By Or With Coating At Joint Interface Of A Formed Part Prior To Bonding Patents (Class 65/43)
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Patent number: 4818264Abstract: A multicapillary gas chromatography column comprising a bundle of single capillary columns each of which have essentially the same internal diameter and which are coated with essentially the same thickness of essentially the same stationary phase so that each column has essentially the same standard retention factor. A method of producing such a column is to cut a single fused silica capillary column into a number of essentially equal lengths and then to bundle the lengths together. Each bundle end can then be inserted into, for example, a graphite ferrule and then the multicapillary column can be conventionally installed into a gas chromatograph. The multicapillary column of the invention has the injection, detection and sample capacity advantages of a relatively large diameter capillary column with the speed and resolving power of a relatively narrow diameter capillary column.Type: GrantFiled: April 30, 1987Date of Patent: April 4, 1989Assignee: The Dow Chemical CompanyInventor: Marsha L. Langhorst
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Patent number: 4792348Abstract: A method of producing a joint between a beta-alumina electrolyte tube and alpha-alumina flange with a glass bonding agent in a solid annular bead form devoid of additives such as a coupling agent or the like capable of being heated when subjected to microwave energy which comprises utilizing in the heating step a source of microwave energy rather than a gas flame or electrical resistance heat source so as to heat the beta-alumina tube by microwave energy for a time period sufficient to enable the heat generated in the beta-alumina tube to be conducted to glass bead and the alpha-alumina flange and heat the glass bead to a temperature above the glass deformation point, and allowing the tube to cool to solidify the glass bead in intimately penetrating relation to the surfaces of the beta-alumina tube and alpha-alumina flange engaged thereby so that the glass forms a bond between the beta-alumina tube and the alpha-alumina flange characterized by a fusion of the glass within the engaged beta-alumina and alpha-alType: GrantFiled: March 2, 1987Date of Patent: December 20, 1988Assignee: Powerplex Technologies, Inc.Inventor: Alina V. Pekarsky
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Patent number: 4788762Abstract: A method for manufacturing a video magnetic head in which two soft magnetic core halves (2a, 2b) of amorphous metal are connected via a non-magnetic gap (5) and the core halves are bilaterally supported by core supports (3a, 3b; 4a, 4b) of ferrite. The core halves with the core supports are combined to a core compound by melting a thin low melting point glass layer (7) which is sputtered on the core halves. The combination process is effected by means of simultaneous influence of temperature and pressure.Type: GrantFiled: August 24, 1987Date of Patent: December 6, 1988Assignee: U.S. Philips CorporationInventors: Horst Gukkenberger, Karl Eberle, Karola Weigel-Krengel
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Patent number: 4786303Abstract: The method of this invention comprises first forming an assembly of a number N of cored glass fibers, separated by a number M of solid glass fibers. After a row of such alternated cored and solid glass fibers is assembled, a uniform pressure is applied to all sides of the assembly. All of the rectangular glass fibers are selected to have the same thermal properties, characterized especially by having the same softening temperature and the same coefficient of expansion. The entire assembly is inserted in an oven subject to a temperature sufficient to soften the glass and thus fuse the parts together. The assembly is cooled and the glass block is removed from the oven. The block can then be cut into thin nozzle wafers and finished to produce the desired jet nozzles. The method may use glass fibers made of two types of glass. The central portion of the fiber comprises a high-temperature glass, this portion surrounding the core.Type: GrantFiled: April 13, 1987Date of Patent: November 22, 1988Assignees: Ricoh Company, Ltd., Ricoh Systems, Inc.Inventor: Marco Padalino
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Patent number: 4746346Abstract: A method for producing an air-tight, heat-resistant plate for a particular use in manufacturing bulbous fluorescent lamp, which comprises: preparing a shaping material by mixing an inorganic filler composed of alumina powder and silica powder in a specified compositional ratio, and glass powder having a thermal expansion coefficient of 8.5 to 11.5.times.10.sup.-6 /.degree.C., both inorganic filler and glass material being blended at a predetermined ratio then, forming the shaping material into a shaped product of any desired configuration by a known shaping method; thereafter heating this shaped body to a temperature, at which the glass powder used becomes molten and fused, thereby rendering it to be a burned body.Type: GrantFiled: January 27, 1987Date of Patent: May 24, 1988Assignee: Mitsubishi Denki Kabushiki KaishaInventors: Tadaki Murakami, Kiyoshi Takata, Kazuharu Kato, Kazuo Okahashi, Hitoshi Yamazaki, Takao Takeda
