Patents Examined by Felisa Hiteshew
  • Patent number: 7323048
    Abstract: A method for producing a single crystal in which when the single crystal is grown by Czochralski method, V/G is controlled by controlling a fluctuation of a temperature gradient G of the crystal which is being pulled without lowering a pulling rate V, thereby the single crystal including a desired defect region over a whole plane in a radial direction of the crystal entirely in a direction of the crystal growth axis can be produced effectively for a short time at a high yield.
    Type: Grant
    Filed: May 28, 2004
    Date of Patent: January 29, 2008
    Assignee: Shin-Etsu Handotai Co., Ltd.
    Inventors: Masahiro Sakurada, Makoto Iida, Nobuaki Mitamura, Atsushi Ozaki
  • Patent number: 7320731
    Abstract: A process for growing a silicon single crystal which is capable of growing a silicon single crystal at a pulling rate which is not lower than the critical pulling rate at which an OSF-generating region will be generated is provided. Such a process for growing a silicon single crystal is characterized by using an atmospheric gas for growing a single crystal which is a hydrogen-containing gas which contains a hydrogen-containing substance, and pulling the silicon single crystal at a pulling rate ranging from a value with which the ratio (a/b) of the diameter (b) of the silicon single crystal and the outer diameter (a) of a ring which consists of the OSF-generating region in the radial direction of the silicon single crystal is not higher than 0.77 to another value with which the OSF-generating region disappears at the center part of the crystal.
    Type: Grant
    Filed: July 17, 2006
    Date of Patent: January 22, 2008
    Assignee: Sumco Corporation
    Inventors: Toshiaki Ono, Wataru Sugimura, Masataka Hourai
  • Patent number: 7318916
    Abstract: A semiconductive GaAs wafer has a diameter of 4 inches or more, and an in-wafer plane dislocation density of 30,000/cm2 or more and 100,000/cm2 or less. A semiconductive GaAs wafer is made by growing a GaAs single crystal under a temperature gradient of 20° C./cm or more and 150° C./cm or less formed in the crystal so that the semiconductive GaAs wafer has an in-wafer plane dislocation density of 30,000/cm2 or more and 100,000/cm2 or less.
    Type: Grant
    Filed: January 30, 2006
    Date of Patent: January 15, 2008
    Assignee: Hitachi Cable, Ltd.
    Inventors: Shinji Yabuki, Michinori Wachi, Kouji Daihou
  • Patent number: 7318865
    Abstract: A manufacturing method of an electronic device includes positioning a processed substrate with respect to a substrate stage of a crystallization apparatus and supporting it with at least one positioning mark previously provided on the processed substrate being used as a references, applying a modulated light beam to a predetermined area of the processed substrate supported by the substrate stage and crystallizing the area, and forming at least one circuit element in the crystallized area of the processed substrate subjected to positioning with the positioning mark being used as a reference.
    Type: Grant
    Filed: December 8, 2004
    Date of Patent: January 15, 2008
    Assignee: Advanced LCD Technologies Development Center Co., Ltd.
    Inventors: Noritaka Akita, Yoshio Takami
  • Patent number: 7316747
    Abstract: A method is disclosed for producing a high quality bulk single crystal of silicon carbide in a seeded growth system and in the absence of a solid silicon carbide source, by reducing the separation between a silicon carbide seed crystal and a seed holder until the conductive heat transfer between the seed crystal and the seed holder dominates the radiative heat transfer between the seed crystal and the seed holder over substantially the entire seed crystal surface that is adjacent the seed holder.
    Type: Grant
    Filed: October 12, 2005
    Date of Patent: January 8, 2008
    Assignee: Cree, Inc.
    Inventors: Jason Ronald Jenny, David Phillip Malta, Hudson McDonald Hobgood, Stephan Georg Mueller, Mark Brady, Robert Tyler Leonard, Adrian Powell, Valeri F. Tsvetkov, George J. Fechko, Jr., Calvin H. Carter, Jr.
