Drying, Dehydration, Oh Removal Or Prevention Patents (Class 65/426)
  • Patent number: 5666454
    Abstract: A single-mode optical fiber preform is produced by a process where a porous glass body of a core rod for a single-mode optical fiber is dehydrated and made into a glass to prepare a core rod for the optical fiber, clad layers are deposited on the circumference of the core rod for the optical fiber so as to give an outer diameter of a desired value, and then these are dehydrated and made into glass. At this time, the diameter of a part corresponding to the core rod for the optical fiber in the optical fiber obtained by drawing the preform for optical fiber is controlled to 1.9 times or more the mode field diameter, which is a diameter that allows light having a wavelength of 1.55 .mu.m to pass therethrough. As a result, a preform for a single-mode optical fiber with which an optical fiber little influenced by defects can be obtained can be produced.
    Type: Grant
    Filed: April 16, 1996
    Date of Patent: September 9, 1997
    Assignee: The Furukawa Electric Co., Ltd.
    Inventors: Jun Terada, Hideaki Chiba, Mituhiro Kawasaki, Tadashi Takahashi
  • Patent number: 5656057
    Abstract: The invention relates to a method of drying and sintering porous optical fiber preforms, especially those consisting of a solid glass core cane surrounded by a layer of cladding soot. After it is dried in a dehydrating atmosphere, the porous preform is heated to a presinter temperature just below that at which it would begin to rapidly densify. The various temperature holds and ramp rates are such that the preform is consolidated in a relatively short time without becoming cloudy or exhibiting other defects that would adversely affect the optical fiber drawn from the consolidated draw blank.
    Type: Grant
    Filed: May 19, 1995
    Date of Patent: August 12, 1997
    Assignee: Corning Incorporated
    Inventors: Gillian L. Brown, Richard M. Fiacco, John C. Walker
  • Patent number: 5609666
    Abstract: During the gradual build-up of porous quartz glass by the combustion of a hydrolysis gas mixture and preferably for a certain period of time thereafter, a drying gas mixture is conducted under positive pressure through the porous tubular deposit from the inside to the outside as it is being built-up. This is accomplished by depositing the quartz on a tubular substrate in which a drying gas is introduced at positive pressure.
    Type: Grant
    Filed: February 16, 1995
    Date of Patent: March 11, 1997
    Assignee: Heraeus Quarzglas GmbH
    Inventor: Walter Heitmann
  • Patent number: 5565014
    Abstract: Sol-gel processing of a silica glass body is facilitated by rapid drying. The body, having been heated to a temperature of about 200.degree. C. in a hermetically sealed vessel, is vented while reducing temperature. Termination of drying coincides with reduction to atmospheric pressure.
    Type: Grant
    Filed: March 31, 1994
    Date of Patent: October 15, 1996
    Assignee: Lucent Technologies Inc.
    Inventor: James W. Fleming, Jr.
  • Patent number: 5562752
    Abstract: Heating a wet colloidal gel body in an autoclave above its 1-atmosphere boiling point, under rigorously defined conditions, avoids shrinkage during subsequent drying. As a consequence, drying rates may be increased, and handling care becomes less critical.
    Type: Grant
    Filed: March 31, 1994
    Date of Patent: October 8, 1996
    Assignee: Lucent Technologies Inc.
    Inventor: James W. Fleming, Jr.
  • Patent number: 5397372
    Abstract: A method for making a glass preform substantially free of OH impurities is disclosed. The method comprises the steps of introducing a moving stream of a vapor mixture including at least one compound glass-forming precursor together with an oxidizing medium into a tube, while generating a hydrogen-free isothermal plasma on an outer surface of the tube to react the mixture and produce a glassy deposit on an inner surface of the tube. The method uses a plasma torch or a radio frequency furnace.
    Type: Grant
    Filed: November 30, 1993
    Date of Patent: March 14, 1995
    Assignee: AT&T Corp.
    Inventors: Fred P. Partus, Gordon A. Thomas