Spray-dried Product, Or Process Of Preparing Patents (Class 510/452)
  • Patent number: 6767880
    Abstract: A process for improving aesthetics of a liquid dishwashing detergent product is disclosed. The process includes the steps of providing a liquid dishwashing detergent composition and adding solid particles to the liquid dishwashing detergent composition. The particles are coated with a polymeric coating. The coating is prepared from materials which are insoluble in the liquid dishwashing detergent composition but soluble in dishwashing wash solution.
    Type: Grant
    Filed: September 24, 2001
    Date of Patent: July 27, 2004
    Assignee: The Procter & Gamble Company
    Inventors: Peter Robert Foley, Brian Xiaoqing Song, Mary Ruth Leyendecker, Eugene Steven Sadlowski, Jeffrey Donald Painter, Joseph Herbert Thien
  • Patent number: 6756353
    Abstract: Detergent compositions or components are formulated with certain hydrophobically modified cellulosic materials, which provide protection of fabrics, whereof at least 80% or even at least 90% have a particle size of below 1000 microns or even below 850 or even 710 microns. Selection of materials of this particle size results in improved dispersability of the cellulosic material and imparts improved appearance and integrity benefits to fabrics and textiles laundered in washing solutions from such compositions.
    Type: Grant
    Filed: December 3, 2001
    Date of Patent: June 29, 2004
    Assignee: The Procter & Gamble Company
    Inventors: Robert Michael Pettifer, Victor Stuart Reid, Paul Sherrington, Shirley Summers
  • Patent number: 6734156
    Abstract: The present invention relates to particles for supporting a surfactant and a process for preparing the same. Further, the present invention relates to high-density detergent particles using the particles for supporting a surfactant, and a process for preparing the same.
    Type: Grant
    Filed: February 14, 2001
    Date of Patent: May 11, 2004
    Assignee: Kao Corporation
    Inventors: Shuji Takana, Hitoshi Takaya, Hiroki Yamaboshi, Yoichi Sugiyama, Hiroshi Kitagaito, Shu Yamaguchi, Hiroyuki Yamashita
  • Publication number: 20040005994
    Abstract: Solid mixtures comprising: (a) a solid carrier, (b) a surfactant component, (c) a component which is liquid at room temperature, and (d) a hydrocolloid are described along with processes for their production and their use.
    Type: Application
    Filed: March 28, 2003
    Publication date: January 8, 2004
    Inventors: Rainer Eskuchen, Franz Wenin
  • Publication number: 20030203832
    Abstract: An improved process having the steps of forming a low organic slurry in a mixer, pumping the low organic slurry to a spray drying tower, spraying the low organic slurry in the spray drying tower, drying the low organic slurry in the spray drying tower to form a low organic granule, and processing the low organic granule to form a detergent composition. The low organic slurry contains less than about 10%, by weight of the low organic slurry, of an organic material.
    Type: Application
    Filed: April 15, 2003
    Publication date: October 30, 2003
    Applicant: The Procter & Gamble Company
    Inventors: Jeffrey Edward Boucher, Rui Shen, Kaiming Zhu
  • Patent number: 6627596
    Abstract: The present invention relates to a cationic particle containing an aqueous cationic surfactant solution adsorbed to a water-insoluble high absorbing material. Preferably, the water-insoluble high absorbing material has an oil absorption (using d-butyl phthalate) of from about 140 mL/100 g to about 400 mL/100 g. A process for making the cationic particle is also described herein. The cationic particle can be incorporated into a particulate detergent composition.
    Type: Grant
    Filed: July 31, 2001
    Date of Patent: September 30, 2003
    Assignee: The Procter & Gamble Company
    Inventors: Manivannan Kandasamy, Kenji Naemura, Daniel James Dufton, Eric San Jose Robles, Aram Armand Dedeyan
  • Publication number: 20030130157
    Abstract: A particulate laundry detergent composition which comprises a detergent base powder comprising surfactant and builder and, as separate particulate components:
    Type: Application
    Filed: October 17, 2002
    Publication date: July 10, 2003
    Applicant: Unilever Home & Personal Care USA, Division of Conopco, Inc.
