Operating Under Inert Or Reducing Conditions Patents (Class 65/32.1)
  • Patent number: 11890698
    Abstract: The present application provides a double-beam laser polishing device and a double-beam laser polishing method for an aluminum alloy, which includes a frame; a rotary workbench and an optical path system, which are arranged on the frame. The optical path system includes: a first fiber laser, a second fiber laser, a first three-dimensional galvanometer, and a second three-dimensional galvanometer. The first three-dimensional galvanometer is connected with the first fiber laser through an optical fiber, and the second three-dimensional galvanometer is connected with the second fiber laser through an optical fiber. The first three-dimensional galvanometer and the second three-dimensional galvanometer are arranged side by side above the rotary workbench in a horizontal direction.
    Type: Grant
    Filed: August 26, 2021
    Date of Patent: February 6, 2024
    Assignee: SHENZHEN INSTITUTE OF INFORMATION TECHNOLOGY
    Inventors: Haibing Xiao, Yunsheng Zhang, Mingjun Liu, Yongquan Zhou, Xinzhong Wang
  • Patent number: 11660841
    Abstract: Described herein are organosilicon modification layers and associated deposition methods and inert gas treatments that may be applied on a sheet, a carrier, or both, to control van der Waals, hydrogen and covalent bonding between a sheet and carrier. The modification layers bond the sheet and carrier together such that a permanent bond is prevented at high temperature processing as well as maintaining a sufficient bond to prevent delamination during high temperature processing.
    Type: Grant
    Filed: September 7, 2021
    Date of Patent: May 30, 2023
    Assignee: Corning Incorporated
    Inventors: Kaveh Adib, Robert Alan Bellman
  • Patent number: 11459814
    Abstract: A vacuum insulated glass product and the method for making the same, wherein the vacuum insulated glass comprises: a first glass substrate; a second glass substrate disposed facing the first glass substrate; a sealing structure provided between the first glass substrate and the second glass substrate and used for airtight binding of the first glass substrate and the second glass substrate to form a vacuum cavity; and a plurality of supports provided inside the vacuum cavity for bearing pressure from the first glass substrate and the second glass substrate. The sealing structure comprises: metal layers which are fixedly formed on facing surfaces of the first glass substrate and the second glass substrate, and an intermediate solder layer which is disposed between and connects the metal layers. The sealing structure has arc-shaped transition structures at the corner areas of the glass substrates.
    Type: Grant
    Filed: November 10, 2017
    Date of Patent: October 4, 2022
    Assignee: Luoyang Landglass Technology Co., Ltd.
    Inventors: Yanbing Li, Zhangsheng Wang
  • Patent number: 10071931
    Abstract: Optical glass that has an Abbe number (Vd) of less than 23 and is suitable for use as a single-lens material constituting a photographic-imaging lens; an optical element including the optical glass; and an imaging lens containing a lens including the optical glass. Optical glass that has an Abbe number (Vd) of less than 23, wherein a flat plate of said optical glass with a thickness of 10 mm exhibits an ISO color contribution index (ISO/CCI) of 0 for blue (B), up to 9 for green (G), and up to 9 for red (R).
    Type: Grant
    Filed: December 2, 2014
    Date of Patent: September 11, 2018
    Assignee: HOYA CORPORATION
    Inventor: Shuhei Mikami
  • Patent number: 9834465
    Abstract: An optical glass may be a phosphate based glass containing at least any one of oxides selected from TiO2, Nb2O5, WO3, and Bi2O2. The total content (HR) of the TiO2, Nb2O5, WO3, and Bi2O2 may be 35 mol % or above, the noble metal content may be less than 2.0 ppm, and the ?OH value, given by the following general formula, may be 0.1 mm-1 or above: ?OH=?[ln(B/A)]/t.
    Type: Grant
    Filed: September 26, 2014
    Date of Patent: December 5, 2017
    Assignee: HOYA CORPORATION
    Inventor: Shuhei Mikami
  • Publication number: 20150135772
    Abstract: An apparatus and method are provided for sintering a hollow cylindrical body of porous synthetic silica. The apparatus comprises a hollow mandrel for supporting the body in a horizontal position, and the mandrel is housed within a vacuum furnace having heating elements arranged to surround the body circumferentially along its entire length. The method includes supporting the body on a hollow horizontally-oriented mandrel in a vacuum furnace in which heating elements are disposed surrounding the body, and heating the body by means of the elements to a sintering temperature.
    Type: Application
    Filed: November 11, 2014
    Publication date: May 21, 2015
    Inventors: Alan Mundy, Ian George Sayce, Richard Benjamin Coapes
  • Publication number: 20150111040
    Abstract: A method capable of forming a sufficiently thick low alkali concentration region without heating glass to a high temperature and even in an atmosphere which is not an atmosphere of plasma formation gas such as helium and argon, is provided. A glass substrate having a pair of main surfaces and being made of glass containing an alkali oxide in its composition, is disposed between a first electrode and a second electrode so that one main surface is separated from the first electrode and the other main surface is brought into contact with the second electrode, and a corona discharge is generated by applying a direct-current voltage to the first electrode as a positive electrode and the second electrode as a negative electrode, in a positive-electrode-side surface layer portion of the glass substrate, at least one positive ion including an alkali ion migrate toward the negative-electrode-side.
