Patents Represented by Attorney Douglas E. McKinley, Jr.
  • Patent number: 5997961
    Abstract: A simple and effective method to bond a thin coating of poly(N-isopropylacylamide) (NIPAAm) on a glass surface by UV photopolymerization, and the use of such a coated surface in nano and micro technology applications. A silane coupling agent with a dithiocarbamate group is provided as a photosensitizer, preferably, (N,N'-diethylamine)dithiocarbamoylpropyl-(trimethoxy)silane (DATMS). The thiocarbamate group of the sensitizer is then bonded to the glass surface by coupling the silane agent with the hydroxyl groups on the glass surface. The modified surface is then exposed to a solution of NIPAAm and a crosslinking agent which may be any organic molecule having an acrylamide group and at least two double bonds in its structure, such as N,N'-methylenebisacrylamide, and a polar solvent which may be any polar liquid which will dissolve the monomer and the crosslinking agent such as acetone, water, ethanol, or combinations thereof.
    Type: Grant
    Filed: March 6, 1998
    Date of Patent: December 7, 1999
    Assignee: Battelle Memorial Institute
    Inventors: Xiangdong Feng, Jun Liu, Liang Liang
  • Patent number: 5958541
    Abstract: Disclosed is a method for storing and retrieving information. More specifically, the present invention is a method for forming predetermined patterns, or data structures, using materials which exhibit enhanced absorption of light at certain wavelengths or, when interrogated with a light having a first wavelength, provide a luminescent response at a second wavelength. These materials may exhibit this response to light inherently, or may be made to exhibit this response by treating the materials with ionizing radiation.
    Type: Grant
    Filed: June 28, 1996
    Date of Patent: September 28, 1999
    Assignee: Battelle Memorial Institute
    Inventors: Steven D. Miller, George W. Endres
  • Patent number: 5863298
    Abstract: Disclosed is a method of sizing and desizing yarn, or more specifically to a method of coating yarn with size and removing size from yarn with liquid carbon dioxide solvent.
    Type: Grant
    Filed: March 6, 1997
    Date of Patent: January 26, 1999
    Assignee: Battelle Memorial Institute
    Inventors: John L. Fulton, Clement R. Yonker, Richard R. Hallen, Eddie G. Baker, Lawrence E. Bowman, Laura J. Silva
  • Patent number: 5803174
    Abstract: A method and apparatus for the remediation of contaminated soil and ground water wherein a reactive pack material is added to the annular fill material utilized in standard well construction techniques.
    Type: Grant
    Filed: December 31, 1996
    Date of Patent: September 8, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Tyler J. Gilmore, George R. Holdren, Jr., Daniel I. Kaplan
  • Patent number: 5778664
    Abstract: A method and apparatus for the destruction of emissions from an internal combustion engine wherein a substrate coated with TiO.sub.2 is exposed to a light source in the exhaust system of an internal combustion engine thereby catalyzing oxidation/reduction reactions between gaseous hydrocarbons, carbon monoxide, nitrogen oxides and oxygen in the exhaust of the internal combustion engine.
    Type: Grant
    Filed: September 20, 1996
    Date of Patent: July 14, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Jiri Janata, Gary L. McVay, Charles H. Peden, Gregory J. Exarhos
  • Patent number: 5777190
    Abstract: A method for the controlled reduction of nitroaromatic compounds such as nitrobenzene and 2,4,6-trinitrotoluene by enzymatic reaction with oxygen sensitive nitroreductase enzymes, such as ferredoxin NADP oxidoreductase.
    Type: Grant
    Filed: May 29, 1997
    Date of Patent: July 7, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Manish M. Shah, James A. Campbell
  • Patent number: 5767512
    Abstract: A method for producing an ion beam having an increased proportion of analyte ions compared to carrier gas ions is disclosed. Specifically, the method has the step of addition of a charge transfer gas to the carrier analyte combination that accepts charge from the carrier gas ions yet minimally accepts charge from the analyte ions thereby selectively neutralizing the carrier gas ions. Also disclosed is the method as employed in various analytical instruments including an inductively coupled plasma mass spectrometer.
    Type: Grant
    Filed: January 5, 1996
    Date of Patent: June 16, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Gregory C. Eiden, Charles J. Barinaga, David W. Koppenaal
  • Patent number: 5749042
    Abstract: A method for separating .sup.213 Bi from a solution of radionuclides wherein the solution contains a concentration of the chloride ions and hydrogen ions adjusted to allow the formation of a chloride complex. The solution is then brought into contact with an anion exchange resin, whereupon .sup.213 Bi is absorbed from the solution and adhered onto the anion exchange resin in the chloride complex. Other non-absorbing radionuclides such as .sup.225 Ra, .sup.225 Ac, and .sup.221 Fr, along with HCl are removed from the anion exchange resin with a scrub solution. The .sup.213 Bi is removed from the anion exchange resin by washing the anion exchange resin with a stripping solution free of chloride ions and with a reduced hydrogen ion concentration which breaks the chloride anionic complex, releasing the .sup.213 Bi as a cation. In a preferred embodiment of the present invention, the anion exchange resin is provided as a thin membrane, allowing for extremely rapid adherence and stripping of the .sup.213 Bi.
    Type: Grant
    Filed: January 28, 1997
    Date of Patent: May 5, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Lane Allan Bray, Jaquetta R. DesChane
  • Patent number: 5731590
    Abstract: The present invention is a method of measuring a radiation dose wherein a radiation responsive material consisting essentially of metal oxide is first exposed to ionizing radiation. The metal oxide is then stimulating with light thereby causing the radiation responsive material to photoluminesce. Photons emitted from the metal oxide as a result of photoluminescence may be counted to provide a measure of the ionizing radiation.