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Patent number: 4710673Abstract: An electron tube comprising a window having a radiation-sensitive layer. The window is laid on a bearing surface of an envelope normal to the tube axis. There is no sealing material in the seam between the bearing surface and the window. The seam is sealed hermetically by a mass of indium or an indium alloy in which a metal wire is embedded along the circumference of the seam. The wire can be soldered with indium or an indium alloy. The seal is made by locally melting the indium or the indium alloy by a heated ultrasonically vibrating heat transfer member. The heat transfer member traverses the circumference of the seam.Type: GrantFiled: June 25, 1986Date of Patent: December 1, 1987Assignee: U.S. Philips CorporationInventor: Gerardus A. H. M. Vrijssen
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Patent number: 4685945Abstract: A method of achieving long-term stability in the transmission properties of high purity low-hydroxyl vitreous silica optical waveguide fibers having preexisting peroxy linkages disposed therein in which the peroxy linkages are exposed to deuterium molecules and the reaction between the deuterium molecules and the peroxy linkages to form deuteroxyl group is substantially enhanced by simultaneously or sequentially exposing the permeated fibers to a light source having an intensity of at least 10 Lambert Units and a wave length of from the short wave length absorption edge of vitreous silica up to about 650 nanometers until the absorption at 1.7 micrometers reaches saturation.Type: GrantFiled: April 21, 1986Date of Patent: August 11, 1987Inventor: Friedemann Freund
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Patent number: 4685200Abstract: A technique for enclosing microelectronic circuit elements in hermetically sealed packages comprising a planar ceramic substrate with a box-like ceramic cover sealed thereto by a fused glass coating. The glass sealant is applied to the substrate in the form of a paste which thereafter is fired at high temperature and cooled to produce a smooth glass coating. With the cover in place on the substrate, the glass coating is remelted by heat developed by infra-red radiation developed by four line-focussed radiant heaters at the four sides of the package. The radiation of each heater is focussed at the interface line between the cover and the substrate. Because the radiant heat is concentrated along the interface line, unwanted heat transfer into the package is minimized, and the temperature is prevented from rising sufficiently to damage heat-sensitive elements.Type: GrantFiled: January 18, 1982Date of Patent: August 11, 1987Assignee: Analog Devices, IncorporatedInventor: Delip R. Bokil
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Patent number: 4682849Abstract: There are disclosed an optical fiber junction device and a method of making the same. The method comprises the steps of providing a central inner pipe or rod of glass, arranging a plurality of optical fibers around the inner pipe or rod, and externally heating the optical fibers and the central inner pipe to form a thermally fused assembly having cores of a sectorial cross section. The inner pipe may include a tapered portion having a reduced diameter. The optical fibers may comprise optical fiber junction units each composed of a plurality of optical fibers.Type: GrantFiled: February 19, 1986Date of Patent: July 28, 1987Assignee: Showa Electric Wire & Cable Co. Ltd.Inventors: Nobuo Kowata, Naoshige Sasano
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Patent number: 4680075Abstract: An integrated circuit package is fabricated by assembling a stack which is comprised of a plurality of thin flat epoxy-glass layers, adhesive layers between the epoxy-glass layers, and a staircase-shaped cavity. This cavity extends from an outer epoxy-glass layer to an internal epoxy-glass layer and goes parallel along a portion of the flat surface of the internal epoxy-glass layer and then penetrates through it. Conductors lie on the internal epoxy-glass layer, including bonding pads on the flat surface portions. After the stack is assembled, a plug is inserted into its cavity. This plug is thermoplastic; and it fits snugly into the cavity and extends over a larger area outside the cavity. While the plug is in the cavity, the stack is laminated at a temperature and pressure which causes the plug to soften and conform to the exact shape of the cavity. This dams the adhesive from flowing onto the bonding pads.Type: GrantFiled: January 21, 1986Date of Patent: July 14, 1987Assignee: UNISYS CorporationInventors: Norman E. McNeal, Richard A. Nagy
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Patent number: 4676817Abstract: A rugged scintillation detector uses a hermetically sealed window assembly welded or otherwise bonded to the detector housing. A method and apparatus useful in forming a reproducible hermetic seal between the glass and an annular metal retaining ring is described. The glass and ring are chosen so that the ring diameter is slightly larger than that of the glass at room temperature. A thin layer of frit at the interface ensures a very tight mechanical seal, and a surface layer of chromium oxide on the ring ensures a secure chemical bond. The assembly device uses pressure and counterpressure to uniformly and reproducibly assemble the glass window into the retainer ring at elevated temperatures.Type: GrantFiled: August 25, 1986Date of Patent: June 30, 1987Assignee: Harshaw/Filtrol PartnershipInventors: Ramesh C. Tailor, Bradley K. Utts
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Method of manufacturing a hermetically sealed component housing, in particular for quartz resonators