    Type: Application
    Filed: December 22, 2014
    Publication date: April 23, 2015
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Shiro FUNATSU, Akio KOIKE, Kiyoshi YAMAMOTO, Yuichi YAMAMOTO, Hiroshi WAKATSUKI, Junji NISHII, Kenji HARADA, Hiroshi IKEDA, Daisuke SAKAI
  • Patent number: 9010152
    Abstract: Ion transport membranes are integrated with a glass melting furnace and a float glass bath. Only feeds of air, steam and hydrocarbon are necessary for producing hot oxygen for the melting furnace and a mixture of nitrogen, carbon dioxide, and hydrogen for the float glass bath.
    Type: Grant
    Filed: December 31, 2012
    Date of Patent: April 21, 2015
    Assignee: L'Air Liquide, Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges Claude
    Inventors: Wei Huang, Youssef Joumani, Remi Pierre Tsiava, Bhadra S. Grover
  • Publication number: 20150104376
    Abstract: A method of annealing at least one sapphire lamina is disclosed. The method comprises at least two different heating steps and produces an annealed sapphire lamina having improved optical properties that can be used for fabricating a cover plate of an electronic device. The cover plate and electronic device comprising the annealed sapphire lamina are also disclosed.
    Type: Application
    Filed: September 18, 2014
    Publication date: April 16, 2015
    Inventors: Scott J. Turchetti, Daniela M. Fredrick
  • Publication number: 20150040612
    Abstract: A method of making a shaped glass article includes placing a glass sheet on top of a mold. A heat exchanger is arranged relative to the mold such that a heat exchange surface of the heat exchanger is in opposing relation to a back surface of the mold and separated from the back surface of the mold by a gap containing a layer of gas. The height of the gap is selected such that the dominant heat transfer between the heat exchange surface and the back surface of the mold is by conduction through the layer of gas. The glass sheet is heated and formed into a shaped glass article with the mold. The heat exchanger is operated to remove heat from at least part of the mold during at least one of heating the glass sheet, forming the shaped glass article, and cooling the shaped glass article.
    Type: Application
    Filed: July 30, 2014
    Publication date: February 12, 2015
    Inventors: Bushra Afzal, Keith Raymond Gaylo, Elias Panides, Kevin Lee Wasson
  • Publication number: 20150038314
    Abstract: Boron-containing network sulfide glass which may be useful in IR transmitting applications, such as IR optics, laser or fiber amplifiers doped with rare earths with emission in the near IR, and methods of making the same.
    Type: Application
    Filed: June 29, 2012
    Publication date: February 5, 2015
    Inventors: Bruce Gardiner Aitken, Stephen Charles Currie, Randall Eugene Youngman
  • Patent number: 8925349
    Abstract: A rare earth ion doped silicate luminescence glass and preparation method thereof are provided. The luminescence glass is the material with the following formula: aM2O.bM?2O3.cSiO2.dRE2O3, wherein M is at least one of Na, K and Li, M? is at least one of Y, Gd, La, Sc and Lu, RE is at least one of Ce, Tm, Tb, Ho, Dy, Er, Nd, Sm, Eu and Pr. The preparation method is: grinding the raw material until mixed uniformly, calcining the raw material at 1200-1500° C. for 1-5 h, cooling to room temperature, annealing at 600-1100° C. for 0.5-24 h, cooling to room temperature again, molding then getting the product. The performance of the product is stable. The product is homogenous, and the luminescence performance is good. The light transmittance is high. The process of the preparation method is simple and with low cost.
    Type: Grant
    Filed: May 19, 2009
    Date of Patent: January 6, 2015
    Assignee: Ocean's King Lighting Science & Technology Co., Ltd.
    Inventors: Mingjie Zhou, Wenbo Ma, Zhaopu Shi, Yanbo Qiao, Qingtao Li
  • Publication number: 20140373571
    Abstract: A fused silica glass article having greater resistance to damage induced by exposure to laser radiation such as laser induced wavefront distortion at deep ultraviolet (DUV) wavelengths, and behaviors such as fluence dependent transmission, which are related to intrinsic defects in the glass. The improved resistance to laser damage may be achieved in some embodiments by loading the glass article with molecular hydrogen (H2) at temperatures of about 400° C. or less, or 350° C. or less. The combined OH and deuteroxyl (OD) concentration may be less than 10 ppm by weight. In other embodiments, the improved resistance may be achieved by providing the glass with 10 to 60 ppm deuteroxyl (OD) species by weight. In still other embodiments, improved resistance to such laser damage may be achieved by both loading the glass article with molecular hydrogen at temperatures of about 350° C. or less and providing the glass with less than 10 ppm combined OH and OD, or 10 to 60 ppm OD by weight.
