Abstract: For conditioning build material for fused filament fabrication, thermal power is both added to and removed from a nozzle in a manner that can reduce sensitivity of the nozzle temperature to fluctuations in build material feed rate. The amount of thermal power added is at least as large as the sum of the amount removed, the amount to condition the material, and losses to the environment. The amount removed may be at least as large as half the thermal power required to condition the material to extrusion temperature, and may be comparable to, or much larger than the conditioning amount. The larger the ratio of the amount removed to the conditioning amount, the less sensitive the nozzle temperature will be to fluctuations in build material feed rate. Fine temperature control arises, enabling building with metal-containing multi-phase materials or other materials that have a narrow working temperature range.
Type:
Grant
Filed:
July 13, 2018
Date of Patent:
February 8, 2022
Assignee:
Desktop Metal, Inc.
Inventors:
Emanuel Michael Sachs, Uwe Bauer, Jonah Samuel Myerberg, Nicholas Graham Bandiera
Abstract: A steel plate for high-strength and high-toughness steel pipes has a chemical composition containing, by mass %, C: 0.03% or more and 0.08% or less, Si: more than 0.05% and 0.50% or less, Mn: 1.5% or more and 2.5% or less, P: 0.001% or more and 0.010% or less, S: 0.0030% or less, Al: 0.01% or more and 0.08% or less, Nb: 0.010% or more and 0.080% or less, Ti: 0.005% or more and 0.025% or less, and N: 0.001% or more and 0.006% or less, and further containing, by mass %, at least one selected from Cu: 0.01% or more and 1.00% or less, Ni: 0.01% or more and 1.00% or less, Cr: 0.01% or more and 1.00% or less, Mo: 0.01% or more and 1.00% or less, V: 0.01% or more and 0.10% or less, and B: 0.0005% or more and 0.0030% or less, with the balance being Fe and inevitable impurities. The steel plate has a microstructure in which an area fraction of ferrite at a ½ position of a thickness of the steel plate is 20% or more and 80% or less and deformed ferrite constitutes 50% or more and 100% or less of the ferrite.
Abstract: The present invention relates to a method for manufacturing a tubular product, characterized in that the tubular product is manufactured from steel comprising chromium in the range of 2.5 to 9.5 wt. % and silicon in an amount of more than 1.0 wt. %, and the method comprises the steps of austenitizing, quenching and tempering at a tempering temperature in the range of 300° C. to 550° C. Furthermore, the invention concerns a tubular product produced by this method.
Type:
Grant
Filed:
February 18, 2020
Date of Patent:
January 25, 2022
Assignee:
Benteler Steel/Tube GmbH
Inventors:
Michael Kaufmann, Marco Walterfang, Ralf Köster
Abstract: A SnAgCuSb-based Pb-free solder alloy is disclosed. The disclosed solder alloy is particularly suitable for, but not limited to, producing solder joints, in the form of solder preforms, solder balls, solder powder, or solder paste (a mixture of solder powder and flux), for harsh environment electronics. An additive selected from 0.1-2.5 wt. % of Bi and/or 0.1-4.5 wt. % of In may be included in the solder alloy.
Abstract: Provided is a ferritic stainless steel sheet excellent in shape of weld zone and corrosion resistance of a weld zone with a material of a different kind formed by performing welding with austenitic stainless steel. A ferritic stainless steel sheet having a chemical composition containing, by mass %, C: 0.003% to 0.020%, Si: 0.01% to 1.00%, Mn: 0.01% to 0.50%, P: 0.040% or less, S: 0.010% or less, Cr: 20.0% to 24.0%, Cu: 0.20% to 0.80%, Ni: 0.01% to 0.60%, Al: 0.01% to 0.08%, N: 0.003% to 0.020%, Nb: 0.40% to 0.80%, Ti: 0.01% to 0.10%, Zr: 0.01% to 0.10%, and the balance being Fe and inevitable impurities, in which relational expression (1) below is satisfied: 3.0?Nb/(2Ti+Zr+0.5Si+5Al)?1.5??(1), here, in relational expression (1), each of the atomic symbols denotes the content (mass %) of the corresponding chemical element.
Abstract: A method for synthesizing a copper-silver alloy includes an ink preparation step, a coating step, a crystal nucleus formation step and a crystal nucleus synthesis step. In the ink preparation step, a copper salt particle, an amine-based solvent, and a silver salt particle are mixed, thereby preparing a copper-silver ink. In the coating step, a member to be coated is coated with the copper-silver ink. In the crystal nucleus formation step, at least one of a crystal nucleus of copper having a crystal grain diameter of 0.2 ?m or less and a crystal nucleus of silver having a crystal grain diameter of 0.2 ?m or less is formed from the copper-silver ink. In the crystal nucleus synthesis step, the crystal nucleus of copper and the crystal nucleus of silver are synthesized.
