Including Solid Member Shaping Means Other Than Seed Or Product (e.g., Edfg Die) Patents (Class 117/209)
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Publication number: 20140202379Abstract: A crucible for growing crystals, the crucible being formed from Molybdenum and Rhenium. A crucible for growing crystals, the crucible being formed from a metal selected from Group V of the Periodic Table of the Elements. A crucible for growing crystals, the crucible comprising a body and a layer formed on at least a portion of the body, the layer being formed out of Molybdenum.Type: ApplicationFiled: February 21, 2014Publication date: July 24, 2014Inventor: Matthew Fonte
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Publication number: 20140182512Abstract: A crystal growth apparatus includes a first housing, a second housing and a controller received in the second housing. The first housing includes a first main body and defines a growth chamber in the first main body. The second housing includes a second main body and a pulling rod. The second main body defines a transmission chamber and a cooling chamber. The pulling rod is mounted in the transmission chamber, and a first seed rod is mounted on the pulling rod. The controller includes a transmission member and a pair of partition assemblies. The second housing includes a separating sheet and a second seed rod. The separating sheet separates the transmission chamber from the growth chamber. The second seed rod is mounted in the cooling chamber. The pair of partition assemblies move enabling the cooling chamber to communicate with the transmission chamber, such that the transmission member exchanges seed rods.Type: ApplicationFiled: December 16, 2013Publication date: July 3, 2014Applicant: HON HAI PRECISION INDUSTRY CO., LTD.Inventor: SHAO-HAN CHANG
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Patent number: 8673075Abstract: A method and apparatus for growing a semiconductor crystal include pulling the semiconductor crystal from melt at a pull speed and modulating the pull speed by combining a periodic pull speed with an average speed. The modulation of the pull speed allows in-situ determination of characteristic temperature gradients in the melt and in the crystal during crystal formation. The temperature gradients may be used to control relevant process parameters that affect morphological stability or intrinsic material properties in the finished crystal such as for instance the target pull speed of the crystal or the melt gap, which determines the thermal gradient in the crystal during growth.Type: GrantFiled: March 29, 2012Date of Patent: March 18, 2014Assignees: Sumco Phoenix Corporation, Sumco CorporationInventors: Benno Orschel, Andrzej Buczkowski, Joel Kearns, Keiichi Takanashi, Volker Todt
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Patent number: 8580036Abstract: The method and apparatus includes a vessel having a bottom and sidewalls arranged to house the material in a molten state. A temperature controlled horizontally oriented, cooling plate is movable into and out of the top of the molten material. When the cooling plate is lowered into the top of the melt, an ingot of solid silicon is solidified downwards.Type: GrantFiled: May 10, 2006Date of Patent: November 12, 2013Assignee: Elkem Solar ASInventor: Kenneth Friestad
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Patent number: 8440017Abstract: To grow a gallium nitride crystal, a seed-crystal substrate is first immersed in a melt mixture containing gallium and sodium. Then, a gallium nitride crystal is grown on the seed-crystal substrate under heating the melt mixture in a pressurized atmosphere containing nitrogen gas and not containing oxygen. At this time, the gallium nitride crystal is grown on the seed-crystal substrate under a first stirring condition of stirring the melt mixture, the first stirring condition being set for providing a rough growth surface, and the gallium nitride crystal is subsequently grown on the seed-crystal substrate under a second stirring condition of stirring the melt mixture, the second stirring condition being set for providing a smooth growth surface.Type: GrantFiled: August 12, 2011Date of Patent: May 14, 2013Assignee: NGK Insulators, Ltd.Inventors: Takanao Shimodaira, Takayuki Hirao, Katsuhiro Imai
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Patent number: 8388751Abstract: A method of growing a ribbon crystal provides a crucible containing molten material and passes string through the molten material to grow the ribbon crystal. The method further directs gas flow around the ribbon crystal such that the gas flows down along the ribbon crystal toward the crucible.Type: GrantFiled: August 17, 2009Date of Patent: March 5, 2013Assignee: Max Era, Inc.Inventors: David Harvey, Weidong Huang, Scott Reitsma, Minh Sy Le