    Type: Application
    Filed: May 5, 2014
    Publication date: December 25, 2014
    Applicant: Corning Incorporated
    Inventors: Kenneth Edward Hrdina, Changyi Lai, Lisa Anne Moore, Ulrich Wilhelm Heinz Neukirch, William Rogers Rosch
  • Publication number: 20140318183
    Abstract: An apparatus for manufacturing a glass optical element includes: a heating unit that heats a glass material; a pressurizing unit that pressurizes the glass material; a cooling unit that cools the glass material; a molding room in which the heating unit, the pressurizing unit, and the cooling unit are located; an inert-gas supplying unit that forms a plurality of flows of an inert gas within the molding room by blowing the inert gas in a plurality of directions crossing each other; and an inert-gas emitting unit that emits, from within the molding room, the inert gas supplied into the molding room by the inert-gas supplying unit.
    Type: Application
    Filed: July 3, 2014
    Publication date: October 30, 2014
    Inventors: Kiyomi Yamada, Takashi Watanabe, Masato Nakahama
  • Patent number: 8771530
    Abstract: A method for producing a polarizing element includes: forming particulate materials of a metal halide on a glass substrate; forming a protective film that covers the particulate materials in a non-plasma environment; stretching the particulate materials by heating and stretching the glass substrate; and forming acicular metal particles by reducing the metal halide constituting the stretched particulate materials.
    Type: Grant
    Filed: February 22, 2013
    Date of Patent: July 8, 2014
    Assignee: Seiko Epson Corporation
    Inventor: Yoshitomo Kumai
  • Publication number: 20140165654
    Abstract: Surface modification layers and associated heat treatments, that may be provided on a sheet, a carrier, or both, to control both room-temperature van der Waals (and/or hydrogen) bonding and high temperature covalent bonding between the thin sheet and carrier. The room-temperature bonding is controlled so as to be sufficient to hold the thin sheet and carrier together during vacuum processing, wet processing, and/or ultrasonic cleaning processing, for example. And at the same time, the high temperature covalent bonding is controlled so as to prevent a permanent bond between the thin sheet and carrier during high temperature processing, as well as maintain a sufficient bond to prevent delamination during high temperature processing.
    Type: Application
    Filed: October 7, 2013
    Publication date: June 19, 2014
    Applicant: Corning Incorporated
    Inventors: Robert Alan Bellman, Dana Craig Bookbinder, Robert George Manley, Prantik Mazumder
  • Patent number: 8640500
    Abstract: Corrosion of the inner surface of the crown of a glassmelting furnace is reduced or avoided by directing at low velocity along that surface a gaseous stream comprising water vapor, or comprising the combustion products of an oxy-fuel burner operated at a stoichiometric ratio of at least 1.0, or the combustion products of a burner operated at a stoichiometric ratio less than 1.0, or by injecting into the furnace interior a gaseous reactant which reacts with alkali species in said space.
    Type: Grant
    Filed: April 14, 2011
    Date of Patent: February 4, 2014
    Assignee: Praxair Technology, Inc.
    Inventors: Kuang-Tsai Wu, Hisashi Kobayashi
  • Patent number: 8635886
    Abstract: It is an object of the present invention to provide a copper-containing silica glass which emits fluorescence having a peak in a wavelength range of from 520 nm to 580 nm under irradiation of ultraviolet light with a wavelength of 400 nm or less, and which is excellent in long term stability even in the high output use. The copper-containing silica glass is made to have copper of from 5 wtppm to 200 wtppm, which emits fluorescence having a peak in a wavelength range of from 520 nm to 580 nm under irradiation of ultraviolet light with a wavelength ranging from 160 nm to 400 nm, and in which an internal transmittance per 2.5 mm thickness at a wavelength of 530 nm is 95% or more.
    Type: Grant
    Filed: July 26, 2012
    Date of Patent: January 28, 2014
    Assignees: Shin-Etsu Quartz Products Co., Ltd., Opto-Electronics Laboratory, Inc.
    Inventors: Tetsuji Ueda, Michinari Ohuchi, Hiroyuki Nishimura, Akira Fujinoki, Masahiro Nakatsuka, Hidetsugu Yoshida
  • Publication number: 20140013803
    Abstract: A device for making a window includes a main body defining a first space and a second space, a first shaft provided in the first space and connected to the main body, a first die provided in the first space and connected to the first shaft, a second shaft connected to the main body, movable relative to the first shaft and extending to the first space from the second space, and a second die provided in the first space and connected to the second shaft.. The device further includes an air-tight chamber surrounding the first and second dies, a gas supply conduit and a gas discharge conduit connected to the chamber, and an actuator connected to the second shaft and configured to move the second shaft relative to the first shaft. At least one of the first and second dies has a flat area and a curved area.
