Treating With Specified Agent (e.g., Heat Exchange Agent, Protective Agent, Decarburizing Agent, Denitriding Agent, Etc.) Or Vacuum Patents (Class 148/606)
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Patent number: 11848132Abstract: One aspect of the present invention is a coil component comprising: a magnetic substrate formed with magnetic metal particles containing Fe, Si and Cr, and a bonding layer containing oxygen and nitrogen that bonds the magnetic metal particles to each other; and a conductor arranged inside or on the surface of the magnetic substrate.Type: GrantFiled: December 6, 2021Date of Patent: December 19, 2023Assignee: Taiyo Yuden Co., Ltd.Inventors: Kinshiro Takadate, Atsushi Tanada, Kengo Tsuchiya
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Patent number: 11065396Abstract: A needle cannula (100) and a method for producing a needle cannula comprising providing a needle cannula tube (10) with an end portion (30). The end portion (30) comprises an outer surface, and a given type of steel comprising carbon (C) in 0.07 to 0.15% by mass, silicon (Si) in 0.50 to 1.00% by mass, manganese (Mn) in 5.0 to 7.5% by mass, phosphorus (P) in 0 to 0.030% by mass, sulfur (S) in less than or equal to 0.015% by mass, chromium (Cr) in 17.5 to 19.5% by mass, nickel (Ni) in 6.5 to 8.5% by mass, and nitrogen (N) in 0.20 to 0.30% by mass. The method further comprises establishing an electrochemical reaction to remove material from the outer surface of the end portion (30), and thereby providing a needle cannula (100) with a tapered end portion.Type: GrantFiled: April 6, 2017Date of Patent: July 20, 2021Assignee: Novo Nordisk A/SInventors: Jacqueline Trosborg, Jens Christian Uggerhoej
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Patent number: 10480043Abstract: A seamless steel pipe for line pipe has a chemical composition consisting, by mass percent, of C: 0.03-0.15%, Si: ?0.50%, Mn: 1.0-2.0%, P: ?0.050%, S: ?0.005%, Cr: 0.1-1.0%, Al: 0.001-0.10%, N: ?0.01%, Ni: 0.05-2.0%, B: 0.0003-0.0015%, Ca: 0.0002-0.0050%, Mo: 0.10-0.50%, Ti: 0.001-0.05%, Cu: 0-2.0%, Nb: 0-0.05%, V: 0-0.10%, the balance: Fe and impurities, and satisfying the conditions of 2Nb+4V+Mo?0.50, wherein a metal micro-structure of the steel pipe contains 50% or more of bainite, in an area fraction, a wall thickness of the steel pipe is 25 mm or larger, and in a scale formed on the surface of the steel pipe, metal particles consisting mainly of Ni or Cu having an average circle-equivalent diameter of 0.1-5 mm exist. A distance from a boundary between the base metal of the steel pipe and the scale to a region in which the metal particles do not exist is 20 mm or longer.Type: GrantFiled: May 12, 2015Date of Patent: November 19, 2019Assignee: NIPPON STEEL CORPORATIONInventors: Yuji Arai, Yukimasa Ueda
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Patent number: 9359665Abstract: A swage mount is manufactured for attaching a head suspension assembly to a head actuator arm for a hard disk drive. A conductive material is deposited on a predetermined part of the swage mount. A coating material is deposited on the swage mount including the predetermined part. Heat is applied to the swage mount, forming a mixture of the conductive material and the coating material. The mixture is conductive and supports a reliable connection between the swage mount and other disk drive components. Furthermore, the mixture enhances cleanliness by reducing particles shed from the swage mount. The conductive material is preferably gold, and the coating material is preferably nickel-based.Type: GrantFiled: July 22, 2015Date of Patent: June 7, 2016Assignee: INTRI-PLEX TECHNOLOGIES, INC.Inventors: David Django Dexter, Ryan John Schmidt, Paul Wesley Smith
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Patent number: 8685257Abstract: A method for controlling microbial growth in potable water stored in a vessel having a metallic surface includes heating the metallic surface to a temperature between about 480° C. (900° F.) and about 870° C. (1600° F.), exposing the metallic surface to oxygen during heating to oxidize potential reduction sites on the metallic surface and charging potable water containing silver ions to the vessel. A vessel having a metallic surface is prepared for long-term storage of potable water containing silver ions by heating the metallic surface to a temperature between about 480° C. (900° F.) and about 870° C. (1600° F.) and exposing the metallic surface to oxygen during heating to oxidize electropositive metals on the metallic surface or by treating the metallic surface with an aqueous solution containing on oxidizing agent to oxidize potential reduction sites on the metallic surface.Type: GrantFiled: December 10, 2009Date of Patent: April 1, 2014Assignee: Hamilton Sundstrand Space Systems International, Inc.Inventors: Durwood Mace Beringer, John W. Steele, Timothy A. Nalette
