Producing Or Purifying Named Magnetic Material Patents (Class 75/348)
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Patent number: 12080895Abstract: A method for making a branched metal nanocatalyst including providing a first metal precursor solution having a first metal precursor, wherein providing the first metal precursor solution includes combining a first metal ion source and a first alkylamine, and providing a second metal precursor solution, wherein providing the second metal precursor solution includes combining a second metal ion source and a second alkylamine, heating the second metal precursor solution, combining the first metal precursor solution with the second metal precursor solution to provide a reaction solution, and holding the reaction solution at an elevated temperature for a reaction time to provide a branched metal nanocatalyst. Also described are nanocatalysts prepared according to the method.Type: GrantFiled: August 9, 2022Date of Patent: September 3, 2024Assignee: HONDA MOTOR CO., LTD.Inventor: Shutang Chen
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Patent number: 11897036Abstract: Methods of forming metal multipod nanostructures. The methods may include providing a mixture that includes a metal acetylacetonate, a reducing agent, and a carboxylic acid. The mixture may be contacted with microwaves to form the metal multipod nanostructures. The methods may offer control over the structure and/or morphology of the metal multipod nanostructures.Type: GrantFiled: October 3, 2022Date of Patent: February 13, 2024Assignee: The Florida State University Research Foundation, Inc.Inventors: Parth Nalin Vakil, Geoffrey F. Strouse
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Patent number: 11705255Abstract: Disclosed herein is a method comprising disposing a first particle in a reactor; the first particle being a magnetic particle or a particle that can be influenced by a magnetic field, an electric field or a combination of an electrical field and a magnetic field; fluidizing the first particle in the reactor; applying a uniform magnetic field, a uniform electrical field or a combination of a uniform magnetic field and uniform electrical field to the reactor; elevating the temperature of the reactor; and fusing the first particles to form a monolithic solid.Type: GrantFiled: March 24, 2021Date of Patent: July 18, 2023Assignee: UNIVERSITY OF FLORIDA RESEARCH FOUNDATION, INC.Inventors: James F. Klausner, Renwei Mei, Ayyoub Mehdizadeh Momen, Kyle Allen
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Patent number: 11416437Abstract: An apparatus is provided, comprising a plurality of memory devices and a buffering device that permits memory devices with a variety of physical dimensions and memory formats to be used in an industry-standard memory module format. The buffering device includes memory interface circuitry and at least one first-in first-out (FIFO) or multiplexer circuit. The apparatus further comprises a parallel bus connecting the buffering device to the plurality of memory devices. The parallel bus includes a plurality of independent control lines, each coupling the memory interface circuitry to a corresponding subset of a plurality of first subsets of the plurality of memory devices. The parallel bus further includes a plurality of independent data channels, each coupling the at least one FIFO circuit or multiplexer circuit to a corresponding subset of a plurality of second subsets of the plurality of memory devices.Type: GrantFiled: December 19, 2019Date of Patent: August 16, 2022Assignee: Micron Technology, Inc.Inventors: Thomas H. Kinsley, George E. Pax, Timothy M. Hollis, Yogesh Sharma, Randon K. Richards, Chan H. Yoo, Gregory A. King, Eric J. Stave
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Patent number: 11014356Abstract: In a case where a direction of ejection of a second liquid is a direction from below to above, the second liquid flows above a first liquid in a pressure chamber. A substrate includes an outflow port located downstream of the pressure chamber in a direction of flow of the first liquid and configured to allow the first liquid to flow out of a liquid flow passage. A wall is located in the liquid flow passage and on a section of the substrate on a side opposite to the pressure chamber across the outflow port, the wall including a portion located higher than a surface of a section of the substrate where the pressure chamber is located on a side opposite to the wall across the outflow port.Type: GrantFiled: July 30, 2019Date of Patent: May 25, 2021Assignee: Canon Kabushiki KaishaInventors: Yoshiyuki Nakagawa, Akiko Hammura
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Patent number: 10790514Abstract: Aspects disclosed herein relate to methods for producing nanostructured metal catalysts that can be used in various alternative fuel applications.Type: GrantFiled: November 4, 2015Date of Patent: September 29, 2020Assignee: Alliance for Sustainable Energy, LLCInventors: Bryan Pivovar, Shaun Alia
