Vaporization (e.g., Evaporation, Distillation, Etc.) Patents (Class 73/61.77)
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Patent number: 11185791Abstract: The present invention provides a rotary evaporator capable of accurately quantifying concentrated liquid and/or distillate. A distillation flask is improved into a structure having a liquid discharge opening formed at the bottom, and/or a spherical collecting flask is improved into a structure having a liquid release opening formed at the bottom. Concentrated liquid and/or distillate can be discharged without dismounting the distillation flask and/or the collecting flask. In addition, fine metering scale tubes and quantitative capacity increase units are disposed at the liquid discharge opening and/or the liquid release opening, there is a valve on the top and another valve on the bottom of each tube, so that the constant subtle changes of the amount of concentrated liquid and/or distillate can be observed, and an accurate amount of concentrated liquid and/or distillate can be discharged.Type: GrantFiled: July 22, 2020Date of Patent: November 30, 2021Assignee: Beijing Normal UniversityInventor: Shuyao Wen
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Patent number: 9005404Abstract: An accelerated vapor recompression apparatus 10 converts incoming flow 35a to a concentrate 35c by developing a concentration profile 146 within a tank 30 holding a liquid 23 containing dissolved solids. The resulting curve 160 of saturation temperature of the stratified liquid 23 (such as a brine 23 or other material 23) moves away from the curve 162 corresponding to fully mixed conditions. The shift 174, 180 in saturation temperature results in increased boiling without increased energy from a heater 70 or compressor 50. A method 90, 200 of control of the system provides interventions 203, 204, 205, 206 at different levels 92, 94, 96, 98 of control, ranging from mass flows 35 to work of a compressor 50, heat from a heater 70, and a predictive processing 215 of feedback 217 for controlling commands 216 algorithmically.Type: GrantFiled: February 13, 2012Date of Patent: April 14, 2015Assignee: Purestream Services, LLCInventors: J. Clair Batty, Neil W. Richardson, David A. Bell, Christopher M. Miller
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Patent number: 8986509Abstract: An accelerated vapor recompression apparatus 10 converts incoming flow 35a to a concentrate 35c by developing a concentration profile 146 within a tank 30 holding a liquid 23 containing dissolved solids. The resulting curve 160 of saturation temperature of the stratified liquid 23 (such as a brine 23 or other material 23) moves away from the curve 162 corresponding to fully mixed conditions. The shift 174, 180 in saturation temperature results in increased boiling without increased energy from a heater 70 or compressor 50. A method 90, 200 of control of the system provides interventions 203, 204, 205, 206 at different levels 92, 94, 96, 98 of control, ranging from mass flows 35 to work of a compressor 50, heat from a heater 70, and a predictive processing 215 of feedback 217 for controlling commands 216 algorithmically.Type: GrantFiled: February 13, 2012Date of Patent: March 24, 2015Assignee: Purestream Services, LLCInventors: J. Clair Batty, Neil W. Richardson, David A. Bell, Christopher M. Miller
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Patent number: 8372247Abstract: Method for automatically distilling liquid specimens in a standardized distillation apparatus containing a heater, a distillation flask, a collecting cylinder and control and regulation means, characterized in that: the specimen is introduced into the distillation flask; this flask is positioned in the distillation apparatus; the specimen to be analysed is classified in a group defined by the standard selected; the distillation is started, with the amount of condensate collected in the collecting cylinder, the temperature of the evaporated vapor, the temperature of the liquid specimen present in the flask, together with an operating parameter of the heater, being constantly measured; and the measured values are sent to the control and regulating means that in return control the operating parameter of the heater so as to obtain, directly and automatically, distillation parameters in accordance with a standard.Type: GrantFiled: February 8, 2008Date of Patent: February 12, 2013Assignee: Instrumentation Scientifique de Laboratoire ISLInventors: Viachaslau Urvantsau, Hervé Cleris
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Patent number: 8205486Abstract: An atmometer device comprises a porous evaporator member, a suction tube communicating water from a reservoir to the porous evaporator member, a sensor measuring a moisture characteristic of soil associated with a crop, a mechanism arranged for controllably varying a rate of evaporation of the water through the porous evaporator member responsive to the moisture characteristic measured by the sensor, and an indicator arranged to indicate water loss in the reservoir. By controlling rate of evaporation of the water through the porous evaporator member responsive to the measured moisture characteristic of the soil, the amount of water loss in the reservoir during the given time period more accurately reflects crop evapotranspiration.Type: GrantFiled: February 22, 2010Date of Patent: June 26, 2012Inventor: Ramanathan Sri Ranjan