    Type: Application
    Filed: January 29, 2013
    Publication date: January 16, 2014
    Applicant: SAMSUNG DISPLAY CO., LTD.
    Inventors: Seong-Jin Hwang, Kwan-Young Han, Dong-Ho Lee, Hyoung-Suk Roh, Mikiya Itakura
  • Patent number: 8592333
    Abstract: A green light-emitting glass and the method of preparing the same are provided. The components with parts by mole of the green light-emitting glass are alkali oxide 25-40, Y2O3 0.01-15, SiO2 40-70, Tb2O3 0.01-15. The method of preparing the glass includes mixing alkali salt with Y2O3, SiO2 and Tb4O7, firing the mixture at 1200° C.-1500° C. for 1-5 hours, cooling the precursor to the room temperature and annealing the precursor in a reducing atmosphere at 600° C.-1200° C. for 1-20 hours. A green light-emitting glass with good transparence, high uniformity, easily being made into big bulk and high stability is provided. The process of capsulation of parts by using the glass is simple. And a method of preparing the glass with simple process and low cost is provided.
    Type: Grant
    Filed: March 25, 2009
    Date of Patent: November 26, 2013
    Assignee: Ocean's King Lighting Science & Technology Co., Ltd.
    Inventors: Mingjie Zhou, Wenbo Ma, Zhaopu Shi, Yanbo Qiao, Qingtao Li
  • Patent number: 8567215
    Abstract: A method for producing a polarizing element includes the steps of: forming an island-shaped film of a metal halide on a glass substrate; forming needle-shaped particles of the metal halide by stretching the glass substrate through heating to elongate the island-shaped film; and forming needle-shaped metal particles composed of a metal by reducing the metal halide of the needle-shaped particles, wherein the metal halide is deposited on the glass substrate by a reactive physical vapor deposition method.
    Type: Grant
    Filed: March 16, 2012
    Date of Patent: October 29, 2013
    Assignee: Seiko Epson Corporation
    Inventor: Yoshitomo Kumai
  • Patent number: 8549880
    Abstract: A method for producing a polarizing element includes the steps of: forming a coating film of a metal on a glass substrate; forming an island-shaped film composed of a metal halide on the glass substrate by partially removing the coating film and also halogenating the metal; forming needle-shaped particles of the metal halide by stretching the glass substrate through heating to elongate the island-shaped film; and forming needle-shaped metal particles composed of a metal by reducing the metal halide of the needle-shaped particles.
    Type: Grant
    Filed: March 15, 2012
    Date of Patent: October 8, 2013
    Assignee: Seiko Epson Corporation
    Inventor: Yoshitomo Kumai
  • Publication number: 20130112919
    Abstract: A white light emitting glass-ceramic. The chemical formula of the glass-ceramic is aSiO2.bAl2O3.cNaF.dCeF3.nDyF3.mAg, wherein a, b, c, d, n and m are, by mol part, 25-50, 15-30, 10-30, 10-25, 0.01-1 and 0.01-1, respectively, and a+b+c+d-100. A method for producing said glass-ceramic is also provided. Silver ion is doped in the glass-ceramic in the form of silver particles by means of sintering and reduction annealing treatment, and thus the luminescence properties of rare earth ion is improved.
    Type: Application
    Filed: July 22, 2010
    Publication date: May 9, 2013
    Inventors: Mingjie Zhou, Wenbo Ma, Fangyi Weng
  • Patent number: 8375747
    Abstract: A sealing apparatus for use in conveying molten glass from a first vessel to a second vessel, wherein at least a portion of the first vessel is nested within the second vessel without contact between the first and second vessels, and a flexible member comprising a gas-tight seal separates an atmosphere enclosed by the sealing apparatus and an ambient atmosphere. The sealing apparatus is useful for flexibly sealing a non-contact joint between conduits for supplying molten glass to a forming body.
    Type: Grant
    Filed: July 3, 2012
    Date of Patent: February 19, 2013
    Assignee: Corning Incorporated
    Inventors: Gilbert De Angelis, Ronald L. Kimball
  • Patent number: 8356493
    Abstract: New and improved compositions of doped fluorophosphate glasses for lasers have a high refractive index (nD) of approximately 1.6 to 1.7, high transmission in the near infrared part of the spectrum and a wide glass forming domain. These glass systems, Ba(PO3)2—Al(PO3)3—BaF2-Dopants, utilize dopants from the group of oxides or fluorides of the rare earth elements Sm, Eu, Nd, Er, Yb, Tm, Tb, Ho and Pr as well as MnO; and mixtures thereof. The composition of glass includes chemical durability, efficiency of laser use in the infrared spectrum and improved duration of luminescence.
