By Or With Coating At Joint Interface Of A Formed Part Prior To Bonding Patents (Class 65/43)
  • Patent number: 4818264
    Abstract: A multicapillary gas chromatography column comprising a bundle of single capillary columns each of which have essentially the same internal diameter and which are coated with essentially the same thickness of essentially the same stationary phase so that each column has essentially the same standard retention factor. A method of producing such a column is to cut a single fused silica capillary column into a number of essentially equal lengths and then to bundle the lengths together. Each bundle end can then be inserted into, for example, a graphite ferrule and then the multicapillary column can be conventionally installed into a gas chromatograph. The multicapillary column of the invention has the injection, detection and sample capacity advantages of a relatively large diameter capillary column with the speed and resolving power of a relatively narrow diameter capillary column.
    Type: Grant
    Filed: April 30, 1987
    Date of Patent: April 4, 1989
    Assignee: The Dow Chemical Company
    Inventor: Marsha L. Langhorst
  • Patent number: 4792348
    Abstract: A method of producing a joint between a beta-alumina electrolyte tube and alpha-alumina flange with a glass bonding agent in a solid annular bead form devoid of additives such as a coupling agent or the like capable of being heated when subjected to microwave energy which comprises utilizing in the heating step a source of microwave energy rather than a gas flame or electrical resistance heat source so as to heat the beta-alumina tube by microwave energy for a time period sufficient to enable the heat generated in the beta-alumina tube to be conducted to glass bead and the alpha-alumina flange and heat the glass bead to a temperature above the glass deformation point, and allowing the tube to cool to solidify the glass bead in intimately penetrating relation to the surfaces of the beta-alumina tube and alpha-alumina flange engaged thereby so that the glass forms a bond between the beta-alumina tube and the alpha-alumina flange characterized by a fusion of the glass within the engaged beta-alumina and alpha-al
    Type: Grant
    Filed: March 2, 1987
    Date of Patent: December 20, 1988
    Assignee: Powerplex Technologies, Inc.
    Inventor: Alina V. Pekarsky
  • Patent number: 4788762
    Abstract: A method for manufacturing a video magnetic head in which two soft magnetic core halves (2a, 2b) of amorphous metal are connected via a non-magnetic gap (5) and the core halves are bilaterally supported by core supports (3a, 3b; 4a, 4b) of ferrite. The core halves with the core supports are combined to a core compound by melting a thin low melting point glass layer (7) which is sputtered on the core halves. The combination process is effected by means of simultaneous influence of temperature and pressure.
    Type: Grant
    Filed: August 24, 1987
    Date of Patent: December 6, 1988
    Assignee: U.S. Philips Corporation
    Inventors: Horst Gukkenberger, Karl Eberle, Karola Weigel-Krengel
  • Patent number: 4786303
    Abstract: The method of this invention comprises first forming an assembly of a number N of cored glass fibers, separated by a number M of solid glass fibers. After a row of such alternated cored and solid glass fibers is assembled, a uniform pressure is applied to all sides of the assembly. All of the rectangular glass fibers are selected to have the same thermal properties, characterized especially by having the same softening temperature and the same coefficient of expansion. The entire assembly is inserted in an oven subject to a temperature sufficient to soften the glass and thus fuse the parts together. The assembly is cooled and the glass block is removed from the oven. The block can then be cut into thin nozzle wafers and finished to produce the desired jet nozzles. The method may use glass fibers made of two types of glass. The central portion of the fiber comprises a high-temperature glass, this portion surrounding the core.
    Type: Grant
    Filed: April 13, 1987
    Date of Patent: November 22, 1988
    Assignees: Ricoh Company, Ltd., Ricoh Systems, Inc.
    Inventor: Marco Padalino
  • Patent number: 4746346
    Abstract: A method for producing an air-tight, heat-resistant plate for a particular use in manufacturing bulbous fluorescent lamp, which comprises: preparing a shaping material by mixing an inorganic filler composed of alumina powder and silica powder in a specified compositional ratio, and glass powder having a thermal expansion coefficient of 8.5 to 11.5.times.10.sup.-6 /.degree.C., both inorganic filler and glass material being blended at a predetermined ratio then, forming the shaping material into a shaped product of any desired configuration by a known shaping method; thereafter heating this shaped body to a temperature, at which the glass powder used becomes molten and fused, thereby rendering it to be a burned body.
    Type: Grant
    Filed: January 27, 1987
    Date of Patent: May 24, 1988
    Assignee: Mitsubishi Denki Kabushiki Kaisha
    Inventors: Tadaki Murakami, Kiyoshi Takata, Kazuharu Kato, Kazuo Okahashi, Hitoshi Yamazaki, Takao Takeda
  • Patent number: 4710673
    Abstract: An electron tube comprising a window having a radiation-sensitive layer. The window is laid on a bearing surface of an envelope normal to the tube axis. There is no sealing material in the seam between the bearing surface and the window. The seam is sealed hermetically by a mass of indium or an indium alloy in which a metal wire is embedded along the circumference of the seam. The wire can be soldered with indium or an indium alloy. The seal is made by locally melting the indium or the indium alloy by a heated ultrasonically vibrating heat transfer member. The heat transfer member traverses the circumference of the seam.
