Patents Assigned to Degussa-Huls AG
  • Patent number: 5958588
    Abstract: A process for the direct preparation of alkali metal cyanide and alkaline earth metal cyanide granules from an HCN-containing gas and an aqueous solution or suspension of an alkali metal or alkaline earth metal hydroxide. The reaction is performed in a reactor for fluidized bed spray granulation, wherein a solution or suspension of the hydroxide is sprayed onto seed granules of the cyanide being prepared and at the same time a hydrogen cyanide-containing gas is supplied to the reactor and water is evaporated by means of a fluidizing gas. The preferred fluidizing gas is steam. The reaction gases from a BMA or Andrussow process may be quenched with water and the gas mixture used as fluidizing gas. By using a CO.sub.2 -free HCN-containing gas, alkali metal cyanide granules with advantageous properties, including a combined concentration of alkali metal carbonate and alkali metal formate of less then 0.4 wt. %, are obtainable.
    Type: Grant
    Filed: February 5, 1998
    Date of Patent: September 28, 1999
    Assignee: Degussa-Huls AG
    Inventors: Rudiger Schutte, Hans Christian Alt, Catrin Becker-Balfanz, Manfred Sauer, Lukas Von Hippel, Oliver Feuer, Jurgen Lorosch