Patent number: 4676816Abstract: The invention relates to a method of manufacturing a hermetically sealed component housing having a tray-like upper portion and a tray-like lower portion of an insulating material, which portions are hermetically sealed to each other, the lead-in conductors to the component being accommodated in the junction between the upper and lower portion of the housing. The lead-in conductors to the component are so formed that they partially extend in a longitudinal direction between the connecting surfaces of the upper portion and the lower portion of the housing, and the housing portions with the intermediate lead-in conductors are interconnected by heating in a high-frequency field the individual lead-in conductors, which are interconnected to form an annular conductor, until the housing portions are interconnected.Type: GrantFiled: June 3, 1986Date of Patent: June 30, 1987Assignee: U.S. Philips CorporationInventor: Franz Fick -
Patent number: 4669814Abstract: An optical fiber comprising a core and cladding having different refractive indices and forming a single-mode guiding region, the core having a non-circular cross-section defining two transverse orthogonal axes which, in combination with the different refractive indices, permit the de-coupling of waves polarized along the axes. The guiding region is located sufficiently close to the surface of the fiber along a selected length of the fiber, to allow coupling to a guided wave. The outer surface of the fiber has a non-circular cross-section with a predetermined geometric relationship to the guiding region and the orthogonal transverse axes so that the location of the guiding region and the orientation of the axes can be ascertained from the geometry of the outer surface.Type: GrantFiled: October 29, 1985Date of Patent: June 2, 1987Assignee: Andrew CorporationInventor: Richard B. Dyott
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Patent number: 4668264Abstract: A method of making an optical fiber, comprising the steps of forming an optical preform having a core and a cladding with different refractive indices, the core being offset from the geometric center of the preform and having a non-circular cross-section defining two transverse orthogonal axes, the core having a longer transverse dimension along one of the orthogonal axes than along the other of the axes for guiding two fundamental modes, which, in combination with the different refractive indices, permits the de-coupling of waves polarized along the axes, the outer surface of the preform having a non-circular cross-section forming an indexing surface with a predetermined geometric relationship to the core and the orthogonal transverse axes so that the location of the core and the orientation of the axes can be ascertained from the geometry of the outer surface, and drawing an optical fiber from the preform with the drawing rate and the temperature of the preform being controlled to produce a fiber with a croType: GrantFiled: September 30, 1985Date of Patent: May 26, 1987Assignee: Andrew CorporationInventor: Richard B. Dyott
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Patent number: 4666548Abstract: A process for making a fluorescent display device capable of accomplishing the mass production of a tipless fluorescent display device with good reliability and productivity is disclosed. The process is adapted to carry out, in a single chamber, a step of hermetically bonding an anode substrate and a casing together to form a hermetic envelope and a step of sealing the envelope in vacua.Type: GrantFiled: March 12, 1985Date of Patent: May 19, 1987Assignee: Futaba Denshi Kogyo Kabushiki KaishaInventors: Goro Eto, Shigeo Itoh, Mikio Yokoyama, Takeshi Tonegawa
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Patent number: 4661079Abstract: An image intensifier tube and a method of making same are disclosed wherein veiling glare caused by the amplification of off-axis light is reduced. A face plate is formed from a fused assembly of a glass rod having a low reflective, light absorbing layer thereon, a cladding tube and a jacket tube. The fused assembly is then cut into wafer-shaped slices and the ends polished.Type: GrantFiled: June 26, 1985Date of Patent: April 28, 1987Assignee: ITT CorporationInventors: James W. Harris, Ronald A. Sink
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Patent number: 4650509Abstract: A method for making a fluid lamp assembly which includes a fiberglass wick, consisting of approximately 100 individual fibers in a bundle, is inserted in a glass tube, adjusted with its tip a desired distance above opening, and fused in place by heating to 600 degrees Centigrade for 20 minutes. Fusing temperatures of from about 500 to 600 degrees Centigrade may be employed, for times of from about 10 minutes to about one hour, with a longer fusing time employed with lower temperatures. This provides a premanent wick that is not consumed in use of the lamp assembly.Type: GrantFiled: February 19, 1985Date of Patent: March 17, 1987Inventor: Willy Vanbragt
