Spray Nozzle Patents (Class 96/203)
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Publication number: 20150135959Abstract: [Problem] To provide a deoxidation apparatus (4) with improved efficiency in absorbing degassing gas and dissolved oxygen in treated water. [Solution] A deoxidation apparatus (4) in which by bringing the degassing gas into contact with the treated water, causes dissolved oxygen in treated water to be absorbed by degassing gas and lowers the dissolved oxygen concentration of the treated water. The deoxidation apparatus includes the following: a gas-liquid contact tower (42) that has the shape of a lower end open container, at least the lower end of which is submerged below the surface of the treated water that is to be treated, forming an internal sealed space (421); a degassing gas supply unit (43) that supplies degassing gas to the sealed space (421), filling the sealed space (421) with degassing gas; and a treated water dispersion unit (41) that disperses the supplied treated water within the sealed space (421) in the form of a mist through a dispersion nozzle unit (412).Type: ApplicationFiled: August 30, 2012Publication date: May 21, 2015Inventors: Masahiro Takatsuka, Hiroshi Okajima, Takahiro Matsumura, Hiromu Akita, Daisuke Koiwai
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Patent number: 8936670Abstract: The invention relates to a device for treating water of the spray type, such as a deaerator or preheater. According to the invention the connection between the vessel (12) and the sprayer (34) and the supply of water to be treated comprises a pipe section (40) having a first open end in fluid communication with a treatment chamber and a second open end provided with a first flange (60) for connecting to a sprayer (34), the sprayer (34) comprising a sprayer flange (68) connected to said first flange (60), the sprayer flange (68) carrying the sprayer (34), which is in fluid communication with a connecting pipe (72) at one end thereof, the connecting pipe (72) extending through the first flange (60) to a coupling flange (74) for connection to the supply of water to be treated.Type: GrantFiled: September 26, 2012Date of Patent: January 20, 2015Assignee: Stork Thermeq B.V.Inventor: Jan Johan Averesch
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Publication number: 20130284019Abstract: A method and apparatus are disclosed for treating process water which is loaded with gaseous compounds and/or possibly with solids and comes from a wet-cleaning installation for cleaning process gas, e.g., from a melt-reduction subassembly or from a direct-reduction subassembly. Process water is introduced in a tank in a first process stage and degassed on the basis of reduced solubility of the dissolved compounds. The tank has, on its upper side, a gas-collecting chamber, in which the separated-off gases are collected and from which these are discharged. Likewise, the treated process water is discharged from the tank via a drainage means.Type: ApplicationFiled: December 6, 2011Publication date: October 31, 2013Inventors: Alois Gstoettenmayr, Hado Heckmann, Kurt Lukschander, Robert Millner, Ulrike Schmidt, Helmut Siegl, Johann Wurm
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Patent number: 8359746Abstract: A spray nozzle assembly and hub combination for operation in a boiler feedwater deaerator is disclosed, the combination including a tubular hub capable of being affixed to a wall of a deaerator tank and a spray nozzle assembly that is removably engageable with the hub, the nozzle assembly including a nozzle body, a twist lock for retaining the nozzle body relative to the hub when the nozzle body is in a fully engaged position, and a spreader moveably coupled to the nozzle body and biased by a spreader spring against opening, the spreader is capable of moving to an open position against the spreader spring bias in response to boiler feedwater pressure to form an annular opening about the spreader, thereby enabling feedwater flow.Type: GrantFiled: December 21, 2011Date of Patent: January 29, 2013Assignee: Crane Environmental, Inc.Inventors: Russell G. Burke, Tao D. Nguyen, Joseph T. Strogus
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Publication number: 20120240761Abstract: To include a boiler 11 that burns fuel F, an air heater 13 that recovers heat of flue gas 18 from the boiler 11, a first precipitator 14 that reduces dust in the flue gas 18 after heat recovery, a desulfurizer 15 that reduces sulfur oxides in the flue gas 18 after dust reduction by an absorbent, a dewaterer 32 that reduces gypsum 31 from desulfurization discharged water 30 discharged from the desulfurizer 15, a spray drying device 34 including an atomizer that atomizes a dewatering filtration fluid 33 discharged from the dewaterer 32, and a flue-gas introducing line L11 that introduces a part of the flue gas 18 into the spray drying device 34.Type: ApplicationFiled: May 31, 2011Publication date: September 27, 2012Applicant: MITSUBISHI HEAVY INDUSTRIES, LTD.Inventors: Nobuyuki Ukai, Seiji Kagawa, Tatsuto Nagayasu, Naoyuki Kamiyama, Toshihiro Fukuda
