Spray-dried Product, Or Process Of Preparing Patents (Class 510/452)
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Patent number: 6767880Abstract: A process for improving aesthetics of a liquid dishwashing detergent product is disclosed. The process includes the steps of providing a liquid dishwashing detergent composition and adding solid particles to the liquid dishwashing detergent composition. The particles are coated with a polymeric coating. The coating is prepared from materials which are insoluble in the liquid dishwashing detergent composition but soluble in dishwashing wash solution.Type: GrantFiled: September 24, 2001Date of Patent: July 27, 2004Assignee: The Procter & Gamble CompanyInventors: Peter Robert Foley, Brian Xiaoqing Song, Mary Ruth Leyendecker, Eugene Steven Sadlowski, Jeffrey Donald Painter, Joseph Herbert Thien
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Patent number: 6756353Abstract: Detergent compositions or components are formulated with certain hydrophobically modified cellulosic materials, which provide protection of fabrics, whereof at least 80% or even at least 90% have a particle size of below 1000 microns or even below 850 or even 710 microns. Selection of materials of this particle size results in improved dispersability of the cellulosic material and imparts improved appearance and integrity benefits to fabrics and textiles laundered in washing solutions from such compositions.Type: GrantFiled: December 3, 2001Date of Patent: June 29, 2004Assignee: The Procter & Gamble CompanyInventors: Robert Michael Pettifer, Victor Stuart Reid, Paul Sherrington, Shirley Summers
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Patent number: 6734156Abstract: The present invention relates to particles for supporting a surfactant and a process for preparing the same. Further, the present invention relates to high-density detergent particles using the particles for supporting a surfactant, and a process for preparing the same.Type: GrantFiled: February 14, 2001Date of Patent: May 11, 2004Assignee: Kao CorporationInventors: Shuji Takana, Hitoshi Takaya, Hiroki Yamaboshi, Yoichi Sugiyama, Hiroshi Kitagaito, Shu Yamaguchi, Hiroyuki Yamashita
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Publication number: 20040005994Abstract: Solid mixtures comprising: (a) a solid carrier, (b) a surfactant component, (c) a component which is liquid at room temperature, and (d) a hydrocolloid are described along with processes for their production and their use.Type: ApplicationFiled: March 28, 2003Publication date: January 8, 2004Inventors: Rainer Eskuchen, Franz Wenin
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Publication number: 20030203832Abstract: An improved process having the steps of forming a low organic slurry in a mixer, pumping the low organic slurry to a spray drying tower, spraying the low organic slurry in the spray drying tower, drying the low organic slurry in the spray drying tower to form a low organic granule, and processing the low organic granule to form a detergent composition. The low organic slurry contains less than about 10%, by weight of the low organic slurry, of an organic material.Type: ApplicationFiled: April 15, 2003Publication date: October 30, 2003Applicant: The Procter & Gamble CompanyInventors: Jeffrey Edward Boucher, Rui Shen, Kaiming Zhu
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Patent number: 6627596Abstract: The present invention relates to a cationic particle containing an aqueous cationic surfactant solution adsorbed to a water-insoluble high absorbing material. Preferably, the water-insoluble high absorbing material has an oil absorption (using d-butyl phthalate) of from about 140 mL/100 g to about 400 mL/100 g. A process for making the cationic particle is also described herein. The cationic particle can be incorporated into a particulate detergent composition.Type: GrantFiled: July 31, 2001Date of Patent: September 30, 2003Assignee: The Procter & Gamble CompanyInventors: Manivannan Kandasamy, Kenji Naemura, Daniel James Dufton, Eric San Jose Robles, Aram Armand Dedeyan
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Publication number: 20030130157Abstract: A particulate laundry detergent composition which comprises a detergent base powder comprising surfactant and builder and, as separate particulate components:Type: ApplicationFiled: October 17, 2002Publication date: July 10, 2003Applicant: Unilever Home & Personal Care USA, Division of Conopco, Inc.Inventors: Prasanna Rao Dontula, Alyn James Parry, Catherine Maria Powell, Karen Robinson, Wiebe Schokker, Gilbert Martin Verschelling, Pieter Broer van der Weg