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Patent number: 4643532Abstract: Disclosed is an electric field-assisted method for bonding one glass (or other inorganic insulator) body, typically a plate, to a similar body, such that the two bodies are spaced apart. The interior volume of such a composite body is advantageously filled with liquid crystal material, to produce a liguid crystal display cell. The method comprises forming a patterned layer of an appropriate bonding material (e.g., Al, Ge, Si, preferably Si) on a major surface of one of the two insulator bodies, placing a major surface of the second insulator body into contact with the bonding material, heating at least the second body to a bonding temperature (typically in the range 250.degree.-600.degree. C.), and applying a voltage (e.g., 500-1500 volt DC, the second body negative) across the thus formed sandwich.Type: GrantFiled: June 24, 1985Date of Patent: February 17, 1987Assignee: AT&T Bell LaboratoriesInventor: Rafael N. Kleiman
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Patent number: 4640700Abstract: A method for attaching a stud pin to a cathode ray tube panel is disclosed, which employs as a frit slurry to attach the stud pin to the cathode ray tube panel, a crystalizing solder glass, a binder and a solvent having a viscosity higher than 10 cps and a boiling point ranging from 200.degree. C. to 320.degree. C.Type: GrantFiled: July 3, 1985Date of Patent: February 3, 1987Assignee: Sony CorporationInventors: Shinzo Takei, Junji Yokoyama, Makoto Takagi
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Patent number: 4629486Abstract: Disclosed are the processes of how to fabricate the microchannel plate for use in electron image intensifying by using a number of glass pipes, each consisting of glass material containing oxides of alkaline earth metals, i.e., magnesium oxide (MgO) or a mixture of magnesium oxide (MgO) and calcium oxide (CaO).Type: GrantFiled: November 18, 1985Date of Patent: December 16, 1986Assignee: Hamamatsu Photonics Kabushiki KaishaInventors: Toshiyuki Uchiyama, Takeo Sugawara, Chiyoshi Okuyama, Yoshihiko Mizushima
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Patent number: 4622084Abstract: A method of sealing an electron gun mount of a cathode-ray tube to a back section thereof comprises the steps of applying a glass frit between an edge of the back section and the mount where the sealing is to be effected, heating the glass frit to a temperature sufficient to cause the frit to become vitreous, thereby sealing the mount to the back section, and flowing a gas containing a reducing agent past the electron gun during the heating step.Type: GrantFiled: January 29, 1985Date of Patent: November 11, 1986Inventors: Kern K. N. Chang, Anthony R. Cooke, Kurt J. Sonneborn
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Patent number: 4612028Abstract: A polarization-preserving single mode fiber coupler, fabricated by a method which does not require mutually aligning the fiber polarization axes provided the actual misalignment angle is not close to 90.degree.. The protective jackets from two or more polarization-preserving single mode birefringent fibers are partially removed and the fibers are twisted around each other to bring them into contact over the jacketless region and provide a coupling length that is large compared to the birefringent beat length of the fibers. Next, the cladding layers of the fibers in the contacting region are partially etched without degrading the birefringent beat length over their coupling length. Then, the etched region is heated to the softening point of the fibers while axial tension is applied to taper and fuse the etched region until a desired coupling of the fibers is achieved. Finally, a mechanical supporting structure is added to the tapered and fused region of the fibers.Type: GrantFiled: October 7, 1985Date of Patent: September 16, 1986Assignee: The United States of America as represented by The Secretary of the NavyInventors: Moges Abebe, William K. Burns, Carl A. Villarruel
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Patent number: 4590492Abstract: A high resolution printing head for a line printer using photographic recording medium has a plurality of modules connected to form a two dimensional printing array. Each module has three fiber optic ribbons bonded together to form a staggered array of fibers. An apertured mask is photolithographically attached to the two dimensional array so that there is one aperture positioned over each fiber. The aperture has a cross-section less than the fiber so there is no overlapping of output light from each fiber and the apertures are also staggered so that a three fold increase in line density is achieved over conventional single ribbon arrays.Type: GrantFiled: June 7, 1983Date of Patent: May 20, 1986Assignee: The United States of America as represented by the Secretary of the Air ForceInventor: Michael J. Meier
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Patent number: 4585972Abstract: An arc discharge lamp is provided using sealing compositions comprising mainly Al.sub.2 O.sub.3 --SiO.sub.2 --MgO. Preferred compositions include between 25 to 28% by weight of MgO and 13 to 21% by weight of Al.sub.2 O.sub.3 since these have lower melting points than others in the group. Additives of B.sub.2 O.sub.3, nucleating agents and HfO.sub.2 and other rare earth oxides are preferred. The sealing compositions are used to seal end closure members of alumina or CERMET to ceramic arc tubes for use in discharge lamps. The compositions are selected to have linear expansion co-efficients compatible with the materials of the end closures and arc tubes. The methods described give scaling times of between 3 and 4 minutes.Type: GrantFiled: January 10, 1985Date of Patent: April 29, 1986Assignee: Thorn EMI LimitedInventor: Peter Hing