    Type: Grant
    Filed: June 25, 1986
    Date of Patent: December 1, 1987
    Assignee: U.S. Philips Corporation
    Inventor: Gerardus A. H. M. Vrijssen
  • Patent number: 4685945
    Abstract: A method of achieving long-term stability in the transmission properties of high purity low-hydroxyl vitreous silica optical waveguide fibers having preexisting peroxy linkages disposed therein in which the peroxy linkages are exposed to deuterium molecules and the reaction between the deuterium molecules and the peroxy linkages to form deuteroxyl group is substantially enhanced by simultaneously or sequentially exposing the permeated fibers to a light source having an intensity of at least 10 Lambert Units and a wave length of from the short wave length absorption edge of vitreous silica up to about 650 nanometers until the absorption at 1.7 micrometers reaches saturation.
    Type: Grant
    Filed: April 21, 1986
    Date of Patent: August 11, 1987
    Inventor: Friedemann Freund
  • Patent number: 4685200
    Abstract: A technique for enclosing microelectronic circuit elements in hermetically sealed packages comprising a planar ceramic substrate with a box-like ceramic cover sealed thereto by a fused glass coating. The glass sealant is applied to the substrate in the form of a paste which thereafter is fired at high temperature and cooled to produce a smooth glass coating. With the cover in place on the substrate, the glass coating is remelted by heat developed by infra-red radiation developed by four line-focussed radiant heaters at the four sides of the package. The radiation of each heater is focussed at the interface line between the cover and the substrate. Because the radiant heat is concentrated along the interface line, unwanted heat transfer into the package is minimized, and the temperature is prevented from rising sufficiently to damage heat-sensitive elements.
    Type: Grant
    Filed: January 18, 1982
    Date of Patent: August 11, 1987
    Assignee: Analog Devices, Incorporated
    Inventor: Delip R. Bokil
  • Patent number: 4682849
    Abstract: There are disclosed an optical fiber junction device and a method of making the same. The method comprises the steps of providing a central inner pipe or rod of glass, arranging a plurality of optical fibers around the inner pipe or rod, and externally heating the optical fibers and the central inner pipe to form a thermally fused assembly having cores of a sectorial cross section. The inner pipe may include a tapered portion having a reduced diameter. The optical fibers may comprise optical fiber junction units each composed of a plurality of optical fibers.
    Type: Grant
    Filed: February 19, 1986
    Date of Patent: July 28, 1987
    Assignee: Showa Electric Wire & Cable Co. Ltd.
    Inventors: Nobuo Kowata, Naoshige Sasano
  • Patent number: 4680075
    Abstract: An integrated circuit package is fabricated by assembling a stack which is comprised of a plurality of thin flat epoxy-glass layers, adhesive layers between the epoxy-glass layers, and a staircase-shaped cavity. This cavity extends from an outer epoxy-glass layer to an internal epoxy-glass layer and goes parallel along a portion of the flat surface of the internal epoxy-glass layer and then penetrates through it. Conductors lie on the internal epoxy-glass layer, including bonding pads on the flat surface portions. After the stack is assembled, a plug is inserted into its cavity. This plug is thermoplastic; and it fits snugly into the cavity and extends over a larger area outside the cavity. While the plug is in the cavity, the stack is laminated at a temperature and pressure which causes the plug to soften and conform to the exact shape of the cavity. This dams the adhesive from flowing onto the bonding pads.
    Type: Grant
    Filed: January 21, 1986
    Date of Patent: July 14, 1987
    Assignee: UNISYS Corporation
    Inventors: Norman E. McNeal, Richard A. Nagy
  • Patent number: 4676817
    Abstract: A rugged scintillation detector uses a hermetically sealed window assembly welded or otherwise bonded to the detector housing. A method and apparatus useful in forming a reproducible hermetic seal between the glass and an annular metal retaining ring is described. The glass and ring are chosen so that the ring diameter is slightly larger than that of the glass at room temperature. A thin layer of frit at the interface ensures a very tight mechanical seal, and a surface layer of chromium oxide on the ring ensures a secure chemical bond. The assembly device uses pressure and counterpressure to uniformly and reproducibly assemble the glass window into the retainer ring at elevated temperatures.