    Inventors: Prasanna Rao Dontula, Alyn James Parry, Catherine Maria Powell, Karen Robinson, Wiebe Schokker, Gilbert Martin Verschelling, Pieter Broer van der Weg
  • Publication number: 20030130156
    Abstract: A particulate laundry detergent composition which comprises, as separate particulate components:
    Type: Application
    Filed: October 17, 2002
    Publication date: July 10, 2003
    Applicant: Unilever Home & Personal Care USA, Division of Conopco, Inc.
    Inventors: Prasanna Rao Dontula, Alyn James Parry, Catherine Maria Powell, Karen Robinson, Wiebe Schokker, Gilbert Martin Verschelling, Pieter Broer van der Weg
  • Publication number: 20030119694
    Abstract: The invention is a solid chemical concentrate system of at least two cooperative shapes. The first shape is an inwardly curved bar having an inner opening. The second shape is an insert which is capable of interlocking with the bar by insertion into the bar inner opening. The solid chemical concentrate provides chemical systems having active constituents which may be the same, different but compatible or functionally and chemically incompatible combined within one matrix to provide at least one substantially continuous surface. The system may also comprise an aqueous soluble or dispersible polymeric film cover.
    Type: Application
    Filed: August 13, 2002
    Publication date: June 26, 2003
    Applicant: Ecolab Inc.
    Inventors: Elizabeth J. Gladfelter, Tina O. Outlaw, James L. Copeland, Rhonda K. Schulz, Daniel K. Boche, Jeff W. Peterson
  • Publication number: 20030114346
    Abstract: Synthetic detergent formulations are made by spray drying an aqueous dispersion or emulsion of a synthetic detergent and a hydrophobic plasticiser and optionally a filler to pr duce a particulate product. In particular the synthetic detergent includes mild surfactants such a fatty isethionate or sulphosuccinate surfactants. By spray drying the emulsion or dispersion, a particularly uniform product is made which can readily be formed into synthetic detergent bars which may include soap to form combination bar products (combi-bars).
    Type: Application
    Filed: October 8, 2002
    Publication date: June 19, 2003
    Applicant: Imperial Chemical Industries PLC
    Inventor: Paul Clignet
  • Publication number: 20030114347
    Abstract: A particulate laundry detergent composition which comprises, as separate particulate components:
    Type: Application
    Filed: October 17, 2002
    Publication date: June 19, 2003
    Applicant: Unilever Home & Personal Care USA, Division of Conopco, Inc.
    Inventors: Prasanna Rao Dontula, Alyn James Parry, Catherine Maria Powell, Karen Robinson, Wiebe Schokker, Gilbert Martin Verschelling, Pieter Broer van der Weg
  • Publication number: 20030109397
    Abstract: Process for reducing the density of solid detergent ingredients by forming said ingredients into hollow-core particles. The density of ingredients such as sodium citrate, sodium carbonate and/or sodium silicate, when formed into such hollow-core particles, allows them to be stably incorporated into non-aqueous liquid laundry detergents.
    Type: Application
    Filed: July 17, 2002
    Publication date: June 12, 2003
    Applicant: The Procter & Gamble Company
    Inventors: Yousef Georges Aouad, Christopher John Lienhart, Diane Parry
  • Publication number: 20030087791
    Abstract: A coloured speckle composition for use in particulate laundry detergent compositions comprising a porous granular carrier and at least 0.01 wt % photobleach, preferably at least 0.05 wt %, more preferably at least 0.1 wt %, based on the active ingredient, the composition having an average bulk density of at most 600 g/l, preferably at most 500 g/l, most preferably at most 400 g/l. The carrier system reduces the staining tendency of the photobleach. The most preferred carrier is spray dried detergent base powder. The most preferred photobleach is a blend of Zn and Al sulphonated phthalocyanine.
    Type: Application
    Filed: August 19, 2002
    Publication date: May 8, 2003
    Applicant: Unilever Home & Personal Care USA, Division of Conopco, Inc.
