With Leaching, Dissolving, Or Washing Patents (Class 75/753)
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Patent number: 7846233Abstract: A method of leaching copper from copper sulphide-containing concentrates, such as chalcopyrite, includes using pyrite as a catalyst for ferric reduction in order to eliminate passivation of the chalcopyrite surface, the process being carried out under conditions whereby the pyrite is not materially oxidized, for example by maintaining the operating solution potential at a suitable level. The leaching is carried out in an acidic sulphate medium and may include oxidation by oxygen-containing gas. The leached copper is then recovered, for example by solvent extraction and electrowinning. The leaching process can result in the virtually complete extraction of copper at atmospheric pressure in as little as four hours.Type: GrantFiled: June 1, 2005Date of Patent: December 7, 2010Assignee: The University of British ColumbiaInventors: David G. Dixon, Alain F. Tshilombo
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Patent number: 7544229Abstract: The present invention discloses a novel method for the production of metallic nano-powder. This cost-effective, simple process is customized for a full-scale production of metallic nano-powders containing a first metal, and comprising the following of forming an alloy comprising said first metal and at least one soluble metal; applying first thermal treatment in the manner homogenized alloy is obtained; applying a cold work to the homogenized alloy so thin strips are obtained; applying a second thermal treatment to the alloy until a phase composition of predetermined characteristics is obtained; subjecting the said alloy to a leaching agent adapted to effectively leach out the least one soluble metal; filtering and washing the powder; washing the powder; drying the powder; coating the powder with chemicals; and then de-agglomerating the coated powder. The present invention also discloses a cost-effective and highly pure metallic powder produced by the method defined above.Type: GrantFiled: June 19, 2003Date of Patent: June 9, 2009Assignee: Cima NanoTech Israel Ltd.Inventors: Arkady Garbar, Fernando De La Vega, Einat Matzner
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Patent number: 6861098Abstract: A method for forming a superhard polycrystalline diamond or diamond-like element with greatly improved resistance to thermal degradation without loss of impact strength. Collectively called PCD elements, these elements are formed with a binder-catalyzing material in a high-temperature, high-pressure process. The PCD element has a plurality of partially bonded diamond or diamond-like crystals forming at least one continuous diamond matrix, and the interstices among the diamond crystals forming at least one continuous interstitial matrix containing a catalyzing material. The element has a working surface and a body, where a portion of the interstitial matrix in the body adjacent to the working surface is substantially free of the catalyzing material to a depth from the working surface, the remaining interstitial matrix contains the catalyzing material, causing a 950 degrees C. temperature at the working surface to be less than 750 degrees C. at the depth.Type: GrantFiled: October 1, 2003Date of Patent: March 1, 2005Assignee: ReedHycalog UK LtdInventors: Nigel Dennis Griffin, Peter Raymond Hughes
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Patent number: 6797326Abstract: Griffin, Nigel, et al78.1081-1.3-29 Disclosed is a method for manufacturing a polycrystalline diamond or diamond-like element with greatly improved wear resistance without loss of impact strength. These elements are formed with a binder-catalyzing material in a high-temperature, high-pressure (HTHP) process. The PCD element has a body with a plurality of bonded diamond or diamond-like crystals forming a continuous diamond matrix that has a diamond volume density greater than 85%. Interstices among the diamond crystals form a continuous interstitial matrix containing a catalyzing material. The diamond matrix table is formed and integrally bonded with a metallic substrate containing the catalyzing material during the HTHP process. The diamond matrix body has a working surface, where a portion of the interstitial matrix in the body adjacent to the working surface is substantially free of the catalyzing material, and the remaining interstitial matrix contains the catalyzing material.Type: GrantFiled: October 9, 2002Date of Patent: September 28, 2004Assignee: Reedhycalog UK Ltd.Inventors: Nigel Dennis Griffin, Peter Raymond Hughes
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Patent number: 6696029Abstract: A method for the recovery of high purity zinc oxide products, and optionally iron-carbon feedstocks, from industrial waste streams containing zinc oxide and/or iron. The waste streams preliminary can be treated by adding carbon and an ammonium chloride solution, separating any undissolved components from the solution, displacing undesired metal ions from the solution using zinc metal, treating the solution to remove therefrom zinc compounds, and further treating the zinc compounds and the undissolved components, as necessary, resulting in the zinc products and the optional iron-carbon feedbacks. Once the zinc oxide has been recovered, the purification process is used to further purify the zinc oxide to obtain zinc oxide which is at least 99.8% pure and which has predeterminable purity and particle characteristics. Various zinc compounds may then be quickly, easily, and economically produced from this recovered zinc oxide.Type: GrantFiled: January 29, 1996Date of Patent: February 24, 2004Inventors: Allan S Myerson, Peter Robinson, Stephan Tabah
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Patent number: 6221129Abstract: A flux which contains irreversibly dehydrated K2AlF5, for soldering light metal materials, in particular aluminum. The flux has the advantages of forming a very uniform flux coating on the workpiece or workpieces to be soldered and exhibiting outstanding flow of the solder. An appropriate soldering process, an aqueous flux suspension and preparation processes for the flux are also disclosed.Type: GrantFiled: April 25, 2000Date of Patent: April 24, 2001Assignee: Solvay Fluor und Derivate GmbHInventors: Heinz-Joachim Belt, Alfred Borinski, Ruediger Sander, Werner Rudolph