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Patent number: 8351660Abstract: A face area is detected from an image captured by an image pickup device, pixel values of the image are adjusted based on information concerning the detected face area, a person area is detected from the adjusted image, and the detected face area is integrated with the detected person area. With this configuration, it is possible to accurately detect an object even in a case, for example, where the brightness is varied.Type: GrantFiled: February 27, 2009Date of Patent: January 8, 2013Assignee: Canon Kabushiki KaishaInventors: Muling Guo, Satoshi Yashiro, Hiroshi Tojo
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Publication number: 20120060748Abstract: A Czochralski (“CZ”) single-crystal growth process system continuously grows crystal boules in a chamber furnace during a single thermal cycle. Finished boules are transferred from the furnace chamber, without need to cool the furnace, to an adjoining cooling chamber for controlled cooling. Controlled cooling is preferably accomplished by transporting boules along a path having an incrementally decreasing temperature. In order to maximize crystal boule yield in a single furnace thermal cycle, the crucible assembly may be recharged with crystal growth aggregate and/or slag may be discharged during the crystal boule growth process without opening the furnace.Type: ApplicationFiled: September 9, 2010Publication date: March 15, 2012Applicant: SIEMENS MEDICAL SOLUTIONS USA, INC.Inventors: James L. Corbeil, Troy Marlar, Piotr Szupryczynski
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Patent number: 7875790Abstract: A method of preparing a thermoelectric material includes the following steps. A thermoelectric raw material can be filled into a cavity of a first mold so that the thermoelectric raw material filled in the cavity has first and second dimensions. The first dimension can be defined in a first direction. The second dimension can be defined in a second direction. The second direction can be perpendicular to the first direction. The first dimension can be equal to or greater than the second dimension. The thermoelectric raw material filled in the cavity can be cooled in a uniaxial direction that is parallel to the second direction at a cooling rate of at least 600° C./min.Type: GrantFiled: August 23, 2006Date of Patent: January 25, 2011Assignee: Yamaha CorporationInventor: Takahiro Hayashi
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Publication number: 20100288186Abstract: Techniques are generally disclosed for forming crystalline bodies. An example system, device or method for forming crystalline bodies may include a crucible for containing molten crystalline material and a support for accommodating a seed on an end thereof, the support being movable along a translation axis in a pull direction to draw the seed crystal from the molten crystalline, thereby initiating growth of a crystalline body along a growth path. Further examples may include one or more nozzles configured to be coupled to a fluid source, the nozzles being positioned relative to the growth path for shaping the crystal body as the molten crystalline is pulled in the pull direction along the growth path.Type: ApplicationFiled: May 18, 2009Publication date: November 18, 2010Inventor: Christopher A. Bang
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Patent number: 7682452Abstract: A method and apparatus for eliminating voids and improving crystal quality in shaped ceramic product, e.g. sapphire fiber or silicon sheet, from a melt by using a sloped die tip. The sloped die tip or array thereof comprises an outer sidewall which is sloped outwardly at an angle of 5° to 40° from the vertical.Type: GrantFiled: April 9, 2007Date of Patent: March 23, 2010Assignee: Sapphire Systems Inc.Inventor: John O. Outwater
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Publication number: 20100058977Abstract: A single crystal seed for use in casting a single crystal article, consisting essentially of, in weight %, about 5.0% to about 40.0% Mo, up to 0.1% C and balance essentially Ni.Type: ApplicationFiled: July 20, 2009Publication date: March 11, 2010Inventors: Steven T. Schaadt, Brad J. Murphy, Lisa K. Koivisto
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Patent number: 7507291Abstract: Methods and apparatus for concurrent growth of multiple crystalline ribbons from a single crucible employ meniscus shapers to facilitate continuous growth of discrete and substantially flat crystalline ribbons having controlled width.Type: GrantFiled: April 3, 2006Date of Patent: March 24, 2009Assignee: Evergreen Solar, Inc.Inventor: Richard Lee Wallace, Jr.
