Patents Examined by Tam M. Nguyen
  • Patent number: 11549074
    Abstract: A device for the descending flow of a hydrocarbon-containing liquid containing solid particles at the bottom of an item of equipment (1) and a process for the conversion of hydrocarbon-containing feedstocks implementing said device.
    Type: Grant
    Filed: December 15, 2020
    Date of Patent: January 10, 2023
    Assignee: IFP Energies Nouvelles
    Inventors: Benjamin Amblard, Joao Marques, Jean-Francois Le Coz
  • Patent number: 11548843
    Abstract: In a propane dehydrogenation (PDH) process, the purpose of the deethanizer and chilling train systems is to separate the cracked gas into a methane-rich tail gas product, a C2, and a C3 process stream. By the use of staged cooling, process-to-process inter-change against propane feed to the reactor and use of high efficiency heat exchangers and distributed distillation techniques, refrigeration power requirements are reduced and a simple and reliable design is provided by the process described herein.
    Type: Grant
    Filed: October 26, 2021
    Date of Patent: January 10, 2023
    Assignee: Kellogg Brown & Root LLC
    Inventor: Rian Reyneke
  • Patent number: 11549061
    Abstract: The invention relates to an improved apparatus and methods for managing and utilizing light hydrocarbons utilized and created during the hydroprocessing of biological feedstocks in the making of middle distillate fuels.
    Type: Grant
    Filed: July 8, 2020
    Date of Patent: January 10, 2023
    Assignee: Axens
    Inventor: Dominic Debonis
  • Patent number: 11542445
    Abstract: Embodiments of the disclosure provide an aqueous reforming system and a method for upgrading heavy hydrocarbons. A hydrocarbon feed and a surfactant stream are combined to produce a first precursor stream. The first precursor stream and an alkali feed are combined to produce a second precursor stream. The second precursor stream and a transition metal feed are combined to produce a catalytic emulsion stream. The catalytic emulsion stream is heated to produce a catalytic suspension and a decomposition gas, where the decomposition gas is separated by a first separator. The catalytic suspension is combined with a preheated water stream to produce an aqueous reformer feed. The aqueous reformer feed is introduced to an aqueous reformer such that the heavy hydrocarbons undergo conversion reactions to produce an effluent stream. The effluent stream is introduced to a second separator to produce a heavy stream and a light stream.
    Type: Grant
    Filed: August 9, 2021
    Date of Patent: January 3, 2023
    Assignee: Saudi Arabian Oil Company
    Inventors: Mazin M. Fathi, Ki-Hyouk Choi, Mohammed R. Aldossary
  • Patent number: 11542243
    Abstract: A method of isomerizing ?9-tetrahydrocannabinol (“?9-THC”) to ?10-tetrahydrocannabinol (“?10-THC”). The method includes the steps of: extracting ?9-THC from cannabis biomass, which optionally contains one or more of the components found in fire retardant such as PHOS-CHEK®; dewaxing of crude extracts by winterization; pH-adjusting extracts by washing the extracts in heptane solution with aqueous solutions of: citric acid, sodium bicarbonate, and brine; isomerizing ?9-THC to ?10-THC by exposure to suitable conditions and in the presence of a catalyst based on the components of fire retardant; vacuum distillation of ?10-THC at a predetermined temperature range and vacuum level; collecting the distillate and redistilling it up to three times to acquire distillate containing less than 60% ?10-THC; and purification of the MO-THC to a purity of 99% or greater by crystallization from n-pentane solution.
    Type: Grant
    Filed: September 28, 2020
    Date of Patent: January 3, 2023
    Inventors: Joshua Jones, Justin Cotham, Nicholas Frilot
  • Patent number: 11530174
    Abstract: The present invention discloses a method for separating propylene, propyne, propane and propadiene from mixed gas, wherein, comprising: a high purity component can be obtained as metal-organic frameworks as adsorbents through adsorptive separation and purification of a mixed gas containing propylene, propyne, propane and propadiene a general structural formula of the metal-organic framework material is [M(C4O4)(H2O)]·1.5H2O, wherein M is metal ions, the metal-organic framework material is a three-dimensional network structure formed by transition metal ions or alkaline earth metal ions and squaric acid through coordination bonds or intermolecular forces. The metal-organic framework materials of the present invention exhibit excellent adsorption and separation performances for propylene, propyne, propane and propadiene. The cheap and available raw materials for the synthesis, simple operation, and low cost make it cost-efficient for preparation of such metal-organic frameworks.
