Abstract: An apparatus and method for monitoring and/or controlling cryogenic cooling by measuring the opacity of the vapor cloud (113) generated from a cryogenic cooling device (112). The opacity is determined by measuring the reduction in intensity of a light beam (127) passed through the vapor cloud (113). The opacity measurements are used to control an operating parameter of the system, such as the cooling rate of the cryogenic cooling device (112). The opacity measurements may be normalized to compensate for variables, other than temperature of the workpiece (119) and cooling rate, which may affect the opacity of the vapor cloud (113).

Abstract: A liquid gas vaporization and measurement system, and associated method, for efficiently vaporizing a continuous sample of liquid gas, such as liquid natural gas (LNG), and accurately determining the constituent components of the gas. A constant flow of liquid gas sampled from a mass storage device is maintained in a vaporizing device. Within the vaporizing device the liquid gas is flash vaporized within heated narrow tubing. The liquid gas is converted to vapor very quickly as it enters one or more independently operating vaporizer stages within the vaporizing device. The vapor gas is provided to a measuring instrument such as a chromatograph and the individual constituent components and the BTU value of the gas are determined to an accuracy of within +/?0.5 mole percent and 1 BTU, respectively.

Abstract: A device for monitoring blockage of a turret in a cryomagnet, at least one monitoring unit that functionally interacts with a state of the inside of the turret of a cryomagnet is provided to monitor the inside of the turret.

Abstract: A temperature alert device to warn of imminent devitrification due to warming of a biological specimen that uses shape memory materials. The temperature induced phase transformation of shape memory materials causes a temperature responsive actuator to extend an alert rod upon warming as the specimen temperature approaches the devitrification temperature (e.g. ?130° C.). The temperature alert device is automatically reset upon immersion in liquid nitrogen.

Abstract: Method for protecting a cryogenic tank, the tank comprising two concentric casings between them delimiting an inter-wall space in which a so-called low pressure obtains, the method involving: a step of detecting an impact on the tank and/or an increase in pressure within the inter-wall space, characterized in that it involves a step of generating a stream of inert gas within the inter-wall space only if an impact on the tank of a determined intensity and/or a determined increase in pressure at the inter-wall space is/are detected.

Abstract: A tank and method for containing a cryogenic liquid in which a purge gas is introduced into an insulation space defined between an outer vessel and an inner vessel to contain insulation material. The inner vessel is used to contain the cryogenic liquid. The purge gas can be cryogenic vapor evolved from the liquid and routed into the insulation space. Control of the purge gas within the insulation space can be provided by a programmable logic controller in which purge gas is vented from the insulation space should the pressure be indicative of a leak within the inner vessel and purge gas is introduced into the insulation space should the pressure be below the ambient to maintain a positive purge gas pressure. An adsorbent bed can also be located within the insulation space to adsorb any moisture.

Abstract: To provide a liquefied gas supply device and supply method that has good operability and a compact structure, and enables stable supply of large flow rates of liquefied gas while managing the consumption amount of liquefied gas promptly in real time. A liquefied gas supply device characterized by having container 1 filled with liquefied gas, load cell 2 for measuring the weight of container 1, halogen lamp unit 3 for heating container 1, and a gas transfer means to transfer gas in the gas-phase section of container1, and arranging halogen lamp unit 3, comprising halogen lamp heater 3a and space 3b for the lamp, and load cell 2 in an integrated structure at bottom section 1a of container 1.

Abstract: In a helium 3 refrigerator-utilizing magnetic property measurement system which enables magnetization measurement to be effected till 0.3 K by utilizing the formerly proposed magnetic property measurement system (MPMS), a main pipe 23, for the object of enabling magnetization measurement to be infallibly effected even when the upper limit of magnetic field the MPMS can induce is applied, includes an upper supporting tube 41 positioned in the uppermost part and allowing a bellows 28 to be connected to the lateral part thereof, a condensing tube 42 supported first in the lower part of the upper supporting tube, an outer tube 44 fixed in the lower part of the condensing tube and adapted to form an outer wall of an insulated vacuum chamber 43 formed between the outer tube and a lower inner tube 45 forming an inner wall of the insulated vacuum chamber 43. In each of the tubes, the lower inner tube 45 is formed of titanium.