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Patent number: 10128031Abstract: Provided is a method for manufacturing magnetic particles, in which an oxidation treatment, a reduction treatment, and a nitriding treatment are performed in that order on raw material particles with a core-shell structure in which a silicon oxide layer is formed on the surfaces of iron microparticles, thereby nitriding the iron microparticles while maintaining the core-shell structure. Due to this configuration, granular magnetic particles with a core-shell structure in which a silicon oxide layer is formed on the surfaces of iron nitride microparticles can be obtained.Type: GrantFiled: January 20, 2015Date of Patent: November 13, 2018Assignees: NISSHIN SEIFUN GROUP INC., NISSHIN ENGINEERING INC.Inventors: Keitaroh Nakamura, Akihiro Kinoshita, Naohito Uemura
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Patent number: 9966593Abstract: A method for the production of SbMx nanoparticles is described that comprises the steps of reducing an antimony salt and optionally an alloying metal with a hydride in an anhydrous polar solvent, separating the solid product formed from the solution, preferably via centrifugation, and washing the product with water. M is an element selected from the group consisting of Sn, Ni, Cu, In, Al, Ge, Pb, Bi, Fe, Co, Ga, and 0?x<2.Type: GrantFiled: June 22, 2015Date of Patent: May 8, 2018Assignee: Belenos Clean Power Holding AGInventors: Maksym V. Kovalenko, Marc Walter
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Patent number: 9821374Abstract: The present invention addresses the problem of providing a method for producing microparticles. Composite microparticles are separated by mixing at least two kinds of fluids to be processed in a thin film fluid that is formed between approachable and separable opposing processing surfaces that relatively rotate, wherein the fluids to be processed are a metal fluid comprising at least two kinds of metal elements that are dissolved in a solvent in the form of metal and/or metal compound and a fluid for separation containing at least one kind of separating substance for separating a composite substance comprising the at least two kinds of metal elements. The molar ratio between the at least two kinds of metal elements contained in the resulting microparticles is controlled by controlling the circumferential speed of the rotation at a confluence where the metal fluid and the fluid for separation merge at this time.Type: GrantFiled: February 20, 2013Date of Patent: November 21, 2017Assignee: M. TECHNIQUE CO., LTD.Inventors: Shiho Aoyagi, Masakazu Enomura
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Patent number: 9581001Abstract: In one aspect, a method of stimulating flow of a fluid present in a subsurface reservoir to a wellbore is provided, which method, in one non-limiting embodiment, may include providing a working fluid that includes a heated base fluid and heated nanoparticles, wherein the nanoparticle have a core and a shell; supplying the working fluid into a selected section of the subsurface reservoir; allowing the heated nanoparticles to transfer heat to the fluid in the subsurface reservoir to stimulate flow of the fluid from the reservoir to the wellbore.Type: GrantFiled: August 19, 2013Date of Patent: February 28, 2017Assignee: BAKER HUGHES INCORPORATEDInventors: Oleg A. Mazyar, Bennett M. Richard
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Patent number: 9545456Abstract: Provided herein are dual contrast agents or nanocomposite particles designed to enhance optoacoustic-ultrasonic imaging. The contrast agents or particles have a core designed to enhance response to incident transient ultrasonic pressure waves and at least two layers disposed around the core. The inner first layer is designed to effectively absorb incident transient optical waves, convert absorbed optical energy into heat and demonstrates significant thermal expansion and/or conversion of thermal energy into acoustic pressure. The outer second layer thermally insulates the inner layer from the surrounding aqueous environment and enhances the generation of transient ultrasonic pressure waves during optoacoustic-ultrasonic imaging and sensing. Also provided are methods of enhancing contrast in a tissue optoacoustic-ultrasonic imaging and producing enhanced optoacoustic images by contacting the tissue with the dual contrast agent or nanocomposite particles.Type: GrantFiled: February 22, 2013Date of Patent: January 17, 2017Assignee: TomoWave Laboratories, Inc.Inventors: Alexander A Oraevsky, Anton Liopo, Sergey A Ermilov
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Patent number: 9378876Abstract: Ferromagnetic particles including an Fe16N2 compound phase in an amount of not less than 80% as measured by Mössbauer spectrum and each having an outer shell in which FeO is present in the form of a film having a thickness of not more than 5 nm. Ferromagnetic particles may be made by subjecting iron oxide or iron oxyhydroxide having an average major axis diameter of 40 to 5000 nm and an aspect ratio (major axis diameter/minor axis diameter) of 1 to 200 as a starting material to dispersing treatment to prepare aggregated particles; subjecting the iron compound particles passed through a mesh to hydrogen reducing treatment at a temperature of 160 to 420° C.; and then subjecting the resulting particles to nitridation treatment at a temperature of 130 to 170° C.Type: GrantFiled: January 19, 2012Date of Patent: June 28, 2016Assignees: TODA KOGYO CORPORATION, TOHOKU UNIVERSITYInventors: Migaku Takahashi, Tomoyuki Ogawa, Yasunobu Ogata, Naoya Kobayashi, Chammika Ruwan Polwatta Gallage, Kaori Kohara