    Type: Grant
    Filed: August 25, 1986
    Date of Patent: June 30, 1987
    Assignee: Harshaw/Filtrol Partnership
    Inventors: Ramesh C. Tailor, Bradley K. Utts
  • Patent number: 4676816
    Abstract: The invention relates to a method of manufacturing a hermetically sealed component housing having a tray-like upper portion and a tray-like lower portion of an insulating material, which portions are hermetically sealed to each other, the lead-in conductors to the component being accommodated in the junction between the upper and lower portion of the housing. The lead-in conductors to the component are so formed that they partially extend in a longitudinal direction between the connecting surfaces of the upper portion and the lower portion of the housing, and the housing portions with the intermediate lead-in conductors are interconnected by heating in a high-frequency field the individual lead-in conductors, which are interconnected to form an annular conductor, until the housing portions are interconnected.
    Type: Grant
    Filed: June 3, 1986
    Date of Patent: June 30, 1987
    Assignee: U.S. Philips Corporation
    Inventor: Franz Fick
  • Patent number: 4669814
    Abstract: An optical fiber comprising a core and cladding having different refractive indices and forming a single-mode guiding region, the core having a non-circular cross-section defining two transverse orthogonal axes which, in combination with the different refractive indices, permit the de-coupling of waves polarized along the axes. The guiding region is located sufficiently close to the surface of the fiber along a selected length of the fiber, to allow coupling to a guided wave. The outer surface of the fiber has a non-circular cross-section with a predetermined geometric relationship to the guiding region and the orthogonal transverse axes so that the location of the guiding region and the orientation of the axes can be ascertained from the geometry of the outer surface.
    Type: Grant
    Filed: October 29, 1985
    Date of Patent: June 2, 1987
    Assignee: Andrew Corporation
    Inventor: Richard B. Dyott
  • Patent number: 4668264
    Abstract: A method of making an optical fiber, comprising the steps of forming an optical preform having a core and a cladding with different refractive indices, the core being offset from the geometric center of the preform and having a non-circular cross-section defining two transverse orthogonal axes, the core having a longer transverse dimension along one of the orthogonal axes than along the other of the axes for guiding two fundamental modes, which, in combination with the different refractive indices, permits the de-coupling of waves polarized along the axes, the outer surface of the preform having a non-circular cross-section forming an indexing surface with a predetermined geometric relationship to the core and the orthogonal transverse axes so that the location of the core and the orientation of the axes can be ascertained from the geometry of the outer surface, and drawing an optical fiber from the preform with the drawing rate and the temperature of the preform being controlled to produce a fiber with a cro
    Type: Grant
    Filed: September 30, 1985
    Date of Patent: May 26, 1987
    Assignee: Andrew Corporation
    Inventor: Richard B. Dyott
  • Patent number: 4666548
    Abstract: A process for making a fluorescent display device capable of accomplishing the mass production of a tipless fluorescent display device with good reliability and productivity is disclosed. The process is adapted to carry out, in a single chamber, a step of hermetically bonding an anode substrate and a casing together to form a hermetic envelope and a step of sealing the envelope in vacua.
    Type: Grant
    Filed: March 12, 1985
    Date of Patent: May 19, 1987
    Assignee: Futaba Denshi Kogyo Kabushiki Kaisha
    Inventors: Goro Eto, Shigeo Itoh, Mikio Yokoyama, Takeshi Tonegawa
  • Patent number: 4661079
    Abstract: An image intensifier tube and a method of making same are disclosed wherein veiling glare caused by the amplification of off-axis light is reduced. A face plate is formed from a fused assembly of a glass rod having a low reflective, light absorbing layer thereon, a cladding tube and a jacket tube. The fused assembly is then cut into wafer-shaped slices and the ends polished.
    Type: Grant
    Filed: June 26, 1985
    Date of Patent: April 28, 1987
    Assignee: ITT Corporation
    Inventors: James W. Harris, Ronald A. Sink
  • Patent number: 4650509
    Abstract: A method for making a fluid lamp assembly which includes a fiberglass wick, consisting of approximately 100 individual fibers in a bundle, is inserted in a glass tube, adjusted with its tip a desired distance above opening, and fused in place by heating to 600 degrees Centigrade for 20 minutes. Fusing temperatures of from about 500 to 600 degrees Centigrade may be employed, for times of from about 10 minutes to about one hour, with a longer fusing time employed with lower temperatures. This provides a premanent wick that is not consumed in use of the lamp assembly.
    Type: Grant
    Filed: February 19, 1985
    Date of Patent: March 17, 1987
    Inventor: Willy Vanbragt
  • Patent number: 4643532
    Abstract: Disclosed is an electric field-assisted method for bonding one glass (or other inorganic insulator) body, typically a plate, to a similar body, such that the two bodies are spaced apart. The interior volume of such a composite body is advantageously filled with liquid crystal material, to produce a liguid crystal display cell. The method comprises forming a patterned layer of an appropriate bonding material (e.g., Al, Ge, Si, preferably Si) on a major surface of one of the two insulator bodies, placing a major surface of the second insulator body into contact with the bonding material, heating at least the second body to a bonding temperature (typically in the range 250.degree.-600.degree. C.), and applying a voltage (e.g., 500-1500 volt DC, the second body negative) across the thus formed sandwich.
