Inside Of Tube Or Hollow Form By Soot Buildup Patents (Class 65/417)
  • Patent number: 11161767
    Abstract: An optical preform manufacturing process is disclosed in which an alkali dopant is deposited between an optical fiber core rod and an optical fiber cladding jacket. Depositing the alkali dopant between the core rod and the cladding jacket permits diffusion of the alkali dopants into the core during fiber draw when the core and the cladding are at their respective transition (or vitrification) temperatures. Introduction of the alkali dopants between the core rod and the cladding jacket also permits decoupling of the alkali doping process from one or more of other optical preform manufacturing processes. The optical preform manufacturing process can also include placing alkali dopants between an optical fiber inner cladding jacket and an optical fiber outer cladding jacket to reduce the glass viscosity during fiber draw.
    Type: Grant
    Filed: January 7, 2019
    Date of Patent: November 2, 2021
    Assignee: OFS FITEL, LLC
    Inventors: David W. Peckham, Patrick W. Wisk, Man F. Yan
  • Patent number: 10758415
    Abstract: A method and system for spot size selection wherein an indication of a spot size selection is received and a spot size is generated corresponding to the spot size selection by propagating an optical signal via one of the claddings of a dual-clad optical fiber. The system for spot size selection includes a plurality of lens arrays, at least one galvanometer, and a plurality of dual-clad fibers to propagate an optical signal from one of the plurality of lens arrays.
    Type: Grant
    Filed: January 17, 2018
    Date of Patent: September 1, 2020
    Assignee: Topcon Medical Systems, Inc.
    Inventor: Chris Sramek
  • Patent number: 10730780
    Abstract: One aspect relates to a process for the preparation of a quartz glass body, including providing a silicon dioxide granulate, wherein the silicon dioxide granulate was made from pyrogenic silicon dioxide powder and the silicon dioxide granulate has a BET surface area in a range from 20 to 40 m2/g, making a glass melt out of silicon dioxide granulate in an oven and making a quartz glass body out of at least part of the glass melt. The oven has at least a first and a further chamber connected to one another via a passage. The temperature in the first chamber is lower than the temperature in the further chambers. One aspect relates to a quartz glass body which is obtainable by this process. One aspect relates to a light guide, an illuminant and a formed body, which are each obtainable by further processing of the quartz glass body.
    Type: Grant
    Filed: December 16, 2016
    Date of Patent: August 4, 2020
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Matthias Otter, Walter Lehmann, Michael Hünermann, Nils Christian Nielsen, Nigel Robert Whippey, Boris Gromann, Abdoul-Gafar Kpebane, Matthias Söhn
  • Patent number: 10544057
    Abstract: A method of manufacturing a glass core preform for an optical fibre comprising: providing a porous soot core preform having an outer surface) and a central hole extending axially therethrough; dehydrating the porous soot core preform at a first temperature by exposing the outer surface of the preform to an atmosphere containing chlorine, and simultaneously consolidating the soot core preform and closing the central hole at a second temperature higher than the first temperature to form a glass core preform, wherein consolidating and closing comprises sequentially alternating flowing chlorine containing gas into the central hole and reducing the internal pressure of the central hole.
    Type: Grant
    Filed: June 12, 2015
    Date of Patent: January 28, 2020
    Assignee: PRYSMIAN S.p.A.
    Inventors: Franco Cocchini, Antonio Adigrat, Valeria Caronna, Marco Antonio Caiata, Antonio Collaro, Antonio Schiaffo
  • Patent number: 9643879
    Abstract: A method for manufacturing a precursor for a primary preform for optical fibers by an internal plasma deposition process including the steps of providing a hollow substrate tube, creating a first plasma reaction zone having first reaction conditions and depositing non-vitrified silica layers along at least a portion of the inner surface of the substrate tube, subsequently creating a second plasma reaction zone having second reaction conditions different from the first reaction conditions and depositing vitrified silica layers along at least a portion of the substrate tube, and cooling the substrate tube to produce the precursor for a primary preform.
    Type: Grant
    Filed: June 24, 2014
    Date of Patent: May 9, 2017
    Assignee: Draka Comteq B.V.
    Inventors: Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Johannes Antoon Hartsuiker, Gertjan Krabshuis
  • Patent number: 9598304
    Abstract: A soot glass deposit body is manufactured by placing a starting rod and a burner 22 for producing glass particulates in a reaction container, introducing a source material gas to the burner 22 through a supplying pipe 26, producing glass particulates by a pyrolytic oxidation reaction of the source material gas in a flame formed by the burner 22, and depositing the produced glass particulates on the starting rod. At the time, the source material gas to be supplied to the burner 22 is a siloxane, the burner 22 is heated so that temperature of the burner 22 falls within the range of from ?30° C. to +30° C. relative to the boiling point of the siloxane, and also temperature of the supplying pipe is controlled within the range of from the boiling point of the siloxane to the boiling point plus 30° C.
