Abstract: The present application provides a preparation method of racemic nicotine, including the following steps: Nicotinyl chloride and methylamine are reacted under alkaline conditions to obtain methylnicotinamide, then condensed with monochloroacetone to obtain N-methyl-N-(2-oxopropyl) nicotinamide, then self-aldol condensed to obtain 1-methyl-5-(pyridin-3-yl)-1,2-dihydro-3H-pyrrol-3-one, and finally reduced to obtain racemic nicotine.

Abstract: The present application discloses a synthesis method of chiral nicotine from nicotinate and ?-butyrolactone, including the following steps: Step S1: performing condensation under an alkaline condition, and performing ring opening reaction with hydrochloric acid; Step S2: reacting with (+)-B-diisopinocampheyl chloroborane to produce a chiral hydroxyl group; Step S3: performing a chlorination reaction; and Step S4: performing cyclization under an alkaline condition to obtain the chiral nicotine. In the present application, nicotinate and ?-butyrolactone, both cheap and readily available, are used as raw materials, so as to reduce the production cost of (S)-nicotine. (+)-B-diisopinocampheyl chloroborane is used to reduce a carbonyl group of an intermediate to obtain a target chiral center.

Abstract: A method for preparing chiral synthetic nicotine includes the following steps: Step S1. condensing nicotinic acid ester and ?-butyrolactone under the action of alkaline condensate in organic solvent I to obtain the first mixture; Step S2. performing a ring-opening reaction to the first mixture obtained in Step S1 by adding an acidic substance to obtain a second mixture; Step S3. separating 4-chloro-1-(3-pyridine)-1-butanone from the second mixture obtained in Step S2, reacting with chiral tert-butyl sulfinamide to obtain chiral N-(4-chloro-1-(pyridin-3-yl)butene) -2-methylpropane-2-sulfinamide; Step S4: reacting the chiral N-(4-chloro-1-(pyridin-3-yl) butene)-2-methylpropane-2-sulfenamide with a reducing agent, and then cyclizing under the action of hydrogen halide to obtain a chiral demethylized nicotine; and Step S5: performing methylamination to the chiral demethylized nicotine to obtain a chiral nicotine.

Abstract: The present invention provides a preparation method for synthesizing S-nicotine from glutarate, including: reacting nicotinate with glutarate in the presence of a base catalyst to obtain 5-carbonyl-5-(pyridin-3-yl)pentanoic acid, reacting with an amination reagent to obtain 5-oxo-5-(pyridin-3-yl)pentanamide, performing Hofmann degradation on to obtain 4-amino-1-(pyridin-3-yl)butanone, reducing a carbonyl group of the 4-amino-1-(pyridin-3-yl)butanone by using (+)-B-diisopinocampheyl chloroborane to obtain (S)-4-amino-1-(pyridin-3-yl)butan-1-ol, performing chlorination and cyclization to obtain S-demethylnicotine, and finally performing amine methylation to obtain S-nicotine.

Abstract: A cable connector includes an outer housing, an inner housing including a first housing and a second housing assembled with each other, and a cable assembly retained between the first housing and the second housing. The cable assembly includes a pair of terminals, two wires, and a sleeve. The second housing defines a group of first holding portions for holding the wires. The first housing and the second housing each define a group of second holding portions for commonly holding the sleeve.

Abstract: Systems and methods are provided for use in providing messaging among different regions, via a distributed event drive architecture. One exemplary method includes receiving, at an event gateway in a region, a network message from a different event gateway in a different region, via a persistent connection between the event gateway and the different event gateway, and validating, by the event gateway, the network message based on at least a certificate associated with the network message. The method also includes, in response to validation of the network message, converting, by the event gateway, the network message to an event and publishing, by the event gateway, the event to the message bus, thereby providing the event associated with the network message to a service to which the network request is directed.

Abstract: An acoustic garbage classification method using a one-dimensional convolutional neural network (1D-CNN) is provided. The method includes: acquiring sound signals generated by falling garbage; preprocessing the sound signals; acquiring and preprocessing the sound signals of different types of garbage, building a sound database for garbage classification, and establishing and training a 1D-CNN model; acquiring a sound signal of garbage to be classified, and inputting the sound signal into the trained 1D-CNN for garbage classification to obtain a classification result. The present disclosure is helpful to assist people in accurate garbage classification, improves the accuracy of garbage classification and recycling, and has high practical and popularization value.