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Publication number: 20030130156Abstract: A particulate laundry detergent composition which comprises, as separate particulate components:Type: ApplicationFiled: October 17, 2002Publication date: July 10, 2003Applicant: Unilever Home & Personal Care USA, Division of Conopco, Inc.Inventors: Prasanna Rao Dontula, Alyn James Parry, Catherine Maria Powell, Karen Robinson, Wiebe Schokker, Gilbert Martin Verschelling, Pieter Broer van der Weg
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Publication number: 20030119694Abstract: The invention is a solid chemical concentrate system of at least two cooperative shapes. The first shape is an inwardly curved bar having an inner opening. The second shape is an insert which is capable of interlocking with the bar by insertion into the bar inner opening. The solid chemical concentrate provides chemical systems having active constituents which may be the same, different but compatible or functionally and chemically incompatible combined within one matrix to provide at least one substantially continuous surface. The system may also comprise an aqueous soluble or dispersible polymeric film cover.Type: ApplicationFiled: August 13, 2002Publication date: June 26, 2003Applicant: Ecolab Inc.Inventors: Elizabeth J. Gladfelter, Tina O. Outlaw, James L. Copeland, Rhonda K. Schulz, Daniel K. Boche, Jeff W. Peterson
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Publication number: 20030114346Abstract: Synthetic detergent formulations are made by spray drying an aqueous dispersion or emulsion of a synthetic detergent and a hydrophobic plasticiser and optionally a filler to pr duce a particulate product. In particular the synthetic detergent includes mild surfactants such a fatty isethionate or sulphosuccinate surfactants. By spray drying the emulsion or dispersion, a particularly uniform product is made which can readily be formed into synthetic detergent bars which may include soap to form combination bar products (combi-bars).Type: ApplicationFiled: October 8, 2002Publication date: June 19, 2003Applicant: Imperial Chemical Industries PLCInventor: Paul Clignet
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Publication number: 20030114347Abstract: A particulate laundry detergent composition which comprises, as separate particulate components:Type: ApplicationFiled: October 17, 2002Publication date: June 19, 2003Applicant: Unilever Home & Personal Care USA, Division of Conopco, Inc.Inventors: Prasanna Rao Dontula, Alyn James Parry, Catherine Maria Powell, Karen Robinson, Wiebe Schokker, Gilbert Martin Verschelling, Pieter Broer van der Weg
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Publication number: 20030109397Abstract: Process for reducing the density of solid detergent ingredients by forming said ingredients into hollow-core particles. The density of ingredients such as sodium citrate, sodium carbonate and/or sodium silicate, when formed into such hollow-core particles, allows them to be stably incorporated into non-aqueous liquid laundry detergents.Type: ApplicationFiled: July 17, 2002Publication date: June 12, 2003Applicant: The Procter & Gamble CompanyInventors: Yousef Georges Aouad, Christopher John Lienhart, Diane Parry
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Publication number: 20030087791Abstract: A coloured speckle composition for use in particulate laundry detergent compositions comprising a porous granular carrier and at least 0.01 wt % photobleach, preferably at least 0.05 wt %, more preferably at least 0.1 wt %, based on the active ingredient, the composition having an average bulk density of at most 600 g/l, preferably at most 500 g/l, most preferably at most 400 g/l. The carrier system reduces the staining tendency of the photobleach. The most preferred carrier is spray dried detergent base powder. The most preferred photobleach is a blend of Zn and Al sulphonated phthalocyanine.Type: ApplicationFiled: August 19, 2002Publication date: May 8, 2003Applicant: Unilever Home & Personal Care USA, Division of Conopco, Inc.Inventors: Juan Jose Bonelli, Marcio Henrique Perissinotto Bonfa, Rudolf Govert Van Driel, Paulo-Enrique De Gusmao, Mario Jovelino Del Nunzio, Paulo Cesar Puelle Andrade