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Patent number: 8663403Abstract: A precipitation-hardened stainless steel alloy comprises, by weight: about 14.0 to about 16.0 percent chromium; about 6.0 to about 8.0 percent nickel; about 1.25 to about 1.75 percent copper; greater than about 1.5 to about 2.0 percent molybdenum; about 0.001 to about 0.025 percent carbon; niobium in an amount greater than about twenty times that of carbon; and the balance iron and incidental impurities. The alloy has an aged microstructure and an ultimate tensile strength of at least about 1100 MPa and a Charpy V-notch toughness of at least about 69 J. In one embodiment, the aged microstructure includes martensite and not more than about 10% reverted austenite. In another embodiment, the alloy includes substantially all martensite and substantially no reverted austenite. The alloy is useful for making turbine airfoils.Type: GrantFiled: June 8, 2011Date of Patent: March 4, 2014Assignee: General Electric CompanyInventors: Jianqiang Chen, Thomas Michael Moors, Jon Conrad Schaeffer
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Patent number: 8339745Abstract: A cylindrical boss portion is press-formed on a baseplate of a disk drive suspension. The boss portion is penetrated by a ball insertion hole relative to the thickness of the baseplate. The baseplate is formed of stainless steel. A chemically-polished surface is formed on an inner circumferential wall of the ball insertion hole by chemically polishing the baseplate after heat-treating it. The boss portion is inserted into a mounting hole of an actuator arm. A ball having a diameter larger than the inside diameter of the ball insertion hole is passed through the ball insertion hole. As the diameter of the boss portion is enlarged by the ball, the boss portion is fixed to the actuator arm.Type: GrantFiled: April 26, 2010Date of Patent: December 25, 2012Assignees: NHK Spring Co., Ltd., Ogaki Seiko Co., Ltd.Inventors: Ryosuke Yabu, Masakazu Sugino
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Publication number: 20110265920Abstract: The present invention provides an alloy-saving type of high purity ferritic stainless steel excellent in corrosion resistance and a method of production of the same. A high purity ferritic stainless steel excellent in corrosion resistance comprised of, by mass %, C: 0.001 to 0.02%, Si: 0.01 to 0.6%, Mn: 0.01 to 0.6%, P: 0.005 to 0.04%, S: 0.0001 to 0.01%, Cr: 13 to 22%, N: 0.001 to 0.02%, Al: 0.005 to 0.05%, Sn: 0.001 to 1%, and a balance of Fe and unavoidable impurities, said steel characterized by satisfying the two relations of the following formula (1) and formula (2) where I(Fe), I(Cr), I(Sn), and I(O) are the X-ray intensities of the Fe oxides, Cr oxides, Sn oxides, and other detected oxides at the steel surface measured by an X-ray photoelectron spectrometer: 0<I(Fe)/I(Cr)<5??formula (1) and 0<I(O)/I(Sn)<3??formula (2) To improve the effect of modification of the coating by addition of Sn, the method comprises annealing at a temperature higher than 800° C.Type: ApplicationFiled: December 7, 2009Publication date: November 3, 2011Inventors: Masaharu Hatano, Akihiko Takahashi, Eiichiro Ishimaru, Shigenori Takahata
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Patent number: 7985306Abstract: A precipitation-hardened stainless steel alloy comprises, by weight: about 14.0 to about 16.0 percent chromium; about 6.0 to about 7.0 percent nickel; about 1.25 to about 1.75 percent copper; about 0.5 to about 2.0 percent molybdenum; about 0.025 to about 0.05 percent carbon; niobium in an amount greater than about twenty times to about twenty-five times that of carbon; and the balance iron and incidental impurities. The alloy has an aged microstructure and an ultimate tensile strength of at least about 1100 MPa and a Charpy V-notch toughness of at least about 69 J. The aged microstructure includes martensite and not more than about 10% reverted austenite and is useful for making turbine airfoils.Type: GrantFiled: February 4, 2009Date of Patent: July 26, 2011Assignee: General Electric CompanyInventors: Jianqiang Chen, Thomas Michael Moors, Jon Conrad Schaeffer