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Patent number: 4545840Abstract: A semiconductor die attach adhesive is provided which is formed of a plurality of spacers formed in a suspension of silver filled glass. In one embodiment of this invention, the spacers are spheres. The spacers utilized in one embodiment of this invention have a melting temperature below the temperature at which the solvents are evaporated from the die attach adhesive. In this manner, as the solvents are driven from the silver filled glass during the die attach operation, thus causing the volume of the silver filled glass to decrease, the spacers utilized in this invention partially melt, thus decreasing their thickness. This decreased thickness of the spacers decreases the separation between the die and the substrate, thus preventing the formation of voids within the die attach adhesive. In one embodiment, the spacers are formed of a lead/tin alloy.Type: GrantFiled: March 8, 1983Date of Patent: October 8, 1985Assignee: Monolithic Memories, Inc.Inventors: Robert Newman, Fred Johnson
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Patent number: 4532171Abstract: Each of the multifibers which are stacked in parallel and compressed together to form a boule during the process of manufacturing microchannel plates is hexagonal in cross-section, and single fibers having thicker channel walls are placed at corners of the hexagon in order to prevent damages to corner fibers which are exposed to the strongest external forces.Type: GrantFiled: December 5, 1983Date of Patent: July 30, 1985Assignee: Varian Associates, Inc.Inventor: John T. Balkwill
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Patent number: 4529459Abstract: An adhesive agent having, as its active components, copper sulfide and at least one member selected from the group consisting of alumina, silica, and kaoline enables the opposed surfaces of two oxide-type ceramic articles to be joined to each other with high adhesive strength, this fast union being accomplished by interposing the adhesive agent between the opposed surfaces of the ceramic articles and heating the adhesive agent to a temperature of not less than 1000.degree. C.Type: GrantFiled: October 18, 1983Date of Patent: July 16, 1985Assignees: Agency of Industrial Science & Technology, Ministry of International Trade & IndustryInventors: Yoshihiro Ebata, Makoto Kinoshita, Ryozo Hayami
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Patent number: 4526598Abstract: A filamentary gathering apparatus, apparatus for forming filaments into a gathered bundle of filaments, and a method of forming gathered filaments into a bundle of filaments according to the present invention result in a reduced tendency of the filaments and/or gathered filaments to wrap around the gathering apparatus. The gathering apparatus is a cylindrically shaped gathering shoe having a height much smaller than the diameter of the shoe and having an annular recess providing for a peripheral groove in the shoe. The groove has a plurality of holes extending radially toward the center of the gathering shoe and up the side of the groove. The apparatus for forming filaments has a fiber forming means, an applicator, one or more rotating gathering shoes and a winder mechanism. The one or more rotatable gathering shoes have the groove with radially extending holes.Type: GrantFiled: December 30, 1983Date of Patent: July 2, 1985Assignee: PPG Industries, Inc.Inventors: Walter J. Reese, George T. Salego
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Patent number: 4486257Abstract: A composition of at least one member selected from the group consisting of sodium fluoride and calcium fluoride and optionally containing kaolin is powerful adhesive for ceramic articles which is used by interposing the adhesive intimately between the opposed surfaces for union of the ceramic articles and heating the adhesive to a temperature equal to or higher than the decomposition temperature of the fluoride used.Type: GrantFiled: September 7, 1982Date of Patent: December 4, 1984Assignee: Agency of Industrial Science & Technology Ministry of International Trade & TechnologyInventors: Yoshihiro Ebata, Saburo Kose, Makoto Kinoshita, Tsutomu Ueno
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Patent number: 4484972Abstract: Adhesion of two silicon nitride parts is accomplished by interposing a layer of calcium fluoride or a mixture of calcium fluoride with kaoline between the two silicon nitride parts and heating the resultant interposed layer.Type: GrantFiled: August 12, 1982Date of Patent: November 27, 1984Assignee: Agency of Industrial Science & Technology Ministry of International Trade & IndustryInventors: Yoshihiro Ebata, Nobuyuki Tamari, Makoto Kinoshita, Yasuo Toibana
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Patent number: 4482579Abstract: For supplying frit slurry to the sealing surface of a funnel portion of a cathode ray tube, air under pressure, preferably saturated with a solvent for the frit slurry, is supplied to a vessel containing the frit slurry, and the latter is transported by the air under pressure out of an outlet of the vessel and through a hose or hoses for deposit on the sealing surface. The flow of frit slurry is regulated by a valve between the vessel outlet and the hoses. The frit slurry contained in the vessel is stirred continuously to maintain a substantially constant slurry viscosity as the slurry leaves the vessel outlet.Type: GrantFiled: January 17, 1983Date of Patent: November 13, 1984Assignee: Sony CorporationInventors: Makoto Fujii, Akira Ikuzawa, Edward C. Sullivan