    Type: Grant
    Filed: June 24, 1985
    Date of Patent: February 17, 1987
    Assignee: AT&T Bell Laboratories
    Inventor: Rafael N. Kleiman
  • Patent number: 4640700
    Abstract: A method for attaching a stud pin to a cathode ray tube panel is disclosed, which employs as a frit slurry to attach the stud pin to the cathode ray tube panel, a crystalizing solder glass, a binder and a solvent having a viscosity higher than 10 cps and a boiling point ranging from 200.degree. C. to 320.degree. C.
    Type: Grant
    Filed: July 3, 1985
    Date of Patent: February 3, 1987
    Assignee: Sony Corporation
    Inventors: Shinzo Takei, Junji Yokoyama, Makoto Takagi
  • Patent number: 4629486
    Abstract: Disclosed are the processes of how to fabricate the microchannel plate for use in electron image intensifying by using a number of glass pipes, each consisting of glass material containing oxides of alkaline earth metals, i.e., magnesium oxide (MgO) or a mixture of magnesium oxide (MgO) and calcium oxide (CaO).
    Type: Grant
    Filed: November 18, 1985
    Date of Patent: December 16, 1986
    Assignee: Hamamatsu Photonics Kabushiki Kaisha
    Inventors: Toshiyuki Uchiyama, Takeo Sugawara, Chiyoshi Okuyama, Yoshihiko Mizushima
  • Patent number: 4622084
    Abstract: A method of sealing an electron gun mount of a cathode-ray tube to a back section thereof comprises the steps of applying a glass frit between an edge of the back section and the mount where the sealing is to be effected, heating the glass frit to a temperature sufficient to cause the frit to become vitreous, thereby sealing the mount to the back section, and flowing a gas containing a reducing agent past the electron gun during the heating step.
    Type: Grant
    Filed: January 29, 1985
    Date of Patent: November 11, 1986
    Inventors: Kern K. N. Chang, Anthony R. Cooke, Kurt J. Sonneborn
  • Patent number: 4612028
    Abstract: A polarization-preserving single mode fiber coupler, fabricated by a method which does not require mutually aligning the fiber polarization axes provided the actual misalignment angle is not close to 90.degree.. The protective jackets from two or more polarization-preserving single mode birefringent fibers are partially removed and the fibers are twisted around each other to bring them into contact over the jacketless region and provide a coupling length that is large compared to the birefringent beat length of the fibers. Next, the cladding layers of the fibers in the contacting region are partially etched without degrading the birefringent beat length over their coupling length. Then, the etched region is heated to the softening point of the fibers while axial tension is applied to taper and fuse the etched region until a desired coupling of the fibers is achieved. Finally, a mechanical supporting structure is added to the tapered and fused region of the fibers.
    Type: Grant
    Filed: October 7, 1985
    Date of Patent: September 16, 1986
    Assignee: The United States of America as represented by The Secretary of the Navy
    Inventors: Moges Abebe, William K. Burns, Carl A. Villarruel
  • Patent number: 4590492
    Abstract: A high resolution printing head for a line printer using photographic recording medium has a plurality of modules connected to form a two dimensional printing array. Each module has three fiber optic ribbons bonded together to form a staggered array of fibers. An apertured mask is photolithographically attached to the two dimensional array so that there is one aperture positioned over each fiber. The aperture has a cross-section less than the fiber so there is no overlapping of output light from each fiber and the apertures are also staggered so that a three fold increase in line density is achieved over conventional single ribbon arrays.
    Type: Grant
    Filed: June 7, 1983
    Date of Patent: May 20, 1986
    Assignee: The United States of America as represented by the Secretary of the Air Force
    Inventor: Michael J. Meier
  • Patent number: 4585972
    Abstract: An arc discharge lamp is provided using sealing compositions comprising mainly Al.sub.2 O.sub.3 --SiO.sub.2 --MgO. Preferred compositions include between 25 to 28% by weight of MgO and 13 to 21% by weight of Al.sub.2 O.sub.3 since these have lower melting points than others in the group. Additives of B.sub.2 O.sub.3, nucleating agents and HfO.sub.2 and other rare earth oxides are preferred. The sealing compositions are used to seal end closure members of alumina or CERMET to ceramic arc tubes for use in discharge lamps. The compositions are selected to have linear expansion co-efficients compatible with the materials of the end closures and arc tubes. The methods described give scaling times of between 3 and 4 minutes.
