Abstract: While high-performance semiconductor devices encapsulated with a resin composition are subject to the problem of wrong operation due to the alpha-particles emitted from the trace amounts of radioactive impurities, e.g. uranium and thorium, contained in the silica filler incorporated in the resin composition, a means for solving this problem is provided by use of a silicon dioxide powder obtained by the pyrolysis of a volatilizable silicon compound free from radioactive impurities in an oxidizing condition and having an average particle diameter in the range from 0.5 to 100 .mu.m in place of the conventional silica fillers.

Abstract: A process for manufacturing an organic silazane polymer which comprises reacting ammonia with a mixture of methyldichlorosilane, methyltrichlorosilane and dimethyldichlorosilane to obtain an ammonolysis product. The ammonolysis product is polymerized in the presence of a basic catalyst capable of deprotonation to obtain an organic silazane polymer. The silazane polymer may be further melted, shaped and infusibilized. The thus infusibilized product is finally sintered to obtain a ceramic material.

Abstract: The invention provides a silicone-coated release paper having a coating surface film of an organopolysiloxane composition curable by irradiation with ultraviolet light or electron beams to give a fully cured film resistant to migration of the organopolysiloxane constituents therefrom on to other surfaces in contact therewith. The composition comprises (a) a diorganopolysiloxane terminatd at both molecular chain ends each with a divinylmethylsilyl group or trivinylsilyl group, (b) an organohydrogenpolysiloxane having at least 2 hydrogen atoms directly bonded to the silicon atoms in a molecule, (c) a catalytic amount of a platinum or rhodium catalyst and, optionally, (d) a compound of a rare earth element such as ceric oxide.

Abstract: A method for quantitative analysis of low molecular weight components which are contained in a protein-containing liquid sample originating from body fluids and are capable of binding to said protein, characterized by incorporating into the liquid sample a compound having the formula (I):X--(Y).sub.p --SO.sub.3 M (I)in which M is hydrogen ion, an alkali metal ion, or ammonium ion; X is a straight or branched alkyl, alkenyl, fluorinated alkyl, or fluorinated alkenyl group containing at least 6 carbon atoms, Y is a divilent organic residue; and p is 0 r 1. The compound represented by formula (I) liberates thyroid hormone from bound protein to facilitate analysis.

Abstract: A room temperature-curable silicone rubber composition having improved heat-resistance is disclosed. The composition is formulated without any siliceous fillers as a reinforcing inorganic filler conventionally used in silicone compositions and, instead, comprises carbon black as a reinforcing filler. Namely, the composition comrises a major amount of a hydroxy-containing organopolysiloxane admixed with a minor amount of an organosilicon compound having at least two hydrolyzable groups per molecule, a curing catalyst, carbon black and iron oxide.

Abstract: There is provided a process for the heat treatment of coal which comprises heating and drying low grade coal such as subbituminous coal and brown coal containing less than 80% of carbon and more than 33% of volatile matter (dry mineral matter-free basis) and having a high moisture content and a particle diameter smaller than 2 inches, with a high-temperature gas containing less than 5% of oxygen in a fluidized bed for 2-10 minutes until the coal temperature reaches 180.degree.-400.degree. C., and subsequently cooling the coal by spraying water in a fluidized bed for 2-10 minutes until the coal temperature decreases to 60.degree. C. or below at which time the coal holds the maximum moisture given by wetting. The heating process may be performed in two steps, in which case coal is heated with a high-temperature gas to 80.degree.-150.degree. C. in the first step so that the moisture of coal is reduced below the inherent moisture.

Abstract: A medium for electrophoresis in the form of an aqueous gel comprising an acrylamide copolymer having at least one specifically selected constitutional repeating unit. This medium is preferably employable for analysis of bipolymers such as proteins.