Abstract: Apparatus and methods for improving the safety and efficiency and decreasing the cost of producing liquid gas, such as liquid oxygen, with a small-scale use liquefaction device, according to various embodiments of the present invention. In one embodiment, liquid oxygen barrier may be added to interface between a cryocooler and a dewar to control rate of liquid oxygen escape upon a tipping of the dewar. A boiloff vessel in fluid communication with the dewar allows expanding gas from a tipped dewar to escape while allowing the liquid to safely settle in the boiloff vessel. A temperature sensing circuit, in proximity with a heat dissipator or cold finger of the cryocooler, is operable to break an electrical power circuit of the cryocooler or cooling fan when a sensed temperature exceeds a predetermined temperature. Oxygen purity of a feed stream of gas may be sensed and/or displayed.

Abstract: A system for sampling cryogenic liquids, and an air separation unit provided with at least one such system. The cryogenic liquid is introduced into a vaporizer, through heat exchange with the compressed air. The liquid passes through the vaporizer generally downwards. The walls of the vaporizer that are intended to come into contact with the cryogenic liquid are maintained at a temperature above the sublimation temperature or the boiling point of the least volatile impurity contained in this liquid. Downstream of the vaporizer, a gaseous phase coming from the vaporization of the cryogenic liquid is withdrawn and at least some of the gaseous phase is sent to an analyzer.

Abstract: A cryogenic fluid distribution device may include a fluid flow passage for distributing cryogenic fluid to an apparatus, an overflow passage positioned downstream of the apparatus, and a sensor coupled to the overflow passage, the sensor having an active component for determining if fluid is present in the overflow passage.

Abstract: This invention provides for an apparatus and a method for operation of a cryogenic hydrogen storage system that contains a porous medium configured to adsorb hydrogen. The hydrogen storage and supply system includes a hydrogen source apparatus and a cryosorptive storage apparatus. Methods and devices that allow for an energy efficient filling of the cryosorptive apparatus from the hydrogen source apparatus are described. The cryosorptive hydrogen storage apparatus is filled with cold, pressurized hydrogen. During the course of filling, heat is generated in the cryosorptive storage device by the process of hydrogen adsorption on to the host medium. Methods and devices are provided for the removal the generated heat and the warm hydrogen. Further provided are devices and methods for the capture and recycle of escaped hydrogen within the hydrogen source apparatus.

Abstract: A dual purpose recirculation valve system for a cryogenic vessel includes a fill line, a delivery line assembly, a recirculation line and a recirculation valve. The cryogenic vessel defines a storage space and includes a pressure monitoring device structured to monitor the pressure in the storage space, as well as an electronic control system structured to receive input from the pressure monitoring device. The fill line is structured to be coupled to a bulk tank, whereby the storage space is filled with a cryogenic fluid. The delivery line assembly has a delivery coupling assembly and the delivery line assembly structured to remove the cryogenic fluid from the storage space and deliver the cryogenic fluid to the delivery coupling assembly. The recirculation line extends between, and is in fluid communication with both, the fill line and the delivery line assembly.

Abstract: The invention relates to a method for storing liquefied zeotropic gas mixtures. To ensure a composition of the liquid phase which meets specifications, the change of the gas phase is determined by means of a differential pressure transducer by comparing the pressure with a calibration mixture. The mixture composition of the liquid phase is regulated by subsequently metering in the mixture components which have the higher partial pressure.

Abstract: This invention provides for an apparatus and a method for operation of a cryogenic hydrogen storage system that contains a porous medium configured to adsorb hydrogen. The hydrogen storage and supply system includes a hydrogen source apparatus and a cryosorptive storage apparatus. Methods and devices that allow for an energy efficient filling of the cryosorptive apparatus from the hydrogen source apparatus are described. The cryosorptive hydrogen storage apparatus is filled with cold, pressurized hydrogen. During the course of filling, heat is generated in the cryosorptive storage device by the process of hydrogen adsorption on to the host medium. Methods and devices are provided for the removal the generated heat and the warm hydrogen. Further provided are devices and methods for the capture and recycle of escaped hydrogen within the hydrogen source apparatus.