    Type: Grant
    Filed: January 10, 1985
    Date of Patent: April 29, 1986
    Assignee: Thorn EMI Limited
    Inventor: Peter Hing
  • Patent number: 4545840
    Abstract: A semiconductor die attach adhesive is provided which is formed of a plurality of spacers formed in a suspension of silver filled glass. In one embodiment of this invention, the spacers are spheres. The spacers utilized in one embodiment of this invention have a melting temperature below the temperature at which the solvents are evaporated from the die attach adhesive. In this manner, as the solvents are driven from the silver filled glass during the die attach operation, thus causing the volume of the silver filled glass to decrease, the spacers utilized in this invention partially melt, thus decreasing their thickness. This decreased thickness of the spacers decreases the separation between the die and the substrate, thus preventing the formation of voids within the die attach adhesive. In one embodiment, the spacers are formed of a lead/tin alloy.
    Type: Grant
    Filed: March 8, 1983
    Date of Patent: October 8, 1985
    Assignee: Monolithic Memories, Inc.
    Inventors: Robert Newman, Fred Johnson
  • Patent number: 4532171
    Abstract: Each of the multifibers which are stacked in parallel and compressed together to form a boule during the process of manufacturing microchannel plates is hexagonal in cross-section, and single fibers having thicker channel walls are placed at corners of the hexagon in order to prevent damages to corner fibers which are exposed to the strongest external forces.
    Type: Grant
    Filed: December 5, 1983
    Date of Patent: July 30, 1985
    Assignee: Varian Associates, Inc.
    Inventor: John T. Balkwill
  • Patent number: 4529459
    Abstract: An adhesive agent having, as its active components, copper sulfide and at least one member selected from the group consisting of alumina, silica, and kaoline enables the opposed surfaces of two oxide-type ceramic articles to be joined to each other with high adhesive strength, this fast union being accomplished by interposing the adhesive agent between the opposed surfaces of the ceramic articles and heating the adhesive agent to a temperature of not less than 1000.degree. C.
    Type: Grant
    Filed: October 18, 1983
    Date of Patent: July 16, 1985
    Assignees: Agency of Industrial Science & Technology, Ministry of International Trade & Industry
    Inventors: Yoshihiro Ebata, Makoto Kinoshita, Ryozo Hayami
  • Patent number: 4526598
    Abstract: A filamentary gathering apparatus, apparatus for forming filaments into a gathered bundle of filaments, and a method of forming gathered filaments into a bundle of filaments according to the present invention result in a reduced tendency of the filaments and/or gathered filaments to wrap around the gathering apparatus. The gathering apparatus is a cylindrically shaped gathering shoe having a height much smaller than the diameter of the shoe and having an annular recess providing for a peripheral groove in the shoe. The groove has a plurality of holes extending radially toward the center of the gathering shoe and up the side of the groove. The apparatus for forming filaments has a fiber forming means, an applicator, one or more rotating gathering shoes and a winder mechanism. The one or more rotatable gathering shoes have the groove with radially extending holes.
    Type: Grant
    Filed: December 30, 1983
    Date of Patent: July 2, 1985
    Assignee: PPG Industries, Inc.
    Inventors: Walter J. Reese, George T. Salego
  • Patent number: 4486257
    Abstract: A composition of at least one member selected from the group consisting of sodium fluoride and calcium fluoride and optionally containing kaolin is powerful adhesive for ceramic articles which is used by interposing the adhesive intimately between the opposed surfaces for union of the ceramic articles and heating the adhesive to a temperature equal to or higher than the decomposition temperature of the fluoride used.
    Type: Grant
    Filed: September 7, 1982
    Date of Patent: December 4, 1984
    Assignee: Agency of Industrial Science & Technology Ministry of International Trade & Technology
    Inventors: Yoshihiro Ebata, Saburo Kose, Makoto Kinoshita, Tsutomu Ueno
  • Patent number: 4484972
    Abstract: Adhesion of two silicon nitride parts is accomplished by interposing a layer of calcium fluoride or a mixture of calcium fluoride with kaoline between the two silicon nitride parts and heating the resultant interposed layer.
    Type: Grant
    Filed: August 12, 1982
    Date of Patent: November 27, 1984
    Assignee: Agency of Industrial Science & Technology Ministry of International Trade & Industry
    Inventors: Yoshihiro Ebata, Nobuyuki Tamari, Makoto Kinoshita, Yasuo Toibana
  • Patent number: 4482579
    Abstract: For supplying frit slurry to the sealing surface of a funnel portion of a cathode ray tube, air under pressure, preferably saturated with a solvent for the frit slurry, is supplied to a vessel containing the frit slurry, and the latter is transported by the air under pressure out of an outlet of the vessel and through a hose or hoses for deposit on the sealing surface. The flow of frit slurry is regulated by a valve between the vessel outlet and the hoses. The frit slurry contained in the vessel is stirred continuously to maintain a substantially constant slurry viscosity as the slurry leaves the vessel outlet.