Abstract: An electrostatographic encapsulated toner comprising a core material which comprises a colorant and a binder and a resin shell enclosing said core material in the form of micro-capsule, which is characterized in that:said binder is an oily binder comprising a solid polymer and an organic solvent capable of dissolving or swelling said polymer and having a boiling point of not lower than 150.degree. C., said oily binder having a viscosity within the range of 1,000-100,000 cp at 25.degree. C.; said resin shell is formed around the core material by a polymerization process selected from the group consisting of an interfacial polymerization process, an inner polymerization process and an outer polymerization process; and the surface of said resin shell is deposited with a polymer of at least one vinyl monomer having a nitrogen-atom.

Abstract: The inventive method is particularly advantageous for the preparation of an unsaturated alcohol or aldehyde by the reduction of a corresponding unsaturated carboxylic acid since the unsaturated double bond in the starting acid is not hydrogenated by the reaction of reduction. The method comprises first reacting the starting acid with an alkyl chloroformate to form an intermediate compound by the dehydrochlorination and the intermediate compound is then reduced by using sodium borohydride as the reducing agent. The proportion of the aldehyde to alcohol in the product mixture can be controlled by modifying the amount of the reducing agent and/or the reaction time.

Abstract: The invention provides a novel polymeric compound having crosslinkability by irradiation with actinic rays, e.g. ultraviolet light, and useful as a polymeric base ingredient of a negative type photoresist composition with high sensitivity and resistance against dry etching. The polymer is obtained by the anionic living polymerization of a vinylsilyl group-containing styrene derivative of the formulaCH.sub.2 .dbd.CH--C.sub.6 H.sub.4 --CH.sub.2).sub.n SiR.sub.2 --CH.dbd.CH.sub.2,in which R is a monovalent hydrocarbon group, e.g. methyl and phenyl, and n is an integer of 0 to 3, in a specific solvent in the presence of a specific polymerization initiator so that the polymerization takes place only at the styrenic vinyl groups leaving the silicon-bonded vinyl groups unpolymerized. Quite unexpectedly, the polymer has a very uniform monodisperse distribution of the molecular weight.

Abstract: The invention relates to a clamping device used for making up or breaking apart joints of drill pipe, drill collars and the like in mouse hole pipe during oil drilling operation. A clamping means of the device firstly clamps the drill pipe therebetween during its moving down and centripetally simultaneously by the self-weight of drill pipe to be clamped, then tightly clamps the drill pipe with a force generated by rollers' moving inwardly to the center of the device along the concavity of the turning plate with the rotation of a kelly. It can be used instead of a back tong when making-up joint in mouse hole pipe with a tong.

Abstract: An integral flat container type analytical instrument for use in the quantitative analysis of an analyte present in a liquid sample which has a reaction chamber and an observation chamber associated with each other so as to allow a liquid to flow therebetween characterized in that: at least part of the wall of said reaction chamber is made of a flexible material; said observation chamber is provided with wall parts which are made of a transparent material and opposed to each other in such a manner that their relative positions are fixed to provide a given light path; and no partition wall preventing the free flow of the liquid substantially exists between said reaction chamber and said observation chamber. A method for optical measurement of an analyte in a liquid sample utilizing said analytical instrument is also disclosed.

Abstract: The invention provides organosilane compounds of a novel class having one or two (phenyl dimethyl carbinyl) groups bonded to the silicon atom as represented by the general formula (PhMe.sub.2 C).sub.p R.sub.q X.sub.r Si, in which Ph is a phenyl group, Me is a methyl group, R is a monovalent hydrocarbon group selected from the class consisting of alkyl, alkenyl and aryl groups, X is a halogen atom or an alkoxy group, p is 1 or 2, q is zero, 1 or 2 and r is zero, 1, 2 or 3 with the proviso that p+q+r=4. The compound can be prepared by the reaction of a Grignard reagent PhMe.sub.2 C. MgY, in which Y is a halogen atom, with a silane compound represented by the general formula R.sub.q SiX.sub.4-q in an organic solvent.

Abstract: The see-through coordinate input tablet is formed of two oppositely facing elements each made of a transparent substrate provided with fine metal wires running in parallel on the inward surface of the substrate, the running directions on the two substrates being perpendicular to each other. At least either one of the elements is provided with a detecting resistor along a side periphery crossing the end portions of the parallel-running metal wires so that the accuracy and reliability in the detection of the coordinates of the inputted point can be improved.