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Patent number: 4482418Abstract: A bonding method which uses two solutions, one being anionic and the other being cationic, to lay down alternating layers of particles of accurate dimension onto members which are to be bonded. Thereafter, the layers are placed in contact, and the members are bonded together by diffusion bonding techniques.Type: GrantFiled: August 17, 1983Date of Patent: November 13, 1984Assignee: International Business Machines CorporationInventor: Eugene B. Rigby
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Patent number: 4452624Abstract: A method for making an airtight seal between a pair of insulator elements, uch as glass plates, without destroying any fine structure etched in the insulator elements. A thin metal film is deposited on one of the elements to be sealed and then placed in intimate contact with the other element to be sealed. The elements are then heated to a temperature well below their softening point, but high enough to significantly enhance the ion mobility in the insulator. A voltage is applied across the interface and the resulting anodic reaction consumes the film at the interface while producing a strong hermetic bond between the insulator elements.Type: GrantFiled: December 21, 1982Date of Patent: June 5, 1984Assignee: The United States of America as represented by the Secretary of the NavyInventors: Henry Wohltjen, John F. Giuliani
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Patent number: 4447283Abstract: An adhesive having as its active component at least one fluoride selected from the group consisting of alkali metal fluorides except for sodium fluoride and alkaline earth metal fluorides except for calcium fluoride or a combination of the aforementioned at least one fluoride with kaolin and an adhesive having as its active component a combination of at least one member selected from the group consisting of yttria and alkaline earth metal compounds except for fluorides, an alkali metal fluoride, and at least one member selected from the group consisting of kaolin and alkaline earth metal fluorides both provide fast adhesion easily between two ceramic articles by a method which comprises the steps of interposing the adhesive between the ceramic articles and heating the ceramic articles with the adhesive therebetween to a temperature equal to or higher than the decomposition temperature of the fluoride in the adhesive.Type: GrantFiled: September 16, 1982Date of Patent: May 8, 1984Assignees: Agency of Industrial Science and Technology, Ministry of International Trade and IndustryInventors: Yoshihiro Ebata, Saburo Kose, Ryozo Hayami
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Patent number: 4433962Abstract: A process for making an envelope for a projection televised tube, that includes a spherically curved electronic beam target surface spaced away from the neck of the tube, a larger reflective surface spherically curved concentrically with the target surface on an end plate located close to the tube neck, a target support that preferably constitutes a face plate for the envelope, and a hollow cylindrical spacer member for closing the side of the tube envelope and for holding the target support accurately spaced from the reflective surface, includes making the ends of the cylindrical member and the abutting peripheral surfaces of the end plate and target concentric with the target and reflective surfaces, so that slight relative lateral motion of the parts during assembly and bonding will not affect tube projection optics, while the relationship between the target and reflective surfaces is precisely maintained in spaced concentric relationship.Type: GrantFiled: September 7, 1982Date of Patent: February 28, 1984Inventor: Henry E. Kloss
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Patent number: 4431694Abstract: Each of the multifibers which are stacked in parallel and compressed together to form a boule during the process of manufacturing microchannel plates is hexagonal in cross-section, and single fibers having thicker channel walls are placed at corners of the hexagon in order to prevent damages to corner fibers which are exposed to the strongest external forces.Type: GrantFiled: May 3, 1982Date of Patent: February 14, 1984Assignee: Varian Associates, Inc.Inventor: John T. Balkwill
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Patent number: 4428763Abstract: A method of transfer molding fiber reinforced glass composite articles is described. The method has particular utility for providing strength in a particular direction in such a composite. The fibers are aligned in a mold cavity in a predetermined orientation to provide composite strength in particular directions, and a glass billet is heated and transferred to the mold. The article is cooled and removed from the mold producing a composite having longitudinal strength along the axes of the aligned fibers in the composite.Type: GrantFiled: May 25, 1982Date of Patent: January 31, 1984Assignee: United Technologies CorporationInventor: George K. Layden
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Patent number: 4427430Abstract: In the thermal cycles utilized for frit sealing glass members together for forming a glass housing and for baking-out such housing, shielding means are provided to protect and shield those portions of the glass members having multiple surfaces which would otherwise be exposed to excess thermal energy, from such thermal energy so as to inhibit the formation of detrimental thermal gradients within the housing structure.Type: GrantFiled: March 25, 1982Date of Patent: January 24, 1984Assignee: Corning Glass WorksInventors: Roger A. Allaire, Edwin J. Simonson
