Patents Assigned to Crystal IS Inc.
  • Patent number: 11251330
    Abstract: In various embodiments, light-emitting devices incorporate smooth contact layers and polarization doping (i.e., underlying layers substantially free of dopant impurities) and exhibit high photon extraction efficiencies.
    Type: Grant
    Filed: March 3, 2017
    Date of Patent: February 15, 2022
    Assignee: CRYSTAL IS, INC.
    Inventors: James R. Grandusky, Leo J. Schowalter, Muhammad Jamil, Mark C. Mendrick, Shawn R. Gibb
  • Patent number: 11225731
    Abstract: Reducing the microvoid (MV) density in AlN ameliorates numerous problems related to cracking during crystal growth, etch pit generation during the polishing, reduction of the optical transparency in an AlN wafer, and, possibly, growth pit formation during epitaxial growth of AlN and/or AlGaN. This facilitates practical crystal production strategies and the formation of large, bulk AlN crystals with low defect densities—e.g., a dislocation density below 104 cm?2 and an inclusion density below 104 cm?3 and/or a MV density below 104 cm?3.
    Type: Grant
    Filed: February 8, 2017
    Date of Patent: January 18, 2022
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert Bondokov, Kenneth E. Morgan, Glen A. Slack, Leo J. Schowalter
  • Patent number: 11183567
    Abstract: Fabrication of doped AlN crystals and/or AlGaN epitaxial layers with high conductivity and mobility is accomplished by, for example, forming mixed crystals including a plurality of impurity species and electrically activating at least a portion of the crystal.
    Type: Grant
    Filed: May 15, 2020
    Date of Patent: November 23, 2021
    Assignee: Crystal IS, Inc.
    Inventors: Glen A. Slack, Leo J. Schowalter
  • Patent number: 11168411
    Abstract: In various embodiments, single-crystal aluminum nitride boules and substrates are formed from the vapor phase with controlled levels of impurities such as carbon. Single-crystal aluminum nitride may be heat treated via quasi-isothermal annealing and controlled cooling to improve its ultraviolet absorption coefficient and/or Urbach energy.
    Type: Grant
    Filed: June 18, 2019
    Date of Patent: November 9, 2021
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert T. Bondokov, James R. Grandusky, Jianfeng Chen, Shichao Wang, Toru Kimura, Thomas Miebach, Keisuke Yamaoka, Leo J. Schowalter
  • Patent number: 11124892
    Abstract: Bulk single crystal of aluminum nitride (AlN) having an areal planar defect density ?100 cm?2. Methods for growing single crystal aluminum nitride include melting an aluminum foil to uniformly wet a foundation with a layer of aluminum, the foundation forming a portion of an AlN seed holder, for an AlN seed to be used for the AlN growth. The holder may consist essentially of a substantially impervious backing plate.
    Type: Grant
    Filed: May 22, 2020
    Date of Patent: September 21, 2021
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert T. Bondokov, Kenneth E. Morgan, Leo J. Schowalter, Glen A. Slack
  • Publication number: 20210202865
    Abstract: Provided is a novel chalcogen-containing organic semiconductor compound having excellent carrier mobility. The compound is represented by Formula (1a) or (1b): [Chem. 1] where in Formulas (1a) and (1b), X represents S, O, or Se, and R1 each independently represents a hydrogen atom, a halogen atom, an alkyl group, an aryl group, an aralkyl group, a pyridyl group, a furyl group, a thienyl group, or a thiazolyl group.
    Type: Application
    Filed: August 29, 2019
    Publication date: July 1, 2021
    Applicants: THE UNIVERSITY OF TOKYO, PI-CRYSTAL INC.
    Inventors: Toshihiro OKAMOTO, Junichi TAKEYA, Masato MITANI, Yosuke ITO, Tomonori MATSUMURO
  • Patent number: 11015263
    Abstract: Bulk single crystal of aluminum nitride (AlN) having an areal planar defect density?100 cm?2. Methods for growing single crystal aluminum nitride include melting an aluminum foil to uniformly wet a foundation with a layer of aluminum, the foundation forming a portion of an AlN seed holder, for an AlN seed to be used for the AlN growth. The holder may consist essentially of a substantially impervious backing plate.
    Type: Grant
    Filed: July 9, 2019
    Date of Patent: May 25, 2021
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert T. Bondokov, Leo J. Schowalter, Kenneth Morgan, Glen A. Slack, Shailaja P. Rao, Shawn Robert Gibb
  • Patent number: 10971665
    Abstract: In various embodiments, a rigid lens is attached to a light-emitting semiconductor die via a layer of encapsulant having a thickness insufficient to prevent propagation of thermal expansion mismatch-induced strain between the rigid lens and the semiconductor die.
    Type: Grant
    Filed: February 26, 2020
    Date of Patent: April 6, 2021
    Assignee: CRYSTAL IS, INC.
    Inventors: Leo J. Schowalter, Jianfeng Chen, James R. Grandusky
  • Patent number: 10954608
    Abstract: In various embodiments, single-crystal aluminum nitride boules and substrates having high transparency to ultraviolet light and low defect density are formed. The single-crystal aluminum nitride may function as a platform for the fabrication of light-emitting devices such as light-emitting diodes and lasers.
    Type: Grant
    Filed: November 9, 2018
    Date of Patent: March 23, 2021
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert T. Bondokov, Jianfeng Chen, Keisuke Yamaoka, Shichao Wang, Shailaja P. Rao, Takashi Suzuki, Leo J. Schowalter
  • Patent number: 10851474
    Abstract: In various embodiments, controlled heating and/or cooling conditions are utilized during the fabrication of aluminum nitride single crystals and aluminum nitride bulk polycrystalline ceramics. Thermal treatments may also be utilized to control properties of aluminum nitride crystals after fabrication.