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Publication number: 20030060394Abstract: A process for producing a water-dispersible non-particulate detergent product includes the step of providing a particulate detergent composition. The process further includes the step of adding a flow aid to the particulate detergent composition in a range of from about 0.1% to about 25% by weight of the particulate detergent composition. The process then includes the step of compacting the particulate detergent composition having the flow aid by applying a pressure in an amount sufficient to form the water-dispersible non-particulate detergent product having a density of at least about 1000 g/l. This process enables the manufacture of a rapidly dispersing non-particulate detergent composition that sinks in water.Type: ApplicationFiled: October 10, 2002Publication date: March 27, 2003Inventors: Adrian John Waynforth Angell, Les Charles Zorb
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Patent number: 6534471Abstract: A process for the production of colored detergent particles. The process is characterized in that a slurry comprising at least one powdering agent and at least one dye is spray dried so that a colored powdering agent is formed. The thus formed colored powdering agent is then applied to detergent particles.Type: GrantFiled: December 4, 2000Date of Patent: March 18, 2003Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Christian Block, Antoni Machin, Hans-Friedrich Kruse
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Patent number: 6528475Abstract: A process for making a solid primary alkyl amine salt, and its use in a powdered laundry detergent.Type: GrantFiled: October 5, 2000Date of Patent: March 4, 2003Assignee: Cognis CorporationInventors: Stephen F. Gross, Robert J. Valesky, Timothy C. Morris, Robert J. Coakley, George Smith
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Patent number: 6511956Abstract: The present invention relates to a process for forming a cleaning composition containing the steps of providing at least one alkaline material and at least one acid active, and adding the acid active and the alkaline material to a mixer. The acid active is substantially neutralized within the mixer to form a neutralized detergent active. At least one acid-sensitive polymer is added to the neutralized detergent active to form a slurry, and the slurry is formed into a cleaning composition. A cleaning composition as formed by the above process is also described herein.Type: GrantFiled: June 19, 2001Date of Patent: January 28, 2003Assignee: The Procter & Gamble CompanyInventors: Tianli Wen, Manivannan Kandasamy
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Patent number: 6503878Abstract: The present invention relates to pellets comprising one or more active ingredients; and either one or both of: (a) one or more binders incorporated within the body of the pellet; and (b) one or more coating materials on the surface of the pellet; characterized in that either one or both of the binders and the coating materials comprise one or more polymers with a Tg in the range −85 to +35°C., and, optionally, wherein the coating and/or binder materials comprise at least one multi-phase polymer and further wherein at least one of the phases of the multi-phase polymer has a Tg in the range −85 to +35° C.Type: GrantFiled: September 22, 2000Date of Patent: January 7, 2003Assignee: Rohm and Haas CompanyInventors: Curtis Schwartz, Steven Michael Baxter
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Patent number: 6498133Abstract: Particulate bleach activators comprising 15 to 60% by weight of an acetonitrile, 20 to 70% by weight of a silicon-containing carrier material and 20 to 30% by weight of water, which are obtained by applying an aqueous solution, saturated at 10 to 40° C., of an acetonitrile onto the carrier material without subsequent drying, where the amount of saturated aqueous solution is measured such that the given limits for acetonitrile, carrier material and water are observed.Type: GrantFiled: November 16, 2001Date of Patent: December 24, 2002Assignee: Clariant GmbHInventors: Georg Borchers, Robert Milbradt, Oliver Mogck, Frank Weinelt