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Patent number: 4426673Abstract: A capacitive pressure transducer comprising a pair of disc shaped members having planar surfaces made from an insulator material, one of the members being several times thinner than the other plate and flexible and constituting a diaphragm and the other thicker plate constituting a stationary plate. A thin conductive film is formed on the surface of each of the members to form the plates of the capacitor. A glass frit is applied on the marginal edge of each member and when the members are held in adjacent relationship, the assembly is fired to seal the two members together while spacing them a predetermined distance apart so that the two conductive plates are opposite each other and are separated by an open gap of a predetermined distance, the two conductive plates being insulated one from the other. Leads are electrically connected to the conductive plate of each disc through the fused glass frit.Type: GrantFiled: March 13, 1980Date of Patent: January 17, 1984Assignee: Kavlico CorporationInventors: Robert L. Bell, Robert Willing, Fred Kavli
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Patent number: 4417913Abstract: An improved lead-free glass or glass plus alumina ceramic sealing material composition for making compression glass sealed electrical leads in semiconductor device packages is described wherein the improved sealing material consists essentially of the following range of ingredients, by weight percent:______________________________________ Pb-Free Glass Element Composition Range Glass Plus Alumina ______________________________________ SiO.sub.2 40-50 34-50 Al.sub.2 O.sub.3 2-12 2-25 K.sub.2 O 2-6 2-6 Na.sub.2 O 5-9 4-9 Li.sub.2 O 2-6 2-6 CaO 0-4 0-4 ZnO 5-12 4-12 BaO 1-5 1-5 TiO.sub.2 2-6 2-6 B.sub.2 O.sub.Type: GrantFiled: May 26, 1982Date of Patent: November 29, 1983Assignee: Motorola, Inc.Inventors: Earl K. Davis, Rafael Landron, Scot W. Taylor
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Patent number: 4414282Abstract: A glass ceramic composition prepared by subjecting a glass composition comprising, by weight, 65-80% SiO.sub.2, 8-16%, Li.sub.2 O, 2-8% , Al.sub.2 O.sub.3, 1-8% K.sub.2 O, 1-5% P.sub.2 O.sub.5 and 1.5-7% B.sub.2 O.sub.3, to the following processing steps of heating the glass composition to a temperature sufficient to crystallize lithium metasilicate therein, holding the glass composition at a temperature and for a time period sufficient to dissolve the lithium metasilicate therein thereby creating cristobalite nucleii, cooling the glass composition and maintaining the composition at a temperature and for a time period sufficient to recrystallize lithium metasilicate therein, and thermally treating the glass composition at a temperature and for a time period sufficient to cause growth of cristobalite and further crystallization of lithium metasilicate producing a glass ceramic composition having a specific thermal expansion coefficient and products containing said composition.Type: GrantFiled: April 19, 1982Date of Patent: November 8, 1983Assignee: The United States of America as represented by the United States Department of EnergyInventors: Howard L. McCollister, Scott T. Reed
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Patent number: 4414009Abstract: A glass faceplate having a central area of required useful diameter surrounded by a narrow ring of opaque glass and an outer glass mounting flange. Light entering the flange or ring is prevented from reaching the central area as stray light or glare in the system and spurious reflections at the interface of the ring and central area are minimized by a refractive index match of the two innermost glasses.Type: GrantFiled: June 11, 1982Date of Patent: November 8, 1983Assignee: Warner Lambert Technologies, Inc.Inventor: Walter P. Siegmund
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Patent number: 4412854Abstract: A method of making fiber reinforced glass composite articles of complex shape is disclosed which overcomes problems associated with the debulking process common with such procedures. Sheets of woven or non-woven fiber reinforcement are impregnated with a layer of thermoplastic binder containing glass powder and optionally, additional carrier liquid. The thus treated sheets are then dried and cut into a plurality of preforms corresponding to the predetermined pattern of the article being fabricated. The thus treated preforms are then stacked in a mold and warm molded to form an intermediate article of near net shape, during which molding operation much of the ultimate debulking occurs. The intermediate article is then hot pressed to form the final fiber reinforced glass matrix article of net shape and high strength and toughness. These multiple heating steps may also be accomplished in a single molding operation.Type: GrantFiled: May 25, 1982Date of Patent: November 1, 1983Assignee: United Technologies CorporationInventor: George K. Layden