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Patent number: 7473317Abstract: A crystal growth crucible made of boron nitride includes a cylindrical tip portion for accommodating a seed crystal, and a cylindrical straight-body portion for growing a crystal, which is formed above the tip portion and has a diameter larger than that of the tip portion. Thickness T1 of the tip portion and thickness T2 of the straight-body portion satisfy a condition of 0.1 mm?T2<T1?5 mm, and inside diameter D2 and length L2 of the straight-body portion satisfy conditions of 100 mm<D2 and 2<L2/D2<5.Type: GrantFiled: March 9, 2006Date of Patent: January 6, 2009Assignee: Sumitomo Electric Industries, Ltd.Inventor: Yoshiaki Hagi
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Publication number: 20080282972Abstract: Previously a number of techniques have been used in order to form single crystal or pre-determined crystallography components and articles. Each one of these techniques has its own particular problems, including susceptibility to error. By utilisation of a bi-crystal experiment to determine melt-back length LM and by consideration of the ingress distance d from potential initiation nucleation points on a perimeter of a seed crystal, it is possible to determine a maximum ingress length d. By ensuring that the maximum ingress length d is less than or equal to a seed crystal diameter R, it is possible to project locus from potential nucleation points C1, C2 in terms of potential radii for stray grain propagation. As the seed crystal will have a known crystalline orientation, it will be possible to consider two divergent growth curves of the crystal in terms of the stray grains propagating from the point C1, C2.Type: ApplicationFiled: July 29, 2008Publication date: November 20, 2008Inventors: Neil J. D'Souza, Philip A. Jennings, Keerthi Devendra
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Publication number: 20080245292Abstract: A method and apparatus for eliminating voids and improving crystal quality in shaped ceramic product, e.g. sapphire fiber or silicon sheet, from a melt by using a sloped die tip. The sloped die tip or array thereof comprises an outer sidewall which is sloped outwardly at an angle of 5° to 40° from the vertical.Type: ApplicationFiled: April 9, 2007Publication date: October 9, 2008Inventor: John O. Outwater
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Publication number: 20080127885Abstract: A crystal growth crucible made of boron nitride includes a cylindrical tip portion for accommodating a seed crystal, and a cylindrical straight-body portion for growing a crystal, which is formed above the tip portion and has a diameter larger than that of the tip portion. Thickness T1 of the tip portion and thickness T2 of the straight-body portion satisfy a condition of 0.1 mm?T2<T1?5 mm, and inside diameter D2 and length L2 of the straight-body portion satisfy conditions of 100 mm<D2 and 2<L2/D2 <5.Type: ApplicationFiled: March 9, 2006Publication date: June 5, 2008Inventor: Yoshiaki Hagi
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Patent number: 7022180Abstract: Methods and apparatus for concurrent growth of multiple crystalline ribbons from a single crucible employ meniscus shapers to facilitate continuous growth of discrete and substantially flat crystalline ribbons having controlled width.Type: GrantFiled: September 16, 2004Date of Patent: April 4, 2006Assignee: Evergreen Solar, Inc.Inventor: Richard Lee Wallace, Jr.
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Patent number: 6896732Abstract: A raw material feeder apparatus for industrial crystal growth systems includes a hopper disposed within a vacuum chamber and adapted to hold a quantity of raw material therein. A slide is disposed adjacent to an opening of the hopper and configured to receive the raw material from the hopper thereon. The slide is selectively moved between an open feeding position and a closed non-feeding position. The slide and a door cooperatively close the opening of the hopper, or in their open state, control the flow of raw material from the hopper. A vibrator associated with the slide feeds the raw material from the slide into an outlet tube for conveyance of the raw material to the crystal growth system.Type: GrantFiled: April 23, 2004Date of Patent: May 24, 2005Inventors: Bryan Fickett, Robert Bushman
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Patent number: 6814802Abstract: Methods and apparatus for concurrent growth of multiple crystalline ribbons from a single crucible employ meniscus shapers to facilitate continuous growth of discrete and substantially flat crystalline ribbons having controlled width.Type: GrantFiled: October 30, 2002Date of Patent: November 9, 2004Assignee: Evergreen Solar, Inc.Inventor: Richard Lee Wallace, Jr.
