Abstract: A process for the production of a metal mixture composition containing lead and tin, and comprising by weight at least 10% tin and 45% lead, at least 90% of tin and lead together, more lead than tin, from 1-5000 ppm of copper, at least 0.42% antimony and at least 0.0001% wt of sulphur, at most 0.1% of the total of chromium, manganese, vanadium, titanium and tungsten, and at most 0.1% of each one of aluminium, nickel, iron and zinc. The process includes a pre-treatment step for producing the metal mixture composition, followed by a vacuum distillation step wherein lead is removed by evaporation and a bottom stream is obtained comprising at least 0.6% wt of lead.

Abstract: A method for recycling a lithium iron phosphate positive plate with low energy consumption and low Al content, including: crushing a lithium iron phosphate positive plate to be recycled into a granular material with a particle size of 1-15 mm by using a crusher; heating the granular material obtained in step (1) to 350-500° C. in an atmosphere furnace in an inert atmosphere; and keeping the granular material at 350-500° C. for 0.5-2 h followed by cooling to a preset temperature to obtain a calcined product; grinding the calcined product obtained in step (2) by using a grinder to obtain a ground product with D50 larger than or equal to 50 ?m; and classifying the ground product obtained in step (3) by using an air classifier to remove Al simple substance to obtain a recovered positive material with an Al content below 200 ppm.

Abstract: A method and a device using pyrolysis for recycling used printed circuit board in which water (moisture) is introduced in the pyrolysis process and a fully sealed low pressure environment is established to ensure that no combustion happens in the pyrolysis process to enhance the safety of the process; pyrolysis gases generated in the process are concentrated and purified to provide useful fuels or chemical materials; therefore, the present invention can reduce process cost, improve recycling efficiency and provide processing device with high safety, thereby enhancing industry usability.

Abstract: A method of reduction treatment of metal oxides characterized by using as a material a powder containing metal oxides and containing alkali metals and halogen elements and further, in accordance with need, carbon, mixing said material with water to produce a slurry, then dehydrating this and charging the dehydrated material, mixed with another material in accordance with need, into a rotary hearth type reduction furnace for reduction.

Abstract: The present invention solves the problem of the bonding strength of a Pb-free alloy solder being inferior to that of the conventional Pb-containing alloy solder and provides a Pb-free alloy solder satisfactory in bonding reliability. An alloy solder is manufactured by adding a predetermined amount of carbon to a Pb-free solder in a high-temperature atmosphere of a temperature in the range of 800° C. to 1200° C. An alloy solder manufacturing method includes a melting process for melting a Pb-free solder by heating the Pb-free solder in a high-temperature atmosphere of a temperature in the range of 800° C. to 1200° C.

Abstract: The present invention describes a method of recycling lead from lead containing waste, the method comprising the steps of mixing the battery paste with aqueous citric acid solution so as to generate lead citrate; isolating lead citrate from the aqueous solution; and converting the lead citrate to lead and/or lead oxide.

Abstract: A method for recovering catalytic metals from fluids containing catalytic metal colloids. Fluid compositions such as rinse solutions or dragout baths containing catalytic metal colloids are passed through a filter that entraps catalytic metal colloids on the filter. The catalytic metal colloids have a high affinity for the filter in contrast to other components of the fluids. The other components of the fluids pass through the filter while the catalytic colloids concentrate on the filter. The filter containing the catalytic metal colloids is burned, and the catalytic metal is retrieved. The method is economically efficient and environmentally friendly.

Abstract: A method for recovering catalytic metals from fluid compositions containing catalytic metal colloids. Fluid compositions such as aqueous rinse solutions or dragout baths containing catalytic metal colloids are passed through a porous metal filter that entraps the catalytic metal colloids. The catalytic metal colloids have a high affinity for the porous metal filter in contrast to other components of the fluids. The other components of the fluids pass through the porous metal filter while the catalytic metal colloids concentrate on the porous metal filter. The catalytic metal colloids that are captured on the porous metal filter are removed from the filter by backwashing the filter with a gas and/or a liquid. The backwashing forces the catalytic metal colloids off of the porous metal filter and through a solids discharge valve and into a solids collection container. The method is economically efficient with high catalytic metal recovery and is environmentally friendly.

Abstract: A method for treating steel works dust in order to recuperate elements capable of being upgraded. The method comprises attrition in water followed by hydraulic grading of the resulting load. The method is characterized in that is further comprises: a washing step to separate the water soluble saline fractions of the insoluble oxides; hot treatment to eliminate metals in the form of free oxides such as zinc and lead; treatment by heating at a temperature ranging between 240 and 800° C.; treatment with sulphuric acid having a concentration between 5 and 8%.