Type:
Grant
Filed:
July 24, 2018
Date of Patent:
January 4, 2022
Assignees:
SENJU METAL INDUSTRY CO., LTD., OSAKA UNIVERSITY
Inventors:
Jinting Jiu, Minoru Ueshima, Katsuaki Suganuma, Wanli Li
Abstract: A steel pipe for fuel injection pipe has a tensile strength of 500 to 900 MPa and a yield ratio of 0.50 to 0.85, and has a critical internal pressure (IP) satisfying [IP?0.41×TS×?] (?=[(D/d)2?1]/[0.776×(D/d)2], where TS: tensile strength (MPa) of the steel pipe, D: steel pipe outer diameter (mm), and d: steel pipe inner diameter (mm)), wherein a circumferential-direction residual stress on an inner surface of the pipe is ?20 MPa or lower after the steel pipe is split in half in a pipe axis direction.
Abstract: In one aspect of the invention, an alloy includes a first element comprising magnesium (Mg), titanium (Ti), zirconium (Zr), chromium (Cr), or nickelaluminum (NiAl), a second element comprising lithium (Li), calcium (Ca), manganese (Mn), aluminum (Al), or a combination thereof, and a third element comprising zinc (Zn). According to the invention, nanoscale precipitates is produced in the magnesium alloy by additions of zinc and specific heat-treatment. These precipitates lower the energy for dislocation movements and increase the number of available slip systems in the magnesium alloy at room temperature and hence improve ductility and formability of the magnesium alloy.
Type:
Grant
Filed:
December 16, 2014
Date of Patent:
December 14, 2021
Assignee:
NORTHWESTERN UNIVERSITY
Inventors:
Morris E. Fine, Semyon Vaynman, Evan T. Hunt, Akio Urakami, Yip-Wah Chung, Johannes Weertman
Abstract: A method of manufacturing a rolled wear-resistant aluminium alloy product including the steps of: (a) providing a rolling feedstock material of an aluminium alloy having Mg 4.20% to 5.5%, Mn 0.50% to 1.1%, Fe up to 0.40%, Si up to 0.30%, Cu up to 0.20%, Cr up to 0.25%, Zr up to 0.25%, Zn up to 0.30%, Ti up to 0.25%, unavoidable impurities and balance aluminium; (b) heating the rolling feedstock; (c) hot-rolling of the feedstock to an intermediate gauge in a range of 15 mm to 40 mm; (d) hot-rolling of the feedstock from intermediate gauge to a final gauge in a range of 3 mm to 15 mm and wherein the hot-mill exit temperature is in a range of 130-285° C.; (e) cooling of the hot-rolled feedstock to ambient temperature.
Type:
Grant
Filed:
November 13, 2017
Date of Patent:
December 7, 2021
Assignee:
Aleris Rolled Products Germany GmbH
Inventors:
Andreas Harald Bach, Bernd Jacoby, Achim Bürger
Abstract: Provided is a soft magnetic alloy including Fe as a main component, in which a slope of an approximate straight line, plotted between cumulative frequencies of 20 to 80% on Fe content in each grid of 80000 grids or more, each of which has 1 nm×1 nm×1 nm, is ?0.1 to ?0.4, provided that Fe content (atom %) of each grid is Y axis, and the cumulative frequencies (%) obtained in descending order of Fe content in each grid is X axis, and an amorphization ratio X is 85% or more.
Abstract: A manufacturing method for a three-dimensional structure includes forming unit layers using at least one of a first flowable composition including first powder and a second flowable composition including second powder and solidifying at least one of the first flowable composition including the first powder and the second flowable composition including the second powder in the unit layers. In the forming the unit layers, both of the first flowable composition and the second flowable composition are caused to be present in plane directions crossing a thickness direction of the unit layers.
Abstract: A process for selectively separating a metallic constituent from other metals and other materials accompanying the metallic constituent in a mixture is described. The process comprises the step of providing the mixture in an aqueous solution such that the metallic constituent forms a complex anion in the solution. One or more of the other metals forms a cation or a complex cation in the solution. Another step includes contacting the solution with one or more additives to form layered double hydroxide (LDH) material in situ such that the complex anion is intercalated within interlayers of the LDH material and wherein one or more of the other metals are incorporated into the LDH material's crystal structure or matrix. Another step involves the addition of an LDH to an aqueous solution.
Type:
Grant
Filed:
April 15, 2016
Date of Patent:
November 30, 2021
Assignee:
COMMONWEALTH SCIENTIFIC AND INDUSTRIAL RESEARCH ORGANISATION
Abstract: The present application provides a hot-work die steel and a preparation method thereof wherein the chemical constituents of the hot-work die steel in mass percentage are as follows: C: 0.20-0.32 wt %, Si: ?0.5 wt %, Mn: ?0.5 wt %, Cr: 1.5-2.8 wt %, Mo: 1.5-2.5 wt %, W: 0.5-1.2 wt %, Ni: 0.5-1.6 wt %, V: 0.15-0.7 wt %, Nb: 0.01-0.1 wt %, and a balance of iron, wherein an alloying degree is 5-7%; a tensile strength of the hot-work die steel at 700° C. is 560-700 MPa; a value of hardness of the hot-work die steel at room temperature is 32-38 HRC after holding at 700° C. for 3-5 h; and the hot-work die steel has an elongation of 14% to 16% at room temperature, a percentage reduction of area of 48% to 65%, and an impact toughness of 52-63 J at room temperature. The hot-work die steel of the present application has an excellent thermal stability as well as a good plasticity and a toughness at room temperature.