    Type: Grant
    Filed: May 13, 2014
    Date of Patent: March 21, 2017
    Assignee: SUMITOMO ELECTRIC INDUSTRIES, LTD.
    Inventors: Takashi Yamazaki, Tomohiro Ishihara
  • Publication number: 20150052952
    Abstract: An apparatus for manufacturing a glass perform, includes: a dummy tube section, a reservoir portion, and a cooling portion; and a glass tube section in which particles of an alkali metal compound or an alkaline earth metal compound which have flowed into the glass tube section from the dummy tube section are heated by a second heat source which performs traverse, and oxides of the particles being deposited on an inner wall and dispersed in the glass tube section. In the cooling portion of the dummy tube section, vapor of the alkali metal compound or the alkaline earth metal compound generated by heating of a first heat source is cooled and condensed by a dry gas flowing into the dummy tube section, and thereby the particles are generated.
    Type: Application
    Filed: October 23, 2014
    Publication date: February 26, 2015
    Applicant: FUJIKURA LTD.
    Inventor: Takayuki KITAMURA
  • Patent number: 8925354
    Abstract: Methods of forming an overclad portion of an optical fiber are described which include positioning a core cane member in an overclad tube to form a rod and tube assembly. Thereafter, glass soot pellets are positioned in the rod and tube assembly between the core cane member and an interior sidewall of the overclad tube. The rod and tube assembly is then redrawn under conditions effective to form the overclad tube and the glass soot pellets into a continuous, void-free glass layer surrounding the core cane member at a sintering time tsinter of at least 1800 seconds thereby forming an overclad portion of an optical fiber.
    Type: Grant
    Filed: November 4, 2009
    Date of Patent: January 6, 2015
    Assignee: Corning Incorporated
    Inventors: Robert Brett Desorcie, Peter Joseph Ronco, Roger A. Rose, Pushkar Tandon
  • Patent number: 8904827
    Abstract: A method for manufacturing an optical preform via an internal vapor deposition process, wherein during the inside deposition process the velocity of the reaction zone is set so that the velocity of the reaction zone over the length of the supply side-to-discharge side is higher than the velocity of the reaction zone over the length of the discharge side-to-supply side.
    Type: Grant
    Filed: March 23, 2012
    Date of Patent: December 9, 2014
    Assignee: Draka Comteq B.V.
    Inventors: Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Johannes Antoon Hartsuiker, Eugen Aldea, Eric Aloysius Kuijpers
  • Patent number: 8857372
    Abstract: An isothermal, low pressure-based process of depositing material within a substrate has been developed and results in creating an extremely narrow reaction zone within which a more uniform and efficient deposition will occur. Sets of isothermal plasma operating conditions have been found that create a narrow deposition zone, assuring that the deposited material is clear glass rather than soot particles. The chemical delivery system, in one arrangement, utilizes rods of solid phase source material (which may otherwise be difficult to obtain in gaseous form). The operating conditions are selected such that the hot plasma does not transfer a substantial amount of heat to the substrate tube, where the presence of such heat has been found to result in vaporizing the reactant material (creating soot) and developing hot spots.
    Type: Grant
    Filed: September 27, 2010
    Date of Patent: October 14, 2014
    Inventors: James Fleming, George Zydzik
  • Patent number: 8844323
    Abstract: A glass preform manufacturing method, includes: preparing a glass element having a rough surface; turning a raw material of an alkali metal compound or a raw material of an alkaline earth metal compound into particles; depositing particles of the alkali metal compound or the alkaline earth metal compound on the rough surface of the glass element; oxidizing the particles of the alkali metal compound or the alkaline earth metal compound while diffusing alkali metal oxide or alkaline earth metal oxide in the glass element; and manufacturing a glass preform into which the alkali metal oxide or the alkaline earth metal oxide is doped.
    Type: Grant
    Filed: September 15, 2011
    Date of Patent: September 30, 2014
    Assignee: Fujikura Ltd.
    Inventor: Takayuki Kitamura
  • Patent number: 8840858
    Abstract: An apparatus for mixing a vaporized precursor with a gas for producing silica particles is provided. The apparatus includes a mixer housing, a precursor delivery chamber having an output in communication with the mixer housing for delivering a vaporized precursor in the mixer housing, and an oxidizing gas delivery chamber having an output in communication with the mixer housing for delivering an oxidizing gas to be mixed with the vaporized precursor. The apparatus further includes a flashback member disposed within the mixer housing and between the output of the precursor delivery chamber and the output of the oxidizing gas delivery chamber. The flashback member is located at a minimum distance from the output of the oxidizing gas delivery chamber defined by Lminimum (cm)=0.453 U (Re)?0.5567, wherein U is the flow rate in cm/sec of precursor and Re is the flow Reynolds number. The flashback member may include a tapered surface on at least one side to reduce recirculation of vaporized gas.