    Inventors: Juan Jose Bonelli, Marcio Henrique Perissinotto Bonfa, Rudolf Govert Van Driel, Paulo-Enrique De Gusmao, Mario Jovelino Del Nunzio, Paulo Cesar Puelle Andrade
  • Publication number: 20030060394
    Abstract: A process for producing a water-dispersible non-particulate detergent product includes the step of providing a particulate detergent composition. The process further includes the step of adding a flow aid to the particulate detergent composition in a range of from about 0.1% to about 25% by weight of the particulate detergent composition. The process then includes the step of compacting the particulate detergent composition having the flow aid by applying a pressure in an amount sufficient to form the water-dispersible non-particulate detergent product having a density of at least about 1000 g/l. This process enables the manufacture of a rapidly dispersing non-particulate detergent composition that sinks in water.
    Type: Application
    Filed: October 10, 2002
    Publication date: March 27, 2003
    Inventors: Adrian John Waynforth Angell, Les Charles Zorb
  • Patent number: 6534471
    Abstract: A process for the production of colored detergent particles. The process is characterized in that a slurry comprising at least one powdering agent and at least one dye is spray dried so that a colored powdering agent is formed. The thus formed colored powdering agent is then applied to detergent particles.
    Type: Grant
    Filed: December 4, 2000
    Date of Patent: March 18, 2003
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Christian Block, Antoni Machin, Hans-Friedrich Kruse
  • Patent number: 6528475
    Abstract: A process for making a solid primary alkyl amine salt, and its use in a powdered laundry detergent.
    Type: Grant
    Filed: October 5, 2000
    Date of Patent: March 4, 2003
    Assignee: Cognis Corporation
    Inventors: Stephen F. Gross, Robert J. Valesky, Timothy C. Morris, Robert J. Coakley, George Smith
  • Patent number: 6511956
    Abstract: The present invention relates to a process for forming a cleaning composition containing the steps of providing at least one alkaline material and at least one acid active, and adding the acid active and the alkaline material to a mixer. The acid active is substantially neutralized within the mixer to form a neutralized detergent active. At least one acid-sensitive polymer is added to the neutralized detergent active to form a slurry, and the slurry is formed into a cleaning composition. A cleaning composition as formed by the above process is also described herein.
    Type: Grant
    Filed: June 19, 2001
    Date of Patent: January 28, 2003
    Assignee: The Procter & Gamble Company
    Inventors: Tianli Wen, Manivannan Kandasamy
  • Patent number: 6503878
    Abstract: The present invention relates to pellets comprising one or more active ingredients; and either one or both of: (a) one or more binders incorporated within the body of the pellet; and (b) one or more coating materials on the surface of the pellet; characterized in that either one or both of the binders and the coating materials comprise one or more polymers with a Tg in the range −85 to +35°C., and, optionally, wherein the coating and/or binder materials comprise at least one multi-phase polymer and further wherein at least one of the phases of the multi-phase polymer has a Tg in the range −85 to +35° C.
    Type: Grant
    Filed: September 22, 2000
    Date of Patent: January 7, 2003
    Assignee: Rohm and Haas Company
    Inventors: Curtis Schwartz, Steven Michael Baxter
  • Patent number: 6498133
    Abstract: Particulate bleach activators comprising 15 to 60% by weight of an acetonitrile, 20 to 70% by weight of a silicon-containing carrier material and 20 to 30% by weight of water, which are obtained by applying an aqueous solution, saturated at 10 to 40° C., of an acetonitrile onto the carrier material without subsequent drying, where the amount of saturated aqueous solution is measured such that the given limits for acetonitrile, carrier material and water are observed.
    Type: Grant
    Filed: November 16, 2001
    Date of Patent: December 24, 2002
    Assignee: Clariant GmbH
    Inventors: Georg Borchers, Robert Milbradt, Oliver Mogck, Frank Weinelt
  • Patent number: 6492320
    Abstract: The present invention relates to a multifunctional pellet aid including one or more binders, wherein at least one binder is an acrylic based polymer having a Tg ranging from −20° C. to +95° C., one or more inorganic solids and one or more organic solids; the particle size of the pellet aid ranging from 100 &mgr;m to 3000 &mgr;m. Adding 0.25 to 10% by weight of the multifunctional pellet aid, based on the total weight of the pellet, to a plurality of ingredients and compacting the pellet aid and ingredients to form a pellet, affords a pellet having improved mechanical strength as a solid and rapidly disintegrating upon contact with an aqueous system.