Type:
Grant
Filed:
September 15, 2020
Date of Patent:
November 23, 2021
Assignee:
University of Science and Technology Beijing
Abstract: A flexible porous metal foil sheet made of a metal porous material which use a solid solution alloy, a metal element of a face-centered cubic structure or a metal element of a body-centered cubic structure as the matrix phase, wherein the thickness of the sheet is greater than 200 ?m and less than or equal to 1500 ?m, the average aperture is 0.05˜100 ?m, and the porosity is 15%˜70%. The method for making the flexible porous metal foil comprises: (1) making viscous suspension or muddy paste of raw material powder that will form the metal porous material using a dispersing agent and a binding agent; (2) injecting the suspension or paste into a mold for making membrane, and drying the suspension or paste to form a homogeneous membrane; (3) pressing the membrane to improve the stacking density of the powder particles; and (4) sintering the pressed membrane to obtain the flexible porous metal foil. The flexible porous metal foil has more uniform aperture distribution, and better flatness of the foil.
Abstract: The present invention provides an additive for tin stripping, comprising 0.1 to 20 wt % of copper corrosion inhibitor and 0.1 to 20 wt % of nickel corrosion inhibitor; wherein said weight percentage is based on the total weight of said additive. The present additive can be used with nitric acid conventionally used for metal-stripping for not only reducing the usage of nitric acid but also improving the efficiency of tin stripping. The present invention also provides a method for Tin recycle and a reaction tank for metal recycle. Both of them are favorable for satisfying the needs of metal recycle (especially, tin recycle) in the field.
Abstract: A manufacturing method for a three-dimensional structure includes forming unit layers using at least one of a first flowable composition including first powder and a second flowable composition including second powder and solidifying at least one of the first flowable composition including the first powder and the second flowable composition including the second powder in the unit layers. In the forming the unit layers, both of the first flowable composition and the second flowable composition are caused to be present in plane directions crossing a thickness direction of the unit layers.
Abstract: A method for fabricating a part by selective melting or sintering of powder beds by high energy beam, the method including a) providing a material in the form of powder particles; b) depositing a first powder layer on a support; c) scanning a region of the first layer with the beam to heat the powder locally to a temperature higher than the powder sintering temperature, such that the powder particles as melted or sintered form a first single-piece element; d) depositing a second powder layer on the first powder layer; e) scanning a region of the second layer with the beam to heat the powder to a temperature higher than the powder sintering temperature, so that the particles of powder as sintered or melted form a second single-piece element; and f) repeating d) and e) for each new powder layer laid over a preceding layer until the part is formed.
Abstract: This high strength austenitic stainless steel having excellent resistance to hydrogen embrittlement includes, in terms of mass %, C: 0.2% or less, Si: 0.2% to 1.5%, Mn: 0.5% to 2.5%, P: 0.06% or less, S: 0.008% or less, Ni: 10.0% to 20.0%, Cr: 16.0% to 25.0%, Mo: 3.5% or less, Cu: 3.5% or less, N: 0.01% to 0.50%; and O: 0.015% or less, with the balance being Fe and unavoidable impurities, in which an average size of precipitates is 100 nm or less and an amount of the precipitates is 0.001% to 1.0% in terms of mass %.
Abstract: Processes for refurbishing a spent sputtering target with a non-circular shape are disclosed. In one form, the processes include the steps of receiving one or more spent sputtering targets, inspecting and weighing the spent sputtering targets, removing any contaminants or other surface impurities from the spent sputtering target surfaces, preparing a hot press die with spacers, disposing the spent sputtering targets in the hot press die, the spacers used to center the spent sputtering targets therein, loading fresh metal refilling powder into the die to account for depleted regions of the spent sputtering targets to produce a powder-filled sputtering target, and applying sufficient heat and force to the filled sputtering target to produce a refurbished sputtering target with homogeneous composition and sufficient adhesion strength.
Type:
Grant
Filed:
May 31, 2016
Date of Patent:
October 19, 2021
Assignee:
Materion Corporation
Inventors:
Longzhou Ma, Xingbo Yang, Matthew J. Komertz, Arthur V. Testanero
Abstract: A die apparatus including a first die element, a plurality of second die elements, a plurality of actuators, and a controller is provided. Each of the plurality of actuators is mounted to one of the plurality of second die elements. The controller is programmed to activate the actuators to contact and compress portions of a blank disposed between the die elements at separate pressures to influence microstructure forming for one of a geometry transition region, a deformation region, and a joining region. One of the separate pressures applied to one of the portions of the blank may be approximately 5 N/mm2 or less to form a soft strength zone. The pressure of approximately 5 N/mm2 or less may be applied to the one of the portions of the blank for approximately one to two seconds.
Type:
Grant
Filed:
June 16, 2017
Date of Patent:
October 12, 2021
Assignee:
Ford Global Technologies, LLC
Inventors:
Raj Sohmshetty, Torsten Hallfeldt, S. George Luckey, Jr.