    Type: Grant
    Filed: October 24, 2019
    Date of Patent: December 20, 2022
    Assignee: ZHEJIANG UNIVERSITY
    Inventors: Zongbi Bao, Liangying Li, Qilong Ren, Zhiguo Zhang, Yiwen Yang, Qiwei Yang
  • Patent number: 11525628
    Abstract: Process for producing biomethane from a biogas stream including methane, carbon dioxide and at least one impurity chosen from ammonia, volatile organic compounds, water, sulfur-based impurities (H2S) and siloxanes. A biogas stream is dried, the at least one impurity is at least partially removed by solidification and removal of the impurity. The methane and the carbon dioxide contained in the biogas obtained from the second step are separated so as to produce a biomethane stream and a CO2 stream.
    Type: Grant
    Filed: September 25, 2019
    Date of Patent: December 13, 2022
    Assignee: L'Air Liquide, Societe Anonyme Pour L'Etude Et L'Exploitation Des Procedes Georges Claude
    Inventors: Guillaume Cardon, Antonio Trueba, Solene Valentin
  • Patent number: 11525091
    Abstract: A method of forming high molecular weight (“HMW”) coal tar can include combining supercritical carbon dioxide (sCO2) and an amount of coal tar, and fractionating the amount of coal tar to form the HMW coal tar. The method can further include forming the amount of coal tar from coal. Forming the amount of coal tar from coal can include extracting the coal tar from an amount of coal using sCO2.
    Type: Grant
    Filed: March 23, 2020
    Date of Patent: December 13, 2022
    Assignee: CARBON HOLDINGS INTELLECTUAL PROPERTIES, LLC
    Inventors: Charles Agee Atkins, Matthew Targett
  • Patent number: 11504693
    Abstract: The present invention relates to an adsorbent comprising an alumina support and at least one alkali element, said adsorbent being obtained by introducing at least one alkali element, identical to or different from sodium, onto an alumina support the sodium content of which, expressed as Na2O equivalent, before the introduction of the alkali element or elements, is comprised between 1000 and 5000 ppm by weight with respect to the total weight of the support. The invention also relates to processes for the preparation of said adsorbent and use thereof in a process for the elimination of acidic molecules such as COS and/or CO2.
    Type: Grant
    Filed: June 22, 2015
    Date of Patent: November 22, 2022
    Assignee: IFP Energies nouvelles
    Inventors: Karin Barthelet, Arnaud Baudot, Marc-Antoine Lelias, Olivier Ducreux
  • Patent number: 11505754
    Abstract: According to one or more embodiments, petrochemical products may be formed from a hydrocarbon material by a method that includes separating crude oil into at least two or more fractions in an atmospheric distillation column, hydrotreating the atmospheric residue to form a hydrotreated atmospheric residue, combining steam with the hydrotreated atmospheric residue, and cracking at least a portion of the hydrotreated atmospheric residue in the presence of a first catalyst to produce a cracking reaction product.
    Type: Grant
    Filed: September 1, 2020
    Date of Patent: November 22, 2022
    Assignee: Saudi Arabian Oil Company
    Inventors: Aaron Chi Akah, Musaed Salem Al-Ghrami
  • Patent number: 11499104
    Abstract: A method is disclosed of purifying a recycled or renewable organic material, wherein the recycled or renewable organic material includes more than 1 ppm silicon as silicon compounds and/or more than 10 ppm phosphorous as phosphorous compounds. The method can include providing a feed of the lipid material; heat treating the organic material in presence of an adsorbent and the filtering organic material and hydrotreating the lipid material in a presence of a hydrotreating catalyst to obtain purified hydrotreated organic material having less than 20% organic material and/or less than 30% of the original phosphorous content of the organic material.