    Type: Grant
    Filed: September 26, 1996
    Date of Patent: March 24, 1998
    Assignee: Battelle Memorial Institute
    Inventor: Steven D. Miller
  • Patent number: 5693941
    Abstract: An ion trap having two end cap electrodes disposed asymmetrically about a center of a ring electrode. The inner surface of the end cap electrodes are conformed to an asymmetric pair of equipotential lines of the harmonic formed by the application of voltages to the electrodes. The asymmetry of the end cap electrodes allows ejection of charged species through the closer of the two electrodes which in turn allows for simultaneously detecting anions and cations expelled from the ion trap through the use of two detectors charged with opposite polarity.
    Type: Grant
    Filed: August 23, 1996
    Date of Patent: December 2, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Stephan E. Barlow, Michael L. Alexander, James C. Follansbee
  • Patent number: 5681615
    Abstract: A method for fabrication of polymer composite layers in a vacuum is disclosed. More specifically, the method of dissolving salts in a monomer solution, vacuum flash evaporating the solution, condensing the flash evaporated solution as a liquid film, and forming the condensed liquid film into a polymer composite layer on a substrate is disclosed.
    Type: Grant
    Filed: July 27, 1995
    Date of Patent: October 28, 1997
    Assignee: Battelle Memorial Institute
    Inventors: John D. Affinito, Mark E. Gross
  • Patent number: 5680423
    Abstract: The instant invention is a method for making and using an apparatus for detecting neutrons. Scintillating optical fibers are fabricated by melting SiO.sub.2 with a thermal neutron capturing substance and a scintillating material in a reducing atmosphere. The melt is then drawn into fibers in an anoxic atmosphere. The fibers may then be coated and used directly in a neutron detection apparatus, or assembled into a geometrical array in a second, hydrogen-rich, scintillating material such as a polymer. Photons generated by interaction with thermal neutrons are trapped within the coated fibers and are directed to photoelectric converters. A measurable electronic signal is generated for each thermal neutron interaction within the fiber. These electronic signals are then manipulated, stored, and interpreted by normal methods to infer the quality and quantity of incident radiation.
    Type: Grant
    Filed: March 24, 1995
    Date of Patent: October 21, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Richard W. Perkins, Paul L. Reeder, Ned A. Wogman, Ray A. Warner, Daniel W. Brite, Wayne C. Richey, Don S. Goldman
  • Patent number: 5658233
    Abstract: An improved method for delivering thermal neutrons to a subsurface cancer or tumor which has been first doped with a dopant having a high cross section for neutron capture. The improvement is the use of a guide tube in cooperation with a capillary neutron focusing apparatus, or neutron focusing lens, for directing neutrons to the tumor, and thereby avoiding damage to surrounding tissue.
    Type: Grant
    Filed: September 19, 1995
    Date of Patent: August 19, 1997
    Assignee: Battelle Memorial Institute
    Inventor: Anthony J. Peurrung
  • Patent number: 5656009
    Abstract: Disclosed is a method for converting spent nuclear fuel and surplus plutonium into a vitreous ceramic final waste form wherein spent nuclear fuel is bound in a crystalline matrix which is in turn bound within glass.
    Type: Grant
    Filed: June 5, 1996
    Date of Patent: August 12, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Xiangdong Feng, Robert E. Einziger
  • Patent number: 5597516
    Abstract: Disclosed is a method for converting spent nuclear fuel and surplus plutonium into a vitreous ceramic final waste form wherein spent nuclear fuel is bound in a crystalline matrix which is in turn bound within glass.
    Type: Grant
    Filed: August 11, 1995
    Date of Patent: January 28, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Xiangdong Feng, Robert E. Einziger
  • Patent number: 5569927
    Abstract: The present invention is a composite material containing a mix of dosimeter material powder and a polymer powder wherein the polymer is transparent to the photon emission of the dosimeter material powder. By mixing dosimeter material powder with polymer powder, less dosimeter material is needed compared to a monolithic dosimeter material chip. Interrogation is done with excitation by visible light.
    Type: Grant
    Filed: September 27, 1995
    Date of Patent: October 29, 1996
    Assignee: Battelle Memorial Institute
    Inventor: Steven D. Miller
  • Patent number: 5567948
    Abstract: The present invention is a composite material containing a mix of dosimeter material powder and a polymer powder wherein the polymer is transparent to the photon emission of the dosimeter material powder. By mixing dosimeter material powder with polymer powder, less dosimeter material is needed compared to a monolithic dosimeter material chip. Interrogation is done with excitation by visible light.
    Type: Grant
    Filed: June 2, 1995
    Date of Patent: October 22, 1996
    Assignee: Battelle Memorial Institute
    Inventor: Steven D. Miller
  • Patent number: 5545794
    Abstract: Disclosed is a method for removing radioactive contaminants from metal surfaces by applying steam containing an inorganic acid and cerium IV. Cerium IV is applied to contaminated metal surfaces by introducing cerium IV in solution into a steam spray directed at contaminated metal surfaces. Cerium IV solution is converted to an essentially atomized or vapor phase by the steam.
    Type: Grant
    Filed: June 19, 1995
    Date of Patent: August 13, 1996
    Assignee: Battelle Memorial Institute
    Inventor: Lane A. Bray