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Patent number: 9233393Abstract: A method for plasmonic structure manufacture and for protecting a plasmonic nanostructure during annealing is provided. The method includes: lithographically forming a plasmonic nanostructure on a substrate; encapsulating the plasmonic nanostructure in high temperature resistant material; annealing the plasmonic nanostructure; and removing the high temperature resistant material to reveal the annealed plasmonic nanostructure.Type: GrantFiled: March 19, 2013Date of Patent: January 12, 2016Assignee: Agency for Science, Technology and ResearchInventors: Joel K. W. Yang, Michel Bosman, Huigao Duan, Karthik Kumar, In Yee Phang
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Patent number: 9221044Abstract: The invention relates to a method of synthesis of substantially pure nanoparticles in a continuous-flow system, in which a precursor substance solution undergoes reduction reaction using a reducing agent solution and nanoparticles are produced, wherein the reduction reaction is terminated by adding an agent neutralizing the reducing agent and a stable nanoparticle colloid is produced. In the method of the invention a need for using surfactants or other organic molecules for nanoparticle stabilization has been eliminated.Type: GrantFiled: September 12, 2014Date of Patent: December 29, 2015Assignee: UNIWERSYTET WARSZAWSKIInventors: Rafal Jurczakowski, Adam Lewera, Pawel Kulboka
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Patent number: 9130214Abstract: An electrode material for lithium secondary battery comprises a nanoheterostructure which contains a lithium-ion conductor and an electrode active substance of which one inorganic component is a matrix, and of which the other inorganic component is three-dimensionally and periodically arranged in the matrix, and has a three-dimensional periodic structure whose average value of one unit length of a repeated structure is 1 nm to 100 nm.Type: GrantFiled: September 14, 2012Date of Patent: September 8, 2015Assignee: KABUSHIKI KAISHA TOYOTA CHUO KENKYUSHOInventors: Hiroaki Wakayama, Hirotaka Yonekura, Yasuaki Kawai
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Publication number: 20150147217Abstract: An article having a nanocomposite magnetic component and method of forming a nanocomposite magnetic component are disclosed. The article includes a plurality of nanocrystalline flake particles bonded along their prior particle boundaries. The nanocrystalline flake particles have a median grain size less than about 30 nanometers and include a first set of grains comprising predominantly permanent magnet phase and a second set of grains comprising predominantly soft magnet phase.Type: ApplicationFiled: November 27, 2013Publication date: May 28, 2015Applicant: General Electric CompanyInventors: Francis Johnson, Wanming Zhang, Min Zou, Christina Hongbing Chen
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Publication number: 20150110664Abstract: A scalable process is detailed for forming bulk quantities of high-purity ?-MnBi phase materials suitable for fabrication of MnBi based permanent magnets.Type: ApplicationFiled: October 22, 2013Publication date: April 23, 2015Applicant: BATTELLE MEMORIAL INSTITUTEInventors: Jung Pyung Choi, Curt A. Lavender, Guosheng Li, Jun Cui
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Publication number: 20150104664Abstract: In a magnetic component, such as an inductor and an antenna, produced with a metal magnetic powder, a complex number component of magnetic permeability that is a loss in the GHz band was high. A magnetic component obtained by molding a soft magnetic metal powder can have a reduced loss factor in the GHz band. The soft magnetic metal powder is characterized by containing iron as a main ingredient, and having an average particle size of not larger than 300 nm, a coercive force (Hc) of 16 to 119 kA/m (200 to 1500 Oe), a saturation magnetization of not less than 90 Am2/kg, and a volume resistivity of not less than 1.0×101 ?·cm. The volume resistivity is determined by measuring, by a four probe method, a molded body formed by vertically pressurizing 1.0 g of the metal powder at 64 MPa (20 kN).Type: ApplicationFiled: March 13, 2013Publication date: April 16, 2015Inventors: Kazumasa Ikari, Masahiro Gotoh, Takayuki Yoshida
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Patent number: 8979973Abstract: A method and a device for recovering hydrogen pulverized powder of a raw-material alloy for rare-earth magnets capable of lowering a possibility that hydrogen pulverized powder after hydrogen was pulverized remains in a recovery chamber and capable of enhancing magnetic properties by reducing an amount of oxygen of an obtained rare-earth magnet, a processing container 50 is carried into a recovery chamber 40 from a processing chamber through a carry-in port after inert gas was introduced into the recovery chamber 40 by inert gas introducing means 12, the raw-material alloy for rare-earth magnets in the processing container 50 is discharged into the recovery chamber 40 after the pressure in the recovery chamber 40 was reduced by evacuating means 33 and thereafter, inert gas is introduced into the recovery chamber 40 by inert gas introducing means 12, and the raw-material alloy for rare-earth magnets is recovered into the recovery container 50 from an discharge port 40a after a pressure in the recovery chamberType: GrantFiled: July 7, 2010Date of Patent: March 17, 2015Assignee: Hitachi Metals, Ltd.Inventors: Shoji Nakayama, Kazuhiro Sonoda, Jyunichi Sanai