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Patent number: 6492320Abstract: The present invention relates to a multifunctional pellet aid including one or more binders, wherein at least one binder is an acrylic based polymer having a Tg ranging from −20° C. to +95° C., one or more inorganic solids and one or more organic solids; the particle size of the pellet aid ranging from 100 &mgr;m to 3000 &mgr;m. Adding 0.25 to 10% by weight of the multifunctional pellet aid, based on the total weight of the pellet, to a plurality of ingredients and compacting the pellet aid and ingredients to form a pellet, affords a pellet having improved mechanical strength as a solid and rapidly disintegrating upon contact with an aqueous system.Type: GrantFiled: December 27, 2000Date of Patent: December 10, 2002Assignee: Rohm and Hass CompanyInventors: Hailan Guo, Wen H. Chia, Curtis Schwartz
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Patent number: 6458755Abstract: A spray-dried amorphous alkali metal silicate compound which provides multiple-cycle washing performance. The silicate compound has a molar ratio of M2O to SiO2 of 1:1.5 to 1:3.3 wherein M represents an alkali metal. The compound contains 0.5 to less than 30% by weight of anionic surfactant and has an absorption capacity for liquid components which is at least 20% higher than that of the same quantity of the alkali metal silicate compound which is free from anionic surfactant.Type: GrantFiled: December 11, 2000Date of Patent: October 1, 2002Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Kathrin Schnepp-Hentrich, Rene-Andres Artiga Gonzalez, Katrin Burmeister, Hubert Freese, Manfred Greger, Bernd Larson, Volker Bauer, Peter Sandkuehler, Wilfried Raehse
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Patent number: 6451224Abstract: A stable free-flowing solid chelant composition is produced by the process comprising the steps of: a) adjusting the pH of an aqueous solution of the chelant to a value of from about 1.2 to about 3.0 by the addition of an inorganic acid; and b) drying the pH adjusted aqueous chelant product.Type: GrantFiled: July 11, 2001Date of Patent: September 17, 2002Assignee: The Dow Chemical CompanyInventor: David A. Wilson
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Publication number: 20020115584Abstract: According to the present invention there is provided polymer-containing granules for addition to detergent compositions, said granule comprising:Type: ApplicationFiled: November 5, 2001Publication date: August 22, 2002Applicant: The Procter & Gamble CompanyInventors: Steven Rene Martha Ongena, Iwein Jozef Marie Jaak Goderis
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Patent number: 6432905Abstract: The present invention relates to a process for preparing granular detergent products in which a liquid binder component comprising an acid precursor of an anionic surfactant and a hydrotrope is contacted with a solid particulate starting material comprising a neutralizing agent in a low shear mixer and the mixture granulated, the hydrotrope being present at a level of at least 1% by weight of the acid precursor of the anionic surfactant.Type: GrantFiled: March 23, 2000Date of Patent: August 13, 2002Assignee: Unilever Home & Personal Care USA division of Conopco, Inc.Inventors: Chandrasekaran Gowrishankaran, Winston Anthony Pereira, Rana Sengupta
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Publication number: 20020086807Abstract: The present invention relates to a coated granular sodium percarbonate for detergent and its manufacturing process, and more particularly to a coated granular sodium percarbonate and its manufacturing process, wherein the surface of said sodium percarbonate establishes a multiple coating layer by being internally coated with a specific composition containing alkali metal silicate while externally coated with a specific composition containing alkali metal sulfate on upper part of said internally coated layer thus providing said sodium percarbonate an excellent dissolving rate in water as well as a good storage stability, preventing it from caking during delivery or storage, and being ultimately utilized as an effective detergent bleach containing zeolite as its detergent builder.Type: ApplicationFiled: January 9, 2002Publication date: July 4, 2002Applicant: Oriental Chemical Industries Co., Ltd.Inventors: Sang Hwa Lee, Yong Il Kim, Sun Ki Shur, Jong Pill Lee