    Type: Grant
    Filed: July 6, 2011
    Date of Patent: September 23, 2014
    Assignee: Corning Incorporated
    Inventors: Lewis A Bernstein, Dana Craig Bookbinder, Jason A Dillard, Jennifer L Porter, Balram Suman, Pushkar Tandon
  • Patent number: 8826699
    Abstract: A method for manufacturing a primary preform for optical fibers using an internal vapor deposition process including the steps of providing a substrate tube having supply and discharge sides, surrounding at least part of the tube by a furnace, supplying glass-forming gases to the interior of the tube via the supply side, creating a reaction zone with conditions such that deposition of glass will take place on the inner surface of the tube, and moving the reaction zone back and forth along the length of the tube between reversal points near the supply and discharge sides to form one or more preform layers on the inner surface of the tube, wherein both reversal points are surrounded by the furnace.
    Type: Grant
    Filed: July 28, 2010
    Date of Patent: September 9, 2014
    Assignee: Draka Comteq B.V.
    Inventors: Johannes Antoon Hartsuiker, Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Eric Aloysius Kuijpers
  • Patent number: 8794038
    Abstract: The invention relates to a multimode optical fiber having a refractive index profile, comprising a light-guiding core surrounded by one or more cladding layers. The present invention furthermore relates to an optical communication system comprising a transmitter, a receiver and a multimode optical fiber.
    Type: Grant
    Filed: August 4, 2008
    Date of Patent: August 5, 2014
    Assignee: Draka Comteq, B.V.
    Inventors: Pieter Matthuse, Mattheus Jacobus Nicolaas Van Stralen, Mark Peter Marie Jetten, Gert-Jan Krabshuis
  • Publication number: 20140157829
    Abstract: A method for activating an inner surface of a hollow glass substrate tube for manufacturing an optical fiber preform including depositing a plurality of activation glass layers on the inner surface of the hollow substrate tube by a PCVD process, wherein a total thickness of the deposited activation glass layers is between 10 microns and 250 microns, and etching the deposited activation glass layers to remove at least 30% of the deposited activation glass layers.
    Type: Application
    Filed: December 10, 2013
    Publication date: June 12, 2014
    Applicant: Draka Comteq B.V.
    Inventors: Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Johannes Antoon Hartsuiker
  • Patent number: 8739575
    Abstract: A method for manufacturing a primary preform for optical fibers using an internal vapor deposition process including the steps of providing a substrate tube having supply and discharge sides, surrounding at least part of the tube by a furnace set at a temperature T0, supplying doped or undoped gases via the supply side, creating a reaction zone to promote deposition, and moving the zone back and forth along the length of the tube between reversal points near the supply and discharge sides to form at least one preform layer, which at least one layer comprises several glass layers.
    Type: Grant
    Filed: July 29, 2010
    Date of Patent: June 3, 2014
    Assignee: Draka Comteq B.V.
    Inventors: Johannes Antoon Hartsuiker, Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Eric Aloysius Kuijpers
  • Publication number: 20140126876
    Abstract: An optical fiber with a shaped tip is covered by a cap that is fused to the optical fiber using doped silica. The doped silica has a melting temperature that is lower than the melting temperature of the optical fiber. The doped silica also has a melting temperature that is lower than the melting temperature of the cap.
    Type: Application
    Filed: November 4, 2013
    Publication date: May 8, 2014
    Inventors: Jie Li, Xiaoguang Sun
  • Patent number: 8667816
    Abstract: The present invention relates to a method for manufacturing a primary preform for optical fibers, using an internal vapor deposition process, wherein a gas flow of doped undoped glass-forming gases is supplied to the interior of a hollow substrate tube having a supply side and a discharge side via the supply side thereof, wherein deposition of glass layers on the interior of the substrate tube is effected as a result of the presence of a reaction zone.
    Type: Grant
    Filed: June 1, 2011
    Date of Patent: March 11, 2014
    Assignee: Draka Comteq B.V.
    Inventors: Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Eugen Aldea
  • Patent number: 8499585
    Abstract: The present invention relates to a device for manufacturing an optical preform by means of an internal vapor deposition process, said device comprising an energy source and a substrate tube, which substrate tube comprises a supply side for supplying glass-forming precursors and a discharge side for discharging constituents that have not been deposited on the interior of the substrate tube, said energy source being movable along the length of the substrate tube between a point of reversal at the supply side and a point of reversal at the discharge side.
    Type: Grant
    Filed: September 28, 2010
    Date of Patent: August 6, 2013
    Assignee: Draka Comteq B.V.