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Patent number: 8940075Abstract: A method for fabricating fine reduced iron powders comprises the following steps: heating fine iron oxide powders having a mean particle size of smaller than 20 ?m to a reduction temperature of over 700° C. to reduce the fine iron oxide powder into iron powders that are partially sintered into iron powder agglomerates; and performing a crushing-spheroidizing process on the iron powder agglomerates to obtain individual iron powders having a mean particle size of smaller than 20 ?m. The method can reduce iron oxide powers into iron powders having a rounded shape and a high packing density and a high tap density, which are suitable for the metal injection molding process and the inductor fabrication process. The reduced iron powder may further be processed using an annealing process and a second crushing-spheroidizing process in sequence to further increase the sphericity, packing density, and tap density of the reduced iron powder.Type: GrantFiled: April 4, 2012Date of Patent: January 27, 2015Assignee: Taiwan Powder Technologies Co., Ltd.Inventors: Kuen-Shyang Hwang, Ching-Yu Chen, Yung-Chung Lu
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Publication number: 20150010426Abstract: Disclosed is an R-T-B—Ga-based magnet material alloy where R is at least one element selected from rare earth metals including Y, and T is one or more transition metals with Fe being an essential element. The R-T-B—Ga-based magnet material alloy includes: an R2T14B phase 3 which is a principal phase, and an R-rich phase (1 and 2) which is a phase enriched with the R, wherein a non-crystalline phase 1 in the R-rich phase has a Ga content (mass %) that is higher than a Ga content (mass %) of a crystalline phase 2 in the R-rich phase. With this, it is possible to enhance the magnetic properties of rare earth magnets that are manufactured from the alloy and reduce variations in the magnetic properties thereof.Type: ApplicationFiled: February 1, 2013Publication date: January 8, 2015Inventors: Akihiko Saguchi, Noriyuki Negi, Mitsuharu Yonemura
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Publication number: 20140345424Abstract: Provided herein are systems, methods, and compositions for magnetic nanoparticles and bulk nanocomposite magnets.Type: ApplicationFiled: June 26, 2014Publication date: November 27, 2014Inventor: J. Ping Liu
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Patent number: 8861663Abstract: A method of operation in an ethernet receiver circuit is disclosed. The method comprises sampling an input signal to generate a sampled signal having a sampled noise component and a sampled data component. The sampled signal is sliced, and a slicer error determined based on the slicing of the sampled signal. A subsequently sampled noise component is filtered based on the slicer error.Type: GrantFiled: January 13, 2012Date of Patent: October 14, 2014Assignee: Aquantia CorporationInventors: Hossein Sedarat, Fadi Saibi
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Patent number: 8852314Abstract: A magnetic powder for magnetic recording medium comprises acicular particles constituted primarily of Fe, wherein the powder contains Co in an amount such that the Co/Fe ratio is 50 at. % or less and the Co is contained in a manner such that the surface portion has a higher concentration than the core portion of the particles, and upon subjecting the magnetic powder for magnetic recording medium to TG measurement, the powder exhibits at least two oxidation starting points: a low-temperature side oxidation starting point and a high-temperature side oxidation starting point. The magnetic powder achieves improved resistance to oxidation without sacrificing magnetic characteristics.Type: GrantFiled: March 3, 2011Date of Patent: October 7, 2014Assignee: Dowa Electronics Materials Co., Ltd.Inventors: Shinichi Konno, Kenichi Inoue, Toshihiko Ueyama, Kenji Masada, Shinya Sasaki
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Patent number: 8808468Abstract: The invention relates to a Fe—Si—La alloy having the atomic composition: (La1-a-a?MmaTRa?)1[(Fe1-b-b?CObMb?)1-x(Si1-cXc)x]13(CdNeH1-d-e)y(R)z(I)f Mm representing a mixture of lanthanum, cerium, neodymium and praseodynium in the weight proportion of 22 to 26% La, 48 to 53% Ce, 17 to 20% Nd and 5 to 7% Pr, the said mixture possibly comprising up to 1% by weight of impurities, TR representing one or more elements of the rare earth family other than lanthanum, M representing one or more type d transition elements of the 3d, 4d and 5d layers X representing a metalloid element selected from Ge, Al, B, Ga and In R representing one or more elements selected from Al, Ca, Mg, K and Na, I representing one or two elements selected from O and S, with: 0?a<0.5 and 0?a?<0.2 0?b?0.2 and 0?b?<0.4 0?c?0.5 and 0?d?1 0?e?1 and f?0.1 0.09?x?0.13 and 0.002?y?4 0.0001?z?0.01 the subscripts b, d, e, x and y being such that the alloy further satisfies the following condition: 6.143b(13(1?x))+4.437y[1?0.Type: GrantFiled: December 15, 2008Date of Patent: August 19, 2014Assignee: Aperam Alloys ImphyInventors: Thierry Waeckerle, Herve Fraisse, Mohamed Balli, Patricia De Rango, Daniel Fruchart, Damien Gignoux, Salvatore Miraglia, Mariana Rosca, Miguel Jose Artigas Alava