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Patent number: 6395703Abstract: A detergent composition is described which is a solid homogeneous, evenly dispersed composition containing anionic and nonionic surfactants, soil suspending agents, chelating or sequestering agents, and alkaline builders. The detergent compositions will contain either active enzymes, an oxygen releasing bleaching agent or both. The active enzymes can be protease, amylase or lipase enzymes. Said composition can be used for laundry washing or hard surface cleaning. Manufacturing procedures and methods of use are described.Type: GrantFiled: December 1, 2000Date of Patent: May 28, 2002Assignee: Sunburst Chemicals, Inc.Inventor: William H. Scepanski
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Patent number: 6395702Abstract: A detergent composition is described which is a solid homogeneous, evenly dispersed composition containing anionic and nonionic surfactants, soil suspending agents, chelating or sequestering agents, and alkaline builders. The detergent compositions will contain either active enzymes, an oxygen releasing bleaching agent or both. The active enzymes can be protease, amylase or lipase enzymes. Said composition can be used for laundry washing or hard surface cleaning. Manufacturing procedures and methods of use are described.Type: GrantFiled: July 16, 2001Date of Patent: May 28, 2002Assignee: Sunburst Chemicals, Inc.Inventor: William H. Scepanski
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Patent number: 6391846Abstract: A particulate zero-phosphate laundry detergent powder, preferably of bulk density 600-900 g/l, contains zeolite MAP and zeolite A in a weight ratio of at least 1:1. The powder may contain at least two different granular components containing organic surfactant and zeolite builder. A first granular component, which is preferably non-spray-dried and has a bulk density of 550-900 g/l, contains zeolite MAP, while a second granular component, which is preferably spray-dried and has a bulk density of 200-450 g/l, contains zeolite A.Type: GrantFiled: June 8, 2000Date of Patent: May 21, 2002Assignee: Unilever Home & Personal Care, USA. division of Conopco, Inc.Inventors: Daniel Pierre Marie Berthod, Christophe Michel Bruno Joyeux, Johannes Hendrikus Langeveld
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Patent number: 6387869Abstract: A granular surfactant composition comprising sodium silicate and linear alkylbenzenesulfonates, wherein the granular surfactant composition has a mean particle diameter of ≧50 &mgr;m and an ffc value of ≧7; a process for the preparation of this granular surfactant composition, its use, and detergents and cleaners which comprise such granular surfactant composition and a process for the making of the same; and, where appropriate, the granular surfactant composition comprises other active ingredients and auxiliaries.Type: GrantFiled: March 30, 2001Date of Patent: May 14, 2002Assignee: Clariant GmbHInventors: Harald Bauer, Josef Holz, Gunther Schimmel
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Patent number: 6376453Abstract: To provide detergent particles having high-speed dissolution capable of dissolving quickly in water after supplying the detergent particles in water, and a method for preparing the detergent particles, and a detergent composition comprising the detergent particles. Detergent particles having an average particle size of from 150 to 500 &mgr;m and a bulk density of 500 g/liter or more, wherein the detergent particles comprising a detergent particle being capable of releasing a bubble from an inner portion of the detergent particles in a process of dissolving the detergent particle in water, the bubble having a size of one-tenth or more of a particle size of the detergent particle, and wherein the detergent particles have a dissolution rate as calculated by Equation (1) of 90% or more, under conditions where the detergent particles are supplied in water at 5° C.Type: GrantFiled: July 22, 1999Date of Patent: April 23, 2002Assignee: Kao CorporationInventors: Teruo Kubota, Hitoshi Takaya, Shu Yamaguchi, Hiroyuki Yamashita, Shuji Takana
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Publication number: 20020002130Abstract: A spray-dried amorphous alkali metal silicate compound which provides multiple-cycle washing performance. The silicate compound has a molar ratio of M2O to SiO2 of 1:1.5 to 1:3.3 wherein M represents an alkali metal. The compound contains 0.5 to less than 30% by weight of anionic surfactant and has an absorption capacity for liquid components which is at least 20% higher than that of the same quantity of the alkali metal silicate compound which is free from anionic surfactant.Type: ApplicationFiled: December 11, 2000Publication date: January 3, 2002Applicant: Henkel Kommanditgesellschaft auf AktienInventors: Kathrin Schnepp-Hentrich, Rene-Andres Artiga Gonzalez, Katrin Burmeister, Hubert Freese, Manfred Greger, Bernd Larson, Volker Bauer, Peter Sandkuehler, Wilfried Raehse