    Type: Grant
    Filed: July 19, 2019
    Date of Patent: November 15, 2022
    Assignee: NESTE OYJ
    Inventors: Blanka Toukoniitty, Ville Paasikallio, Jukka-Pekka Pasanen, Jouni Touronen, Meri Hovi, Antti Pasanen, Salla Likander, Sami Toppinen, Pekka Aalto, Kari Jansson, Marina Lindblad, Mats Käldström, Kaisa Lamminpää
  • Patent number: 11499103
    Abstract: A process for the hydroconversion of heavy oil products includes the following steps where heavy oil products and hydrogen are supplied to a slurry hydroconversion section having a molybdenum-based catalyst: separating the reaction effluent into a vapour phase and a slurry phase; and sending the slurry phase to a separation section having the function of separating the Vacuum Gas Oil, Heavy Vacuum Gas Oil, Light Vacuum Gas Oil, and Atmospheric Gas Oil fractions, from a stream of heavy organic products which contains asphaltenes, unconverted feed, catalyst, and solid formed during the hydroconversion reaction. This stream is partly sent to the reaction section and partly forms a purge stream, which is heated and made fluid between 185° C.-220° C., and subjected to a static settling unit up to at least 100° C. From the settling unit two new products, clarified component and cake, are obtained. The clarified component is recycled to the hydroconversion reaction section.
    Type: Grant
    Filed: September 24, 2019
    Date of Patent: November 15, 2022
    Assignee: ENI S.P.A.
    Inventors: Stefania Guidetti, Alberto Malandrino, Simone Cattaneo
  • Patent number: 11498836
    Abstract: A method for producing an iron pigment and hydrochloric acid with reduced or substantially eliminated waste streams includes: providing an iron chloride solution, wherein the iron chloride solution includes one or both of iron (II) chloride and iron (III) chloride; neutralizing the iron chloride solution with one or both of ammonia and ammonium hydroxide to form a slurry of an iron oxide solid component and an ammonium chloride solution; separating the iron oxide solid component from the ammonium chloride solution; drying the iron oxide solid component to form an iron pigment or pigment intermediate; reacting the ammonium chloride solution with an alkaline-earth metal solid to form an alkaline-earth metal chloride solution and to evolve ammonia as a vapor, wherein at least a portion of the evolved ammonia reacts with water to form ammonium hydroxide; recycling one or both of the evolved ammonia and the formed ammonium chloride for use in connection with the neutralization step; and pyrohydrolyzing the alkalin
    Type: Grant
    Filed: June 11, 2020
    Date of Patent: November 15, 2022
    Assignee: L3 Développement de procédés Inc.
    Inventors: Tommee Metivier-Larochelle, Eric F. Larochelle
  • Patent number: 11491466
    Abstract: A regeneration solvent comprised of one or more ethylene amines may contact an adsorbent bed that has been used to remove sulfur compounds from a hydrocarbon stream to extract adsorbed sulfur compounds from the adsorbent material in the bed to regenerate it. The one or more ethyleneamines may have structure (I), (II), or (III): where R1, R2, R5 and R6 are, to the extent chemically possible, independently H, C1-C4 linear or branched alkyl, amido (RRNC?O), or hydroxyalkyl, where each R in the amido group is independently H or C1 alkyl, where R3 and R4 are alkylene of from 1 to 4 carbon atoms, where x ranges from 0 to 3, y ranges from 1 to 6. The regenerated adsorbent bed may be reused, either alone or in combination with a liquid-liquid extraction column, to remove sulfur compounds from a hydrocarbon stream.
    Type: Grant
    Filed: April 29, 2021
    Date of Patent: November 8, 2022
    Assignee: Baker Hughes Oilfield Operations LLC
    Inventors: Sai Reddy Pinappu, Jerry J. Weers
  • Patent number: 11485692
    Abstract: A method for preparing ethylene including: feeding a thermally cracked compressed stream to a first distillation apparatus selectively operating as a first deethanizer or a depropanizer; and feeding an overhead discharge stream of the first distillation apparatus to a second distillation apparatus. When the first distillation apparatus is operated as the first deethanizer, a bottom discharge stream of the second distillation apparatus is fed to a C2 separator. When the first distillation apparatus is operated as the depropanizer, the bottom discharge stream of the second distillation apparatus is passed through a third distillation apparatus and fed to the C2 separator.