    Type: Grant
    Filed: December 16, 2019
    Date of Patent: December 1, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert T. Bondokov, Jianfeng Chen, Keisuke Yamaoka, Shichao Wang, Shailaja P. Rao, Takashi Suzuki, Leo J. Schowalter
  • Patent number: 10801127
    Abstract: In various embodiments, methods of forming single-crystal AlN include providing a substantially undoped polycrystalline AlN ceramic having an oxygen concentration less than approximately 100 ppm, forming a single-crystal bulk AlN crystal by a sublimation-recondensation process at a temperature greater than approximately 2000° C., and cooling the bulk AlN crystal to a first temperature between approximately 1500° C. and approximately 1800° C. at a first rate less than approximately 250° C./hour.
    Type: Grant
    Filed: April 26, 2019
    Date of Patent: October 13, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: Sandra B. Schujman, Shailaja P. Rao, Robert T. Bondokov, Kenneth E. Morgan, Glen A. Slack, Leo J. Schowalter
  • Patent number: 10777706
    Abstract: In various embodiments, an electrochemical process is utilized to remove at least a portion of a substrate from multiple singulated or unsingulated electronic-device or optoelectronic-device dies. The dies may be attached to a submount for the removal process, and the dies may be immersed in or non-immersively contact an electrolyte during the removal process.
    Type: Grant
    Filed: October 16, 2018
    Date of Patent: September 15, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: Ken Kitamura, Jianfeng Chen, Leo J. Schowalter
  • Patent number: 10756234
    Abstract: In various embodiments, extraction efficiency of light-emitting devices fabricated on aluminum nitride substrates is enhanced via removal of at least a portion of the substrate.
    Type: Grant
    Filed: May 11, 2018
    Date of Patent: August 25, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: James R. Grandusky, Leo J. Schowalter, Craig Moe
  • Patent number: 10700237
    Abstract: In various embodiments, light-emitting devices incorporate graded layers with compositional offsets at one or both end points of the graded layer to promote formation of two-dimensional carrier gases and polarization doping, thereby enhancing device performance.
    Type: Grant
    Filed: January 4, 2019
    Date of Patent: June 30, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: Craig Moe, James R. Grandusky, Shawn R. Gibb, Leo J. Schowalter, Kosuke Sato, Tomohiro Morishita
  • Patent number: 10697085
    Abstract: Bulk single crystal of aluminum nitride (AlN) having an areal planar defect density?100 cm=2. Methods for growing single crystal aluminum nitride include melting an aluminum foil to uniformly wet a foundation with a layer of aluminum, the foundation forming a portion of an AlN seed holder, for an AlN seed to be used for the AlN growth. The holder may consist essentially of a substantially impervious backing plate.
    Type: Grant
    Filed: October 15, 2018
    Date of Patent: June 30, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert T. Bondokov, Kenneth E. Morgan, Leo J. Schowalter, Glen A. Slack
  • Patent number: 10692980
    Abstract: Fabrication of doped AlN crystals and/or AlGaN epitaxial layers with high conductivity and mobility is accomplished by, for example, forming mixed crystals including a plurality of impurity species and electrically activating at least a portion of the crystal.
    Type: Grant
    Filed: August 6, 2018
    Date of Patent: June 23, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: Glen A. Slack, Leo J. Schowalter
  • Patent number: 10612156
    Abstract: In various embodiments, growth of large, high-quality single crystals of aluminum nitride is enabled via a two-stage process utilizing two different crystalline seeds.
    Type: Grant
    Filed: July 17, 2019
    Date of Patent: April 7, 2020
    Assignee: Crystal IS, Inc.
    Inventors: Leo J. Schowalter, Robert T. Bondokov, James R. Grandusky
  • Patent number: 10615322
    Abstract: In various embodiments, a rigid lens is attached to a light-emitting semiconductor die via a layer of encapsulant having a thickness insufficient to prevent propagation of thermal expansion mismatch-induced strain between the rigid lens and the semiconductor die.
    Type: Grant
    Filed: August 9, 2018
    Date of Patent: April 7, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: Leo J. Schowalter, Jianfeng Chen, James R. Grandusky
  • Patent number: 10550493
    Abstract: In various embodiments, controlled heating and/or cooling conditions are utilized during the fabrication of aluminum nitride single crystals and aluminum nitride bulk polycrystalline ceramics. Thermal treatments may also be utilized to control properties of aluminum nitride crystals after fabrication.
    Type: Grant
    Filed: November 9, 2018
    Date of Patent: February 4, 2020
    Assignee: CRYSTAL IS, INC.
    Inventors: Robert T. Bondokov, Jianfeng Chen, Keisuke Yamaoka, Shichao Wang, Shailaja P. Rao, Takashi Suzuki, Leo J. Schowalter
  • Patent number: 10451943
    Abstract: Active matrix array devices are constituted by devices that have a function such as those of a display/light emitting device, a sensor, a memory or an actuator, and are arranged in a matrix array shape, and the expansion of usage in various fields and applications is expected. However, there is little similarity and compatibility in the forming process and materials between a device such as a display/light emitting device, a sensor, a memory, or an actuator, and a circuit portion that controls such a device in the matrix element, and therefore the device and the circuit portion are mutually restricting factors. This results in an increase in the manufacturing cost and limitation of the function. A conventional active matrix array device is manufactured by performing various process steps on the same substrate. Control circuit portions each including a transistor are formed in some of the process steps.
    Type: Grant
    Filed: April 20, 2016
    Date of Patent: October 22, 2019
    Assignee: PI-CRYSTAL INC.
    Inventors: Seiichiro Yamaguchi, Junichi Takeya, Masataka Itoh, Norikazu Shomoto, Mina Uematsu