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Patent number: 8241459Abstract: A vessel header comprising a plurality of lateral flow tubes arranged in a parallel configuration and entering the vessel header through alternating header penetrations with a single header penetration per lateral flow tube. A method of increasing the throughput of a polymerization reaction comprising conducting the polymerization reaction in a reaction vessel comprising a plurality of lateral flow tubes arranged in a parallel configuration and entering the vessel header through alternating header penetrations with a single header penetration per lateral flow tube wherein the polymerization reaction displays an increase in throughput of 10% and a decrease in volatiles of from 5% to 10% when compared to a polymerization reaction carried out in a reaction vessel lacking a plurality of lateral flow tubes arranged in a parallel configuration and entering the vessel header through alternating header penetrations with a single header penetration per lateral flow tube.Type: GrantFiled: September 21, 2006Date of Patent: August 14, 2012Assignee: Fina Technology, Inc.Inventors: John Tomlinson, Roy Kennedy, Jose M. Sosa
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Publication number: 20120187050Abstract: An aeration apparatus that is immersed in diluted used seawater, which is water to be treated, and generates fine air bubbles in the diluted used seawater. This aeration apparatus includes: an air supply line L5 that supplies air 122 through blowers 121A to 121D (in an embodiment of the present invention, four blowers) serving as discharge units; a pressure gauge 125 installed in the air supply line L5; and aeration nozzles 123A each including a diffuser membrane 11 having slits for supplying the air, so that when air supply pressure exceeds a predetermined threshold value based on a result of measurement by the pressure gauge 125, supply of the air by the discharge unit is temporarily suspended.Type: ApplicationFiled: August 16, 2011Publication date: July 26, 2012Inventors: Keisuke SONODA, Shozo Nagao
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Patent number: 8114202Abstract: A spray nozzle assembly and hub combination for operation in a boiler feedwater deaerator is disclosed, the combination including a tubular hub capable of being affixed to a wall of a deaerator tank and a spray nozzle assembly that is removably engageable with the hub, the nozzle assembly including a nozzle body, a twist lock for retaining the nozzle body relative to the hub when the nozzle body is in a fully engaged position, and a spreader moveably coupled to the nozzle body and biased by a spreader spring against opening, the spreader is capable of moving to an open position against the spreader spring bias in response to boiler feedwater pressure to form an annular opening about the spreader, thereby enabling feedwater flow.Type: GrantFiled: March 9, 2009Date of Patent: February 14, 2012Assignee: Crane Environmental, Inc.Inventors: Russell G. Burke, Tao D. Nguyen, Joseph T. Strogus
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Publication number: 20100300296Abstract: Degasser including a shell and nozzles for spraying liquid into the shell, and plates within the shell to receive liquid sprayed by the nozzles. The plates disposed to enable running the liquid from upper plates to lower plates. The degasser including a port for steam entry into the shell and conveyor means for directing the steam between the plates. The steam is directed from the lower plates to the upper plates. The degasser including at least one first outlet to extract the degassed liquid from the degasser bottom and to enable a layer of degassed liquid to form on the container bottom when in use; and at least one second outlet to enable extracting a minimum part of the steam plus degassed gases from the shell interior. The conveyor means conveying entering steam to make it bubble through the layer of degassed liquid, to further reduce its dissolved gas concentration.Type: ApplicationFiled: November 27, 2008Publication date: December 2, 2010Applicant: TERMOCHIMICA IMPIANTI S.r.l.Inventor: Antonio Venturelli
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Publication number: 20100199670Abstract: A power generation plant includes a steam turbine and an electrical generator driven thereby. A condenser is downstream from the steam turbine. Moreover, the power generation plant includes a steam source and an inert gas source. A deaerator downstream from the condenser and is operable to perform deaeration using the inert gas source and is also selectively operable to perform deaeration using the steam source.Type: ApplicationFiled: February 6, 2009Publication date: August 12, 2010Applicant: Siemens Energy, Inc.Inventors: Teri J. Robertson, James C. Bellows
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Patent number: 7650938Abstract: A Residential In-well Internal Water Aerator for reducing/eliminating iron, Hydrogen sulfide, and radon gas is a device that hangs within the well casing. Its support is achieved by the well cap. It is capable of degassing hydrogen sulfide and radon gas and precipitation of the iron to become a solid and attaching its self to the interior walls and drip screens of the Residential In-well Internal Water Aerator within the well, thus reducing/eliminating the stained fixtures, bad smell and the risk of radon gas from within the residence.Type: GrantFiled: October 21, 2005Date of Patent: January 26, 2010Inventors: Thomas G. Hall, Veta B. Hall