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Patent number: 6329334Abstract: The invention relates to the use of crosslinked polyvinylpyrrolidone as an additive to compact, particulate detergents and cleansers for the purpose of increasing the rate of disintegration thereof when brought into contact with water, to the particles of crosslinked polyvinylpyrrolidone having a particle size of from 50 to 400 &mgr;m, to a process for the preparation of the compact, particulate detergents and cleansers, and also to the compact, particulate detergents and cleansers themselves.Type: GrantFiled: March 14, 2000Date of Patent: December 11, 2001Assignee: BASF AktiengesellschaftInventors: Werner Bertleff, Folker Ruchatz, Richard Baur, Robert Heinz, Peter Palm
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Publication number: 20010034317Abstract: A water-containing solid detergent having a delayed, controllable and variable hardening time after addition of all the components produced by providingType: ApplicationFiled: March 24, 1999Publication date: October 25, 2001Inventors: DIETER HEMM, GUENTER HELLMANN
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Patent number: 6303558Abstract: A particulate detergent composition or component of high bulk density (at least 600 g/l), comprising at least 10% by weight of detergent surfactant and from 10 to 70% by weight of detergency builder, is composed of at least two, and preferably at least three, different granular components: (i) granules comprising at least 60% by weight of anionic surfactant, (ii) granules comprising at least 20% by weight of nonionic surfactant, and less than 10% by weight of aluminosilicate. (iii)optionally, granules comprising detergency builder.Type: GrantFiled: May 26, 1998Date of Patent: October 16, 2001Assignee: Lever Brothers Co., division of ConopcoInventors: William Derek Emery, Pauline Farnworth, Georgina Hawkes, Terry Instone, Seeng Djiang Liem, John Lloyd, Gilbert Martin Verschelling
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Patent number: 6294512Abstract: Detergent compositions contain sticky particles with at least 45% by weight of a sticky surfactant and non-sticky particles with less than about 1% by weight of sticky surfactant. The particles are further characterized by their size ranges and bulk densities. Compositions containing potassium ions are described. Dissolution of the compositions in aqueous media is optimized.Type: GrantFiled: June 30, 2000Date of Patent: September 25, 2001Assignee: The Procter & Gamble CompanyInventors: Paul R Mort, III, Kevin Todd Norwood
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Publication number: 20010009897Abstract: The invention relates to a granular alkali metal phyllosilicate compound which comprises a crystalline alkali metal phyllosilicate, a colorant and an additive. The invention also relates to a process for its preparation, and to detergents and cleaners which comprise such a granular alkali metal phyllosilicate compound.Type: ApplicationFiled: December 15, 2000Publication date: July 26, 2001Applicant: Clariant GmbHInventors: Harald Bauer, Josef Holz, Gunther Schimmel
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Patent number: 6232284Abstract: The present invention relates to tablets comprising a core and a coating, the core being formed by compressing a particulate material, the particulate material comprising surfactant and detergent builder, and the coating comprising a material, or mixture of materials, such as a fatty alcohol, which is substantially insoluble in water at 25° C. The tablets are provided with means, such as effervescent agents, which aid in their disintegration in wash liquors.Type: GrantFiled: June 4, 1999Date of Patent: May 15, 2001Assignee: The Procter & Gamble CompanyInventors: Paul Irma Albertus Van Dijk, Jose Luis Vega