  • Patent number: 7314523
    Abstract: A method for manufacturing a SiC single crystal from a SiC seed crystal is provided. The method includes the steps of: measuring a diameter of the SiC single crystal during a crystal growth of the SiC single crystal; and controlling the diameter of the SiC single crystal to be a predetermined diameter on the basis of the measured diameter. The method provides the SiC single crystal with high quality and large size.
    Type: Grant
    Filed: August 26, 2005
    Date of Patent: January 1, 2008
    Assignee: DENSO CORPORATION
    Inventors: Kouki Futatsuyama, Yasuo Kitou
  • Patent number: 7314515
    Abstract: An apparatus for fabricating a GaN single crystal and a fabrication method for producing GaN single crystal ingot are provided. The apparatus includes: a reactor including a ceiling, a floor and a wall with a predetermined height encompassing an internal space between the ceiling and the floor, wherein the ceiling is opposite to the floor; a quartz vessel on the floor containing Ga metal; a mount installed on the ceiling on which a GaN substrate is mounted, the GaN substrate being opposite to the quartz vessel; a first gas supplying unit supplying the quartz vessel with hydrogen chloride (HCl) gas; a second gas supplying unit supplying the internal space of the reactor with ammonia (NH3) gas; and a heating unit installed in conjunction with the wall of the reactor for heating the internal space, wherein the lower portion of the internal space is heated to a higher temperature than the upper portion.
    Type: Grant
    Filed: September 8, 2005
    Date of Patent: January 1, 2008
    Assignee: Samsung Corning Co., Ltd.
    Inventor: Jai-yong Han
  • Patent number: 7314517
    Abstract: An improved mineralizer used for a process for obtaining bulk mono-crystalline gallium-containing nitride of a general formula of AlxGa1-xN, where 0?×<1 in an environment of supercritical ammonia-containing solution has been now proposed. According to the invention growth rate and quality of the product obtained can be controlled by suitable selection of mineralizer, so as to ensure presence of ions of Group I element (IUPAC 1989), preferably sodium in combination with other components selected from the group consisting of Group I elements (IUPAC 1989), ions of Group II elements (IUPAC 1989), one or more substances containing oxygen-free species causing some weakening of the ammono-basic nature of the supereritical solvent, optionally in combination with Group II elements (JUPAC 1989), preferably calcium or magnesium.
    Type: Grant
    Filed: December 11, 2003
    Date of Patent: January 1, 2008
    Assignees: Ammono Sp. Z.O.O., Nichia Corporation
    Inventors: Robert Dwilinski, Roman Doradzinski, Jerzy Garczynski, Leszek Sierzputowski, Yasuo Kanbara
  • Patent number: 7314522
    Abstract: An apparatus having a crucible (1) for holding a raw material, a heating means (11) for heating the raw material in the crucible (1) and a crystal transporting means (17) for transporting a seed crystal (13) upwards from the inside of the crucible (1), which further comprises a heat conducting member (3) which extends upwards at least from the vicinity of the upper end of the crucible (1), surrounds a single crystal (15) formed, and is made of a material having heat conductivity, and an interface portion radiation heat blocking member (7) for blocking, at least during cooling after the formation of a single crystal, the radiation heat toward an upper portion above the interface between a taper portion (15a) of the formed single crystal (15) connecting with the seed crystal (13) and a straight bulge portion (15b) having a cylindrical shape connecting with the taper portion (15a) of the formed single crystal (15).
    Type: Grant
    Filed: June 12, 2003
    Date of Patent: January 1, 2008
    Assignee: Hitachi Chemical Co., Ltd.
    Inventors: Shigeki Hirasawa, Masato Ikegawa, Hiroyuki Ishibashi, Akihiro Gunji
  • Patent number: 7314520
    Abstract: A high quality single crystal wafer of SiC is disclosed having a diameter of at least about 3 inches and a 1 c screw dislocation density of less than about 2000 cm?2.
    Type: Grant
    Filed: October 4, 2004
    Date of Patent: January 1, 2008
    Assignee: Cree, Inc.