Abstract: In the inventive touch-operated see-through coordinate input unit, the contacting wires embedded in the upper and lower substrate sheets in a relative perpendicular disposition are divided into groups each of at least two of the adjacent wires and the wires belonging to the same group are bonded to the same electrode. When the upper sheet is depressed with a finger tip or stylus point at a crossing point of the wires on the upper and lower sheets, electrical contact can be obtained at two points or more between wires so that, different from conventional coordinate input units in which electrical contact is obtained at only a single point by a pushing stroke, the reliability of the input operation can be greatly improved also with decreased fatigue of the operator in continuous working of long time.

Abstract: The silicone-based antifoam composition having excellent durability of the antifoam activity even under vigorous agitation or under an alkaline condition comprises three kinds of diorganopolysiloxanes, of which the first is free from aliphatic unsaturation, the second is terminated at both molecular chain ends each with a vinyl diorganosilyl group and the third is terminated at both molecular chain ends each with a diorganosilyl group having a silicon-bonded hydrogen atom, a finely divided silica powder, a platinum compound to catalyze the addition reaction between the silicon-bonded vinyl groups and silicon-bonded hydrogen atoms in the second and the third diorganopolysiloxanes, respectively, and an organosilane compound of the formula R.sup.1.sub.a Y.sub.b Si, in which R.sup.1 is a monovalent hydrocarbon group, Y is a hydroxy, carboxyl or hydrolyzable group and a and b are each 1, 2 or 3 with the proviso that a+b=4.

Abstract: The curable organopolysiloxane composition of the invention is formulated with two kinds of crosslinking agents including an organosilane compound having 2 or 3 isopropenyloxy groups in a molecule and an organopolysiloxane having at least 2 mercapto groups in a molecule added to the base ingredient of a hydroxy-terminated diorganopolysiloxane together with a curing catalyst and a photosensitizer. The composition has two-way curability by the condensation reaction in the presence of atmospheric moisture between the silanolic hydroxy groups and the isopropenyloxy groups and by the ultraviolet-induced addition reaction between the isopropenyloxy groups and the mercapto groups to exhibit very reliable curing behavior giving a cured rubbery elastomer having excellent properties.

Abstract: A liquid sample-spotting apparatus having a base, a holder which is mounted on the base by an elastic body such as a spring in such a manner that said holder is movable downward against an action of the elastic body for recovering the original form, and a manually operable micropipette which is detachably supported by the holder. A process for spotting a liquid sample on an analytical element using said apparatus, which comprises steps of moving downward the holder and the micropipette with a droplet of the liquid sample formed on the pointed end against the recovering action of the elastic body; stopping the downward movement of the micropipette when the droplet of the liquid sample bridges the micropipette and the surface of the analytical element to spot the droplet on the element; and elevating the micropipette to the original position by the recoverable action of the elastic body.

Abstract: An element for electrophoresis suitably employable for electrophoresis of biopolymers such as proteins, as well as for the determination of the base sequence of DNA, RNA, their fragments, and their derivatives, which comprises a plastic support, a nonconductive metal oxide layer, and an electrophoresis medium layer comprising an aqueous polyacrylamide gel formed by crosslinking polymerization of an acrylamide compound and a crosslinking agent in the presence of water, which are superposed in this order. The electrophoresis medium layer may contain a water-soluble polymer and agarose. The medium layer may contain a modifier such as an anionic surfactant, formamide or urea.

Abstract: An element for electrophoresis suitably employable for electrophoresis of biopolymers such as proteins, as well as for determination of base sequence of DNA, RNA, their fragments, and their derivatives, which comprises a plastic support, an adhesive layer containing a cellulose derivative, and an electrophoresis medium layer comprising an aqueous polyacrylamide gel formed by crosslinking polymerization of an acrylamide compound and a crosslinking agent in the presence of water, which are superposed in this order. The electrophoresis medium layer may contain a water-soluble polymer and agarose. The medium layer may contain a modifier such as an anionic surfactant, formamide or urea.