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Patent number: 6562132Abstract: An improved mechanical arrangement controls the introduction of silicon particles into an EFG (Edge-defined Film-fed Growth) crucible/die unit for melt replenishment during a crystal growth run. A feeder unit injects silicon particles upwardly through a center hub of the crucible/die unit and the mechanical arrangement intercepts the injected particles and directs them so that they drop into the melt in a selected region of the crucible and at velocity which reduces splashing, whereby to reduce the likelihood of interruption of the growth process due to formation of a solid mass of silicon on the center hub and adjoining components. The invention also comprises use of a Faraday ring to alter the ratio of the electrical currents flowing through primary and secondary induction heating coils that heat the crucible die unit and the mechanical arrangement.Type: GrantFiled: April 4, 2001Date of Patent: May 13, 2003Assignee: ASE Americas, Inc.Inventors: Brian H. Mackintosh, Marc Ouellette
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Publication number: 20020144649Abstract: An improved mechanical arrangement controls the introduction of silicon particles into an EFG (Edge-defined Film-fed Growth) crucible/die unit for melt replenishment during a crystal growth run. A feeder unit injects silicon particles upwardly through a center hub of the crucible/die unit and the mechanical arrangement intercepts the injected particles and directs them so that they drop into the melt in a selected region of the crucible and at velocity which reduces splashing, whereby to reduce the likelihood of interruption of the growth process due to formation of a solid mass of silicon on the center hub and adjoining components. The invention also comprises use of a Faraday ring to alter the ratio of the electrical currents flowing through primary and secondary induction heating coils that heat the crucible die unit and the mechanical arrangement.Type: ApplicationFiled: April 4, 2001Publication date: October 10, 2002Applicant: ASE Americas, Inc.Inventors: Brian H. Mackintosh, Marc Ouellette
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Patent number: 6325852Abstract: A die for drawing crystals from a molten bath, has a body bored with at least one longitudinal capillary channel arranged between a lower face of the body. The die is intended to be immersed in the molten bath and an upper face of the body intended to support the liquid coming from the molten bath through the capillary channel. The die upper face has a flat surface onto which the capillary channel emerges, and this flat surface forms an angle &thgr; less than 90° with the longitudinal axis of the capillary channel.Type: GrantFiled: June 8, 2000Date of Patent: December 4, 2001Assignee: Commissariat a l'Energie AtomiqueInventors: Fred Theodore, Jean Delepine, Jean-Philippe Nabot, Vladimir Kurlov
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Patent number: 5919304Abstract: When producing an oxide-series single crystal by continuously pulling downwardly by .mu. pulling down method, the composition of the single crystal can properly and quickly controlled to continuously produce the single crystal of a constant composition by changing the pulling rate of the single crystal. Preferably, the pulling rate is 20-300 mm/hr, and the pulling rate is decreased with the proceeding of growing of the single crystal.Type: GrantFiled: August 23, 1996Date of Patent: July 6, 1999Assignee: NGK Insulators, Ltd.Inventors: Minoru Imaeda, Katsuhiro Imai, Tsuguo Fukuda
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Patent number: 5885345Abstract: A shaper (2) is arranged within a shaping vessel (1). A raw material for a crystal is inserted into the shaping vessel (1) and a crystal melt (5) is formed by setting it in a predetermined atmosphere and heating it. A mechanical force F1 is applied to the crystal melt (5), which is present on the upper surface of the shaper (2), by a pressuring member (4) from above. The crystal melt (5) has nowhere to escape but a gap (3) formed by the shaper(2), so it is injected into that gap (3) as shown by the arrow. This method of fabricating a shaped crystal is suitable for fabricating a monocrystal or multicrystal semiconductor from a material such as silicon, germanium, or bismuth telluride.Type: GrantFiled: May 21, 1997Date of Patent: March 23, 1999Assignee: Union Material Inc.Inventor: Shiro Sakuragi