    Type: Grant
    Filed: December 27, 2000
    Date of Patent: December 10, 2002
    Assignee: Rohm and Hass Company
    Inventors: Hailan Guo, Wen H. Chia, Curtis Schwartz
  • Patent number: 6458755
    Abstract: A spray-dried amorphous alkali metal silicate compound which provides multiple-cycle washing performance. The silicate compound has a molar ratio of M2O to SiO2 of 1:1.5 to 1:3.3 wherein M represents an alkali metal. The compound contains 0.5 to less than 30% by weight of anionic surfactant and has an absorption capacity for liquid components which is at least 20% higher than that of the same quantity of the alkali metal silicate compound which is free from anionic surfactant.
    Type: Grant
    Filed: December 11, 2000
    Date of Patent: October 1, 2002
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Kathrin Schnepp-Hentrich, Rene-Andres Artiga Gonzalez, Katrin Burmeister, Hubert Freese, Manfred Greger, Bernd Larson, Volker Bauer, Peter Sandkuehler, Wilfried Raehse
  • Patent number: 6451224
    Abstract: A stable free-flowing solid chelant composition is produced by the process comprising the steps of: a) adjusting the pH of an aqueous solution of the chelant to a value of from about 1.2 to about 3.0 by the addition of an inorganic acid; and b) drying the pH adjusted aqueous chelant product.
    Type: Grant
    Filed: July 11, 2001
    Date of Patent: September 17, 2002
    Assignee: The Dow Chemical Company
    Inventor: David A. Wilson
  • Publication number: 20020115584
    Abstract: According to the present invention there is provided polymer-containing granules for addition to detergent compositions, said granule comprising:
    Type: Application
    Filed: November 5, 2001
    Publication date: August 22, 2002
    Applicant: The Procter & Gamble Company
    Inventors: Steven Rene Martha Ongena, Iwein Jozef Marie Jaak Goderis
  • Patent number: 6432905
    Abstract: The present invention relates to a process for preparing granular detergent products in which a liquid binder component comprising an acid precursor of an anionic surfactant and a hydrotrope is contacted with a solid particulate starting material comprising a neutralizing agent in a low shear mixer and the mixture granulated, the hydrotrope being present at a level of at least 1% by weight of the acid precursor of the anionic surfactant.
    Type: Grant
    Filed: March 23, 2000
    Date of Patent: August 13, 2002
    Assignee: Unilever Home & Personal Care USA division of Conopco, Inc.
    Inventors: Chandrasekaran Gowrishankaran, Winston Anthony Pereira, Rana Sengupta
  • Publication number: 20020086807
    Abstract: The present invention relates to a coated granular sodium percarbonate for detergent and its manufacturing process, and more particularly to a coated granular sodium percarbonate and its manufacturing process, wherein the surface of said sodium percarbonate establishes a multiple coating layer by being internally coated with a specific composition containing alkali metal silicate while externally coated with a specific composition containing alkali metal sulfate on upper part of said internally coated layer thus providing said sodium percarbonate an excellent dissolving rate in water as well as a good storage stability, preventing it from caking during delivery or storage, and being ultimately utilized as an effective detergent bleach containing zeolite as its detergent builder.
    Type: Application
    Filed: January 9, 2002
    Publication date: July 4, 2002
    Applicant: Oriental Chemical Industries Co., Ltd.
    Inventors: Sang Hwa Lee, Yong Il Kim, Sun Ki Shur, Jong Pill Lee
  • Patent number: 6395703
    Abstract: A detergent composition is described which is a solid homogeneous, evenly dispersed composition containing anionic and nonionic surfactants, soil suspending agents, chelating or sequestering agents, and alkaline builders. The detergent compositions will contain either active enzymes, an oxygen releasing bleaching agent or both. The active enzymes can be protease, amylase or lipase enzymes. Said composition can be used for laundry washing or hard surface cleaning. Manufacturing procedures and methods of use are described.
    Type: Grant
    Filed: December 1, 2000
    Date of Patent: May 28, 2002
    Assignee: Sunburst Chemicals, Inc.