Abstract: An offshore floating structure such as a wind turbine includes a number of improvements. The floating structure can include a chain engaging system configured to prevent any lengthwise movement of a mooring chain. The floating structure can also include a mooring fixture pivotally coupled to the hull to prevent shock loads from being transmitted directly from the mooring line to the hull. The floating structure can also include installation aid structures that provide additional water plane area and/or buoyancy to the structure. The floating structure can also have a hull that is optimized for use as an offshore wind turbine.

Abstract: Methods are disclosed for manufacturing a Micro-ElectroMechanical Systems (MEMS) scanning mirror. In an embodiment, one method includes depositing a hinge material on a substrate and removing first and second portions of the substrate to form an outer frame, an inner frame, and a mirror plate in the substrate. First and second portions of the hinge material rotationally couple the outer frame to the inner frame and the inner frame to the mirror plate for rotation about first and second orthogonal axes of rotation. In another embodiment, a third portion of the substrate rotationally couples the inner frame to the mirror plate. In still another embodiment, an elastomer material is configured as a bending hinge that rotationally couples the outer frame to the inner frame.

Abstract: A soft electrohydrodynamic actuator includes an actuating unit. The actuating unit includes a flexible pouch, a rod electrode, a dielectric fluid, an enameled wire, a hose and a planar flexible electrode. The inner cavity of the flexible pouch is provided with the rod electrode and filled with the dielectric fluid. The hose is hermetically connected to a side of the flexible pouch. The enameled wire is hermetically sleeved in the hose. One end of the enameled wire extends into the inner cavity of the flexible pouch through the hose and is electrically connected to an end of the rod electrode. The other end of the enameled wire is connected to a high-voltage positive electrode. The outer surface of the flexible pouch is coated with a layer of conductive soft material as the planar flexible electrode, or a water environment around the flexible pouch is used as the planar flexible electrode.

Abstract: Provided is an extension module for independently storing calibration data, including: a first interface, adapted to receive a first external input signal; a second interface, adapted to output the first output signal of the extension module; a signal processing circuit, connected between the first interface and the second interface; and a first memory, the first memory storing first calibration data, and the first calibration data being associated with the extension module. Furthermore, also provided is a component using the above extension module, and a component calibration method. On the one hand, the extension module of an embodiment may share an ADC sampling circuit on a main module, so that the manufacturing cost of the extension module is reduced. On the other hand, an embodiment can facilitate the replacement of different extension modules for the main module without repeated calibration.

Abstract: A plug connector includes an insulative plug housing with a plurality of plug contacts retained thereto. The plug housing forms a plug mating portion with a mating surface thereon. The plug contacts include front blade contacting sections extending beyond the mating surface and are arranged along the first direction with one another. Viewed along the first direction, the mating surface is curved with a bulged middle section. The receptacle connector includes a receptacle housing with a plurality of receptacle contacts retained thereto. The receptacle housing forms therein a mating cavity in which a receptacle mating portion extends along the mating direction wherein the receptacle mating portion forms a mating face behind which the receptacle contacts are located. During mating, the plug mating portion is snugly received within the mating cavity with the mating surface of the plug connector is spaced from the mating face of the receptacle connector.

Abstract: An offshore floating structure such as a wind turbine includes a number of improvements. The floating structure can include a chain engaging system configured to prevent any lengthwise movement of a mooring chain. The floating structure can also include a mooring fixture pivotally coupled to the hull to prevent shock loads from being transmitted directly from the mooring line to the hull. The floating structure can also include installation aid structures that provide additional water plane area and/or buoyancy to the structure. The floating structure can also have a hull that is optimized for use as an offshore wind turbine.

Abstract: High volume-rate three-dimensional (“3D”) ultrasound imaging using fast acoustic steering via tilting electromechanical reflectors is described. Ultrasound beams are directed towards one or more tilting reflectors, which are scanned through a range of tilt angles in order to image a 3D field-of-view with a high volume rate.