    Inventors: Mattheus Jacobus Nicolaas Van Stralen, Martinus Johannes Marinu Jozeph Swarts, Igor Milicevic, Marco Korsten
  • Patent number: 8484996
    Abstract: The present invention relates to a method for manufacturing a preform for optical fibers, wherein deposition of glass-forming compounds on the substrate takes place. The present invention furthermore relates to a method for manufacturing optical fibers, wherein one end of a solid preform is heated, after which an optical fiber is drawn from said heated end.
    Type: Grant
    Filed: August 24, 2011
    Date of Patent: July 16, 2013
    Assignee: Draka Comteq B.V.
    Inventors: Dennis Robert Simons, Jelle Philip Terpsma, Frans Gooijer
  • Patent number: 8464556
    Abstract: Method of making a microstructured optical fiber. Silica glass based soot is deposited on a substrate to form at least a portion of an optical fiber preform by traversing a soot deposition burner with respect to said substrate at a burner traverse rate greater than 3 cm/sec, thereby depositing a layer of soot having a thickness less than 20 microns for each of a plurality of burner passes. At least a portion of the soot preform is then consolidated inside a furnace to remove greater than 50 percent of the air trapped in said soot preform, said consolidating taking place in a gaseous atmosphere containing krypton, nitrogen, or mixtures thereof under conditions which are effective to trap a portion of said gaseous atmosphere in said preform during said consolidation step, thereby forming a consolidated preform which when viewed in cross section will exhibit at least 50 voids therein.
    Type: Grant
    Filed: May 5, 2008
    Date of Patent: June 18, 2013
    Assignee: Corning Incorporated
    Inventors: Dana Craig Bookbinder, Robert Brett Desorcie, Mark Alan McDermott, Pushkar Tandon
  • Patent number: 8443630
    Abstract: A method for manufacturing a primary preform for optical fibers using an internal vapor deposition process, including the steps of: i) providing a hollow glass substrate tube having a supply side and a discharge side, ii) surrounding at least part of the hollow glass substrate tube by a furnace, iii) supplying a gas flow, doped or undoped, of glass-forming gases to the interior of the hollow glass substrate tube via the supply side thereof, iv) creating a reaction zone in which conditions such that deposition of glass will take place on the interior of the hollow glass tube are created, and v) moving the reaction zone back and forth in longitudinal direction over the hollow glass substrate tube between a reversal point located near the supply side and a reversal point located near the discharge side of the hollow glass substrate tube.
    Type: Grant
    Filed: April 7, 2011
    Date of Patent: May 21, 2013
    Assignee: Draka Comteq, B.V.
    Inventors: Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Johannes Antoon Hartsuiker, Eugen Aldea, Eric Aloysius Kuijpers
  • Publication number: 20130081430
    Abstract: Provided is a method of manufacturing an optical fiber base material using a MCVD method, including: a step of heating a glass tube while rotating the glass tube and supplying a gas into a through-hole of the glass tube, wherein in at least a part of the step, the inside of the through-hole is pressurized so that an outer diameter of the glass tube increases.
    Type: Application
    Filed: September 28, 2012
    Publication date: April 4, 2013
    Applicant: FUJIKURA LTD.
    Inventor: FUJIKURA LTD.
  • Patent number: 8402792
    Abstract: A method for manufacturing a primary preform for optical fibers using an internal vapor deposition process, including the steps of: i) providing a hollow glass substrate tube having a supply side and a discharge side, ii) surrounding at least part of the hollow glass substrate tube by a furnace, iii) supplying doped or undoped glass-forming gases to the interior of the hollow glass substrate tube via the supply side thereof, iv) creating a reaction zone in which conditions such that deposition of glass will take place on the interior of the hollow glass tube are created, and v) moving the reaction zone back and forth along the length of the hollow glass substrate tube between a reversal point located near the supply side and a reversal point located near the discharge side of the hollow glass substrate tube, wherein, during at least part of step v), the gas flow comprises a first concentration of fluorine-containing compound when the reaction zone is moving in the direction of the discharge side.
    Type: Grant
    Filed: April 7, 2011
    Date of Patent: March 26, 2013
    Assignee: Draka Comteq B.V.
    Inventors: Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Johannes Antoon Hartsuiker, Eugen Aldea
  • Patent number: 8381549
    Abstract: The present invention relates to an optical fiber preform fabricating method that makes it possible to implement a reduction in iron impurities at a low cost. The optical fiber preform fabricating method comprises a glass synthesis step for forming a glass region constituting at least a part of the core area of the optical fiber. The glass synthesis step includes a deposition step of depositing glass particles containing the Al-element inside the glass pipe by means of chemical vapor deposition, and a consolidation step of obtaining a transparent glass body from the glass soot body thus obtained. In other words, the deposition step synthesizes glass particles on the inside wall of a glass pipe by feeding raw material gas, in which the content ratio (O/Al) of the O-element and Al-element is 20 or less, into the glass pipe. Furthermore, the consolidation step obtains a transparent glass body from the glass soot body by heating the glass soot body.