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Patent number: 6200949Abstract: Described is a process for forming controllably releasable fragrance-containing consumable articles, for example, encapsulated fragrances in detergents or fabric softener articles and compositions. The process includes the steps of: (a) forming an aqueous fragrance emulsion, including a modified starch; (b) spray drying or freeze drying the emulsion to form a fragrance-containing powder; and (c) mixing a solid consumable article base (e.g., detergent or fabric softener base) with the fragrance-containing powder. Also described are products produced by means of such processes as well as uses thereof.Type: GrantFiled: December 21, 1999Date of Patent: March 13, 2001Assignee: International Flavors and Fragrances Inc.Inventors: Henricus Gerardus Maria Reijmer, Adi Shefer
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Patent number: 6194367Abstract: The present invention discloses an alkaline cleaning composition for cleaning heavily soiled metal surfaces such as food fryers, baking pans, high temperature pasteurizers, and beer kettles, ceramic surfaces such as restaurant grade ceramic china plates and platters, and plastic surfaces. The cleaning composition is noncaustic and includes a peroxygen compound, a chelate, and a metasilicate and/or sesquisilicate. A preferred cleaning composition further includes a surfactant and hydrated builder.Type: GrantFiled: April 27, 1999Date of Patent: February 27, 2001Assignee: Charvid Limited Liability Co.Inventor: Charles Bullick Talley
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Patent number: 6191096Abstract: A spray-dried amorphous alkali metal silicate compound which provides multiple-cycle washing performance. The silicate compound has a molar ratio of M2O to SiO2 of 1:1.5 to 1:3.3 wherein M represents an alkali metal. The compound contains 0.5 to less than 30% by weight of anionic surfactant and has an absorption capacity for liquid components which is at least 20% higher than that of the same quantity of the alkali metal silicate compound which is free from anionic surfactant.Type: GrantFiled: August 18, 1997Date of Patent: February 20, 2001Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Kathrin Schnepp-Hentrich, Rene-Andres Artiga Gonzalez, Katrin Burmeister, Hubert Freese, Manfred Greger, Bernd Larson, Volker Bauer, Peter Sandkuehler, Wilfried Raehse
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Patent number: 6165972Abstract: A solid surfactant mixture, comprising one or more fatty acid polyhydroxyamides of the formula IRCONR.sup.1 Z (1)in which R is C.sub.7 -C.sub.31 -alkyl or C.sub.7 -C.sub.31 -alkenyl, Z is a polyhydroxyhydrocarbon group having at least two hydroxyl groups, which may also be alkoxylated, and R.sup.1 is C.sub.1 -C.sub.8 -alkyl or a group of the formula --(CH.sub.2).sub.x NR.sup.2 R.sup.3 or R.sup.4 O(CH.sub.2).sub.n --, R.sup.2 and R.sup.3 are C.sub.1 -C.sub.4 -alkyl or C.sub.2 -C.sub.4 -hydroxyalkyl, R.sup.4 is C.sub.1 -C.sub.4 -alkyl and x is a number from 1 to 10 and n is a number from 2 to 4, one or more other nonionic surfactants and/or one or more anionic surfactants.Type: GrantFiled: September 2, 1999Date of Patent: December 26, 2000Assignee: Clariant GmbHInventors: Frank Weinelt, Helmut Keck
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Patent number: 6162781Abstract: Foam control granules, for use in particulate laundry detergent compositions, comprise a mobile hydrophobic foam control agent, preferably silicone oil in admixture with hydrophobic silica, optionally combined with a mixture of a hydrocarbon such as petroleum jelly and an alkylphosphoric acid salt, sorbed onto a porous absorbent inorganic carrier comprising or consisting of anhydrous sodium carbonate, preferably light soda ash. When such granules are prepared by mixing and granulating in a high shear mixer/granulator, the addition of from 1 to 10 wt % water after mixing and granulation results in granules having improved flow properties.Type: GrantFiled: August 12, 1999Date of Patent: December 19, 2000Assignee: Lever Brothers Company, div. of Conopco Inc.Inventors: Marinela Buscan, Francois Delwel, Angela Di-Pietro
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Patent number: 6162780Abstract: A carbonate-based detergent having improved properties is provided. Preferably, a base detergent includes an alkali metal carbonate builder, an anionic surfactant, an inert diluent, a copolymer, and a chlorine scavenger. The base detergent is mixed with an agglomerate including nonionic surfactants and a builder such as an alkali metal carbonate. The detergent has improved color retention properties. A method of preparing the improved detergent composition is also provided.Type: GrantFiled: August 9, 1999Date of Patent: December 19, 2000Assignee: The Dial CorporationInventors: Terrell L. Partee, Charles Varker, Elaine T. Morse, Ronald D. Morgan