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Publication number: 20140225696Abstract: The invention relates to a method for producing a magnetic material, said magnetic material consisting of a starting material that comprises a rare earth metal (SE) and at least one transition metal. The rare earth metal content is 15 to 20 wt. %, and the method has the following steps:—hydrogenating the starting material,—disproportioning the starting material,—desorption, and—recombination. A soft magnetic material is added after the starting material is disproportioned.Type: ApplicationFiled: June 20, 2012Publication date: August 14, 2014Applicant: ROBERT BOSCH GmbHInventors: Konrad Güth, Oliver Gutfleisch
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Publication number: 20140170014Abstract: Disclosed is a method for producing a magnetic powder comprising: a first step of producing a R—Fe—B-based rare earth isotropic magnetic powder using a scrap rare earth magnet through a HDDR process; and a second step of mixing the R—Fe—B-based rare earth isotropic magnetic powder with an anisotropic magnetic powder, and a method for producing a magnet using the magnetic powder.Type: ApplicationFiled: May 1, 2013Publication date: June 19, 2014Applicants: KOREA INSTITUTE OF MACHINERY & MATERIALS, HYUNDAI MOTOR COMPANYInventors: Jae Ryung Lee, Ji Hun Yu, Jung Goo Lee
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Patent number: 8734714Abstract: The present invention discloses a method for recovering rare earth particulate material from an assembly comprising a rare earth magnet and comprises the steps of exposing the assembly to hydrogen gas to effect hydrogen decrepitation of the rare earth magnet to produce a rare earth particulate material, and separating the rare earth particulate material from the rest of the assembly. The invention also resides in an apparatus for separating rare earth particulate material from an assembly comprising a rare earth magnet. The apparatus comprises a reaction vessel having an opening which can be closed to form a gas-tight seal, a separation means for separating the rare earth particulate material from the assembly, and a collection means for collecting the rare earth particulate material. The reaction vessel is connected to a vacuum pump and a gas control system, and the gas control system controls the supply of hydrogen gas to the reaction vessel.Type: GrantFiled: June 27, 2011Date of Patent: May 27, 2014Assignee: The University of BirminghamInventors: Ivor Rex Harris, Andrew Williams, Allan Walton, John Speight
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Patent number: 8617290Abstract: The present invention relates to a method for manufacturing a Fe—Si alloy powder. A method for manufacturing a Fe—Si alloy powder includes: providing a mixture of an Al2O3 powder, an active agent powder, a Si powder, and a Fe powder; heating the mixture with a temperature of 700° C. to 1200° C. in the hydrogen atomosphere; magnetically separating a Fe-containing material from the mixture; and separating a Fe—Si alloy powder by soaking the Fe-containing material in an alkali solution. In the heating of the mixture, the Si powder is deposited on the surface of the Fe powder and diffused into the Fe powder.Type: GrantFiled: October 22, 2010Date of Patent: December 31, 2013Assignee: Korea Institute of Science and TechnologyInventors: Ji-Young Byun, Yoon-Bae Kim, Hyun-Kwang Seok, Jang-Won Kim, Dow-Bin Hyun, Heon-Phil Ha, Do-Hyung Kim
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Publication number: 20130195767Abstract: A magnetic nanoparticle includes a magnetic core and a superparamagnetic outer shell, in which the outer shell enhances magnetic properties of the nanoparticle. The enhanced magnetic properties of the magnetic nanoparticle allow for highly sensitive detection as well as diminished non-specific aggregation of nanoparticles.Type: ApplicationFiled: May 26, 2011Publication date: August 1, 2013Inventors: Ralph Weissleder, Hakho Lee, Tae-Jong Yoon
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Publication number: 20130186238Abstract: In a manufacturing method of magnetic alloy powder including an alloy of Fe and Ni, a precursor made of powdered chloride expressed as FeCl2·2H2O·NiCl2·2H2O is prepared, and the precursor is reduced by heating with calcium hydride to form the, magnetic alloy powder having a coercivity of greater than or equal to 40 kA/m.Type: ApplicationFiled: January 21, 2013Publication date: July 25, 2013Applicant: DENSO CORPORATIONInventor: DENSO CORPORATION
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Patent number: 8398741Abstract: Fine composite metal particle comprising a metal core and a coating layer of carbon, and being obtained by reducing metal oxide powder with carbon powder.Type: GrantFiled: January 4, 2011Date of Patent: March 19, 2013Assignee: Hitachi Metals, Ltd.Inventors: Yasushi Kaneko, Shigeo Fujii, Hisato Tokoro