    Inventors: Adrian Powell, Mark Brady, Stephen G. Mueller, Valeri F. Tsvetkov, Robert T. Leonard
  • Patent number: 7314521
    Abstract: A high quality single crystal wafer of SiC is disclosed having a diameter of at least about 100 mm and a micropipe density of less than about 25 cm?2.
    Type: Grant
    Filed: October 4, 2004
    Date of Patent: January 1, 2008
    Assignee: Cree, Inc.
    Inventors: Adrian Powell, Mark Brady, Robert Tyler Leonard
  • Patent number: 7314518
    Abstract: A crystal growth furnace for a compound semiconductor single crystal has: a small diameter section for placing a seed crystal therein; an increasing diameter section that has diameters to increase from the small diameter section to upward; and a constant diameter section that extends from the increasing diameter section to upward. The increasing diameter section has an angle of 120 degrees or more and less than 160 degrees between inner walls opposed to each other.
    Type: Grant
    Filed: January 13, 2005
    Date of Patent: January 1, 2008
    Assignee: Hitachi Cable, Ltd.
    Inventors: Michinori Wachi, Hiroshi Sasabe, Shunsuke Yamamoto
  • Patent number: 7311772
    Abstract: Means for supplying raw material in additional charging or recharging of solid granular raw material into molten material in the crucible, comprises a raw material supply tube to be filled with said material, a metallic support member which runs through the inside of the tube, connects with the bottom lid, and serves for descending the lid and for ascending the tube and the lid, and a configuration avoiding metallic contamination, whereby the lower-end aperture of the tube is opened for charging said material therein into the crucible in uniform circumferential distribution and in large quantity, thus achieving efficient supply operation to be widely applied for growing silicon single crystals.
    Type: Grant
    Filed: September 20, 2005
    Date of Patent: December 25, 2007
    Assignee: Sumco Corporation
    Inventors: Katsunori Nakashima, Koji Toma, Manabu Moroishi
  • Patent number: 7311778
    Abstract: A method of processing a polycrystalline film on a substrate includes generating a plurality of laser beam pulses, positioning the film on a support capable of movement in at least one direction, directing the plurality of laser beam pulses through a mask to generate patterned laser beams; each of said beams having a length l?, a width w? and a spacing between adjacent beams d?, irradiating a region of the film with the patterned beams, said beams having an intensity that is sufficient to melt an irradiated portion of the film to induce crystallization of the irradiated portion of the film, wherein the film region is irradiated n times; and after irradiation of each film portion, translating either the film or the mask, or both, a distance in the x- and y-directions, where the distance of translation in the y-direction is in the range of about 1?/n-?, where ? is a value selected to form overlapping the beamlets from the one irradiation step to the next, and where the distance of translation in the x-direction
    Type: Grant
    Filed: September 17, 2004
    Date of Patent: December 25, 2007
    Assignee: The Trustees of Columbia University in the City of New York
    Inventors: James S. Im, Paul Christiaan van der Wilt
  • Patent number: 7311977
    Abstract: A highly-oriented diamond film which has a flat surface but does not have non-oriented crystals in the surface can be provided by depositing a first diamond layer on a substrate by {111} sector growth of diamond crystals by a CVD method using a gaseous mixture of methane and hydrogen as material gas, and then depositing a second diamond layer on the first diamond layer by {100} sector growth of diamond crystals by a plasma CVD method using a gaseous mixture of methane, hydrogen, and oxygen as material gas under the conditions that the pressure of the material gas is 133 hPa or more; the material gas composition is determined such that ([C]?[O])/[CH3+H2+O2] is ?0.2×10?2 or more and [O]/[C] is 1.2 or less; and the substrate temperature is between 750° C. and 1000° C.