    Inventor: William H. Scepanski
  • Patent number: 6395702
    Abstract: A detergent composition is described which is a solid homogeneous, evenly dispersed composition containing anionic and nonionic surfactants, soil suspending agents, chelating or sequestering agents, and alkaline builders. The detergent compositions will contain either active enzymes, an oxygen releasing bleaching agent or both. The active enzymes can be protease, amylase or lipase enzymes. Said composition can be used for laundry washing or hard surface cleaning. Manufacturing procedures and methods of use are described.
    Type: Grant
    Filed: July 16, 2001
    Date of Patent: May 28, 2002
    Assignee: Sunburst Chemicals, Inc.
    Inventor: William H. Scepanski
  • Patent number: 6391846
    Abstract: A particulate zero-phosphate laundry detergent powder, preferably of bulk density 600-900 g/l, contains zeolite MAP and zeolite A in a weight ratio of at least 1:1. The powder may contain at least two different granular components containing organic surfactant and zeolite builder. A first granular component, which is preferably non-spray-dried and has a bulk density of 550-900 g/l, contains zeolite MAP, while a second granular component, which is preferably spray-dried and has a bulk density of 200-450 g/l, contains zeolite A.
    Type: Grant
    Filed: June 8, 2000
    Date of Patent: May 21, 2002
    Assignee: Unilever Home & Personal Care, USA. division of Conopco, Inc.
    Inventors: Daniel Pierre Marie Berthod, Christophe Michel Bruno Joyeux, Johannes Hendrikus Langeveld
  • Patent number: 6387869
    Abstract: A granular surfactant composition comprising sodium silicate and linear alkylbenzenesulfonates, wherein the granular surfactant composition has a mean particle diameter of ≧50 &mgr;m and an ffc value of ≧7; a process for the preparation of this granular surfactant composition, its use, and detergents and cleaners which comprise such granular surfactant composition and a process for the making of the same; and, where appropriate, the granular surfactant composition comprises other active ingredients and auxiliaries.
    Type: Grant
    Filed: March 30, 2001
    Date of Patent: May 14, 2002
    Assignee: Clariant GmbH
    Inventors: Harald Bauer, Josef Holz, Gunther Schimmel
  • Patent number: 6376453
    Abstract: To provide detergent particles having high-speed dissolution capable of dissolving quickly in water after supplying the detergent particles in water, and a method for preparing the detergent particles, and a detergent composition comprising the detergent particles. Detergent particles having an average particle size of from 150 to 500 &mgr;m and a bulk density of 500 g/liter or more, wherein the detergent particles comprising a detergent particle being capable of releasing a bubble from an inner portion of the detergent particles in a process of dissolving the detergent particle in water, the bubble having a size of one-tenth or more of a particle size of the detergent particle, and wherein the detergent particles have a dissolution rate as calculated by Equation (1) of 90% or more, under conditions where the detergent particles are supplied in water at 5° C.
    Type: Grant
    Filed: July 22, 1999
    Date of Patent: April 23, 2002
    Assignee: Kao Corporation
    Inventors: Teruo Kubota, Hitoshi Takaya, Shu Yamaguchi, Hiroyuki Yamashita, Shuji Takana
  • Publication number: 20020002130
    Abstract: A spray-dried amorphous alkali metal silicate compound which provides multiple-cycle washing performance. The silicate compound has a molar ratio of M2O to SiO2 of 1:1.5 to 1:3.3 wherein M represents an alkali metal. The compound contains 0.5 to less than 30% by weight of anionic surfactant and has an absorption capacity for liquid components which is at least 20% higher than that of the same quantity of the alkali metal silicate compound which is free from anionic surfactant.
    Type: Application
    Filed: December 11, 2000
    Publication date: January 3, 2002
    Applicant: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Kathrin Schnepp-Hentrich, Rene-Andres Artiga Gonzalez, Katrin Burmeister, Hubert Freese, Manfred Greger, Bernd Larson, Volker Bauer, Peter Sandkuehler, Wilfried Raehse
  • Patent number: 6329334
    Abstract: The invention relates to the use of crosslinked polyvinylpyrrolidone as an additive to compact, particulate detergents and cleansers for the purpose of increasing the rate of disintegration thereof when brought into contact with water, to the particles of crosslinked polyvinylpyrrolidone having a particle size of from 50 to 400 &mgr;m, to a process for the preparation of the compact, particulate detergents and cleansers, and also to the compact, particulate detergents and cleansers themselves.