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Patent number: 8357222Abstract: A metal magnetic powder for a magnetic recording medium is provided whose particles have a metal magnetic phase, composed mainly of Fe or Fe plus Co, and an oxide layer, wherein the average major axis length of the powder particles is 10-50 nm, the average particle volume including the oxide layer is 5,000 nm3 or less, the atomic ratio (R+Al+Si)/(Fe+Co) calculated using the content values (at. %) of the elements contained in the powder particles is 20% or less, where R is rare earth element (Y being treated as a rare earth element). The metal magnetic powder is obtained by using a complexing agent and a reducing agent to elute nonmagnetic constituents after firing. The metal magnetic powder exhibits a large saturation magnetization as for its particle volume while maintaining weatherability comparable to the conventional level and is suitable for a coated-type magnetic recording medium.Type: GrantFiled: November 23, 2010Date of Patent: January 22, 2013Assignee: DOWA Electronics Materials Co., Ltd.Inventors: Takayuki Yoshida, Masatoshi Nakayama, Ryota Igarashi
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Publication number: 20120328467Abstract: Method for the production of mixed oxides and permanent magnetic particles, based on rare earths-transition metals to produce RETM magnetic materials, comprising the preparation of a parent compounds mixture; introducing the parent compound mixture into a reactor with heat energy input, where the atomization die generates fine droplets as spray or aerosol; subjecting the fine droplets formed to pyrolysis and combustion, and; reducing the mixed oxide particles formed and collected as homogenous powder, obtaining permanent magnetic particles; being a simple method and allowing to obtain homogeneous and versatile compositions, especially for Rare Earth-Transition Metal (RETM) type permanent magnets, where RE (rare earth) can be, for example, an element such as neodymium, praseodymium, dysprosium or a combination thereof, among other possibilities, and TM (transition metal) can be, for example, iron, cobalt, nickel or a combination thereof.Type: ApplicationFiled: April 23, 2012Publication date: December 27, 2012Inventors: Claudio FERNANDEZ ACEVEDO, Luis Martinez De Morentin Osaba, Tamara Oroz Mateo, Cristina Salazar Castro, Angelica Perez Manso, Ana Carmen Esparza Hermoso
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Patent number: 8323374Abstract: Fine composite metal particle comprising a metal core and a coating layer of carbon, and being obtained by reducing metal oxide powder with carbon powder.Type: GrantFiled: January 4, 2011Date of Patent: December 4, 2012Assignee: Hitachi Metals, Ltd.Inventors: Yasushi Kaneko, Shigeo Fujii, Hisato Tokoro, Takeo Oku
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Patent number: 8252124Abstract: The present invention provides a powder magnetic core low in the loss and high in the saturation magnetic flux density and a method for manufacturing the same. More specifically, the present invention provides a powder magnetic core that comprises a soft magnetic metal powder having an average particle size (D50) of 0.5 to 5 ?m, a half width of diffraction peak in a <110> direction of ?-Fe as measured by X-ray powder diffraction of 0.2 to 5.0°, and an Fe content of 97.0% by mass or more, the core having an oxygen content of 2.0% by mass or more.Type: GrantFiled: March 11, 2011Date of Patent: August 28, 2012Assignee: TDK CorporationInventors: Masahito Koeda, Tomofumi Kuroda, Tomokazu Ishikura, Akihiro Harada, Hiroyuki Ono, Osamu Kido, Satoko Ueda
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Patent number: 8157889Abstract: A magnetic metal powder having fluidity is provided which is composed of FePt nanoparticles synthesized by the polyol synthesis method that possess fct (face-centered tetragonal) structure and exhibit crystal magnetic anisotropy from immediately after synthesis. Specifically, there is provided a magnetic metal powder having fluidity which is composed of magnetic metal particles whose main components and the contents thereof are represented by the following general formula (1): [TXM1?X]YZ1?Y??(1), where T is one or both of Fe and Co, M is one or both of Pt and Pd, Z is at least one member selected from the group composed of Ag, Cu, Bi, Sb, Pb and Sn, X represents 0.3˜0.7, and Y represents 0.7˜1.Type: GrantFiled: November 12, 2008Date of Patent: April 17, 2012Assignee: Dowa Electronics Materials Co., Ltd.Inventor: Kazuyuki Tohji
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Patent number: 8110048Abstract: A method for producing a magnetic powder comprised chiefly of Fe16N2 comprising providing a starting powder comprising an oxy-hydroxide or oxide of iron and an amount of noble metal. The starting powder is reduced into an iron powder by a dry method using a hydrogen gas; and the iron powder is nitrided into a magnetic powder comprised chiefly of Fe16N2 particles using a nitrogen-containing gas at a temperature not higher than 200° C. The amount of noble metal is such that an amount that the atomic percent ratio of the noble metal content to Fe in the magnetic powder is 0.01-10.Type: GrantFiled: January 7, 2011Date of Patent: February 7, 2012Assignee: Dowa Electronics Materials Co., Ltd.Inventors: Kenji Masada, Yuzo Ishikawa, Hiroshi Kimura