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Publication number: 20090229465Abstract: The present invention has as an object to render a photochromic coating layer free from air bubbles and obtain a uniform layer without film thickness unevenness in the coating layer. In the prevent invention, entrained air in a coating fluid stored in a vessel of a coating unit comprising the vessel, a check valve for preventing back-flow of the coating fluid connected to the vessel, and optionally an ejection nozzle connected to the check valve; air existing inside of the check valve; and optionally air existing inside of the ejection nozzle are removed by plugging an outlet of the coating fluid existing downstream of the check valve and then rotating the coating unit on an axis of the vessel and orbiting the coating unit on a revolution axis simultaneously.Type: ApplicationFiled: October 16, 2006Publication date: September 17, 2009Applicant: Tokuyama CorporationInventor: Naoto Takahashi
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Publication number: 20090165652Abstract: The invention relates to a purification device for flue gases a purification device for flue gases comprising a primary purification tower, a washing tower and an adsorption tower which are connected in sequence. The washing tower is a spray tower and the adsorption tower includes a plurality of standard flashboards inserted into its flue gases duct. A plurality of washing nozzles are placed in a central part of an inner space of the spray tower, a plurality of sieve plates are placed in a lower part of an inner space of the spray tower and a gas-liquid segregating unit is placed in an upper part of an inner space of the spray tower. The device is simple in technique, convenient in operation and can completely remove the harmful ingredients from the flue gases, and thereby reducing the harm of flue gases upon human bodies and environment.Type: ApplicationFiled: May 9, 2008Publication date: July 2, 2009Applicant: Haisibote ( Beijing ) Science and Technology Co., Ltd.Inventor: Guangliang Chen
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Patent number: 7503961Abstract: A nitrogen sweep stream for use in a deaerator during deaerator operations to disperse and remove oxygen and carbon dioxide from boiler feed water prior to being fed to a boiler. The nitrogen sweep stream substantially reduces the amount of oxygen and carbon dioxide in the water supply system. The water supply system can be sent to a deaerator stripper or can be heated using a heat exchanger. A heat water supply stream can also be sent directly to the deaerator water tank. The nitrogen sweep stream reduces the amount of oxygen contained with the boiler feed water stream to less than 7 ppb and reduces the amount of carbon dioxide to nondetectable levels. The nitrogen sweep may be provided to an existing deaerator, not having been previously provided with a nitrogen sweep, while the deaerator is running without shutting down the deaerator.Type: GrantFiled: December 6, 2005Date of Patent: March 17, 2009Assignee: Westlake Chemical CorporationInventors: Ken M. Istre, David C. Payne
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Patent number: 6960294Abstract: The present invention relates to methods and apparatus for separation of solids from liquids and separation of liquids from liquids (such as oil from water) by dissolved gas floatation. A dissolved gas floatation clarifier is described as is a liquid-gas mixer, a liquid-liquid mixer, and solid-liquid chemical feeders. The methods and apparatus of the present invention are particularly suitable for supplying dissolved air and mixing of chemicals for use in separation of solids in dissolved air floatation clarifiers.Type: GrantFiled: December 11, 2002Date of Patent: November 1, 2005Assignee: Hydrotreat, Inc.Inventor: Johnny Arnaud
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Patent number: 6669843Abstract: An apparatus is provided for separation of suspended solid particles from fluids, for separation and mixing of fluids, and for dissolving gases in aqueous fluids. The apparatus employs a grooved ring to divide the fluid stream and impart a high velocity on each of the divided or sub-streams. A grooved ring with any number of grooves that may be spiral in shape is used to create a high velocity circular motion on a divided stream for separation of suspended solid particles by centrifugal force in a cyclone filter and for saturation of liquid with gases in a fluid mixer where gases are introduced through a diffuser. A grooved ring with any number of grooves that may be radial is used in a fluid mixer to divide a stream of fluid, produce a high velocity flow through each groove, introduce a second fluid through an orifice into the first fluid flowing through each groove, and direct the fluid mixture to a center impact zone where the various streams collide to complete the mixing.Type: GrantFiled: June 12, 2001Date of Patent: December 30, 2003Assignee: Hydrotreat, Inc.Inventor: Johnny Arnaud
