HN=Xbulk/Xpart. A process for producing the detergent is also provided.Type: GrantFiled: September 24, 1999Date of Patent: June 14, 2005Assignee: The Procter & Gamble CompanyInventors: Scott William Capeci, Mark William Ridyard, Paur R. Mort, III
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Patent number: 6900169Abstract: A process for preparing coated detergent granules in a fluidized bed. The fluidized bed is operated at a flux number of at least about 4 and at a Stokes Number of 10 to about 1000 using a coating solution or slurry having a viscosity from about 300 to about 100,000 centipoise, measured at 60° C. Upon drying, the resultant detergent particles have improved appearance and flow properties and may be packaged and sold as a detergent material or mixed with various other detergent ingredients to provide a fully formulated detergent composition.Type: GrantFiled: June 30, 2004Date of Patent: May 31, 2005Assignee: The Procter & Gamble CompanyInventors: Matthew Israel Wasserman, Mark William Ridyard, Scott William Capeci, Wayne Edward Beimesch, Paul R Mort, III
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Patent number: 6900170Abstract: In order to improve the dispersion of nonionic surfactant into wash water from a granule in which the nonionic surfactant is carried on a water-insoluble granular material, the nonionic surfactant is intimately blended with a water-insoluble liquid. Preferred water-insoluble liquids include hydrocarbons, for example, paraffins.Type: GrantFiled: May 14, 2002Date of Patent: May 31, 2005Assignee: Unilever Home Products and Care USA, a division of Conopco, Inc.Inventors: Terry Instone, Rafiq Mohammed Nabi, John Edley Wilson
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Patent number: 6894018Abstract: A process for the production of granular detergent compositions is provided wherein fluid bed granulation is employed in conjunction with selected recycle of oversized particles to control the uniformity of the resulting detergent composition. The process comprises feeding starting ingredients into a fluid bed granulator to at least partially granulate the feed material while employing the fluid bed to control undersized particle generation and sizing in conjunction with recycle to control oversized particles.Type: GrantFiled: June 20, 2000Date of Patent: May 17, 2005Assignee: The Procter & Gamble CompanyInventors: Wayne Edward Beimesch, Scott William Capeci, G. Gregory Spontak, Matthew Israel Wasserman, Robert Gary Welch
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Patent number: 6878680Abstract: Detergent compositions comprising bleach catalysts or perfumes are disclosed. In particular, components comprising the bleach catalysts or perfumes are disclosed. In particular, the bleach catalysts are formed into stable particles having low moisture content and low moisture pick-up. Particles are also described having low surface area. Particles containing bleach catalysts or perfumes are also described comprising a protective agent which reacts with water to form non-water reaction products, particularly preferred protective agents being bleach activators.Type: GrantFiled: April 30, 2003Date of Patent: April 12, 2005Assignee: Procter & GambleInventors: David Johnathan Kitko, Colin Stephenson
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Patent number: 6858572Abstract: A process for preparing detergent particles having a coating layer of a water-soluble inorganic material is provided. The detergent particle comprises a particle core of a detergent active material. This particle core is then at least partially covered by a particle coating layer of a water soluble inorganic material. Particularly preferred are non-hydratable inorganic coating materials including double salt combinations of alkali metal carbonates and sulfates. The particle coating layer may also include detergent adjunct ingredients such as brighteners, chelants, nonionic surfactants, co-builders, etc. The process includes the steps of passing the particle core through a coating mixer such as a low speed mixer or fluid bed mixer and coating the particle core with a coating solution or slurry of the water soluble inorganic material.Type: GrantFiled: March 8, 2000Date of Patent: February 22, 2005Assignee: The Procter & Gamble CompanyInventor: Paul R Mort, III
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Patent number: 6849590Abstract: The present invention relates to a process for preparing particles for supporting a surfactant, comprising a step of giving a defect to a coating film containing a water-soluble component, wherein the coating film is formed on surfaces of raw material particles; and a process for preparing detergent particles comprising a step of mixing a surfactant composition and the particles for supporting a surfactant obtained by the above process, under conditions that the surfactant composition shows a liquid state. By using the process of the present invention, there can be obtained particles for supporting a surfactant, in which the supporting ability of the particles is improved, without lowering the detergency. In addition, by using the particles for supporting a surfactant, there can be obtained detergent particles having excellent detergency.Type: GrantFiled: December 28, 1999Date of Patent: February 1, 2005Assignee: KAO CorporationInventors: Hiroki Yamaboshi, Shuji Takana, Teruo Kubota, Hitoshi Takaya, Hiroyuki Yamashita, Hideichi Nitta
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Patent number: 6846796Abstract: Surfactant granules are made by the process comprising the steps of (1) mixing an aqueous nonionic surfactant paste and an aqueous solution of an organic polymeric carrier; (2) simultaneously granulating and drying the mixture from step (1) in a fluidized bed to form a granulated nonionic surfactant. The surfactant granules are dust-free, flowable, storage-stable, show no tendency toward clumping and are readily soluble in cold water.Type: GrantFiled: April 6, 2001Date of Patent: January 25, 2005Assignee: Cognis Deutschland GmbH & Co. KGInventor: Karl Heinz Schmid