    Type: Grant
    Filed: July 4, 2019
    Date of Patent: November 1, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Tae Woo Kim, Sung Kyu Lee, In Seop Kim, Joon Ho Shin, Yeon Uk Choo
  • Patent number: 11485914
    Abstract: This invention relates to the recovery of hydrocarbons i.e. to a process and system for the production of synthetic crude oil from unconventional oil sources such as oil sands, oil shale, and similar materials. The process comprises pyrolysing the feedstock in a pyrolysis liquid comprising molten metal(s) or molten salt (s).
    Type: Grant
    Filed: March 20, 2020
    Date of Patent: November 1, 2022
    Assignee: COMPOSITE RECYCLING CORP.
    Inventors: Roman Cintula, Frank Riedewald
  • Patent number: 11479522
    Abstract: The present invention relates to a method for the purification of alkanes, especially methane, wherein an alkane comprising impurities, especially methane, is reacted with an active compound, optionally in the presence of sulfur trioxide, whereby the impurities are removed. The present invention furthermore relates to the use of the active compound and sulfur trioxide in the purification of alkanes, especially methane.
    Type: Grant
    Filed: March 17, 2020
    Date of Patent: October 25, 2022
    Assignee: BASF SE
    Inventor: Timo Ott
  • Patent number: 11473020
    Abstract: A method for fluid catalytic cracking (FCC) of petroleum oil feedstock includes reacting the petroleum oil feedstock with a catalyst mixture in a reaction zone of an FCC unit to obtain a product stream including desulfurized hydrocarbon product, unreacted petroleum oil feedstock, and spent catalyst. During the reacting a process control system develops a process model based on data collected during the reacting, the process model characterizing a relationship among the feed rate of the base cracking catalyst, the feed rate of the FCC additive, the operating conditions, the composition of the product stream, and emissions from the reaction; and one or more of (i) a target feed rate of the base cracking catalyst, (ii) a target feed rate of the FCC additive, and (iii) one or more target operating conditions of the reaction in the reaction zone to reduce the emissions from the FCC unit and to increase a yield of the desulfurized hydrocarbon product in the product stream are determined.
    Type: Grant
    Filed: January 7, 2021
    Date of Patent: October 18, 2022
    Assignee: Saudi Arabian Oil Company
    Inventors: Saeed Al-Alloush, Othman Taha
  • Patent number: 11460454
    Abstract: A method for monitoring, evaluating and controlling a cyclic chromatographic purification process that involves at least two adsorbers. According to the method, one step is monitoring of the chromatogram, including the measurement of at least one current concentration-proportional signal in the liquid. Another step is conducting an evaluation of the chromatogram, including a comparison of at least one of the current concentration-proportional signals measured in the monitoring step with a threshold value thereof. A further step is controlling the chromatographic purification process by adapting the termination of the currently running phase as a function of the comparison of the evaluation step and initiating the next phase. Finally, according to the method, the sequence of steps is carried out in given order at least twice.
    Type: Grant
    Filed: November 6, 2018
    Date of Patent: October 4, 2022
    Assignee: ChromaCon AG
    Inventors: Lars Aumann, Thomas Müller-Späth, Michael Bavand
  • Patent number: 11459516
    Abstract: Systems and methods include an aromatics complex (ARC), the ARC in fluid communication with a naphtha reforming unit (NREF) and operable to receive a reformate stream produced by the NREF, and the ARC further operable to separate the reformate stream into a gasoline pool stream, an aromatics stream, and an aromatic bottoms stream; and a hydrodearylation unit operable to receive heavy, non-condensed, alkyl-bridged, multi-aromatic compounds from the aromatic bottoms stream, the hydrodearylation unit further operable to hydrogenate and hydrocrack the heavy, non-condensed, alkyl-bridged, multi-aromatic compounds to produce a stream suitable for recycle to the NREF or the reformate stream, where the hydrodearylation unit is further operable to receive hydrogen produced in the NREF.
    Type: Grant
    Filed: May 24, 2021
    Date of Patent: October 4, 2022
    Inventors: Robert Peter Hodgkins, Omer Refa Koseoglu, Frederick Adam