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Patent number: 6375718Abstract: Connected in a water circuit for cooling or heating gaseous fuel in a fuel system for a gas turbine plant is a gas/liquid separation apparatus which serves to separate gases contained in the water from the water, and to detect them. The container of the separation apparatus is split up by a partition into a water entry chamber and a water exit chamber. The incoming water flow is split up in the water entry chamber into an upward-flowing and a downward-flowing water flow. Located above the water is a gas-filled space into which gas bubbles disperse. The upward-flowing water flows over an overflow weir, and the downward-flowing water flows into the water exit chamber through openings in the lower region of the partition. The separation apparatus thus includes a calm, free water level in the water entry chamber, and an irrotational flow from the water exit chamber.Type: GrantFiled: June 21, 2000Date of Patent: April 23, 2002Assignee: Alstom (Switzerland) LtdInventors: Francisco Blangetti, Stephan Werner Doehler, Erhard Liebig, Rainer Schlageter
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Patent number: 6291232Abstract: Anaerobic digestion system and process in which the raw digester gas containing methane and other gaseous components is cooled at atmospheric pressure in the presence of a liquid to a temperature at which the other gaseous components have a substantially higher solubility in the liquid than methane and are substantially all absorbed into the liquid, leaving pure, dry methane gas. That methane gas is then used in other parts of the system, including the digester and a refrigeration system for cooling the raw gas.Type: GrantFiled: October 8, 1999Date of Patent: September 18, 2001Inventor: Herman P. Miller, III
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Patent number: 6123750Abstract: An aeration system for removing radon and other volatile compounds from a water or other liquid source. Water supplied from a well and/or water pressure/storage tank enters an aeration tank and is sprayed through a clog resistant nozzle. The nozzle creates a cone shaped spray of very fine water droplets or particles. Such spraying exposes the maximum amount of water surface area to the air stream and hence removes about 50% of the existing radon and other volatile compounds contained within the water. The sprayed water is then collected and fills the aeration tank and the collected water is then exposed to a source of high pressure, filtered air which is blown through a conventional sparger to vigorously agitate and aerate the sprayed and collected water in the aeration tank thereby removing any remaining radon and other volatile compounds from the water.Type: GrantFiled: October 30, 1998Date of Patent: September 26, 2000Assignee: New England Radon, LtdInventor: Daniel Espinal
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Patent number: 5919289Abstract: There is disclosed a deaeration tank which can sufficiently deaerate object water, is decreased in size, and has high treatment capability. The deaeration tank includes a tank body which defines a deaeration chamber and receives object water, an air injection device disposed within the deaeration chamber for injecting air, a discharge passage for discharging object water from the deaeration chamber, and a bubble-scavenging member disposed in the discharge passage for scavenging fine bubbles contained in the object water which passes through the discharge passage. When object water is fed into the deaeration chamber, and air is injected into the deaeration chamber, thus-injected air ascends in the object water in the form of coarse bubbles and is then released from the surface of the object water. During this ascent of coarse bubbles within the deaeration chamber, through contact with the object water, coarse bubbles attract fine bubbles contained in the object water, so that the object water is deaerated.Type: GrantFiled: August 25, 1997Date of Patent: July 6, 1999Assignee: Sumitomo Heavy Industries, Ltd.Inventors: Kihachiro Misawa, Yoshio Okumoto
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Patent number: 5766321Abstract: Disclosed is a dissolved oxygen reducing apparatus which enables supplying a liquid containing very small amounts of dissolved oxygen. The dissolved oxygen reducing apparatus includes a bubbling vessel (24) having a liquid charge inlet (21), a liquid discharge outlet (22) and an inert gas discharge port (23), an inert gas sparger (25) provided within the bubbling vessel (24), and a liquid discharge pipe (26) connected to the liquid discharge outlet (22). The bubbling vessel (24) and the liquid discharge pipe (26) have a coefficient of oxygen permeability of not higher than 10.sup.-9 cc.multidot.cm/cm.sup.2 .multidot.sec.multidot.atm at 25.degree. C.Type: GrantFiled: December 12, 1994Date of Patent: June 16, 1998Assignee: Nippon Sanso CorporationInventors: Yoshio Ishihara, Hiroshi Yamazaki, Sumiyo Yamane, Koh Matsumoto
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Patent number: 5753189Abstract: An apparatus and process for the removal of sulfur, in the form of hydrogen sulfide (H.sub.2 S), from gas, such as natural gas or industrial gas streams, in which the sulfur is removed and separated in the form of particulate elemental sulfur. The apparatus and process are advantageously configured so as to maintain control over the development of undesired concentrations of particulate sulfur in the precipitation catalyst solution with which the sulfur is separated from the gas stream.Type: GrantFiled: October 7, 1996Date of Patent: May 19, 1998Assignee: Gas Research InstituteInventor: Amirali G. Rehmat