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Patent number: 7820015Abstract: A device for recording the boiling curve of liquids, in particular petroleum products, made of a distillation apparatus which includes a distillation column and a condenser, a sample dish connected to the distillation apparatus and a pump connected to the sample dish to fill the sample dish, wherein the filling means and the condenser are made of well heat-conducting material and the filling means and the condenser are connected to a temperature controller.Type: GrantFiled: June 26, 2008Date of Patent: October 26, 2010Assignee: Grabner Instruments Messtechnik Nfg. Gesellschaft m.b.H. & Co. KG.Inventors: Matthias Burian, Roland Aschauer
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Publication number: 20100206960Abstract: Dispensers and refills for volatile liquids, such as fragrances, are disclosed. Dispensers and refills in combination with dispensers according to the present invention may comprise a volatile liquid and a housing. In certain embodiments, the volatile liquid of the present invention has a predetermined evaporation rate, measured and calculated by the method described herein. In other embodiments, the volatile liquid exhibits a predefined relative evaporation rate. In addition to the housing, the present invention includes optional components, such as a motorized fan and/or a wick, to facilitate release of the volatile liquid into the atmosphere.Type: ApplicationFiled: April 30, 2010Publication date: August 19, 2010Inventors: Padma Prabodh Varanasi, Joel E. Adair, Michael C. Liptrot, Qing Song
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Patent number: 7556716Abstract: Described is a method for recording the boiling curve of liquids, in particular petroleum products and/or solvents, in which a sample amount of the liquid to be analyzed is evaporated and subsequently condensed, wherein the vapor temperature and the respectively evaporated amount of liquid are monitored, the sample amount is dosed by a a pump, for example, wherein the pump and the condensate collection chamber are brought to a defined, and preferably identical, temperature level. The condensed volume is determined volumetrically and the distillation residue of the sample amount is determined by weighing.Type: GrantFiled: April 23, 2003Date of Patent: July 7, 2009Assignee: Grabner Instruments Messtechnik NFG. Gesellschaft m.b.H. & Co. KGInventors: Matthias Burian, Roland Aschauer
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Publication number: 20090095056Abstract: An evaporation rate potential is determined to show the feasibility of evaporation within an environment. The environment includes air and a material, such as wood or other building material. The temperature and vapor pressure differences determine the flow of sensible and latent energy from the air to the material, and vice versa. Using these values, the evaporation rate potential is determined for different conditions within the environment so that evaporation and drying can be improved.Type: ApplicationFiled: May 14, 2008Publication date: April 16, 2009Inventors: Charles Dewald, III, Jerry Blaylock
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Patent number: 7364696Abstract: Disclosed devices and methods for droplet microchromatograhy are aimed at optical monitoring and rapid analysis of a drying droplet. The device includes droplet deposition component preferably made as a modified disk adapted to fit in a modified CD disk drive, an optical recorder, and a computer control and image analysis. Recorded timed sequence of images of the process of drying of the droplet is digitally filtered and analyzed using windows selected in each image. Changes of predetermined parameters in each window for each image are calculated to assess temporal and spatial dynamics within the sequence of images reflecting sedimentary pattern formation of a drying droplet. Humidity can be selectively controlled to slow down the drying process allowing “zooming” onto the critical periods of drying of the droplet. Various chemical coatings of the deposition means can be used to enhance the test further.Type: GrantFiled: September 5, 2006Date of Patent: April 29, 2008Assignee: Artann Laboratories, Inc.Inventor: Armen P. Sarvazyan
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Patent number: 7351312Abstract: A vessel is provided for collecting a process stream and fractionating the process stream into a liquid and gas phase in the vessel. Cooling may be provided by an internal bath and/or an external bath. The liquid phase retained in the vessel and the gas phase collected in lots from the vessel may be delivered to a lab for analysis.Type: GrantFiled: December 17, 2003Date of Patent: April 1, 2008Assignee: UOP LLCInventor: Jessy E. Trucko
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Patent number: 6881585Abstract: In one embodiment, the present method includes the steps of introducing a volume of a sample into a vapor delivery line and volatilizing at least a portion of the volume as it is carried through the vapor delivery line. At least a portion of the volatilized volume contacts a sensor element, which produces a signal that is monitored to reveal information about the sample. All components upstream of the sensor element are substantially free of sorbent materials so that the sample volume does not contact a substantially sorbent material before contacting the sensor element.Type: GrantFiled: March 6, 2000Date of Patent: April 19, 2005Assignee: General Electric CompanyInventors: Radislav Alexandrovich Potyrailo, James Claude Carnahan, Ralph Joseph May, John Patrick Lemmon