    Type: Grant
    Filed: January 17, 1983
    Date of Patent: November 13, 1984
    Assignee: Sony Corporation
    Inventors: Makoto Fujii, Akira Ikuzawa, Edward C. Sullivan
  • Patent number: 4482418
    Abstract: A bonding method which uses two solutions, one being anionic and the other being cationic, to lay down alternating layers of particles of accurate dimension onto members which are to be bonded. Thereafter, the layers are placed in contact, and the members are bonded together by diffusion bonding techniques.
    Type: Grant
    Filed: August 17, 1983
    Date of Patent: November 13, 1984
    Assignee: International Business Machines Corporation
    Inventor: Eugene B. Rigby
  • Patent number: 4452624
    Abstract: A method for making an airtight seal between a pair of insulator elements, uch as glass plates, without destroying any fine structure etched in the insulator elements. A thin metal film is deposited on one of the elements to be sealed and then placed in intimate contact with the other element to be sealed. The elements are then heated to a temperature well below their softening point, but high enough to significantly enhance the ion mobility in the insulator. A voltage is applied across the interface and the resulting anodic reaction consumes the film at the interface while producing a strong hermetic bond between the insulator elements.
    Type: Grant
    Filed: December 21, 1982
    Date of Patent: June 5, 1984
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Henry Wohltjen, John F. Giuliani
  • Patent number: 4447283
    Abstract: An adhesive having as its active component at least one fluoride selected from the group consisting of alkali metal fluorides except for sodium fluoride and alkaline earth metal fluorides except for calcium fluoride or a combination of the aforementioned at least one fluoride with kaolin and an adhesive having as its active component a combination of at least one member selected from the group consisting of yttria and alkaline earth metal compounds except for fluorides, an alkali metal fluoride, and at least one member selected from the group consisting of kaolin and alkaline earth metal fluorides both provide fast adhesion easily between two ceramic articles by a method which comprises the steps of interposing the adhesive between the ceramic articles and heating the ceramic articles with the adhesive therebetween to a temperature equal to or higher than the decomposition temperature of the fluoride in the adhesive.
    Type: Grant
    Filed: September 16, 1982
    Date of Patent: May 8, 1984
    Assignees: Agency of Industrial Science and Technology, Ministry of International Trade and Industry
    Inventors: Yoshihiro Ebata, Saburo Kose, Ryozo Hayami
  • Patent number: 4433962
    Abstract: A process for making an envelope for a projection televised tube, that includes a spherically curved electronic beam target surface spaced away from the neck of the tube, a larger reflective surface spherically curved concentrically with the target surface on an end plate located close to the tube neck, a target support that preferably constitutes a face plate for the envelope, and a hollow cylindrical spacer member for closing the side of the tube envelope and for holding the target support accurately spaced from the reflective surface, includes making the ends of the cylindrical member and the abutting peripheral surfaces of the end plate and target concentric with the target and reflective surfaces, so that slight relative lateral motion of the parts during assembly and bonding will not affect tube projection optics, while the relationship between the target and reflective surfaces is precisely maintained in spaced concentric relationship.
    Type: Grant
    Filed: September 7, 1982
    Date of Patent: February 28, 1984
    Inventor: Henry E. Kloss
  • Patent number: 4431694
    Abstract: Each of the multifibers which are stacked in parallel and compressed together to form a boule during the process of manufacturing microchannel plates is hexagonal in cross-section, and single fibers having thicker channel walls are placed at corners of the hexagon in order to prevent damages to corner fibers which are exposed to the strongest external forces.
    Type: Grant
    Filed: May 3, 1982
    Date of Patent: February 14, 1984
    Assignee: Varian Associates, Inc.
    Inventor: John T. Balkwill
  • Patent number: 4428763
    Abstract: A method of transfer molding fiber reinforced glass composite articles is described. The method has particular utility for providing strength in a particular direction in such a composite. The fibers are aligned in a mold cavity in a predetermined orientation to provide composite strength in particular directions, and a glass billet is heated and transferred to the mold. The article is cooled and removed from the mold producing a composite having longitudinal strength along the axes of the aligned fibers in the composite.
    Type: Grant
    Filed: May 25, 1982
    Date of Patent: January 31, 1984
    Assignee: United Technologies Corporation
    Inventor: George K. Layden
  • Patent number: 4427430
    Abstract: In the thermal cycles utilized for frit sealing glass members together for forming a glass housing and for baking-out such housing, shielding means are provided to protect and shield those portions of the glass members having multiple surfaces which would otherwise be exposed to excess thermal energy, from such thermal energy so as to inhibit the formation of detrimental thermal gradients within the housing structure.