    Type: Grant
    Filed: November 18, 2005
    Date of Patent: December 25, 2007
    Assignee: Kabushiki Kaisha Kobe Seiko Sho
    Inventors: Yoshihiro Yokota, Kazushi Hayashi, Takeshi Tachibana, Koji Kobashi
  • Patent number: 7311775
    Abstract: This method for heat-treating a silicon wafer includes: a step of subjecting a silicon wafer to a high-temperature heat treatment in an ambient gas atmosphere of hydrogen gas, argon gas or a mixture thereof; and a step of lowering a temperature at a rate of 2° C./min or less in a nitrogen-gas-containing ambient atmosphere in a portion or all of a process of lowering a temperature to a wafer removal temperature following said high-temperature heat treatment. This silicon wafer has a defect-free layer which is formed by a high-temperature heat treatment and is included in a surface thereof, wherein an average iron concentration in said surface is 1×1010 atoms/cm3 or less.
    Type: Grant
    Filed: August 4, 2005
    Date of Patent: December 25, 2007
    Assignee: Sumco Corporation
    Inventors: Tatsumi Kusaba, Hidehiko Okuda, Yoshihisa Nonogaki
  • Patent number: 7311888
    Abstract: The present invention provides an annealed wafer which has a wafer surface layer serving as a device fabricating region and having an excellent oxide film dielectric breakdown characteristic, and a wafer bulk layer in which oxide precipitates are present at a high density at the stage before the wafer is loaded into the device fabrication processes to give an excellent IG capability, and a method for manufacturing the annealed wafer. The present invention is directed to an annealed wafer obtained by performing heat treatment on a silicon wafer manufactured from a silicon single crystal grown by the Czochralski method, wherein a good chip yield of an oxide film dielectric breakdown characteristic in a region having at least a depth of up to 5 ?m from a wafer surface is 95% or more, and a density of oxide precipitates detectable in the wafer bulk and each having a size not smaller than a size showing a gettering capability is not less than 1×109/cm3.
    Type: Grant
    Filed: September 29, 2003
    Date of Patent: December 25, 2007
    Assignee: Shin-Etsu Handotai Co., Ltd.
    Inventors: Hiroshi Takeno, Masahiro Sakurada, Takeshi Kobayashi
  • Patent number: 7309393
    Abstract: Bulk Aluminum Antimonide (AlSb)-based single crystal materials have been prepared for use as ambient (room) temperature X-ray and Gamma-ray radiation detection.
    Type: Grant
    Filed: January 21, 2005
    Date of Patent: December 18, 2007
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: John W. Sherohman, Arthur W. Coombs, III, Jick H. Yee
  • Patent number: 7306676
    Abstract: This apparatus for manufacturing a semiconductor single crystal includes: a crucible; a heater; a crucible driving unit; a chamber for housing the crucible and the heater; and a hydrogen mixed gas supplying device for supplying into the chamber a hydrogen mixed gas including an inert gas in admixture with a hydrogen-containing gas that contains hydrogen atoms, wherein the hydrogen mixed gas supplying device includes: a hydrogen-containing gas supply unit; an inert gas supply unit; a hydrogen-containing gas flow rate controller; an inert gas flow rate controller; and a buffer tank for mixing together the hydrogen-containing gas and the inert gas so as to form a hydrogen mixed gas and for holding the hydrogen mixed gas.
    Type: Grant
    Filed: January 10, 2006
    Date of Patent: December 11, 2007
    Assignee: Sumco Corporation
    Inventors: Wataru Sugimura, Toshiaki Ono, Masataka Hourai
  • Patent number: 7303627
    Abstract: A method is described for making an especially not-(111)-oriented low-stress large-volume crystal having a glide plane with reduced stress birefringence and more uniform refractive index. The method includes growing and tempering the crystal while heating and/or cooling to form a temperature gradient in order to relax stresses arising along the glide plane. During the tempering the heating and/or cooling occurs by heat transfer in a heat transfer direction and the heat transfer direction or temperature gradient is oriented at an angle of from 5° to 90° to the glide plane. Crystals with a uniform refractive index with variations of less than 0.025×10?6 (RMS value) are produced by the method.
    Type: Grant
    Filed: February 22, 2005
    Date of Patent: December 4, 2007
    Assignee: Schott AG
    Inventors: Lutz Parthier, Joerg Staeblein, Gunther Wehrhan, Christian Kusch