    Type: Grant
    Filed: April 11, 2011
    Date of Patent: January 22, 2013
    Inventor: Alfred A. Margaryan
  • Patent number: 8336332
    Abstract: Provided are a process for the production of a precision press-molded article having a high transmittance a method of treating a glass to color or decolor the glass, the process comprising heat-treating a press-molded article containing at least one selected from WO3, Nb2O5 or TiO2 in an oxidizing atmosphere to produce a glass molded article, and the method comprising heat-treating a colored glass containing at least one oxide of WO3 and Nb2O5 in an oxidizing atmosphere to decolor the glass, or heat-treating a glass containing at least one oxide selected from WO3, Nb2O5 or TiO2 in a non-oxidizing atmosphere to color the glass.
    Type: Grant
    Filed: March 1, 2012
    Date of Patent: December 25, 2012
    Assignee: Hoya Corporation
    Inventors: Kazutaka Hayashi, Hiromasa Tawarayama, Xuelu Zou, Hiroshi Kawazoe
  • Patent number: 8333089
    Abstract: New and improved compositions of doped fluorophosphate glasses for lasers have a high refractive index (nD) of approximately 1.6 to 1.7, high transmission in the near infrared part of the spectrum and a wide glass forming domain. These glass systems, Ba(PO3)2—Al(PO3)3—BaF2-Dopants, utilize dopants from the group of oxides or fluorides of the rare earth elements Sm, Eu, Nd, Er, Yb, Tm, Tb, Ho and Pr as well as MnO; and mixtures thereof. The composition of glass includes chemical durability, efficiency of laser use in the infrared spectrum and improved duration of luminescence.
    Type: Grant
    Filed: April 11, 2011
    Date of Patent: December 18, 2012
    Inventor: Alfred A. Margaryan
  • Patent number: 8324124
    Abstract: A process for producing a glass substrate, which includes forming molten glass obtained by melting raw materials into a glass ribbon in a float bath, annealing the glass ribbon by a cooling apparatus, and cutting the glass ribbon to form the glass substrate, where the hydrogen concentration in the atmosphere of a float bath exceeds 3%, and the glass retention time in the float bath is from 4 to 15 minutes.
    Type: Grant
    Filed: June 20, 2011
    Date of Patent: December 4, 2012
    Assignee: Asahi Glass Company, Limited
    Inventors: Kensuke Nagai, Yuichi Kuroki, Kei Maeda
  • Patent number: 8181483
    Abstract: Discloses are processes for preparing conductive glass-ceramics employ segregation or ion exchange.
    Type: Grant
    Filed: June 1, 2007
    Date of Patent: May 22, 2012
    Assignee: Schott AG
    Inventors: Mark Davis, Paula Vullo
  • Publication number: 20120010067
    Abstract: A green light-emitting glass and the method of preparing the same are provided. The components with parts by mole of the green light-emitting glass are alkali oxide 25-40, Y2O3 0.01-15, SiO2 40-70, Tb2O3 0.01-15. The method of preparing the glass includes mixing alkali salt with Y2O3, SiO2 and Tb4O7, firing the mixture at 1200° C-1500° C. for 1-5 hours, cooling the precursor to the room temperature and annealing the precursor in a reducing atmosphere at 600° C-1200° C. for 1-20 hours. A green light-emitting glass with good transparence, high uniformity, easily being made into big bulk and high stability is provided. The process of capsulation of parts by using the glass is simple. And a method of preparing the glass with simple process and low cost is provided.
    Type: Application
    Filed: March 25, 2009
    Publication date: January 12, 2012
    Inventors: Mingjie Zhou, Wenbo Ma, Zhaopu Shi, Yanbo Qia, Qingtao Li
  • Publication number: 20120000247
    Abstract: A method for processing a coated glass substrate may include a high-temperature activation process.
    Type: Application
    Filed: June 28, 2011
    Publication date: January 5, 2012
    Inventors: Daniel Burgard, Joshua Conley, James Hinkle, Stephen Murphy, Thomas Truman
  • Publication number: 20110303290
    Abstract: The present disclosure provides a method and apparatus for manufacturing a silicon substrate using inert gas blowing during continuous casting to provide excellent productivity and surface quality. The apparatus includes a raw silicon feeder through which raw silicon is fed, a silicon melting unit disposed under the raw silicon feeder and melting the raw silicon to form molten silicon, a molten silicon storage unit storing the molten silicon supplied from the silicon melting unit and tapping the molten silicon to provide a silicon melt having a constant thickness, a transfer unit transferring the silicon melt tapped from the molten silicon storage unit, and a cooling unit cooling the silicon melt transferred by the transfer unit. Here, the cooling unit cools the silicon melt by blowing inert gas at a rate of 0.1˜2.5 Nm3/h.
