Abstract: The invention concerns an iron powder characterised by spherical form and a porous structure throughout. The powder particles have an average particle diameter between 10 and 300 &mgr;m, a specific surface area of at least 100 m2/kg, a flowability of at least 35 s/50 g, a reactivity of less than 5 minutes and an apparent density lower than about 4 g/cm3. The iron powder is prepared by subjecting a dry powder of essentially spherical iron-containing agglomerates to a heat treatment in a reducing atmosphere at a temperature and time sufficient for obtaining particles essentially consisting of metallic iron and having a porous structure throughout. The obtained particles may then be subjected to sintering at a time and temperature sufficient for obtaining the required strength.

Abstract: A solder ball having a diameter of 1.2 mm or less, a dispersion of a diameter distribution of 5% or less and sphericity of 0.95 or more, an area ratio of the maximum dendrite being 80% or less of a cross section including a center of the solder ball, comprises a first additional element of 0.5-8 mass % of Ag and/or 0.1-3 mass % of Cu, and 0.006-10 mass %, in total, of at least one second additional element selected from the group consisting of Bi, Ge, Ni, P, Mn, Au, Pd, Pt, S, In and Sb, the balance being substantially Sn. The solder ball is produced by a uniform droplet-spraying method comprising the steps of vibrating a melt of a solder alloy in a crucible under pressure to force the melt to drop through orifices of the crucible; permitting the melt dropping through the orifices to become spherical droplets in a non-oxidizing gas atmosphere; and rapidly solidifying them.

Abstract: Method for manufacturing solder balls is disclosed. The apparatus comprises a tundish, a vibrator, a cooling liquid tank, an inactive atmospheric chamber, a molten metal receiving tray, a ball collecting barrel and a cooling liquid reservoir. The tundish has orifices at its bottom. The vibrator is immersed in the molten metal of the tundish and generates vibrations. The cooling liquid tank is situated under the tundish and is provided with a cooling liquid heater at its upper and middle outer surface and a cooling liquid cooler at its lower outer surface. The inactive atmospheric chamber is interposed between the bottom of the tundish and the top surface of the cooling liquid. The molten metal receiving tray is seated on a portion of the inactive atmospheric chamber and is horizontally movable. The ball collecting barrel is positioned under the cooling liquid tank and is provided with a cut-off valve at its top, a ball removing valve at its bottom and a cooling liquid supply conduit at its upper portion.

Abstract: Ultrafine spherical nickel powder for use in a laminate ceramics capacitor is produced through a process employing a vapor phase chemical reaction between nickel chloride and hydrogen. The process includes the steps of: i) charging a reaction vessel with nickel chloride and evaporating the nickel chloride to generate vapor of nickel chloride; ii) mixing an inert gas with the vapor of the nickel chloride to form a mixture gas having a nickel chloride gas concentration of 0.05 to 0.3, and sending the mixture gas to a reaction zone; iii) bringing, in the reaction zone, the mixture gas into contact and mixing with hydrogen which is supplied from a nozzle at a temperature of 1004.degree. C. to 1453.degree. C., in such a manner that the flow rate ratio of the hydrogen to the mixture gas meets the condition of (H.sub.2 /(NiCl.sub.2 +inert gas)) <1, thereby causing the chemical reaction; and iv) cooling the generated ultrafine nickel powder together with the gas and collecting the ultrafine nickel powder.

Abstract: Ferrous powder particles are coated with vaporized phosphorus in a fluid-bed reactor to obtain homogeneous coatings of phosphorus. The coated powders are useful feed for pressed structural parts, exhibiting improved green density, compressibility and sintered density thus improving magnetic and tensile properties.

Abstract: A pressure medium composed of plural kinds of fluids each of which have a different density is charged in a pressure chamber forming, for example, fluid layers. A material is suspended by way of buoyancy brought by this pressure medium. By properly controlling the density of the pressure medium of plural kinds of fluids, various kinds of materials having different densities can be supported in a suspending state at an almost constant pressure. The apparatus and the method processes the material under a state of compensated-gravitation, and is capable of forming an easy-handling weightless state for a long period of time at low cost in a simple manner for ease of handling of the material being processed and can contribute to developing useful materials and novel materials and to the supplying of them in bulk.

Abstract: A compacted, single phase or multiphase composite article. Particles for use in the compacted article are produced by providing a precursor compound containing at least one or at least two metals and a coordinating ligand. The compound is heated to remove the coordinating ligand therefrom and increase the surface area thereof. It may then be reacted so that at least one metal forms a metal-containing compound. The particles may be consolidated to form a compacted article, and for this purpose may be used in combination with graphite or diamonds. The metal-containing compound may be a nonmetallic compound including carbides, nitrides and carbonitrides of a refractory metal, such as tungsten. The metal-containing compound may be dispersed in a metal matrix, such as iron, nickel or cobalt. The dispersed nonmetallic compound particles are no larger than about 0.1 micron in particle size and have a volume fraction greater than about 0.15 within the metal matrix.

Abstract: Method for making hollow microspheres of substantially uniform diameter and of substantially uniform wall thickness is disclosed. The walls of the hollow microspheres comprise sintered together particles which define interconnecting voids within the walls and a single central cavity in the interior of the microspheres and inner and outer microsphere wall surfaces. The interconnecting voids are continuous and extend from the outer wall surface to the inner wall surface. The walls have substantially uniform void content and the interconnecting voids are substantially uniformly distributed in the walls of the hollow microspheres and the walls of the hollow microspheres are free of latent solid or liquid blowing gas materials and are substantially free of relatively thinned wall portions and bubbles. The method includes heating the microspheres for a sufficient period of time to close and seal the interconnecting void.

Abstract: The invention relates to a method of heat processing particles of glass. A first current of a mixture of a combustible gas and a gas capable of oxidizing the combustible gas is introduced into a substantially cylindrical chamber from its lower end. The combustible gas is ignited to form a flame in which the gases have a speed of less than 10 m/s. The resulting flame creates a heat processing zone in the chamber. A quenching zone is provided by a second current of gas introduced into the chamber adjacent the chamber side wall such that it swirls around the flame. Particles of glass are then introduced at the lower end of the chamber and these particles contact the flame in the heat processing zone and are then directed to the quenching zone where they are hardened and from which they are collected.