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Patent number: 6833346Abstract: Methods for making articulate detergents are disclosed. The detergent particulates are formed from a combination of pre-formed detergent particulates and other detergent ingredients may also be preformed such as blown powders, extrudates or agglomerates or particulate raw materials. Selection of the feed streams into a low or moderate shear mixing process enable of the finished detergent particle to be controlled without requiring careful control of the conditions.Type: GrantFiled: November 14, 2001Date of Patent: December 21, 2004Assignee: The Procter & Gamble CompanyInventors: Christopher Andrew Morrison, Scott John Donoghue, Graham Simpson
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Patent number: 6831054Abstract: The dimensionally stable alkaline solid block warewashing detergent uses an E-form binder forming a solid comprising a sodium carbonate source of alkalinity, a sequestrant, a surfactant package and other optional material. The solid block is dimensionally stable and highly effective in removing soil from the surfaces of dishware in the institutional and industrial environment. The E-form hydrate comprises an organic phosphonate and a hydrated carbonate.Type: GrantFiled: May 8, 2003Date of Patent: December 14, 2004Assignee: Ecolab Inc.Inventors: Steven E. Lentsch, Keith E. Olson, G. Jason Wei
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Patent number: 6818605Abstract: The present invention relates to a granular detergent composition having easy measurability and distributivity suitable for spoon measurement, a bulk density thereof being 500 g/L or more, containing a surfactant, a water-insoluble inorganic compound and a water-soluble salt, wherein the granular detergent composition has a variance of powder dropping rate V of 1.0 or less, an inserting pressure P of 80 gf/cm or less, a &Dgr; dropping ratio D of 14% of les, and an index K of from 30 to 230, the index K being represented by the equation: K=P×exp (0.135×D), wherein P stands for an inserting pressure (gf/cm), and D stands for a &Dgr; dropping ratio (%); and a process for preparing the same.Type: GrantFiled: December 13, 2001Date of Patent: November 16, 2004Assignee: Kao CorporationInventors: Takeshi Ban, Teruo Kubota, Shu Yamaguchi, Hiroyuki Saijo, Hiroyuki Yamashita
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Patent number: 6797687Abstract: Mixtures comprising: (a) a gemini surfactant of the formula (I) R1—CHOH—CH2—[OCH2CH2]x—O—CH2—CHOH—R (I) wherein each of R and R1 is a linear or branched alkyl and/or alkenyl group having from 4 to 22 carbon atoms and x is a number from about 5 to about 400; (b) polyethylene glycol are useful as components in laundry detergents, dishwashing detergents and cleaners and for improving the wetting behavior on various surfaces.Type: GrantFiled: August 7, 2002Date of Patent: September 28, 2004Assignee: Cognis Deutschland GmbH & Co. KGInventors: Ditmar Kischkel, Hans-Christian Raths, Manfred Weuthen, Michael Elsner
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Patent number: 6794354Abstract: A continuous process for preparing granular detergent composition including a first step of dry neutralizing an acid precursor of an anionic surfactant with a particulate water-soluble alkaline material in a high speed mixer for a mean residence time of about 0.2 to about 50 seconds, thereby partly or totally neutralizing the acid precursor and producing a dry neutralized material containing the anionic surfactant, in the form of a free-flowing powder; and a second stop of agglomerating the free-flowing powder into a detergent agglomerate using an agglomeration binder. The agglomeration binder is preferably a viscous surfactant paste binder. The resulting agglomerates are dry, free-flowing, and have a substantially more narrow particle size distribution, compared to the free-flowing powder, with reduced fine particles and over-sized particles that generally are recycled.Type: GrantFiled: March 12, 2001Date of Patent: September 21, 2004Assignee: The Procter & Gamble CompanyInventors: Paul R Mort, III, Millard Edward Sullivan
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Patent number: 6790821Abstract: A process for preparing coated detergent granules in a fluidized bed is provided. The fluidized bed is operated at a flux number of at least about 3.5 and/or a Stokes Number of greater than 1.0. Upon drying, the resultant detergent particles have improved appearance and flow properties and may be packaged and sold as a detergent material or mixed with various other detergent ingredients to provide a fully formulated detergent composition.Type: GrantFiled: November 30, 2001Date of Patent: September 14, 2004Assignee: The Procter & Gamble CompanyInventors: Matthew Israel Wasserman, Mark William Ridyard, Scott William Capeci, Wayne Edward Beimesch, Paul R Mort, III
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Patent number: 6784151Abstract: A multi-step process for making a granular detergent composition. The processing steps include adding to a mixer a first feed stream selected from a first powder, a first liquid, and mixtures thereof, to form a second feed stream. The second feed stream is added to a fluid bed dryer to form the granular detergent composition, and optionally, a third feed stream selected from a second powder, a second liquid, and mixtures thereof can be added to the fluid bed dryer. The granular detergent composition contains at least about 50% by weight of particles having a geometric mean particle diameter of from about 500 microns to about 1500 microns with a geometric standard deviation of from about 1 to about 2. Further, at least a portion of the particles contain a detersive surfactant or a detergent builder.Type: GrantFiled: January 8, 2003Date of Patent: August 31, 2004Assignee: The Procter & Gamble CompanyInventors: Scott William Capeci, Steven Matthew Gabriel, Girish Jagannath, Scott John Donoghue, Christopher Andrew Morrison