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Patent number: 5558712Abstract: An apparatus for growing hollow crystalline bodies by the EFG process, comprising an EFG die having a top surface shaped for growing a hollow crystalline body having a cross-sectional configuration in the shape of a polygon having n faces, and a radiation shield adjacent to and surrounded by the top end surface of the die, characterized in that the shield has an inner edge defining a similar polygon with n sides, and the inner edge of the shield is notched so that the spacing between the n faces and the n sides is greatest between the central portions of the n faces and the n sides, whereby the greater spacing at the central portions helps to reduce lateral temperature gradients in the crystalline body that is grown by use of the die.Type: GrantFiled: November 4, 1994Date of Patent: September 24, 1996Assignee: ASE Americas, Inc.Inventor: Juris P. Kalejs
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Patent number: 5551977Abstract: An improved susceptor for a crucible/die assembly for growing tubular crystalline structures by the EFG process is provided. The crucible/die assembly comprises a die having a substantially polygonally-shaped top end surface for supporting a film of silicon feed material that is replenished from a melt in the crucible through capillary action. A hollow crystalline body is grown from the film of silicon material on the top end surface of the die. The heat susceptor is made of graphite or similar material, and has a peripheral configuration similar to that of the die. Further, the upper surface of the heat susceptor has a central land and a plurality of circumferentially-spaced upwardly extending projections.Type: GrantFiled: November 14, 1994Date of Patent: September 3, 1996Assignee: ASE Americas, Inc.Inventor: Andrew A. Menna
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Patent number: 5431124Abstract: A rutile single crystal with no grain boundaries of large inclination is obtained by an EFG crystal growth process wherein a die provided with slits is incorporated in a feed melt 2 to deliver up the melt through the slits until it reaches the upper face of the die, thereby obtaining a single crystal conforming in configuration to the die by pulling growth.Type: GrantFiled: January 18, 1994Date of Patent: July 11, 1995Assignee: Chichibu Cement Co., Ltd.Inventors: Hiroshi Machida, Tsuguo Fukuda, Keigo Hoshikawa
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Patent number: 5398640Abstract: A single crystal dome is formed from a surface of revolution and grown from a liquid material on a linear die surface wettable by the molten material. A seed crystal is supported in a position spaced from an axis of revolution which lies in the plane of the wettable surface, and the seed crystal is rotated around the axis of revolution to generate a curved surface having a predetermined radius of curvature. The seed crystal is supported in a predetermined orientation of one of its axes with respect to the wetted surface of commencement of growth.Type: GrantFiled: March 1, 1993Date of Patent: March 21, 1995Assignee: Saphikon, Inc.Inventors: John W. Locher, Joseph E. Madsen
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Patent number: 5370078Abstract: Growth of monocrystalline rods from a bulk melt is carried out by a modified Czochralski process using a float which floats on the bulk melt held in a crucible. Melt flows through a passageway in the float to a crystal growth zone at a rate which prevents diffusion of dopant from the growth zone to the bulk melt. The shape of the crystal may be determined by a shaper wall in the float which defines the growth zone, in which case the crystal body is pulled from the float as it grows without rotating the crystal. The temperature of the float near the shaper wall may be monitored and controlled to control the crystallization process.Type: GrantFiled: December 1, 1992Date of Patent: December 6, 1994Assignee: Wisconsin Alumni Research FoundationInventors: Sindo Kou, Ming-Hsien Lin