    Type: Grant
    Filed: June 21, 2007
    Date of Patent: February 26, 2013
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Tetsuya Nakanishi, Tetsuya Haruna, Shinji Ishikawa
  • Patent number: 8265440
    Abstract: A method for manufacturing an optical fiber preform includes the steps of depositing an inner cladding and a central core inside a fluorine doped silica tube and thereafter collapsing the silica tube to form a primary preform. The fluorine doped silica tube has a cross section area that is no more than about 15 percent smaller than the cross section area of the resulting primary preform. The present method facilitates reduced-cost manufacturing of a high-capacity optical fiber preform, which may be drawn to produce an optical fiber having reduced transmission losses.
    Type: Grant
    Filed: April 12, 2010
    Date of Patent: September 11, 2012
    Assignee: Draka Comteq, B.V.
    Inventors: Cedric Gonnet, Elise Regnier, Frans Gooijer, Pascale Nouchi
  • Patent number: 8252387
    Abstract: An isothermal, low pressure-based process of depositing material within a substrate has been developed, and is particularly useful in forming an optical fiber preform results in creating an extremely narrow reaction zone within which a more uniform and efficient deposition will occur. Sets of isothermal plasma operating conditions have been found that create a narrow deposition zone, assuring that the deposited material is clear glass rather than soot particles. The exhaust end of the tube is connected to a vacuum system which is in turn connected to a scrubber apparatus for removal and neutralization of reaction by-products. The operating conditions are selected such that the hot plasma does not transfer a substantial amount of heat to the substrate tube, where the presence of such heat has been found to result in vaporizing the reactant material (creating soot) and developing hot spots.
    Type: Grant
    Filed: December 10, 2007
    Date of Patent: August 28, 2012
    Assignee: OFS Fitel, LLC
    Inventors: James W. Fleming, George J. Zydzik
  • Patent number: 8192808
    Abstract: The present invention relates to an apparatus and related method for manufacturing an optical preform. The present invention embraces a novel insert tube that is strategically positioned within a quartz substrate tube during the internal vapor deposition process.
    Type: Grant
    Filed: April 22, 2008
    Date of Patent: June 5, 2012
    Assignee: Draka Comteq, B.V.
    Inventors: Marco Korsten, Marc Jansen, Eric Aloysius Kuijpers
  • Patent number: 8168267
    Abstract: A method for manufacturing a preform for optical fibers by a vapor deposition process wherein an intermediate step is carried out between one deposition phase and the next deposition phase(s), wherein the intermediate step includes supplying an etching gas to the supply side of the hollow substrate tube.
    Type: Grant
    Filed: June 27, 2008
    Date of Patent: May 1, 2012
    Assignee: Draka Comteq B.V.
    Inventors: Johannes Antoon Hartsuiker, Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Rob Hubertus Matheus Deckers, Marco Korsten
  • Publication number: 20120040184
    Abstract: A method of manufacturing an optical fiber preform includes preparing from a first deposition tube a first rod that includes a central core and preparing from a second deposition tube a second rod that includes a buried trench. The method further includes fitting the second rod as a sleeve over the first rod. This disclosed method facilitates the manufacture of large-capacity fiber preforms using deposition benches having small and/or medium deposition capacity.
    Type: Application
    Filed: August 10, 2011
    Publication date: February 16, 2012
    Applicant: DRAKA COMTEQ B.V.
    Inventors: Louis-Anne de Montmorillon, Frans Gooijer, Pierre Sillard
  • Publication number: 20110302966
    Abstract: The present invention relates to a method for manufacturing a primary preform for optical fibres, using an internal vapour deposition process, wherein a gas flow of doped undoped glass-forming gases is supplied to the interior of a hollow substrate tube having a supply side and a discharge side via the supply side thereof, wherein deposition of glass layers on the interior of the substrate tube is effected as a result of the presence of a reaction zone.
    Type: Application
    Filed: June 1, 2011
    Publication date: December 15, 2011
    Applicant: DRAKA COMTEQ B.V.
    Inventors: Igor MILICEVIC, Mattheus Jacobus Nicolaas VAN STRALEN, Eugen ALDEA
  • Patent number: 8069690
    Abstract: A method of fabricating a glass body that includes a multiplicity of constituents, at least one of which is a dopant (e.g., a rare-earth element) having a low vapor pressure (LVP) precursor comprises the steps of: (a) generating an aerosol from the LVP precursor; (b) separately generating vapors of the other constituents; (c) convecting the aerosol and vapors to deposition system including a substrate; and (d) forming at least one doped layer on a surface of the substrate. In one embodiment, the method also includes filtering the aerosol so as to remove aerosol particles outside of a particular range of sizes. Also described is a unique aerosol generator that is particularly useful in generating aerosols of rare-earth dopants. Particular embodiments directed to the fabrication of Yb-doped optical fibers are described.