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Patent number: 6159920Abstract: A detergent composition comprises detergent particles, each particle having a substantially anhydrous coating comprising a fluorescent whitening agent and a nonionic surfactant. A process for the preparation of the said detergent composition comprises spraying base detergent particles with a substantially anhydrous mixture comprising the fluorescent whitening agent and the nonionic surfactant.Type: GrantFiled: November 9, 1999Date of Patent: December 12, 2000Assignee: The Proctor & Gamble CompanyInventor: Mark William Ridyard
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Patent number: 6153574Abstract: The speed of disintegration of tablets containing a water-softening agent, especially water-insoluble, water-softening agent intended as detergency builder for fabric washing is enhanced by incorporating spray-dried partially hydrated sodium acetate alone or jointly with sodium citrate dihydrate and/or crystallized sodium acetate trihydrate.Type: GrantFiled: October 7, 1999Date of Patent: November 28, 2000Assignee: Unilever Home & Personal Care USA division of Conopco, Inc.Inventor: Roger Joseph Anna Janssen
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Patent number: 6147046Abstract: A method and apparatus is disclosed for producing a fragrance-containing solid particle, capable of controllably releasing the fragrance to the environment in which the particle is contained, for incorporation into laundry detergents, fabric softener compositions and drier-added fabric softener articles.Type: GrantFiled: December 30, 1999Date of Patent: November 14, 2000Assignee: International Flavors & Fragrances Inc.Inventors: Adi Shefer, Shmuel David Shefer, Maureen S. Santoro
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Patent number: 6142398Abstract: A method and apparatus is disclosed for producing a fragrance-containing solid particle, capable of controllably releasing the fragrance to the environment in which the particle is contained, for incorporation into laundry detergents, fabric softener compositions and drier-added fabric softener articles.Type: GrantFiled: December 30, 1999Date of Patent: November 7, 2000Assignee: International Flavors & Fragrances Inc.Inventors: Adi Shefer, Shmuel David Shefer, Maureen S. Santoro
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Patent number: 6140292Abstract: Detergent compositions and fabric laundering and treating methods utilize certain polyamide-polyamines as fabric treatment agents that can impart fabric appearance benefits to fabric laundered or treated in washing or soaking solutions which contain such agents. Such polyamide-polyamine fabric treatment agents include adipic acid-diethylenetriamine-epichlorohydrin adducts.Type: GrantFiled: June 30, 1999Date of Patent: October 31, 2000Assignee: The Procter & Gamble CompanyInventors: Sherri Lynn Randall, Rajan Keshav Panandiker
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Patent number: 6133216Abstract: The invention relates to coated bleach activator granules of ammonium nitriles, which have been obtained by coating ammonium nitrile base granules with a water-soluble coating substance. The base granules are preferably thermally conditioned during or after the coating with the coating substance.Type: GrantFiled: September 15, 1998Date of Patent: October 17, 2000Assignee: Clariant GmbHInventors: Matthias Loffler, Gerd Reinhardt
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Patent number: 6069124Abstract: A detergent composition having a bulk density of at least 550 kg/m.sup.3 comprises a mixture of:(a) a granulate, preferably a mechanically mixed granulate, of bulk density 450 kg/m.sup.3 to 1300 kg/m.sup.3, comprising surfactant and inorganic material, and(b) a spray-dried adjunct comprising inorganic material, preferably sodium sesquicarbonate or Burkeite,component (a) being present in an amount of from 35% to 85% by weight of the total granular product.The adjunct allows the bulk density of the final composition to be adjusted to any chosen value without detriment to other properties, thus providing flexibility to formulate at a range of bulk densities.Type: GrantFiled: May 26, 1998Date of Patent: May 30, 2000Assignee: Lever Brothers Company Division of Conopco, Inc.Inventors: Peter Willem Appel, Marcel van der Kraan