    Type: Application
    Filed: June 13, 2011
    Publication date: December 15, 2011
    Applicant: KOREA INSTITUTE OF ENERGY RESEARCH
    Inventors: Bo-Yun JANG, Jin-Seok LEE, Young-Soo AHN
  • Patent number: 8071494
    Abstract: The present invention provides a glass substrate for flat panel display in which yellowing occurring in a case of forming silver electrodes on glass substrate surface is inhibited. A glass substrate for flat panel display, which is formed by a float method, which has a composition consisting essentially of, in terms of oxide amount in mass %: SiO2 50 to 72%, Al2O3 0.15 to 15%, MgO + CaO + SrO + BaO 4 to 30%, Na2O more than 0% and at most 10%, K2O 1 to 21%, Li2O 0 to 1%, Na2O + K2O + Li2O 6 to 25%, ZrO2 0 to 10%, and Fe2O3 0.0725 to 0.15%; and wherein the average Fe2+ content in a surface layer of the glass substrate within a depth of 10 ?m from the a top surface is at most 0.0725% in terms of Fe2O3 amount.
    Type: Grant
    Filed: May 8, 2009
    Date of Patent: December 6, 2011
    Assignee: Asahi Glass Company, Limited
    Inventors: Kensuke Nagai, Tetsuya Nakashima, Kei Maeda, Ryoji Akiyama, Akira Kondo, Daiki Akie
  • Patent number: 8012894
    Abstract: A fused silica glass and a fused silica article having a combined concentration of at least one of OH and OD of up to about 50 ppm. The fused silica glass is formed by drying a fused silica soot blank or preform in an inert atmosphere containing a drying agent, followed by removal of residual drying agent from the dried soot blank by heating the dried soot blank in an atmosphere comprising an inert gas and of oxygen.
    Type: Grant
    Filed: May 5, 2008
    Date of Patent: September 6, 2011
    Assignee: Corning Incorporated
    Inventors: Dana Craig Bookbinder, Richard Michael Fiacco, Kenneth Edward Hrdina, Rostislav Radievich Khrapko
  • Publication number: 20110181953
    Abstract: A polarizing element includes fine metal particles formed in numerous regions that were occupied by respective substantially needle-like metal halide fine particles before reduction that are oriented and dispersed in a glass substrate such that the lengthwise directions thereof are almost the same, the fine metal particles being produced by heat-treating the glass substrate in a reducing atmosphere to reduce the substantially needle-like metal halide fine particles. The number of fine metal particles present in at least some of the numerous regions is two or more in each region, 90% or more of the regions each have a volume of 2,500 to 2,500,000 nm3, and the individual volumes of the fine metal particles present in each region are 4 to 40% of the volume of the region in 90% or more of the total number of the regions.
    Type: Application
    Filed: January 31, 2011
    Publication date: July 28, 2011
    Applicant: HOYA CANDEO OPTRONICS CORPORATION
    Inventors: Yoshitaka YONEDA, Michiyori Miura, Toshiaki Sonehara
  • Patent number: 7841211
    Abstract: First of all, there is provided a production process of a synthetic quartz glass which has less impurity, has a high-temperature viscosity characteristic equal to or more than that of a natural quartz glass, and hardly deforms even in a high-temperature environment, and especially a production process of a highly heat resistant synthetic quartz glass which is free from the generation of bubbles and is dense. Secondly, there is provided a highly heat resistant synthetic quartz glass body which is easily obtained by the production process of the present invention, and especially a transparent or black quartz glass body which is free from the generation of bubbles, is dense, has high infrared absorption rate and emission rate, and has an extremely high effect for preventing diffusion of alkali metal. The process is a process of producing a highly heat resistant quartz glass body having an absorption coefficient at 245 nm of 0.
    Type: Grant
    Filed: November 28, 2003
    Date of Patent: November 30, 2010
    Assignee: Shin-Etsu Quartz Products Co., Ltd.
    Inventors: Tatsuhiro Sato, Takahiro Kaitou, Akira Fujinoki, Toshiyuki Kato, Tohru Segawa, Nobumasa Yoshida
  • Publication number: 20100281919
    Abstract: The present invention is directed to a device and method for shaping optical components with improved uniformity and higher throughput. A curved oven provides a plurality of sequential chambers arranged in a curved path, with walls separating the chambers. The walls of the chambers may have openings shaped to match the profile of shaping molds and pedestals which are transported through the oven. An optional dual temperature control system may provide for the separate temperature regulation of upper and lower regions of the chambers. Optical components, such as for solar energy sytems, are manufactured by conveying material and molds on a transport system through the curved oven and shaping them by controlled heat and vacuum assisted slumping. The chambers may be grouped into regions, with the materials undergoing different processes as they traverse each region.
    Type: Application
    Filed: May 6, 2009
    Publication date: November 11, 2010
    Applicant: SOLFOCUS, INC.
