Containing The Structure P-(x-*acyl), P-(x-*z) Or P-(x-*cyano) Wherein Z Is Other Than C, H, Or A Salt Forming Moiety And * Indicates A Direct Bond To The Adjacent X Atom (9/165a9; 9/165a9+m; 9/165a9+q; 9/165a9+u) Patents (Class 987/211)
  • Method of preparing malononitrile oxime ether compound and intermediate compound
    Patent number: 11952355
    Abstract: Provided are a method of preparing a malononitrile oxime ether compound and an intermediate compound. The malononitrile oxime ether compound has a structure as shown in formula (VII), wherein W is selected from aryl or heteroaryl. The preparation method comprises: reacting a first raw material with a second raw material in the presence of a first solvent and a catalyst to obtain the intermediate compound, wherein the first raw material has a structure as shown in formula (IV), and the second raw material has a structure as shown in formula (V); and subjecting the intermediate compound, and a dehydrant to a dehydration reaction in the present of a second solvent to obtain the malononitrile oxime ether compound. Furthermore, the malononitrile oxime ether compound is obtained through one-step dehydration reaction. using the preparation method, is advantageous for improving the yield of malononitrile oxime ethers and reducing the cost.
    Type: Grant
    Filed: June 17, 2019
    Date of Patent: April 9, 2024
    Assignee: Shenyang Sinochem Agrochemicals R&D Co., Ltd.
    Inventors: Hongfei Wu, Xueming Cheng, Libao Xu, Chunxiao Guo, Jingbo Xu, Ningning Sun, Haibo Yu