Abstract: A soldering ball fabrication method includes the steps of: (1) drawing a metal wire rod into the desired thickness, (2) cutting the metal wire thus obtained into pieces subject to the desired length, (3) washing the pieces of metal wire to remove dust, (4) processing the pieces of metal wire into balls, (5) washing the balls thus obtained, (6) using a screen to select the balls, (7) inspecting selected balls, and (8) obtaining approved soldering balls.

Abstract: A treating method of recovering zinc in the metal state from a waste containing the zinc in the oxide state, lead, chlorine, fluorine, and water comprising a mixing process 90 of obtaining a to-be-treated mixed material 70 by mixing a steel dust 7 and a reducing material 8 together; a chlorine recovery process 91 of recovering the chlorine and the water by heating the to-be-treated mixed material 70; a lead recovery process 92 of recovering fluorine and lead by heating the to-be-treated mixed material 70 under vacuum; a zinc recovery process 93 of recovering metallic zinc by heating the to-be-treated mixed material 70 at a temperature higher than that in the lead recovery process 92 with the vacuum state maintained so as to reduce and vaporize zinc; and a residue recovery process 94 of recovering a residue 79 of the to-be-treated mixed material 70. This construction allows the metallic zinc to be recovered at a high purity from a zinc oxide-containing waste and an on-site treatment to be accomplished.

Abstract: An improved method for the recovery of lead from exhausted lead-acid storage batteries, comprising removal from the storage battery of the sulphuric acid solution, the coating element, the separators between the electrodes and the metal part i.e. grids, connectors and poles and milling of the remaining electrode paste of the storage battery to obtain an extremely fine powder (pastel),characterised by the following operations:a) treatment of the resulting powder with an aqueous saline solution, with a pH of between 0 and 8, capable of solubilising Pb (II) sulphate and oxide, leaving Pb (IV) oxide unsolubilised;b) reduction to metal lead of the bivalent lead ion, present in the soluble fraction, using metal iron, preferably in slight excess with respect to the stoichiometric proportions;c) reduction of the tetravalent lead oxide; andd) recovery of the salts used in the process step a) by elimination of the iron sulphate that has formed. FIG.

Abstract: A method of recovering lead is proposed, wherein preliminarily crushed recycable raw material composed of spent lead-sulphuric acid storage batteries is subjected to treatment with an alkaline solution, as a result of which metallic lead, taken out of the process, and pulp, to be subjected to mechanical separation, are obtained. As a result of the separation, a lead-containing (as inclusions) polymer material and a suspension, which is a mixture of a sodium sulfate solution having lead oxide particles therein, are obtained. The suspension is separated, as a result of which lead oxides are taken out of the process, while the sodium sulfate solution is subjected to electrochemical treatment, as a result of which sulphuric acid and an alkaline solution are obtained, the alkaline solution being fed for treatment of the lead-containing (as inclusions) polymer material.

Abstract: It has been found that Ambrosia sp. and Apocynum sp. accumulate lead in the leaves, stems, and roots when it grows in soil containing organic or inorganic species of lead. Lead is accumulated in the leaves and stems to a greater extent than in most other plants. Lead can be economically recovered from contaminated soil and sludge by harvesting Ambrosia sp. or Apocynum sp. grown in media containing high concentrations of lead.

Abstract: Indium-containing feedstocks, such as flue dusts from a refining or smelting process, are treated to increase the concentration of indium and at the same time to reduce the concentrations of lead, copper, and arsenic. The flue dusts are treated in a sodium-doped lead bath at temperatures of 675.degree. to 800.degree. C. Soda ash in the amount of 15 to 35 weight percent is blended with the feed stock and added to the sodium-doped lead bullion. The sodium reacts with the dusts to form a liquid dross, which is removed, cooled, and crushed. The powdered dross is water leached to remove the sodium salts. The indium remains in the filler cake and can be processed by conventional methods for the recovery of indium. About 95% of the indium reports to the filter cake, while lead retention in the filter cake is only about 5-15% of the initial lead content in the dust. A majority of the zinc also reports to the filter cake.

Abstract: This invention concerns a process for recovering metal values from jarosite-containing materials by leaching with a calcium chloride solution at a temperature above about the atmospheric boiling point of the solution and under at least the autogenous pressure.