Abstract: In a method for the disposal of the boil-off gas in a cryotank, an energy-converting unit is temporarily operated even in phases of non-use in order to burn the boil-off gas. Preferably the start-up and/or the duration of the operation of the energy-converting unit is controlled by an electronic monitor module according to the pressure level in the cryotank. A preferred case of operation is represented by a motor vehicle with a cryotank for supplying a vehicle driving unit or a fuel cell for the generation of electrical energy, wherein the drive unit or the fuel cell of the shut-down, unused motor vehicle is automatically started up temporarily automatically in order to burn boil-off gas.

Abstract: The invention relates to a method for storing liquefied zeotropic gas mixtures. To ensure a composition of the liquid phase which meets specifications, the change of the gas phase is determined by means of a differential pressure transducer by comparing the pressure with a calibration mixture. The mixture composition of the liquid phase is regulated by subsequently metering in the mixture components which have the higher partial pressure.

Abstract: This invention provides for an apparatus and a method for operation of a cryogenic hydrogen storage system that contains a porous medium configured to adsorb hydrogen. The hydrogen storage and supply system includes a hydrogen source apparatus and a cryosorptive storage apparatus. Methods and devices that allow for an energy efficient filling of the cryosorptive apparatus from the hydrogen source apparatus are described. The cryosorptive hydrogen storage apparatus is filled with cold, pressurized hydrogen. During the course of filling, heat is generated in the cryosorptive storage device by the process of hydrogen adsorption on to the host medium. Methods and devices are provided for the removal the generated heat and the warm hydrogen. Further provided are devices and methods for the capture and recycle of escaped hydrogen within the hydrogen source apparatus.

Abstract: A fluid delivery system, for e.g. a vehicle, includes a tank for holding fluid product, such as propane, a pump for pumping the fluid product from the tank, the pump being driven by hydraulic fluid, and a heat exchanger for using the fluid product to cool the hydraulic fluid. The heat exchanger also causes the fluid product to increase in temperature. The heated fluid product is returned to the tank, in the form of a vapor, for example. Embodiments of the invention provide a number of advantages, including increased pump flow rates, reduced cavitation, increased pump life, and elimination of a heat-exchanger fan.

Abstract: In order to avoid evaporation of the propellant gas during the pressure-free filling of an aerosol formulation provided with a readily volatile propellant gas, the product to be filled is cooled prior to being fed into a metering means. In this context, fluoro-chlorinated hydrocarbons such as, for instance, R11 have been used up until now as the coolant, but their use is no longer permitted in Germany and in other nations.

Abstract: A delivery system for transferring a delivery fluid from a delivery tank to a customer tank while maintaining a predetermined vessel pressure in the delivery tank, including a pump assembly pumping fluid from the delivery tank and a piping system passing the pumped fluid to the customer tank. A diverter diverts a slip stream portion of the pumped delivery fluid and a heat exchanger assembly selectively heats or cools the slip stream portion for return to the delivery tank. A sensor monitors a selected condition in the delivery tank and a controller responds to the sensor to control the amount and thermal condition of the slip stream returned to the delivery tank.

Abstract: A method is provided for delivering gaseous hydrogen to end users, the hydrogen being delivered in reusable storage tanks containing a plurality of carbon nanotubes. Liquid hydrogen is introduced into the tank, and the nanotubes absorb the hydrogen. The tanks are then warmed to normal temperatures and distributed to end users. The tanks are connected to the end-user system and are preferably installed within an air-tight enclosure, which may have an inert atmosphere. Alternatively, an inerting system monitors the air within the enclosure for free hydrogen and can release an inerting gas if free hydrogen is detected. The hydrogen is selectively released by heating the storage tank or by injecting a catalyst into the tank. When the usable hydrogen is depleted, the tank is retrieved from the end user for refurbishment and refilling.

