Silicon Containing Treating Agent (e.g., Sodium Silicate, Etc.) Patents (Class 554/196)
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Patent number: 10968414Abstract: A method for refining vegetable oil is used to reduce formation of soaps. An acid-treated vegetable oil mixture is passed through a low shear mixing device prior to being fed to a static hydrodynamic reactor. The static hydrodynamic reactor induces a neutralization reaction that forms soaps in a pressurized vegetable oil mixture. The reacted mixture is discharged from the reactor to a downstream system for separating the formed soaps from the reacted mixture to form a refined vegetable oil having reduced soaps content.Type: GrantFiled: January 13, 2020Date of Patent: April 6, 2021Assignee: ARISDYNE SYSTEMS, INC.Inventors: Oleg Kozyuk, Peter Reimers
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Patent number: 10640729Abstract: A method for refining vegetable oil is used to reduce formation of soaps. An acid-treated vegetable oil mixture is passed through a low shear mixing device prior to being fed to an static hydrodynamic reactor. The static hydrodynamic reactor induces a neutralization reaction that forms soaps in a pressurized vegetable oil mixture. The reacted mixture is discharged from the reactor to a downstream system for separating the formed soaps from the reacted mixture to form a refined vegetable oil having reduced soaps content.Type: GrantFiled: February 28, 2019Date of Patent: May 5, 2020Inventors: Oleg Kozyuk, Peter Reimers
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Patent number: 8680305Abstract: A method of obtaining a polyunsaturated fatty acid derivative comprises contacting a mixture of fatty acid derivatives with a silver salt aqueous solution, and adjusting the free fatty acid content in the silver salt aqueous solution to 0.2 meq or less per gram of silver when repeatedly using the silver salt aqueous solution. A polyunsaturated fatty acid derivative having high purity and excellent quality can thus be economically obtained.Type: GrantFiled: September 2, 2009Date of Patent: March 25, 2014Assignees: Q.P. Corporation, Bizen Chemical Co., Ltd.Inventors: Hiroyuki Sakaguchi, Hideaki Kobayashi, Yoshihisa Misawa, Keisuke Uryu, Yoshio Shimizu
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Patent number: 8642824Abstract: Various methods are provided for metathesizing a feedstock. In one aspect, a method includes providing a feedstock comprising a natural oil, chemically treating the feedstock under conditions sufficient to diminish catalyst poisons in the feedstock, and, following the treating, combining a metathesis catalyst with the feedstock under conditions sufficient to metathesize the feedstock.Type: GrantFiled: August 11, 2008Date of Patent: February 4, 2014Assignee: Elevance Renewable Sciences, Inc.Inventors: Daniel W. Lemke, Kevin D. Uptain, Francis Amore, Tim Abraham
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Patent number: 8063235Abstract: Method for improving the performance of a preparative batchwise Super Critical Fluid Chromatographic separation for the recovery of a target fatty acid or derivative thereof, or of a group of target fatty acids or of derivatives thereof from a mixture, characterized in that the said Super Critical Fluid Chromatographic separation employs a chromatographic column charged with a stationary phase chosen from the group consisting of aluminium oxide or aluminium oxides, titanium oxide or titanium oxides, silica gel or silica gels, amino propyl modified silica gels, diol modified silica gels, phenyl modified silica gels and “reversed phase” phases, the former in turn chosen from the group consisting of RP18, RP8 and RP3, and in that the said Super Critical Fluid Chromatographic Separation further employs a mobile phase chosen from the group consisting of ethylene, propane, ammonia, dinitrogen dioxide and CO2, wherein in the said method, during the run of the said mixture on the chromatographic column, a pressure anType: GrantFiled: June 19, 2007Date of Patent: November 22, 2011Assignee: K.D. Pharma Bexbach GmbHInventors: Rudolf Krumbholz, Peter Lembke, Norbert Schirra
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Publication number: 20110207953Abstract: Methods for producing refined rice bran oil that include caustic treatment step(s) in an amount that is less than or equal to a theoretical amount of caustic required to neutralize practically all of the free fatty acids in the rice bran oil, but avoiding addition of excess caustic. An objective is to retain a high level of oryzanol in the refined oil.Type: ApplicationFiled: February 22, 2010Publication date: August 25, 2011Applicant: Riceland Foods, INC.Inventors: Larry D. Corley, Nahid Rutherford, Gary E. Nelms, Don R. McCaskill
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Patent number: 7034086Abstract: This invention relates to a crosslinking composition comprising a compound having the structure of Formula I: where Z is a hydrogen, an alkyl of 1 to about 18 carbon atoms, an aryl of about 6 to about 24 carbon atoms, an aralkyl of about 7 to about 24 carbon atoms, or —NR2R2; each R2 is independently hydrogen, an alkyl, aryl or an aralkyl of 1 to about 18 carbon atoms or R3; where R3 is —CHROR1 or where R is alkyl, halogenated alkyl, aryl, aralkyl, halogenated aralkyl, alkoxyalkyl or an alkaryl having from 1 to about 24 carbon atoms; R1 is a hydrogen, alkyl, aryl, aralkyl, alkoxyalkyl or an alkaryl having from 1 to about 24 carbon atoms; and where the alkyl or aryl groups in each radical may optionally have heteroatoms in their structure; B is a residue of a poly(alkylaldehyde) with n aldehyde groups; n is an integer of 2 to about 4; and A is an amino moiety derived from the group consisting of guanamine and melamine.Type: GrantFiled: March 31, 2003Date of Patent: April 25, 2006Assignee: Cytec Technology Corp.Inventors: Lon-Tang Wilson Lin, William Jacobs, III, Dimitri Verhage, Kuang-Jong Wu