    Type: Grant
    Filed: March 25, 1982
    Date of Patent: January 24, 1984
    Assignee: Corning Glass Works
    Inventors: Roger A. Allaire, Edwin J. Simonson
  • Patent number: 4426673
    Abstract: A capacitive pressure transducer comprising a pair of disc shaped members having planar surfaces made from an insulator material, one of the members being several times thinner than the other plate and flexible and constituting a diaphragm and the other thicker plate constituting a stationary plate. A thin conductive film is formed on the surface of each of the members to form the plates of the capacitor. A glass frit is applied on the marginal edge of each member and when the members are held in adjacent relationship, the assembly is fired to seal the two members together while spacing them a predetermined distance apart so that the two conductive plates are opposite each other and are separated by an open gap of a predetermined distance, the two conductive plates being insulated one from the other. Leads are electrically connected to the conductive plate of each disc through the fused glass frit.
    Type: Grant
    Filed: March 13, 1980
    Date of Patent: January 17, 1984
    Assignee: Kavlico Corporation
    Inventors: Robert L. Bell, Robert Willing, Fred Kavli
  • Patent number: 4417913
    Abstract: An improved lead-free glass or glass plus alumina ceramic sealing material composition for making compression glass sealed electrical leads in semiconductor device packages is described wherein the improved sealing material consists essentially of the following range of ingredients, by weight percent:______________________________________ Pb-Free Glass Element Composition Range Glass Plus Alumina ______________________________________ SiO.sub.2 40-50 34-50 Al.sub.2 O.sub.3 2-12 2-25 K.sub.2 O 2-6 2-6 Na.sub.2 O 5-9 4-9 Li.sub.2 O 2-6 2-6 CaO 0-4 0-4 ZnO 5-12 4-12 BaO 1-5 1-5 TiO.sub.2 2-6 2-6 B.sub.2 O.sub.
    Type: Grant
    Filed: May 26, 1982
    Date of Patent: November 29, 1983
    Assignee: Motorola, Inc.
    Inventors: Earl K. Davis, Rafael Landron, Scot W. Taylor
  • Patent number: 4414282
    Abstract: A glass ceramic composition prepared by subjecting a glass composition comprising, by weight, 65-80% SiO.sub.2, 8-16%, Li.sub.2 O, 2-8% , Al.sub.2 O.sub.3, 1-8% K.sub.2 O, 1-5% P.sub.2 O.sub.5 and 1.5-7% B.sub.2 O.sub.3, to the following processing steps of heating the glass composition to a temperature sufficient to crystallize lithium metasilicate therein, holding the glass composition at a temperature and for a time period sufficient to dissolve the lithium metasilicate therein thereby creating cristobalite nucleii, cooling the glass composition and maintaining the composition at a temperature and for a time period sufficient to recrystallize lithium metasilicate therein, and thermally treating the glass composition at a temperature and for a time period sufficient to cause growth of cristobalite and further crystallization of lithium metasilicate producing a glass ceramic composition having a specific thermal expansion coefficient and products containing said composition.
    Type: Grant
    Filed: April 19, 1982
    Date of Patent: November 8, 1983
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Howard L. McCollister, Scott T. Reed
  • Patent number: 4414009
    Abstract: A glass faceplate having a central area of required useful diameter surrounded by a narrow ring of opaque glass and an outer glass mounting flange. Light entering the flange or ring is prevented from reaching the central area as stray light or glare in the system and spurious reflections at the interface of the ring and central area are minimized by a refractive index match of the two innermost glasses.
    Type: Grant
    Filed: June 11, 1982
    Date of Patent: November 8, 1983
    Assignee: Warner Lambert Technologies, Inc.
    Inventor: Walter P. Siegmund
  • Patent number: 4412854
    Abstract: A method of making fiber reinforced glass composite articles of complex shape is disclosed which overcomes problems associated with the debulking process common with such procedures. Sheets of woven or non-woven fiber reinforcement are impregnated with a layer of thermoplastic binder containing glass powder and optionally, additional carrier liquid. The thus treated sheets are then dried and cut into a plurality of preforms corresponding to the predetermined pattern of the article being fabricated. The thus treated preforms are then stacked in a mold and warm molded to form an intermediate article of near net shape, during which molding operation much of the ultimate debulking occurs. The intermediate article is then hot pressed to form the final fiber reinforced glass matrix article of net shape and high strength and toughness. These multiple heating steps may also be accomplished in a single molding operation.