Abstract: A system stores densely dissolved methane-base gas and supplies gas of a predetermined composition. A container (10) stores methane-base gas dissolved in hydrocarbon solvent and supplies it to means for adjusting composition, through which an object of regulated contents is obtained. Preferably, the means for adjusting composition is means for maintaining the tank in a supercritical state, or piping (48) for extracting substances at a predetermined ratio from the gas phase (12) and liquid phase (16) in the container.

Abstract: The methods and apparatus for transporting compressed gas includes a gas storage system having a plurality of pipes connected by a manifold whereby the gas storage system is designed to operate in the range of the optimum compressibility factor for a given composition of gas. The pipe for the gas storage system is preferably large diameter pipe made of a high strength material whereby a low temperature is selected which can be withstood by the material of the pipe. Knowing the compressibility factor of the gas, the temperature, and the diameter of the pipe, the wall thickness of the pipe may be calculated for the pressure range of the gas at the selected temperature. The gas storage system may either be modular or be part of the structure of a vessel for transporting the gas to the storage system. Since the pipe provides a bulkhead around the gas, the gas storage system may be used in a single hull vessel. The gas storage system further includes enclosing the pipes in a nitrogen atmosphere.

Abstract: A method and a system for supplying pressurized gas from a liquefied-gas (LG) storage tank, the method including the steps of: (a) providing a system including: (i) a storage tank for storing liquefied gas, the tank having a lower liquid region and a vapor region thereover; (ii) a heat exchanger external to the storage tank; (iii) pumping means driven by a liquid; (iv) a line for directly transferring the vaporized gas from the heat exchanger to the consumer; (b) pumping at least a portion of the liquefied gas from the lower region to the heat exchanger using the pumping means; (c) heating the liquefied gas in the heat exchanger to produce the vaporized gas; and (d) supplying the vaporized gas directly to the consumer, according to consumer demand.

Abstract: A system, method, and computer program products and associated apparatus, to monitor and determine the polarization level of a quantity of hyperpolarized gas during transport. A portable device is configured to transmit an excitation pulse and analyze a response signal in transit to provide a polarization level corresponding to the hyperpolarized gas. Preferably, the monitoring system can provide magnetic field fluctuation feedback to the transport unit and adjust operating current to a solenoid. The system also can compensate for NMR frequency shifts that may appear in the measured response signal to provide a more accurate polarization level or “real” T1 for the hyperpolarized gas.

Abstract: This invention is directed to a method for delivering a liquefied compressed gas with a high rate of flow comprising passing a liquefied compressed high-purity semiconductor gas into a storage vessel; positioning a temperature measuring means onto the wall of the compressed gas storage vessel; positioning at least one heating means proximate to the storage vessel; monitoring the resulting temperature with the temperature measuring means; positioning a pressure measuring means at the outlet of the storage vessel and monitoring the vessel pressure; adjusting the heat output of the heating means to heat the liquefied compressed gas in the storage vessel to control the evaporation of the liquefied compressed gas in the storage vessel; and controlling the flow of the gas from the storage vessel.

Abstract: Methods of dispensing meted quantities of hyperpolarized gas to form a hyperpolarized gas mixture include pre-filling a gas syringe with a quantity of non-polarized gas, then introducing the hyperpolarized gas therein while the non-polarized gas is held therein, and expelling both the hyperpolarized gas and non-polarized gas from the syringe. Methods of inhibiting the presence of oxygen in gas flow paths and extraction systems are also described.

Abstract: A method of supplying vaporized gas from a storage tank storing the gas in liquified form in a lower liquid region and having a vapor region thereover, the method including employing an external source of heat to heat a heat exchange liquid to no more than about 35° C., bringing the heat exchange liquid into heat exchange relation with at least a portion of the liquified gas so as to transfer heat from the external source of heat to the liquified gas, and supplying vaporized gas to the consumer, according to the consumer demand, directly from the vapor region of the storage tank. The heat exchange relation is controlled such that the at least portion of the liquified gas which is heated remains mostly in a liquified state but that the temperature of the liquified gas is prevented from falling below a predefined minimum operational temperature.