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Patent number: 5728200Abstract: A compact deaerator unit used in combination with a boiler feedwater receiver to eliminate corrosion in the feedwater receiver and in other components of a boiler system. The deaerator unit is mounted external to the feedwater receiver for receiving makeup water and return condensate through a spray nozzle, the deaerator unit in one embodiment having a water level overflow supplying the feedwater receiver with deaerated water and a submerged steam supply and temperature control for maintaining water in the deaerator unit at deaeration temperature, with the water level overflow being separated from the spray nozzle by a baffle, the steam supplied to the deaerator unit first passing through the feedwater receiver to continuously purge the receiver of any corrosive gases and maintain a positive steam pressure.Type: GrantFiled: July 31, 1996Date of Patent: March 17, 1998Inventor: Martin Bekedam
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Patent number: 5653873Abstract: A system and method for reducing the volume of the liquid hazardous waste stream generated as a byproduct of the dry cleaning process combines an air atomization apparatus, and a temperature controlled water injection apparatus. The air atomization apparatus disposes of separator water by misting. The temperature controlled injection apparatus uses dry cleaning separator water to create and boil an azeotropic mixture in the still of the dry cleaning machine itself. Consequently, the storage and disposal of separator water is eliminated and almost no solvent is left in the residue of the still before disposal.Type: GrantFiled: August 3, 1995Date of Patent: August 5, 1997Inventor: Bruce Grossman
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Patent number: 5439509Abstract: Solute gas-rich absorbing media formed in scrubbing a solute gas from an off-gas stream prior to discharge of the same are regenerated to solute gas-lean absorbing medium for recycle to the scrubbing operation. Hot solute gas-rich absorbing media is formed into one or more spray patterns of very small liquid droplets in a flowing purge steam stream in a chamber into which the solute gas is desorbed from the droplets. The droplets are coalesced to form a regenerated absorption medium, the solute gas-containing gas stream is cooled to condense out the steam and a pure solute gas stream is recovered. The operation may be effected in multiple stripping stages, which may utilize cocurrent flow of solute gas laden absorbing medium and purge steam within a single chamber or in multiple chambers. Multiple stripping steps may be effected within a single stripping stage.Type: GrantFiled: December 2, 1993Date of Patent: August 8, 1995Assignee: Turbotak Inc.Inventors: Donald R. Spink, Kim D. Nguyen
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Patent number: 5437714Abstract: A combined vertical column and shallow tray semicontinuous deodoriser for edible oils and fats and comprising a column (10) of discrete vessels and a deodorising vessel (13) disposed within or valve-connective thereto. In the operation of the device, heated oil from a vessel (12) is supplied to deodorising vessel (13) wherein it is circulated by steam injection at (33) through a lift tube (29), between a plurality of vertically separated self draining shallow trays (26, 27, 28). The entire oil content of deodorising vessel (13) is circulated therethrough approximately once a minute for a period in the region of eighteen minutes to strip free fatty acids and other volatile components from the oil by falling curtain and steam sparge techniques, and then the oil batch is discharged to a heat recovery vessel (14) and a cooling vessel (15) before product discharge.Type: GrantFiled: October 31, 1994Date of Patent: August 1, 1995Assignee: Ebortec LimitedInventors: Raymond Cook, Donald G. Sewell
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Patent number: 5405435Abstract: An economical deaerator unit for use in boiler feedwater systems for eliminating non-condensible gases, the unit having a containment vessel with a divided internal chamber with an upper scrubbing section and a lower heating and deaerating section with gases flowing from the lower section to the upper section for venting, and with water flowing from the upper section to the lower section for supply to a boiler system with water circulation in the deaerator unit being accomplished by gravity without a transfer pump.Type: GrantFiled: March 1, 1994Date of Patent: April 11, 1995Inventor: Martin Bekedam