    Type: Grant
    Filed: March 14, 2000
    Date of Patent: December 11, 2001
    Assignee: BASF Aktiengesellschaft
    Inventors: Werner Bertleff, Folker Ruchatz, Richard Baur, Robert Heinz, Peter Palm
  • Publication number: 20010034317
    Abstract: A water-containing solid detergent having a delayed, controllable and variable hardening time after addition of all the components produced by providing
    Type: Application
    Filed: March 24, 1999
    Publication date: October 25, 2001
    Inventors: DIETER HEMM, GUENTER HELLMANN
  • Patent number: 6303558
    Abstract: A particulate detergent composition or component of high bulk density (at least 600 g/l), comprising at least 10% by weight of detergent surfactant and from 10 to 70% by weight of detergency builder, is composed of at least two, and preferably at least three, different granular components: (i) granules comprising at least 60% by weight of anionic surfactant, (ii) granules comprising at least 20% by weight of nonionic surfactant, and less than 10% by weight of aluminosilicate. (iii)optionally, granules comprising detergency builder.
    Type: Grant
    Filed: May 26, 1998
    Date of Patent: October 16, 2001
    Assignee: Lever Brothers Co., division of Conopco
    Inventors: William Derek Emery, Pauline Farnworth, Georgina Hawkes, Terry Instone, Seeng Djiang Liem, John Lloyd, Gilbert Martin Verschelling
  • Patent number: 6294512
    Abstract: Detergent compositions contain sticky particles with at least 45% by weight of a sticky surfactant and non-sticky particles with less than about 1% by weight of sticky surfactant. The particles are further characterized by their size ranges and bulk densities. Compositions containing potassium ions are described. Dissolution of the compositions in aqueous media is optimized.
    Type: Grant
    Filed: June 30, 2000
    Date of Patent: September 25, 2001
    Assignee: The Procter & Gamble Company
    Inventors: Paul R Mort, III, Kevin Todd Norwood
  • Publication number: 20010009897
    Abstract: The invention relates to a granular alkali metal phyllosilicate compound which comprises a crystalline alkali metal phyllosilicate, a colorant and an additive. The invention also relates to a process for its preparation, and to detergents and cleaners which comprise such a granular alkali metal phyllosilicate compound.
    Type: Application
    Filed: December 15, 2000
    Publication date: July 26, 2001
    Applicant: Clariant GmbH
    Inventors: Harald Bauer, Josef Holz, Gunther Schimmel
  • Patent number: 6232284
    Abstract: The present invention relates to tablets comprising a core and a coating, the core being formed by compressing a particulate material, the particulate material comprising surfactant and detergent builder, and the coating comprising a material, or mixture of materials, such as a fatty alcohol, which is substantially insoluble in water at 25° C. The tablets are provided with means, such as effervescent agents, which aid in their disintegration in wash liquors.
    Type: Grant
    Filed: June 4, 1999
    Date of Patent: May 15, 2001
    Assignee: The Procter & Gamble Company
    Inventors: Paul Irma Albertus Van Dijk, Jose Luis Vega
  • Patent number: 6200949
    Abstract: Described is a process for forming controllably releasable fragrance-containing consumable articles, for example, encapsulated fragrances in detergents or fabric softener articles and compositions. The process includes the steps of: (a) forming an aqueous fragrance emulsion, including a modified starch; (b) spray drying or freeze drying the emulsion to form a fragrance-containing powder; and (c) mixing a solid consumable article base (e.g., detergent or fabric softener base) with the fragrance-containing powder. Also described are products produced by means of such processes as well as uses thereof.
    Type: Grant
    Filed: December 21, 1999
    Date of Patent: March 13, 2001
    Assignee: International Flavors and Fragrances Inc.