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Patent number: 6033579Abstract: The invention covers a process for dehydration/filtration, and washing of red mud, if applicable with addition of sand, particularly from the Bayer process for aluminum production from bauxite, in which filters are used and caustic is washed out on the filter. The invention is basically characterized by washing and dehydration being effected under pressure above atmospheric with regeneration of bound caustic and production of a residue with a high solids concentration. In addition, the invention covers a plant for the implementation of the process.Type: GrantFiled: October 16, 1997Date of Patent: March 7, 2000Assignee: Andritz-Patentverwaltungs-Gesellschaft m.b.HInventors: Hubert Riemer, Nils Oeberg, Heinz Perchthaler, Paolo Murgia, Mario Noriega
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Patent number: 5942198Abstract: The beneficiation of an electric arc furnace (EAF) dust waste stream comprising zinc compounds by collecting and combining dust from two or more EAF batches with coal fines to form briquettes, adding the briquettes to a final EAF batch with the charge, and collecting the dust from the final EAF batch, so that the zinc in the beneficiated dust is of a greater proportion than in a typical batch of EAF dust. Alternatively, the EAF dust can be split into two dust streams, one of which is returned to the EAF, while the other is treated in a hydrometallurgical process. Either waste stream preliminary can be treated by adding carbon and an ammonium chloride solution, separating any undissolved components from the solution, displacing undesired metal ions from the solution using zinc metal, treating the solution to remove therefrom zinc compounds, and further treating the zinc compounds and the undissolved components resulting in zinc products and an optional iron-carbon feedback.Type: GrantFiled: June 27, 1996Date of Patent: August 24, 1999Assignee: Metals Recycling Technologies Corp.Inventors: Allan S. Myerson, Peter Robinson
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Patent number: 5820653Abstract: This invention relates to a process for making a shaped copper article directly from a copper-bearing material, comprising: (A) contacting said copper-bearing material with an effective amount of at least one aqueous leaching solution to dissolve copper ions into said leaching solution and form a copper-rich aqueous leaching solution; (B) contacting said copper-rich aqueous leaching solution with an effective amount of at least one water-insoluble extractant to transfer copper ions from said copper-rich aqueous leaching solution to said extractant to form a copper-rich extractant and a copper-depleted aqueous leaching solution; (C) separating said copper-rich extractant from said copper-depleted aqueous leaching solution; (D) contacting said copper-rich extractant with an effective amount of at least one aqueous stripping solution to transfer copper ions from said extractant to said stripping solution to form a copper-rich stripping solution and a copper-depleted extractant; (E) separating said copper-rich stType: GrantFiled: April 18, 1996Date of Patent: October 13, 1998Assignee: ElectroCopper Products LimitedInventors: Michael A. Eamon, Robert J. Fedor, Sharon K. Young, Susan S. Enos, Wendy M. Gort, Roger N. Wright, Stephen J. Kohut
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Patent number: 5582631Abstract: A method for the production of an iron-based feedstock suitable for use as the feedstock for steel mills, from industrial waste streams containing iron, by combining an iron poor material such as exhaust fumes from metals production processes with the waste streams, treating the combined waste stream with an ammonium chloride leaching solution, separating the undissolved precipitates comprising iron compounds from the leachant solution, and further treating the undissolved precipitants by elevated temperature roasting, resulting in the iron-based feedstocks.Type: GrantFiled: January 31, 1995Date of Patent: December 10, 1996Assignee: Metals Recycling Technologies Corp.Inventors: Allan S. Myerson, Charles A. Burrows, Charles Sanzenbacher, Paul R. DiBella
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Patent number: 5571306Abstract: A method for the production of an enriched iron product, specifically direct reduced iron and iron oxide suitable for use as the feedstock for steel mills, from industrial waste streams containing iron, by combining an iron oxide rich material such as mill scale and/or used batteries with the waste streams, treating the combined waste stream with an ammonium chloride leaching solution, separating the undissolved precipitates comprising iron compounds from the leachant solution, and further treating the undissolved precipitants by elevated temperature roasting, resulting in the iron feedstocks.Type: GrantFiled: December 21, 1994Date of Patent: November 5, 1996Assignee: Metals Recycling Technologies Corp.Inventors: Allan S. Myerson, Charles A. Burrows, Paul R. DiBella
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Patent number: 5458746Abstract: This invention is directed to a process for making copper metal powder from copper-bearing material, comprising: (A) contacting said copper-bearing material with an effective amount of at least one aqueous leaching solution to dissolve copper ions in said leaching solution and form a copper-rich aqueous leaching solution; (B) contacting said copper-rich aqueous leaching solution with an effective amount of at least one water-insoluble extractant to transfer copper ions from said copper-rich aqueous leaching solution to said extractant to form a copper-rich extractant and a copper-depleted aqueous leaching solution, said extractant comprising (i) at least one oxime characterized by a hydrocarbon linkage with at least one --OH group and at least one .dbd.Type: GrantFiled: August 9, 1994Date of Patent: October 17, 1995Assignees: Magma Copper Company, Gould Electronics Inc.Inventors: David P. Burgess, Wendy M. Gort, Ronald K. Haines, Jackson G. Jenkins, Stephen J. Kohut, Peter Peckham