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Patent number: 5340383Abstract: In accordance with the method of this invention, sulfur is removed from the gas stream exiting a sulfur storage tank through condensation and impingement of droplets and/or particles of elemental sulfur on the baffles and wall(s) of indirectly cooled scrubber-condenser. In order to effect the melting and return to the liquid sulfur storage tank of any sulfur collected on the baffles and wall(s) of the scrubber-condenser, said baffles and wall(s) are periodically heated, preferably with indirect steam. The scrubber-condenser apparatus of this invention is designed to effect the condensation and solidification of sulfur from the gas stream and to maximize the impingement of sulfur droplets and particles upon its baffles and internal wall(s) by repeatedly changing the flow direction of said gas stream. The scrubber-condenser is vertically mounted on a liquid sulfur storage tank and is connected directly to a vent located on top of the tank.Type: GrantFiled: November 12, 1993Date of Patent: August 23, 1994Assignee: Freeport-McMoran Inc.Inventor: James T. Womack
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Patent number: 5310417Abstract: An atmospheric deaerator unit having a vessel divided into an atmospheric section and a low pressure section, the low pressure section containing steam supply line for deaerating a water spray circulated from the atmospheric section through a water circulating line using a series of spray heads for spraying water into the low pressure section, the circulating line communicating between the low pressure section and the atmospheric section, the atmospheric section having a vent open to atmosphere with a vent condenser to purge vented non-condensible gases from the atmospheric section, and, the low pressure section being pressure protected by a water column conduit communicating between the vessel sections to return overflow water and blow-through excess pressurized steam and vapor from the pressurized section to the atmospheric section, the unit being controlled by a steam control valve using pressure of the pressurized section or water temperature in the atmospheric section.Type: GrantFiled: March 15, 1993Date of Patent: May 10, 1994Inventor: Martin Bekedam
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Patent number: 5308384Abstract: A deaeration vessel has a partition wall dividing the hollow vessel body into first and second portions, and defining a weir with a top surface establishing the level of pulp suspension in the vessel body. Turbulence in the deaerated pulp is minimized by providing the outlet for deaerated pulp immediately adjacent the partition wall, in the bottom of the vessel body first portion (on the same side of the weir as the inlet conduits for the suspension being deaerated). The weir is preferably configured so that the top surface, defining the liquid level within the vessel, overlies the outlet. A partition wall may extend substantially linearly at an angle of about 60.degree. to the bottom of the vessel, or it may have a vertical bottom with a top extending at an angle to the bottom, or it may be continuously curved from the vessel bottom to the top surface, about a horizontal and/or vertical axis.Type: GrantFiled: October 1, 1992Date of Patent: May 3, 1994Assignee: A. Ahlstrom CorporationInventors: Kari Kapanen, Seppo Lukkarinen, Jouni Parviainen, Pentti Vikio
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Patent number: 5269832Abstract: A method and apparatus for continuously monitoring the concentration of a target chemical in a solution, such as chlorine dioxide in sewage or waste water, includes a holding tank, a bubbler chamber, and an air pump for directing air bubbles through the solution held in the bubbler chamber. Gases discharged from the solution by the air bubbles are collected in the bubbler chamber. These discharged gases include a quantity of the target chemical present in the solution as a dissolved gas. The concentration of the chemical in the discharged gases is then measured with a sensor such as a polarographic probe. This concentration along with the measured temperature of the solution is used as an analog to determine the concentration of the chemical in the solution.Type: GrantFiled: June 3, 1992Date of Patent: December 14, 1993Assignee: Winfield IndustriesInventor: Robert S. Meijer
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Method and apparatus for extracting dissolved, volatile substances from liquids into the vapor phase
Patent number: 5258057Abstract: In a method for extracting volatile substances from a vaporized liquid in which the vaporized liquid is withdrawn from an extraction chamber, a method of producing the vaporized liquid. The method includes the steps of introducing a carrier gas into the extraction chamber to form a vapor space, and spraying a liquid into the vapor space to form a vaporized liquid. An apparatus for practicing the method includes an extraction chamber in fluid communication with a liquid specimen source, and a liquid injection arrangement extending into the extraction chamber for spraying the liquid from the liquid specimen source in the vapor space to form a vaporized liquid. A carrier gas supply arrangement is provided adjacent to the extraction chamber for introducing carrier gas into the chamber to form a vapor space. The apparatus may further include a specimen chamber for collecting a predetermined amount of liquid prior to spraying.Type: GrantFiled: November 18, 1992Date of Patent: November 2, 1993Assignee: Bruker-Franzen Analytik GmbHInventor: Goekhan Baykut