    Inventors: Henricus Gerardus Maria Reijmer, Adi Shefer
  • Patent number: 6194367
    Abstract: The present invention discloses an alkaline cleaning composition for cleaning heavily soiled metal surfaces such as food fryers, baking pans, high temperature pasteurizers, and beer kettles, ceramic surfaces such as restaurant grade ceramic china plates and platters, and plastic surfaces. The cleaning composition is noncaustic and includes a peroxygen compound, a chelate, and a metasilicate and/or sesquisilicate. A preferred cleaning composition further includes a surfactant and hydrated builder.
    Type: Grant
    Filed: April 27, 1999
    Date of Patent: February 27, 2001
    Assignee: Charvid Limited Liability Co.
    Inventor: Charles Bullick Talley
  • Patent number: 6191096
    Abstract: A spray-dried amorphous alkali metal silicate compound which provides multiple-cycle washing performance. The silicate compound has a molar ratio of M2O to SiO2 of 1:1.5 to 1:3.3 wherein M represents an alkali metal. The compound contains 0.5 to less than 30% by weight of anionic surfactant and has an absorption capacity for liquid components which is at least 20% higher than that of the same quantity of the alkali metal silicate compound which is free from anionic surfactant.
    Type: Grant
    Filed: August 18, 1997
    Date of Patent: February 20, 2001
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Kathrin Schnepp-Hentrich, Rene-Andres Artiga Gonzalez, Katrin Burmeister, Hubert Freese, Manfred Greger, Bernd Larson, Volker Bauer, Peter Sandkuehler, Wilfried Raehse
  • Patent number: 6165972
    Abstract: A solid surfactant mixture, comprising one or more fatty acid polyhydroxyamides of the formula IRCONR.sup.1 Z (1)in which R is C.sub.7 -C.sub.31 -alkyl or C.sub.7 -C.sub.31 -alkenyl, Z is a polyhydroxyhydrocarbon group having at least two hydroxyl groups, which may also be alkoxylated, and R.sup.1 is C.sub.1 -C.sub.8 -alkyl or a group of the formula --(CH.sub.2).sub.x NR.sup.2 R.sup.3 or R.sup.4 O(CH.sub.2).sub.n --, R.sup.2 and R.sup.3 are C.sub.1 -C.sub.4 -alkyl or C.sub.2 -C.sub.4 -hydroxyalkyl, R.sup.4 is C.sub.1 -C.sub.4 -alkyl and x is a number from 1 to 10 and n is a number from 2 to 4, one or more other nonionic surfactants and/or one or more anionic surfactants.
    Type: Grant
    Filed: September 2, 1999
    Date of Patent: December 26, 2000
    Assignee: Clariant GmbH
    Inventors: Frank Weinelt, Helmut Keck
  • Patent number: 6162781
    Abstract: Foam control granules, for use in particulate laundry detergent compositions, comprise a mobile hydrophobic foam control agent, preferably silicone oil in admixture with hydrophobic silica, optionally combined with a mixture of a hydrocarbon such as petroleum jelly and an alkylphosphoric acid salt, sorbed onto a porous absorbent inorganic carrier comprising or consisting of anhydrous sodium carbonate, preferably light soda ash. When such granules are prepared by mixing and granulating in a high shear mixer/granulator, the addition of from 1 to 10 wt % water after mixing and granulation results in granules having improved flow properties.
    Type: Grant
    Filed: August 12, 1999
    Date of Patent: December 19, 2000
    Assignee: Lever Brothers Company, div. of Conopco Inc.
    Inventors: Marinela Buscan, Francois Delwel, Angela Di-Pietro
  • Patent number: 6162780
    Abstract: A carbonate-based detergent having improved properties is provided. Preferably, a base detergent includes an alkali metal carbonate builder, an anionic surfactant, an inert diluent, a copolymer, and a chlorine scavenger. The base detergent is mixed with an agglomerate including nonionic surfactants and a builder such as an alkali metal carbonate. The detergent has improved color retention properties. A method of preparing the improved detergent composition is also provided.