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Patent number: 4412963Abstract: The invention provides a method of producing discharge lamp arc tubes of ceramic material complete with metal cermet end closure members using initially incompletely fired sintered components and a sealing composition selected from silica, alumina and magnesia in proportions such that the composition falls within the accompanying ternary phase diagram BCDEFXYZPQ. The sealing compositions may also contain up to 5% by weight of nucleating agents such as phosphorous pentoxide, rare earth oxides, titania, zirconia or chromia. The inclusion of up to 5% by weight of boric oxide improves the flow characteristics and up to 10% by weight of Y.sub.2 O.sub.3, Yb.sub.2 O.sub.3, La.sub.2 O.sub.3, Dy.sub.2 O.sub.3, Eu.sub.2 O.sub.3, HfO.sub.2 improves the thermal and mechanical properties of the seals. The invention eliminates the need to make a first end seal by separate sintering and sealing operations.Type: GrantFiled: December 18, 1981Date of Patent: November 1, 1983Inventor: Peter Hing
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Patent number: 4388668Abstract: A capacitive pressure transducer comprising a pair of disc shaped members having planar surfaces made from an insulator material, one of the members being several times thinner than the other plate and flexible and constituting a diaphragm and the other thicker plate constituting a stationary plate. A thin conductive film is formed on the surface of each of the members to form the plates of the capacitor. A glass frit is applied on the marginal edge of each member and when the members are held in adjacent relationship, the assembly is fired to seal the two members together while spacing them a predetermined distance apart so that the two conductive plates are opposite each other and are separated by an open gap of a predetermined distance, the two conductive plates being insulated one from the other. Leads are electrically connected to the conductive plate of each disc through the fused glass frit.Type: GrantFiled: December 3, 1979Date of Patent: June 14, 1983Assignee: Kaylico CorporationInventors: Robert L. Bell, Robert Willing, Fred Kavli
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Patent number: 4385092Abstract: A macroboule is disclosed, formed of a bundle of hollow channel elements of fusible material and of different internal diameters. They are arranged with the elements of smallest diameter positioned in the center of the bundle and those of largest internal diameter constituting the outer row of the bundle with uniform or step by step graduation between these extremes. The macroboule is useful for forming a channel multiplier.Type: GrantFiled: September 24, 1965Date of Patent: May 24, 1983Assignee: Ni-Tec, Inc.Inventor: Joseph Singer, Jr.
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Patent number: 4353966Abstract: A process of bonding a plurality of thermally stable, high strength graphite fiber reinforced glass matrix composite materials is described. The process comprises applying to the surface of at least one of the composite materials to be bonded, a mixture of low softening point glaze such as high lead oxide containing glaze, a high melting point low coefficient of thermal expansion material such as beta-spodumene and colloidal silica followed by hot pressing the composite materials to be bonded together. The resultant bonded articles and the glass compositions particularly adapted for this bonding process are also described.Type: GrantFiled: December 12, 1980Date of Patent: October 12, 1982Assignee: United Technologies CorporationInventors: Elias Snitzer, James F. Bacon
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Patent number: 4351104Abstract: In the method for manufacturing annular portions of magnetic heads, a gap between the confronting end surfaces of the magnetic heads is filled with glass. In one of the conventional processes, the glass is sucked into the gap by a capillary action of the gap, but bubbles are liable to form in the glass. The method according to the present invention comprises a step of heating the glass to a relatively low temperature capable of causing the glass to be flowable and applying a centrifugal force to the glass being heated in a rotatable support of a heating furnace. As a result of the centrifugal force, the tendency to form bubbles is considerably reduced as compared with the conventional methods.Type: GrantFiled: November 10, 1980Date of Patent: September 28, 1982Assignee: TDK Electronics Co., Ltd.Inventors: Kiyoshi Klagane, Masao Kakizaki
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Patent number: 4350514Abstract: When fusing together a panel having a fluorescent film and a metallic reflective film, and a funnel with an electroconductive film in a baking furnace for manufacturing a cathode ray tube, oxygen containing air is forced into the furnace.Type: GrantFiled: May 14, 1981Date of Patent: September 21, 1982Assignee: Hitachi, Ltd.Inventors: Masatoshi Akiyama, Shigeki Kitamura, Junichi Tetsu, Koichi Nakazato
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Patent number: 4350515Abstract: A glass edge multiple glazed unit having fillets of substantially uniform thickness is produced by the application of heat to marginal edge portions of adjacent sheets, followed by a delay sufficient to establish a substantially uniform, greater than fusing temperature condition in the body of fillet-forming glass. The fused sheets are thereafter drawn apart a preselected distance to a spaced-apart face-to-face relation to form a glass-edge multiple glazed unit.Type: GrantFiled: January 30, 1981Date of Patent: September 21, 1982Assignee: PPG Industries, Inc.Inventor: John L. Stewart