    Inventors: Darrel Bailey, Gary Kackley
  • Publication number: 20100251772
    Abstract: The present invention is to provide a molten glass producing apparatus realizing simultaneously the production of a glass article of high quality and save-energy in producing molten glass, a molten glass producing method employing the molten glass producing apparatus and a method for producing a glass article. In the molten glass producing apparatus having a vacuum degassing apparatus, the melting tank is provided with a separating means for separating the area for circulating the molten glass in the melting tank into an upstream circulation flow and a downstream circulation flow, the distance from the separating means to the downstream end of the molten glass flow path in the melting tank is from 0.1 LE to 0.
    Type: Application
    Filed: June 22, 2010
    Publication date: October 7, 2010
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Hajime Itoh, Hironobu Yamamichi, Toru Nishikawa, Kazuo Ninomiya, Hiroaki Hamamoto
  • Patent number: 7790078
    Abstract: A process for producing a transparent or opaque silica glass product including mixing a silica fine powder and a cellulose derivative and injection molding the mixture, followed by degreasing treatment and baking treatment, which is characterized in that the cellulose derivative is a cellulose derivative which causes reversible thermal gelation in an aqueous solution of at least one member selected from methyl cellulose, hydroxypropylmethyl cellulose and hydroxyethylmethyl cellulose; in producing a transparent silica glass product, the cellulose derivative is added in water heated at a gelation temperature thereof or higher, and after cooling, the formed aqueous solution is kneaded with the silica fine powder; and in producing an opaque silica glass product, the cellulose derivative is added in a silica slurry containing a silica powder and heated at a gelation temperature of the cellulose derivative or higher.
    Type: Grant
    Filed: February 9, 2006
    Date of Patent: September 7, 2010
    Assignees: Shin-Etsu Quartz Products Co., Ltd., Shin-Etsu Chemical Co., Ltd.
    Inventors: Hiroyuki Watanabe, Akira Fujinoki, Takayuki Imaizumi, Kazuhisa Hayakawa, Shingo Niinobe
  • Publication number: 20100126219
    Abstract: This invention pertains to a process of bonding a magnesium aluminate spinel article or articles and a germanate glass article or articles including the step of heating them together above the softening temperature of the glass.
    Type: Application
    Filed: January 14, 2010
    Publication date: May 27, 2010
    Applicant: The Government of the USA, as represented by the Secretary of the Navy
    Inventors: Shyam S. Bayya, Jasbinder S. Sanghera, Guillermo Villalobos, Geoffrey Chin, Ishwar D. Aggarwal
  • Patent number: 7682537
    Abstract: A mold-press forming apparatus for applying a molding pressure to a mold containing a forming material to perform press forming includes a loading chamber (that is, an airtight chamber) P1 kept airtight. The loading chamber P1 is connected to a pressure reducing member which includes evacuating members 14 and 13 arranged in an evacuating path 7 connected to the loading chamber P1 for evacuating a gas in the loading chamber P1, and a plurality of valves 11 and 12 arranged in the evacuating path 7 in parallel to each other. When the loading chamber P1 is evacuated, the pressure reducing member changes a pressure reducing rate in the course of pressure reduction.
    Type: Grant
    Filed: September 21, 2005
    Date of Patent: March 23, 2010
    Assignee: Hoya Corporation
    Inventor: Tadayuki Fujimoto
  • Patent number: 7552601
    Abstract: Starting from an optical component of quartz glass for transmitting ultraviolet radiation of a wavelength between 190 nm and 250 nm, with a glass structure essentially without oxygen defects, a hydrogen content ranging from 0.1×1016 molecules/cm3 to 5.0×1016 molecules/cm3, and with a content of SiH groups of less than 5×1016 molecules/cm3, to provide such a component which is particularly well suited for use with linearly polarized UV laser radiation, the present invention suggests that the component should have a content of hydroxyl groups ranging from 10 to 250 wt ppm and a fictive temperature above 1000° C.
    Type: Grant
    Filed: March 30, 2005
    Date of Patent: June 30, 2009
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Bodo Kühn, Stephan Thomas, Steffen Kaiser
  • Publication number: 20090104454
    Abstract: A process for the manufacture of a substantially bubble-free article of synthetic vitreous silica free from localised variations in refractive index (striae) and suitable for optical applications, wherein an ingot of synthetic vitreous silica containing unacceptable bubbles is submitted to a first heat treatment process consisting of hot isostatic pressing at a temperature in the range 1,250° C. to 1,500° C. at a pressure in the range 10 MPa to 250 MPa, followed by a second heat treatment process at a pressure in the range 0.01 to 1 MPa and at a temperature in the range 1,550° C. to 1,850° C.
    Type: Application
    Filed: March 15, 2007
    Publication date: April 23, 2009
    Applicant: SAINT-GOBAIN QUARTZ PLC
    Inventor: Ian George Sayce
  • Patent number: 7506521
    Abstract: Disclosed are high purity synthetic silica material having an internal transmission at 193 nm of at least 99.65%/cm and method of preparing such material. The material is also featured by a high compositional homogeneity in a plane transverse to the intended optical axis. The soot-to-glass process for making the material includes a step of consolidating the soot preform in the presence of H2O and/or O2.