    Type: Grant
    Filed: May 25, 1982
    Date of Patent: November 1, 1983
    Assignee: United Technologies Corporation
    Inventor: George K. Layden
  • Patent number: 4412963
    Abstract: The invention provides a method of producing discharge lamp arc tubes of ceramic material complete with metal cermet end closure members using initially incompletely fired sintered components and a sealing composition selected from silica, alumina and magnesia in proportions such that the composition falls within the accompanying ternary phase diagram BCDEFXYZPQ. The sealing compositions may also contain up to 5% by weight of nucleating agents such as phosphorous pentoxide, rare earth oxides, titania, zirconia or chromia. The inclusion of up to 5% by weight of boric oxide improves the flow characteristics and up to 10% by weight of Y.sub.2 O.sub.3, Yb.sub.2 O.sub.3, La.sub.2 O.sub.3, Dy.sub.2 O.sub.3, Eu.sub.2 O.sub.3, HfO.sub.2 improves the thermal and mechanical properties of the seals. The invention eliminates the need to make a first end seal by separate sintering and sealing operations.
    Type: Grant
    Filed: December 18, 1981
    Date of Patent: November 1, 1983
    Inventor: Peter Hing
  • Patent number: 4388668
    Abstract: A capacitive pressure transducer comprising a pair of disc shaped members having planar surfaces made from an insulator material, one of the members being several times thinner than the other plate and flexible and constituting a diaphragm and the other thicker plate constituting a stationary plate. A thin conductive film is formed on the surface of each of the members to form the plates of the capacitor. A glass frit is applied on the marginal edge of each member and when the members are held in adjacent relationship, the assembly is fired to seal the two members together while spacing them a predetermined distance apart so that the two conductive plates are opposite each other and are separated by an open gap of a predetermined distance, the two conductive plates being insulated one from the other. Leads are electrically connected to the conductive plate of each disc through the fused glass frit.
    Type: Grant
    Filed: December 3, 1979
    Date of Patent: June 14, 1983
    Assignee: Kaylico Corporation
    Inventors: Robert L. Bell, Robert Willing, Fred Kavli
  • Patent number: 4385092
    Abstract: A macroboule is disclosed, formed of a bundle of hollow channel elements of fusible material and of different internal diameters. They are arranged with the elements of smallest diameter positioned in the center of the bundle and those of largest internal diameter constituting the outer row of the bundle with uniform or step by step graduation between these extremes. The macroboule is useful for forming a channel multiplier.
    Type: Grant
    Filed: September 24, 1965
    Date of Patent: May 24, 1983
    Assignee: Ni-Tec, Inc.
    Inventor: Joseph Singer, Jr.
  • Patent number: 4353966
    Abstract: A process of bonding a plurality of thermally stable, high strength graphite fiber reinforced glass matrix composite materials is described. The process comprises applying to the surface of at least one of the composite materials to be bonded, a mixture of low softening point glaze such as high lead oxide containing glaze, a high melting point low coefficient of thermal expansion material such as beta-spodumene and colloidal silica followed by hot pressing the composite materials to be bonded together. The resultant bonded articles and the glass compositions particularly adapted for this bonding process are also described.
    Type: Grant
    Filed: December 12, 1980
    Date of Patent: October 12, 1982
    Assignee: United Technologies Corporation
    Inventors: Elias Snitzer, James F. Bacon
  • Patent number: 4351104
    Abstract: In the method for manufacturing annular portions of magnetic heads, a gap between the confronting end surfaces of the magnetic heads is filled with glass. In one of the conventional processes, the glass is sucked into the gap by a capillary action of the gap, but bubbles are liable to form in the glass. The method according to the present invention comprises a step of heating the glass to a relatively low temperature capable of causing the glass to be flowable and applying a centrifugal force to the glass being heated in a rotatable support of a heating furnace. As a result of the centrifugal force, the tendency to form bubbles is considerably reduced as compared with the conventional methods.
    Type: Grant
    Filed: November 10, 1980
    Date of Patent: September 28, 1982
    Assignee: TDK Electronics Co., Ltd.
    Inventors: Kiyoshi Klagane, Masao Kakizaki
  • Patent number: 4350514
    Abstract: When fusing together a panel having a fluorescent film and a metallic reflective film, and a funnel with an electroconductive film in a baking furnace for manufacturing a cathode ray tube, oxygen containing air is forced into the furnace.
    Type: Grant
    Filed: May 14, 1981
    Date of Patent: September 21, 1982
    Assignee: Hitachi, Ltd.
    Inventors: Masatoshi Akiyama, Shigeki Kitamura, Junichi Tetsu, Koichi Nakazato
  • Patent number: 4350515
    Abstract: A glass edge multiple glazed unit having fillets of substantially uniform thickness is produced by the application of heat to marginal edge portions of adjacent sheets, followed by a delay sufficient to establish a substantially uniform, greater than fusing temperature condition in the body of fillet-forming glass. The fused sheets are thereafter drawn apart a preselected distance to a spaced-apart face-to-face relation to form a glass-edge multiple glazed unit.
    Type: Grant
    Filed: January 30, 1981
    Date of Patent: September 21, 1982
    Assignee: PPG Industries, Inc.
    Inventor: John L. Stewart