    Type: Grant
    Filed: August 9, 1999
    Date of Patent: December 19, 2000
    Assignee: The Dial Corporation
    Inventors: Terrell L. Partee, Charles Varker, Elaine T. Morse, Ronald D. Morgan
  • Patent number: 6159920
    Abstract: A detergent composition comprises detergent particles, each particle having a substantially anhydrous coating comprising a fluorescent whitening agent and a nonionic surfactant. A process for the preparation of the said detergent composition comprises spraying base detergent particles with a substantially anhydrous mixture comprising the fluorescent whitening agent and the nonionic surfactant.
    Type: Grant
    Filed: November 9, 1999
    Date of Patent: December 12, 2000
    Assignee: The Proctor & Gamble Company
    Inventor: Mark William Ridyard
  • Patent number: 6153574
    Abstract: The speed of disintegration of tablets containing a water-softening agent, especially water-insoluble, water-softening agent intended as detergency builder for fabric washing is enhanced by incorporating spray-dried partially hydrated sodium acetate alone or jointly with sodium citrate dihydrate and/or crystallized sodium acetate trihydrate.
    Type: Grant
    Filed: October 7, 1999
    Date of Patent: November 28, 2000
    Assignee: Unilever Home & Personal Care USA division of Conopco, Inc.
    Inventor: Roger Joseph Anna Janssen
  • Patent number: 6147046
    Abstract: A method and apparatus is disclosed for producing a fragrance-containing solid particle, capable of controllably releasing the fragrance to the environment in which the particle is contained, for incorporation into laundry detergents, fabric softener compositions and drier-added fabric softener articles.
    Type: Grant
    Filed: December 30, 1999
    Date of Patent: November 14, 2000
    Assignee: International Flavors & Fragrances Inc.
    Inventors: Adi Shefer, Shmuel David Shefer, Maureen S. Santoro
  • Patent number: 6142398
    Abstract: A method and apparatus is disclosed for producing a fragrance-containing solid particle, capable of controllably releasing the fragrance to the environment in which the particle is contained, for incorporation into laundry detergents, fabric softener compositions and drier-added fabric softener articles.
    Type: Grant
    Filed: December 30, 1999
    Date of Patent: November 7, 2000
    Assignee: International Flavors & Fragrances Inc.
    Inventors: Adi Shefer, Shmuel David Shefer, Maureen S. Santoro
  • Patent number: 6140292
    Abstract: Detergent compositions and fabric laundering and treating methods utilize certain polyamide-polyamines as fabric treatment agents that can impart fabric appearance benefits to fabric laundered or treated in washing or soaking solutions which contain such agents. Such polyamide-polyamine fabric treatment agents include adipic acid-diethylenetriamine-epichlorohydrin adducts.
    Type: Grant
    Filed: June 30, 1999
    Date of Patent: October 31, 2000
    Assignee: The Procter & Gamble Company
    Inventors: Sherri Lynn Randall, Rajan Keshav Panandiker
  • Patent number: 6133216
    Abstract: The invention relates to coated bleach activator granules of ammonium nitriles, which have been obtained by coating ammonium nitrile base granules with a water-soluble coating substance. The base granules are preferably thermally conditioned during or after the coating with the coating substance.
    Type: Grant
    Filed: September 15, 1998
    Date of Patent: October 17, 2000
    Assignee: Clariant GmbH
    Inventors: Matthias Loffler, Gerd Reinhardt
  • Patent number: 6069124
    Abstract: A detergent composition having a bulk density of at least 550 kg/m.sup.3 comprises a mixture of:(a) a granulate, preferably a mechanically mixed granulate, of bulk density 450 kg/m.sup.3 to 1300 kg/m.sup.3, comprising surfactant and inorganic material, and(b) a spray-dried adjunct comprising inorganic material, preferably sodium sesquicarbonate or Burkeite,component (a) being present in an amount of from 35% to 85% by weight of the total granular product.The adjunct allows the bulk density of the final composition to be adjusted to any chosen value without detriment to other properties, thus providing flexibility to formulate at a range of bulk densities.
    Type: Grant
    Filed: May 26, 1998
    Date of Patent: May 30, 2000
    Assignee: Lever Brothers Company Division of Conopco, Inc.
    Inventors: Peter Willem Appel, Marcel van der Kraan