    Type: Grant
    Filed: December 5, 2006
    Date of Patent: December 6, 2011
    Assignee: OFS Fitel, LLC
    Inventors: Anthony Michael DeSantolo, Robert Scott Windeler
  • Patent number: 8051683
    Abstract: The present invention relates to a method for manufacturing a preform for optical fibers via a vapor deposition process in which the position of the reversal point near the substrate tube's supply side shifts along the longitudinal axis of the substrate tube during at least part of the deposition process.
    Type: Grant
    Filed: April 25, 2008
    Date of Patent: November 8, 2011
    Assignee: Draka Comteq, B.V.
    Inventors: Rob Hubertus Matheus Deckers, Marco Korsten, Robert Martinus Marie Cremers, Koen de Jongh
  • Publication number: 20110244154
    Abstract: In a known method for producing a dimensionally stable semi-finished product for use in producing fibers from synthetic quartz glass, an SiO2 soot layer is applied to the outer wall of a quartz glass inner cylinder and is subjected to a sintering treatment, wherein a sintering zone moves through the SiO2 soot layer from the outside to the inside. In order to achieve dimensionally accurate and low-deformation production as well as high cost efficiency based on said known method, it is proposed that the sintering treatment be interrupted before the sintering zone reaches the outer wall of the inner cylinder so that an intermediate layer made of synthetic quartz glass containing pores remains at the inner cylinder outer wall. The semi-finished product obtained in such a way is elongated into the optical component, wherein the intermediate layer sinters completely into transparent quartz glass.
    Type: Application
    Filed: October 29, 2009
    Publication date: October 6, 2011
    Applicant: Heraeus Quarzglas GmbH & Co KG
    Inventors: Thomas Krause, Martin Trommer
  • Patent number: 8020410
    Abstract: A method of making an optical fiber preform includes depositing silica glass on the inside of a tube substrate via a plasma chemical vapor deposition (PCVD) operation. The parameters of the PCVD operation are controlled such that the silica glass deposited on the interior of the tube substrate contains a non-periodic array of voids in a cladding region of the optical fiber preform. The optical fiber preform may be used to produce an optical fiber having a core and a void containing cladding. The core of the optical fiber has a first index of refraction and the cladding has a second index of refraction less than that of the core.
    Type: Grant
    Filed: November 19, 2007
    Date of Patent: September 20, 2011
    Assignee: Corning Incorporated
    Inventors: Dana Craig Bookbinder, Robert Brett Desorcie, Pushkar Tandon
  • Patent number: 8015845
    Abstract: In a glass processing method according to the invention, in the case of performing chemical vapor deposition or diameter shrinkage of a substrate glass tube G by relatively moving a heating furnace 20 comprising a heating element 21 for annularly enclosing the circumference of the substrate glass tube in a longitudinal direction of the substrate glass tube G with respect to the substrate glass tube G in which an outer diameter is 30 mm or more and a wall thickness is 3 mm or more and is less than 15 mm and an ovality of the outer diameter is 1.0% or less using a glass processing apparatus 1, a temperature of at least one of the heating element 21 and the substrate glass tube G is measured and the amount of heat generation of the heating element 21 is adjusted based on the measured temperature.
    Type: Grant
    Filed: May 27, 2010
    Date of Patent: September 13, 2011
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Tetsuya Nakanishi, Masashi Onishi, Tomoyuki Yokokawa, Masaaki Hirano, Nobuyuki Taira
  • Patent number: 8006518
    Abstract: The present invention relates to a method for manufacturing a preform for optical fibers, wherein deposition of glass-forming compounds on the substrate takes place. The present invention furthermore relates to a method for manufacturing optical fibers, wherein one end of a solid preform is heated, after which an optical fibre is drawn from said heated end.
    Type: Grant
    Filed: October 7, 2004
    Date of Patent: August 30, 2011
    Assignee: Draka Comteq, B.V.
    Inventors: Dennis Robert Simons, Jelle Philip Terpsma, Frans Gooijer
  • Patent number: 7946134
    Abstract: The specification describes methods for the manufacture of very large optical fiber preforms wherein the core material is produced by MCVD. Previous limitations on preform size inherent in having the MCVD starting tube as part of the preform process are eliminated by removing the MCVD starting tube material from the collapsed MCVD rod by etching or mechanical grinding. Doped overcladding tubes are used to provide the outer segments of the refractive index profile thus making most effective use of the MCVD produced glass and allowing the production of significantly larger MCVD preforms than previously possible.