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Patent number: 8038762Abstract: A process for production of a chain metal powder, which comprises the steps of reducing metal ions contained in an aqueous solution, while applying a magnetic filed to the solution, in the presence of both a reducing agent capable of generating a gas during the reduction of metal ions and a foamable water soluble compound, through the generation of a gas, a bubble layer on the surface of the aqueous solution to form a chain metal powder, separating the bubble layer formed on the surface of the aqueous solution from the solution, and collecting the chain metal powder contained in the bubble layer.Type: GrantFiled: January 13, 2010Date of Patent: October 18, 2011Assignee: Sumitomo Electric Industries, Ltd.Inventors: Tetsuya Kuwabara, Hideaki Toshioka, Hideki Kashihara, Keiji Koyama, Takashi Sakai
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Publication number: 20110061496Abstract: A metal magnetic powder for a magnetic recording medium is provided whose particles have a metal magnetic phase, composed mainly of Fe or Fe plus Co, and an oxide layer, wherein the average major axis length of the powder particles is 10-50 nm, the average particle volume including the oxide layer is 5,000 nm3 or less, the atomic ratio (R+Al+Si)/(Fe+Co) calculated using the content values (at. %) of the elements contained in the powder particles is 20% or less, where R is rare earth element (Y being treated as a rare earth element). The metal magnetic powder is obtained by using a complexing agent and a reducing agent to elute nonmagnetic constituents after firing. The metal magnetic powder exhibits a large saturation magnetization as for its particle volume while maintaining weatherability comparable to the conventional level and is suitable for a coated-type magnetic recording medium.Type: ApplicationFiled: November 23, 2010Publication date: March 17, 2011Applicant: DOWA ELECTRONICS MATERIALS CO., LTD.Inventors: Takayuki YOSHIDA, Masatoshi NAKAYAMA, Ryota IGARASHI
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Patent number: 7892316Abstract: Fine composite metal particle comprising a metal core and a coating layer of carbon, and being obtained by reducing metal oxide powder with carbon powder.Type: GrantFiled: March 1, 2007Date of Patent: February 22, 2011Assignee: Hitachi Metals, Ltd.Inventors: Yasushi Kaneko, Shigeo Fujii, Hisato Tokoro
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Patent number: 7850760Abstract: A chain metal powder, which is free from branches and has a small distribution of the chain length, can be produced by a process of reducing metal ions contained in an aqueous solution, while applying a magnetic field to the solution containing ferromagnetic ions, in the presence of a polymer compound comprising repeating units of the formula (1): and repeating unit of the formula (2): or repeating unit of the formula (4); or a process which comprises the steps of reducing metal ions contained in an aqueous solution, while applying a magnetic filed to the solution, in the presence of both a reducing agent capable of generating a gas during the reduction of metal ions and a foamable water soluble compound, through the generation of a gas, a bubble layer on the surface of the aqueous solution to form a chain metal powder, separating the bubble layer formed on the surface of the aqueous solution from the solution, and collecting the chain metal powder contained in the bubble layer.Type: GrantFiled: April 27, 2005Date of Patent: December 14, 2010Assignee: Sumitomo Electric Industries, Ltd.Inventors: Tetsuya Kuwabara, Hideaki Toshioka, Hideki Kashihara, Keiji Koyama, Takashi Sakai
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Patent number: 7763094Abstract: A precursor particle having a particle size of 10 nm or more and 1 ?m or less, and comprising a first compound selected from an alkoxide, a hydroxide, a sulfate, a nitrate, a carbonate, or a carboxylate of magnetic metal containing at least one metal of Fe and Co, and a second compound selected from an alkoxide or a hydroxide, a sulfate, a nitrate, a carbonate, or a carboxylate of a metal element for forming an oxide, is prepared. Then the precursor particle is heated in a reducing atmosphere to form an insulating particle made of an oxide of the metal element by decomposing the second compound, and to precipitate a particle of the magnetic metal in the insulating particle at a particle size of 1 nm or more and 100 nm or less, thereby manufacturing a high frequency magnetic material.Type: GrantFiled: July 23, 2007Date of Patent: July 27, 2010Assignee: Kabushiki Kaisha ToshibaInventors: Tomohiro Suetsuna, Seiichi Suenaga, Kouichi Harada, Maki Yonetsu
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Patent number: 7744673Abstract: In accordance with invention, there are methods for fabricating hollow spheres and nanofoams. The method for making hollow spheres can include providing a homogeneous precursor solution including a first solvent and one or more anhydrous precursor species and forming aerosol droplets having a first size distribution using the homogeneous precursor solution in an anhydrous carrier gas. The method can also include transporting the aerosol droplets through an aerosol reactor including a reactant to form a plurality of hollow spheres, wherein each of the plurality of hollow spheres can be formed by one or more chemical reactions occurring at a surface of the aerosol droplet. The method can further include controlling size and thickness of the hollow spheres by one or more of the precursor solution concentration, aerosol droplet size, temperature, residence time of the aerosol droplets in the aerosol reactor, and the reactant distribution in the aerosol reactor.Type: GrantFiled: October 22, 2007Date of Patent: June 29, 2010Assignee: STC.UNMInventors: Xingmao Jiang, Charles Jeffrey Brinker