    Type: Grant
    Filed: June 8, 2005
    Date of Patent: March 24, 2009
    Assignee: Corning Incorporated
    Inventors: Dana Craig Bookbinder, Richard Michael Fiacco, Kenneth Edward Hrdina, Lisa Anne Moore, Susan Lee Schiefelbein
  • Patent number: 7506522
    Abstract: Disclosed are high purity synthetic silica glass material having a high OH concentration homogeneity in a plane perpendicular to the optical axis, and process of making the same. The glass has high refractive index homogeneity. The glass can have high internal transmission of at least 99.65%/cm at 193 nm. The process does not require a post-sintering homogenization step. The controlling factors for high compositional homogeneity, thus high refractive index homogeneity, include high initial local soot density uniformity in the soot preform and slow sintering, notably isothermal treatment during consolidation.
    Type: Grant
    Filed: June 8, 2005
    Date of Patent: March 24, 2009
    Assignee: Corning Incorporated
    Inventors: Daniel Joseph Bleaking, Dana C. Bookbinder, Richard M. Fiacco, Kenneth E. Hrdina, Pushkar Tandon, John E. Maxon, Kimberly Ann Wilbert
  • Patent number: 7487649
    Abstract: The present invention provides a manufacturing method of a glass substrate for an image display device having high picture quality. The reducing force in a float furnace is controlled to be decreased so that Sn++ content on a surface of the glass substrate forming an Ag electrode is a predetermined value or less. When the resultant Sn++ content on the surface of the glass substrate forming the Ag electrode exceeds the predetermined value, the surface is partially removed to decrease the Sn++ content to the predetermined value or less to suppress the occurrence of yellowing of the glass substrate.
    Type: Grant
    Filed: November 27, 2003
    Date of Patent: February 10, 2009
    Assignee: Panasonic Corporation
    Inventors: Daisuke Adachi, Hiroyasu Tsuji, Keisuke Sumida
  • Patent number: 7485593
    Abstract: To provide titania-silica glass which is transparent glass of low thermal expansion, in particular, is of a low thermal expansion coefficient over a wide range of temperatures of 0 to 100° C. (an operating temperature range) when it is used as a photomask or a mirror material in extreme ultraviolet ray lithography, and which is excellent in homogeneity within the field and stability. Titania-silica glass is used which has 8 to 10% by weight of titania and 90 to 92% by weight of silica, where a Ti3+ concentration is 10 to 60 ppm by weight.
    Type: Grant
    Filed: October 18, 2007
    Date of Patent: February 3, 2009
    Assignee: Covalent Materials Corporation
    Inventors: Masanobu Ezaki, Masashi Kobata, Sachiko Kato
  • Publication number: 20080282734
    Abstract: The invention relates to a method and apparatus for the production of high-melting glass materials or high-melting glass ceramic materials by a process during which a temperature of a molten mass exceeds 1,760° C., wherein a shard material or raw material is molten to a molten mass, the molten mass is fined, and the molten mass emerges via a tubular outlet made of iridium or an iridium alloy having an iridium content of at least 50 wt.-%. According to the invention the temperature of a section of said tubular outlet, which is in contact with the ambient atmosphere having a natural gas composition, is controlled or regulated such that said temperature is held below 1,000° C. except during pouring out the molten mass out of said tubular outlet. Thus, an oxidative decomposition of the apparatus can be prevented.
    Type: Application
    Filed: May 12, 2008
    Publication date: November 20, 2008
    Inventors: Uwe Kolberg, Thomas Kirsch, Paul Kissl
  • Publication number: 20080287279
    Abstract: A fused silica glass and a fused silica article having a combined concentration of at least one of OH and OD of up to about 50 ppm. The fused silica glass is formed by drying a fused silica soot blank or preform in an inert atmosphere containing a drying agent, followed by removal of residual drying agent from the dried soot blank by heating the dried soot blank in an atmosphere comprising an inert gas and of oxygen.
    Type: Application
    Filed: May 5, 2008
    Publication date: November 20, 2008
    Inventors: Dana Craig Bookbinder, Richard Michael Fiacco, Kenneth Edward Hrdina, Rostislav Radievich Khrapko
  • Patent number: 7373792
    Abstract: For producing large volume optical components of high optical quality from synthetic quartz glass blanks, the latter are heated in a component mold in a furnace with a protective gas atmosphere to a temperature 50° to 170° K above the softening point, this temperature being held for 20 to 90 minutes and, during this holding time, the quartz glass blank being pressed into the component mold. By these means, a gentle treatment of the quartz glass, a good yield, a decrease in the energy input and a complete filling up of the component mold are achieved.
    Type: Grant
    Filed: August 14, 2002
    Date of Patent: May 20, 2008
    Assignee: Schott AG
    Inventors: Andreas Menzel, Frank Elsmann, Norman Schoenherr