    Type: Grant
    Filed: April 27, 2010
    Date of Patent: May 24, 2011
    Assignee: OFS Fitel, LLC
    Inventors: Robert M. Atkins, James W. Fleming, Paul F Glodis, Man F. Yan
  • Patent number: 7946135
    Abstract: Disclosed is a method of heat treating quartz glass deposition tubes at between 900° C. and 1200° C. for at least 115 hours. The resulting deposition tubes are useful in forming optical preforms that can yield optical fibers having reduced added loss.
    Type: Grant
    Filed: January 2, 2008
    Date of Patent: May 24, 2011
    Assignees: Draka Comteq, B.V., Momentive Performance Materials, Inc.
    Inventors: Guangjun Xu, Larry Zeng, Ivo Flammer, Dennis Robert Simons, Cedric Gonnet, Rob Hubertus Matheus Deckers
  • Patent number: 7930903
    Abstract: A method for manufacturing a preform for optical fibers by means of a vapor deposition process, wherein plasma conditions are created and wherein the plasma is moved back and forth along the longitudinal axis of the hollow substrate tube between a reversal point near the supply side and a reversal point near the discharge side of the hollow substrate tube, so that the location where the soot deposition associated with one phase takes place is axially spaced from the location where the soot deposition associated with the other phase(s) takes place.
    Type: Grant
    Filed: April 25, 2008
    Date of Patent: April 26, 2011
    Assignee: Draka Comteq B.V.
    Inventors: Johannes Antoon Hartsuiker, Igor Milicevic, Mattheus Jacobus Nicolaas Van Stralen, Rob Hubertus Matheus Deckers, Marco Korsten
  • Patent number: 7921675
    Abstract: A method of making an optical fiber preform includes depositing silica glass soot on the inside of a substrate tube via a chemical vapor deposition operation. The silica glass soot is consolidated into silica glass under controlled conditions such that the consolidated silica glass on the interior of the substrate tube contains a non-periodic array of gaseous voids in a cladding region of the optical fiber preform. The optical fiber preform may be used to produce an optical fiber having a core and a cladding containing voids formed from the gaseous voids of the cladding region of the optical fiber preform. The core of the optical fiber has a first index of refraction and the cladding has a second index of refraction less than that of the core.
    Type: Grant
    Filed: November 16, 2007
    Date of Patent: April 12, 2011
    Assignee: Corning Incorporated
    Inventors: Dana Craig Bookbinder, Robert Brett Desorcie, Pushkar Tandon
  • Patent number: 7891217
    Abstract: Glass can be synthesized and deposited at a high rate by the inside CVD method using a plasma burner in a manner such that unconsolidated portions or bubbles are little generated. The method includes a step of depositing a glass film on the inner wall surface of a starting pipe. In a first aspect, temperature the pipe is controlled not to exceed (1800 +100xd)° C., a temperature of (1100 +100xd)° C. or higher being continued for 20 seconds or more at each point of the pipe, where d (mm) represents the wall thickness of the pipe. In a second aspect, the burner includes at least two inlets and has an inner diameter of 80 mm or more, and the deposition step is performed in the relationship, 150 mm/s <(Total flow rate of the gases introduced into the burner)/(Sectional area of the burner) <600 mm/s.
    Type: Grant
    Filed: October 20, 2005
    Date of Patent: February 22, 2011
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Tetsuya Nakanishi, Masaaki Hirano
  • Publication number: 20110023552
    Abstract: The present invention relates to a device for manufacturing an optical preform by means of an internal vapour deposition process, said device comprising an energy source and a substrate tube, which substrate tube comprises a supply side for supplying glass-forming precursors and a discharge side for discharging constituents that have not been deposited on the interior of the substrate tube, said energy source being movable along the length of the substrate tube between a point of reversal at the supply side and a point of reversal at the discharge side.
    Type: Application
    Filed: September 28, 2010
    Publication date: February 3, 2011
    Applicant: DRAKA COMTEQ B.V.
    Inventors: Mattheus Jacobus Nicolaas VAN STRALEN, Martinus Johannes Marinus Jozeph Swarts, Igor Milicevic, Marco Korsten
  • Patent number: 7866188
    Abstract: The present invention relates to an apparatus for carrying out a PCVD deposition process, wherein one or more doped or undoped layers are coated onto the interior of a glass substrate tube, which apparatus comprises an applicator having an inner and an outer wall and a microwave guide which opens into the applicator, which applicator extends around a cylindrical axis and which is provided with a passage adjacent to the inner wall, through which the microwaves can exit, over which cylindrical axis the substrate tube can be positioned, and wherein at least one choke of annular shape having a length l and a width w is centred around the cylindrical axis within the applicator.
    Type: Grant
    Filed: December 30, 2004
    Date of Patent: January 11, 2011
    Assignee: Draka Comteq, B.V.