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Patent number: 7708910Abstract: The present invention relates to ink jet printing ink consisting of an independently dispersed metal ultrafine particles-containing liquid dispersion in which the metal ultrafine particles having a particle size of not more than 100 nm are independently and uniformly dispersed and which is excellent in characteristic properties required for ink. The ink is used in the printing or the formation of conductive circuits using an ink jet printer.Type: GrantFiled: October 21, 2001Date of Patent: May 4, 2010Assignee: ULVAC, Inc.Inventors: Noriyuki Abe, Masaaki Oda
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Patent number: 7704297Abstract: A melt of nickel nitrate hydrate is introduced as droplets or liquid flow into a heated reaction vessel and thermally decomposed in a gas phase at a temperature of 1200° C. or more and at an oxygen partial pressure equal to or below the equilibrium oxygen pressure of nickel-nickel oxide at that temperature to manufacture a highly crystalline fine nickel powder with an extremely narrow particle size distribution. The oxygen partial pressure during the thermal decomposition is preferably 10?2 Pa or less, and a metal other than nickel, a semimetal and/or a compound of these may be added to the nickel nitrate hydrate melt to manufacture a highly crystalline nickel alloy powder or highly crystalline nickel composite powder. The resultant powder is suited in particular to thick film pastes such as conductor pastes for manufacturing ceramic multilayer electronic components.Type: GrantFiled: April 3, 2007Date of Patent: April 27, 2010Assignee: Shoei Chemical Inc.Inventors: Yuji Akimoto, Kazuro Nagashima, Hidenori Ieda, Tetsuya Kimura
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Publication number: 20100035087Abstract: The present invention relates to ferromagnetic metal particles having an average major axis diameter (L) of 10 to 100 nm which satisfy a relationship between the average major axis diameter (L) and a particle SFD represented by the following formula: Particle SFD?0.0001 L2?0.0217 L+1.75; a process for producing the ferromagnetic metal particles; and a magnetic recording medium using the ferromagnetic metal particles.Type: ApplicationFiled: August 5, 2009Publication date: February 11, 2010Applicant: TODA KOGYO CORPORATIONInventors: Hiroko Morii, Keisuke Iwasaki, Seiji Ishitani, Mineko Ohsugi, Shinji Horie, Toshiharu Harada, Takehiro Matsuo, Yosuke Yamamoto, Kazuyuki Hayashi
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Patent number: 7648555Abstract: Disclosed is a method for carrying out a reaction in a microreaction chamber. Nanoparticles which have been advantageously subjected to specific reactions in the microreaction chamber are used for carrying out the reaction. The obtained reaction product, which is preferably also provided in the form of nanoparticles. can then be removed from the microreaction chamber. Advantageously, the ongoing reaction can be specifically influenced by using the microreaction chamber. Both endothermic and exothermic reactions can be carried out with an accurately predictable result by feeding energy in a dosed manner into/out of the reaction chamber.Type: GrantFiled: September 27, 2006Date of Patent: January 19, 2010Assignee: Siemens AktiengesellschaftInventors: Frank Arndt, Jens Dahl Jensen, Ursus Krüger, Hendrik Rönsch
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Patent number: 7544230Abstract: The solution I is spouted from a first nozzle into a mixing chamber as a high-pressure jet stream of not less than 1 MPa and as a turbulent flow having a Reynolds number of not less than 10000 during the flow into the mixing chamber, and the solution II having a lower pressure than the solution I is spouted from a second nozzle into the mixing chamber as an orthogonal flow which intersects the solution I almost at right angles. The two solutions are mixed together and caused to react with each other, with the result that a mixed reaction solution Z containing alloy particles Z is formed.Type: GrantFiled: March 4, 2004Date of Patent: June 9, 2009Assignee: FUJIFILM CorporationInventors: Fumiko Shiraishi, Yasunori Ichikawa, Koukichi Waki, Yasushi Hattori
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Patent number: 7497892Abstract: Magnetic particles of the present invention comprising monocrystals of rare earth element-transition metal-metalloid having particle diameters of 5 nm to 50 nm. The magnetic particles are produced by a producing method comprising a step of fabricating a quenched thin band comprising rare earth element-transition metal-metalloid. A magnetic recording medium of the present invention includes the magnetic layer which contains therein the magnetic particles and the binder, and which is formed on the non-magnetic substrate.Type: GrantFiled: September 30, 2005Date of Patent: March 3, 2009Assignee: FUJIFILM CorporationInventor: Yasushi Hattori