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Patent number: 6248911Abstract: A process and composition for removing trace contaminants from glyceride oils utilizes a metal-substituted silica xerogel having a pH of at least 7.5 to adsorb at least a portion of the contaminants. The process of the invention includes contacting a glyceride oil with such an adsorbent and then separating the adsorbent from the contaminant-depleted glyceride oil, for example, by filtration. The composition of the present invention includes a metal-substituted silica xerogel having a pH of at least 7.5 and an organic acid blended with the xerogel. Preferably, the organic acid is citric acid. Contaminants which can be removed from glyceride oils during the refinement of such oils by the adsorbent include phospholipids, soaps, detrimental metals, and chlorophyll.Type: GrantFiled: August 14, 1998Date of Patent: June 19, 2001Assignee: PQ CorporationInventors: Carlos E. Canessa, Adam J. Brozzetti
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Patent number: 5840945Abstract: A method of refining and manufacturing a fat and oil containing polyunsaturated fatty acids which prevents production of peculiar fishy smells when such a fat and oil is added to food materials and while it is stored by preventing oxidation of PUFA's and restraining conversion of odor-emanating precursors into odor-emanating substances. A fat and oil, such as a marine animal oil, containing polyunsaturated fatty acids with 18 or more carbon atoms and three or more double bonds such as EPA and DHA is alkali refined and bleached. The thus alkali refined and bleached fat and oil is refined by bringing 100 parts by weight of it into contact for 10 minutes or more at 5.degree.-80.degree. C. with not less than 0.1 part by weight of powdered or granulated diatomaceous earth formed by calcining with a flux added such as sodium carbonate or sodium chloride. The fat and oil thus obtained is filtered and deodorized by steam distillation under vacuum.Type: GrantFiled: October 31, 1996Date of Patent: November 24, 1998Assignee: Ueda Oils and Fats Mfg. Co., Ltd.Inventors: Yoshikazu Tsujiwaki, Hiroshi Yamamoto, Kazuko Hirata, Satoru Kamigasa
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Patent number: 5434281Abstract: Process for the stereospecific synthesis of leukotriene B.sub.4 (LTB.sub.4) of 6Z, 8E, 10E configuration of formula ##STR1## in which a dibenzoate triether is prepared which is subjected to a reductive elimination according to the diagram ##STR2## so as to obtain a triether which is converted in order to obtain the leukotriene B.sub.4.Type: GrantFiled: May 31, 1994Date of Patent: July 18, 1995Assignee: L'OrealInventors: Guy Solladie, Guy Stone, Antonio Urbano-Pujol, Jean Maignan
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Patent number: 5391385Abstract: The treatment of cooking oil with a combination of alumina and amorphous silica is disclosed. This combination, preferably with a silica hydrogel and a hydrated alumina, reduces all contaminants known to degrade the oil without introducing metals or increasing undesirable soaps.Type: GrantFiled: July 13, 1993Date of Patent: February 21, 1995Assignee: The PQ CorporationInventor: Jed C. Seybold
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Patent number: 5264597Abstract: The invention relates to a process for refining glyceride oil comprising the steps of contacting the oil with amorphous silica, wherein said silica is selected from the group of precipitated amorphous silicas having a surface area of at least 400 m.sup.2 /g in pores with a diameter from at least 2 nm. Preferably said precipitated amorphous silicas have a pore volume in the range of about 1.3 to 2.5 ml/g, in pores having a pore diameter in the range of 3.6 to 1000 nm.Type: GrantFiled: June 15, 1992Date of Patent: November 23, 1993Assignee: Van den Bergh Foods, Co., Division of Conopco, Inc.Inventors: Josef P. Van Dalen, Jannes G. Lammers, Derek Aldcroft
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Patent number: 5252762Abstract: Adsorbents are provided which are suitable for use in the removal of contaminants selected from the group consisting of free fatty acids, soaps, phosphorus, metal ions and color bodies. The adsorbents comprise inorganic porous supports selected from the group consisting of substantially amorphous alumina, diatomaceous earth, clays, magnesium silicates, aluminum silicates and amorphous silica, treated with a base in such a manner that at least a portion of said base is retained in at least some of the pores of the support to yield base-treated inorganic porous adsorbents. Processes for removing free fatty acids, etc., from glyceride oils using these adsorbents are also provided.Type: GrantFiled: April 3, 1991Date of Patent: October 12, 1993Assignee: W. R. Grace & Co.-Conn.Inventor: Dean A. Denton