Abstract: An electrical connector assembly includes a first connector and a second connector mateable with each other wherein each of the first connector and the second connector has an insulative housing essentially composed of a bottom wall, a side wall and a pair of end walls wherein all the bottom wall and the side wall are rectangular while the end walls are right triangular. The first connector and he second connector are coupled with each other in a complementary manner with the corresponding hypotenuses of the right triangles confronting each other. A sealing member of a frame structure is located at an interface between the coupled edges of the housings in an oblique manner.

Abstract: An electrical connector assembly includes a plug connector and a receptacle connector. A plug connector includes an insulative plug housing and a plurality of blade type male contacts retained in the plug housing. Each of the blade type male contacts includes a contacting section composed of two opposite primary mating planes and two opposite side locking planes. Correspondingly, a receptacle connector includes an insulative receptacle housing and a plurality of clip type female contacts retained in the receptacle housing. Each of the clip type female contacts includes a pair of contacting portions sandwiching the two opposite primary mating planes of the corresponding blade type male contact therebetween in a first horizontal direction. A metallic blade type locking piece retained in the receptacle housing, includes a pair of locking arms sandwiching the two opposite side locking planes therebetween in a second horizontal direction perpendicular to the first horizontal direction.

Abstract: The present disclosure provides a method and a device for detecting and evaluating a defect with electromagnetic multi-field coupling. The method includes magnetizing a pipeline with the electromagnetic multi-field coupling; detecting a defect of the pipeline along an axial direction of the pipeline at a constant speed; collecting signals at a position of the defect to obtain magnetic leakage signals in three dimensions and an electrical impedance signal; pre-processing the collected signals; decoupling the pre-processed signals, to obtain decoupled magnetic leakage signals and a decoupled electrical impedance signal; performing impedance analysis on the decoupled electrical impedance signal, and determining a type of the defect based on a phase angle of the decoupled electrical impedance signal; and performing quantification analysis on the decoupled magnetic leakage signals and performing quantification evaluation on a size of the defect using a neural network defect quantification method.

Abstract: A communication method includes: determining, by a first device, a first synchronization signal, where the first synchronization signal is used by a second device for symbol timing alignment and frequency synchronization; and sending, by the first device, the first synchronization signal on each group of subcarriers of M groups of subcarriers, where M is a positive integer greater than or equal to 2. According to the communication method in this application, the first device sends the first synchronization signal on each group of subcarriers of a plurality of groups of subcarriers, so that the second device can select, based on a reception capability of the second device, an appropriate bandwidth to receive the first synchronization signal.

Abstract: A plug connector includes an insulative plug housing with a plurality of plug contacts retained thereto. The plug housing forms a plug mating portion with a mating surface thereon. The plug contacts include front blade contacting sections extending beyond the mating surface and are arranged along the first direction with one another. Viewed along the first direction, the mating surface is curved with a bulged middle section. The receptacle connector includes a receptacle housing with a plurality of receptacle contacts retained thereto. The receptacle housing forms therein a mating cavity in which a receptacle mating portion extends along the mating direction wherein the receptacle mating portion forms a mating face behind which the receptacle contacts are located. During mating, the plug mating portion is snugly received within the mating cavity with the mating surface of the plug connector is spaced from the mating face of the receptacle connector.

Abstract: An electrical connector assembly includes a plug connector and a receptacle connector. A plug connector includes an insulative plug housing and a plurality of blade type male contacts retained in the plug housing. Each of the blade type male contacts includes a contacting section composed of two opposite primary mating planes and two opposite side locking planes. Correspondingly, a receptacle connector includes an insulative receptacle housing and a plurality of clip type female contacts retained in the receptacle housing. Each of the clip type female contacts includes a pair of contacting portions sandwiching the two opposite primary mating planes of the corresponding blade type male contact therebetween in a first horizontal direction. A metallic blade type locking piece retained in the receptacle housing, includes a pair of locking arms sandwiching the two opposite side locking planes therebetween in a second horizontal direction perpendicular to the first horizontal direction.