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Patent number: 6836732Abstract: An apparatus and method for ensuring effective and efficient vehicle vapor recovery performance, storage tank system integrity relative to both vapor and liquid containment and for reducing the probability that inaccurate information causes companies to undertake unnecessary, expensive and wasteful loss investigations at gasoline dispensing facilities. A fuel storage and delivery system is transformed from an “open system” communicating directly with the environment to a “closed system” which ensures capture, containment and accurate accounting of both hydrocarbon vapors and liquid phase product.Type: GrantFiled: June 26, 2002Date of Patent: December 28, 2004Assignee: Arid Technologies, Inc.Inventor: Tedmund P. Tiberi
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Patent number: 6817342Abstract: A wall film can form around a temperature sensor as a result of the temperature sensor being fitted in the intake port of the internal combustion engine, in such a manner that at least some of the fuel jet from the injection valve is sprayed onto it. The reduction in temperature that occurs as a result of the enthalpy of vaporization at the temperature sensor is measured and used as a criterion for determining the quality of the fuel supplied to the internal combustion engine. This information can be used to correct the change in injection time exclusively or in addition to adapting the starting quantity and/or using the lack-of-smoothness method.Type: GrantFiled: June 20, 2002Date of Patent: November 16, 2004Assignee: Siemens AktiengesellschaftInventor: Harry Schüle
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Patent number: 6651487Abstract: A reactive test strip having a pre-exposure color is used to measure and indicate the concentration of copper ions in brake fluid in terms of a readily visible color change. The strip is immersed in the fluid within a brake fluid container and any resulting color change is compared to a color chart and a known test standard representative of the maximum metal concentration determined empirically to correspond to a boiling point considered safe for normal operation. If the color change indicates a higher copper concentration than the known test standard, then the fluid is considered inadequate for safe operation and thus recommended for replacement without any further tests. Similar copper or metal strips can also be used in a similar test to determine iron or zinc concentration within the brake fluid so as to also determine suitability of the brake fluid for ensuring safe operation.Type: GrantFiled: January 3, 2002Date of Patent: November 25, 2003Assignee: Phoenix Systems, L.L.C.Inventor: Jon A. Petty
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Patent number: 6588253Abstract: A method and apparatus for determining a volatility of a fuel sample. A fuel sample is collected in a container and heated for a time period using a heater device. Periodically during the heating, the capacitance of the fuel sample and the temperature of the heater device are determined. After a time period passes, the volatility of the fuel sample is determined using the capacitance decrease and the temperature increase. Specifically, a voltage across the heater device is used, along with the current through the heater device to determine the resistance of the heater device, which gives the temperature of the heater device and the sample. The capacitance and temperature are compared to values derived from experimentation for fuels of varying DI. The first measurement of capacitance with a known sample volume can be used to determine the MTBE or ethanol content in gasoline fuels.Type: GrantFiled: August 17, 2001Date of Patent: July 8, 2003Assignee: Delphi Technologies, Inc.Inventors: David K. Lambert, Charles Robert Harrington, Han-Sheng Lee, Da Yu Wang
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Patent number: 6581443Abstract: “Process for determining the distillation characteristics of liquid petroleum products by express mini-distillation and apparatus permitting implementation of this process” Apparatus characterized by the fact that it includes: a distillation flask dimensioned to receive 5 to 15 ml of a sample to be analysed, organs for heating the distillation flask, with an adjustable constant heating intensity, two inertialess temperature sensors permitting continuous measurement on the one hand of the true value of the temperature of a sample in the course of distillation in the liquid phase and the true value of the temperature of this sample in the vapor phase, a device for continuous measurement of the pressure in the vapor phase of a sample in the course of distillation which includes a pressure detector and a capillary tube, and organs for reception and exploitation of signals transmitted by the temperature sensors and the pressure detector.Type: GrantFiled: October 17, 2001Date of Patent: June 24, 2003Assignee: Instrumentation Scientifique de Laboratoire I.S.L. SAInventors: Guenrikh Abaev, Raissa Andreeva, Viachaslau Urvantsau, Aliaksandr Spirydonau, Victor Kalesnik
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Publication number: 20030037603Abstract: Apparatus characterized by the fact that it includes:Type: ApplicationFiled: October 17, 2001Publication date: February 27, 2003Inventors: Guenrikh Abaev, Raissa Andreeva, Viachaslau Urvantsau, Aliaksandr Spirydonau, Victor Kalesnik