Abstract: An apparatus and method for disinfecting a microtome and cryostat is provided. The cryostat comprises a chamber, a pump communicating with the chamber, an ozone generator and an ozone destroyer. A microtome is located in the chamber. Oxygen molecules in ambient air are converted to ozone that is injected into the cryostat chamber, disinfecting the chamber and the microtome. After disinfection, the air and ozone present in the chamber is directed to an ozone destroying unit that eliminates any remaining ozone. This eliminates the risk of ozone exposure to nearby operators and minimizes damage to the cryostat and microtome from extended ozone contact.

Abstract: A compact portable transport unit for shipping hyperpolarized noble gases and shielding same from electromagnetic interference and/or external magnetic fields includes a means for shifting the resonance frequency of the hyperpolarized gas outside the bandwidth of typical frequencies associated with prevalent time-dependent fields produced by electrical sources. Preferably the transport unit includes a magnetic holding field which is generated from a solenoid in the transport unit. The solenoid includes a plurality of coil segments and is sized and configured to receive the gas chamber of a container. The gas container is configured with a valve, a spherical body, and an extending capillary stem between the valve and the body. The gas container or hyperpolarized product container can also be formed as a resilient bag.

Abstract: A delivery system for transferring a delivery fluid from a delivery tank to a customer tank while maintaining a predetermined vessel pressure in the delivery tank, including a pump assembly pumping fluid from the delivery tank and a piping system passing the pumped fluid to the customer tank. A diverter diverts a slip stream portion of the pumped delivery fluid and a heat exchanger assembly selectively heats or cools the slip stream portion for return to the delivery tank. A sensor monitors a selected condition in the delivery tank and a controller responds to the sensor to control the amount and thermal condition of the slip stream returned to the delivery tank.

Abstract: Methods of dispensing meted quantities of hyperpolarized gas to form a hyperpolarized gas mixture include pre-filling a gas syringe with a quantity of non-polarized gas, then introducing the hyperpolarized gas therein while the non-polarized gas is held therein, and expelling both the hyperpolarized gas and non-polarized gas from the syringe. Methods of inhibiting the presence of oxygen in gas flow paths and extraction systems are also described.

Abstract: A fluid storage and dispensing system including a fluid storage and dispensing vessel enclosing an interior volume for holding a fluid. The vessel includes a fluid discharge port for discharging fluid from the vessel. A pressure regulating element in the interior volume of the fluid storage and dispensing vessel is arranged to flow fluid therethrough to the fluid discharge port at a set pressure for dispensing thereof. A controller external of the fluid storage and dispensing vessel is arranged to transmit a control input into the vessel to cause the pressure regulating element to change the set pressure of the fluid flowed from the pressure regulating element to the fluid discharge port. By such arrangement, the respective storage and dispensing operations can have differing regulator set point pressures, as for example a subatmospheric pressure set point for storage and a super atmospheric pressure set point for dispensing.

Abstract: Methods of extracting and removing hyperpolarized gas from a container include introducing an extraction fluid into the container to force the hyperpolarized gas out of an exit port. The hyperpolarized gas is forced out of the container separate and apart from the extraction fluid. Alternatively, if the fluid is a gas, a portion of the gas is mixed with the hyperpolarized gas to form a sterile mixed fluid product suitable for introduction to a patient. An additional method includes engaging a gas transfer source such as a syringe to a transport container and pulling a quantity of the hyperpolarized gas out of the container in a controlled manner. Alternatively, one or more gas syringes can be employed to mete out predictable quantities of hyperpolarized gas or gas mixtures including quantities of buffer gases.

Abstract: A dry ice dispenser apparatus for dispensing a metered volume of dry ice into a receiving well. The apparatus includes a dry ice source, such as a hopper, or a dry ice producing apparatus for supplying dry ice to a metering carriage. The metering carriage delivers a metered volume of dry ice to a receiving well. The metering carriage is contained in a carriage slide assembly which includes a pair of guide walls, a closed floor portion connection to a bottom portion of the guide walls and a discharge opening located above the receiving well. The apparatus may contain a pellet press for forming dry ice pellets when the dry ice is delivered to the receiving well.