    Inventors: Mattheus Jacobus Nicolaas Van Stralen, Rob Hubertus Matheus Deckers
  • Patent number: 7854148
    Abstract: The present invention relates to a device for manufacturing an optical preform by means of an internal vapour deposition process, said device comprising an energy source and a substrate tube, which substrate tube comprises a supply side for supplying glass-forming precursors and a discharge side for discharging constituents that have rot been deposited on the interior of the substrate tube, said energy source being movable along the length of the substrate tube between a point of reversal at the supply side and a point of reversal at the discharge side.
    Type: Grant
    Filed: December 19, 2006
    Date of Patent: December 21, 2010
    Assignee: Draka Comteq B.V.
    Inventors: Mattheus Jacobus Nicolaas Van Stralen, Martinus Johannes Marinus Jozeph Swarts, Igor Milicevic, Marco Korsten
  • Patent number: 7854149
    Abstract: In general, in one aspect, the invention features a method that includes exposing a surface to a first gas composition under conditions sufficient to deposit a layer of a first chalcogenide glass on the surface, and exposing the layer of the first chalcogenide glass to a second gas composition under conditions sufficient to deposit a layer of a second glass on the layer of the first chalcogenide glass, wherein the second glass is different from the first chalcogenide glass.
    Type: Grant
    Filed: June 8, 2007
    Date of Patent: December 21, 2010
    Assignee: OmniGuide, Inc.
    Inventor: Vladimir Fuflyigin
  • Publication number: 20100287993
    Abstract: The specification describes methods for the manufacture of very large optical fiber preforms wherein the core material is produced by MCVD. Previous limitations on preform size inherent in having the MCVD starting tube as part of the preform process are eliminated by removing the MCVD starting tube material from the collapsed MCVD rod by etching or mechanical grinding. Doped overcladding tubes are used to provide the outer segments of the refractive index profile thus making most effective use of the MCVD produced glass and allowing the production of significantly larger MCVD preforms than previously possible.
    Type: Application
    Filed: April 27, 2010
    Publication date: November 18, 2010
    Inventors: Robert M. Atkins, James W. Fleming, Paul F. Glodis, Man F. Yan
  • Patent number: 7797966
    Abstract: Fused silica injected or created by pyrolysis of SiCl4 are introduced in a powder state into a vacuum chamber. Pluralities of jet streams of fused silica are directed towards a plurality of heated substrates. The particles attach on the substrates and form shaped bodies of fused silica called preforms. For uniformity the substrates are rotated. Dopant is be added in order to alter the index of refraction of the fused silica. Prepared soot preforms are vitrified in situ. Particles are heated, surface softened and agglomerated in mass and are collected in a heated crucible and are softened and flowed through a heated lower throat. The material is processed into quartz plates and rods for wafer processing and optical windows.
    Type: Grant
    Filed: June 15, 2001
    Date of Patent: September 21, 2010
    Assignee: Single Crystal Technologies, Inc.
    Inventor: Kiril A. Pandelisev
  • Patent number: 7752870
    Abstract: A method of forming an optical fiber preform using, for example, an MCVD process, is modified to reduce the presence of hydrogen-induced transmission losses in an optical fiber drawn from the preform. A relatively porous, unsintered soot layer is first formed (similar to the initial soot layer commonly associated with the solution-doped process of the prior art) and then subjected to a flow of a metal halide (such as SiCl4) to reduce the presence of excess oxygen. It is imperative that the metal halide treatment occur in the absence of oxygen. Sintering of the treated layer, followed by a conventional collapsing process is then used to form the inventive preform. In accordance with the present invention, both the sintering and collapsing steps are performed in a non-oxygen based ambient. When the drawn fiber is then later exposed to hydrogen, the lack of oxygen thus eliminates the formation of Si—OH and the associated attenuation problems.
    Type: Grant
    Filed: October 16, 2003
    Date of Patent: July 13, 2010
    Assignee: Baker Hughes Incorporated
    Inventor: Daniel Scott Homa
  • Patent number: 7637125
    Abstract: In a glass processing method according to the invention, in the case of performing chemical vapor deposition or diameter shrinkage of a substrate glass tube G by relatively moving a heating furnace 20 comprising a heating element 21 for annularly enclosing the circumference of the substrate glass tube in a longitudinal direction of the substrate glass tube G with respect to the substrate glass tube G in which an outer diameter is 30 mm or more and a wall thickness is 3 mm or more and is less than 15 mm and an ovality of the outer diameter is 1.0% or less using a glass processing apparatus 1, a temperature of at least one of the heating element 21 and the substrate glass tube G is measured and the amount of heat generation of the heating element 21 is adjusted based on the measured temperature.
    Type: Grant
    Filed: November 19, 2004
    Date of Patent: December 29, 2009
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Tetsuya Nakanishi, Masashi Onishi, Tomoyuki Yokokawa, Masaaki Hirano, Nobuyuki Taira