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Patent number: 7926180Abstract: A method for making gas and liquid storage tanks such as automotive fuel tanks includes providing two or more blanks of air hardenable martensitic stainless steel in the annealed condition. The steel blanks have a thickness in the range of 0.5-5.0 mm., and are formed utilizing stamping, forging, pressing, or roller forming techniques or the like into the form of a tank shell components. The shell components are hardened and assembled into a storage tank. The shell components are hardened by application of heat, preferably to between 950° C. and 1100° C. for standard air hardenable martensitic stainless steels. Thereafter, the automotive fuel tank is preferably cooled at a rate greater than 25° C. per minute to achieve a Rockwell C hardness of at least 39. The automotive fuel tank may undergo additional heat treating processes including high temperature or low temperature tempering processes which may incorporate electro-coating.Type: GrantFiled: October 4, 2006Date of Patent: April 19, 2011Inventors: Edward J. McCrink, Danny Codd
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Patent number: 7914630Abstract: The subject of the invention is a process for the continuous manufacture of an austenitic stainless steel strip having a dull surface appearance, consisting in subjecting an austenitic stainless steel strip to a heat treatment in a bright annealing furnace inside which an inert or reducing flushing gas circulates, which gas has a dew point above ?15° C., and then in pickling the strip using a suitable acid pickling solution.Type: GrantFiled: March 9, 2005Date of Patent: March 29, 2011Assignee: Ugine & Alz FranceInventors: Arnaud Dessis, Henri Giraud, Caroline Dhondt
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Patent number: 7879400Abstract: There is provided a substrate processing apparatus equipped with a metallic component, with at least a part of its metallic surface exposed to an inside of a processing chamber and subjected to baking treatment at a pressure less than atmospheric pressure. As a result of this baking treatment, a film which does not react with various types of reactive gases, and which can block the out diffusion of metals, is formed on the surface of the above-mentioned metallic component.Type: GrantFiled: October 10, 2007Date of Patent: February 1, 2011Assignee: Hitachi Kokusal Electric Inc.Inventors: Takahiro Maeda, Kiyohiko Maeda, Takashi Ozaki
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Patent number: 7875235Abstract: A method is described for batchwise heat treatment of goods to be annealed which are heated in a heating chamber after scavenging air with a scavenging gas under protective gas to a predetermined treatment temperature, with the protective gas being conveyed through the heating chamber depending on the occurrence of impurities in different quantities. In order to enable the economic use of protective gas, it is proposed that the protective gas which is withdrawn from the heating chamber after the main occurrence of impurities and which is loaded with a residual quantity of impurities is conveyed, optionally after intermediate storage, into the heating chamber during the main occurrence of impurities of a subsequent batch before non-loaded protective gas is introduced into the heating chamber.Type: GrantFiled: May 11, 2006Date of Patent: January 25, 2011Assignee: Ebner Industrieofenbau Gesellschaft m.b.H.Inventors: Peter Ebner, Heribert Lochner
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Publication number: 20100196799Abstract: The present invention relates to the use of the A286 alloy grade for the manufacture of a sheet, optionally surfaced, making it possible to obtain a conducting plate of mono polar or bipolar type for a fuel cell element. The invention also relates to this optional surface treatment process, which comprises a cold-rolling step followed by a continuous annealing step in an oxidizing atmosphere and by an acid pickling step.Type: ApplicationFiled: June 19, 2007Publication date: August 5, 2010Applicants: L'Air Liquide Societe Anonyme Pour L'Etude et L'Exploration DesProcedes George Claude, Arcelormittal-Stainless & Nickel Alloys, Alfa Laval Corporate ABInventors: Eric Claude, Richard Bousquet, Gilles Platen, Claude Roussel
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Patent number: 7658883Abstract: Novel carbon-plus-nitrogen corrosion-resistant ferrous and austenitic alloys, apparatus incorporating an inventive alloy, and methods of making and using the apparatus are described. The corrosion-resistant ferrous and austenitic alloys comprise no greater than about 4 wt. % nickel, are characterized by a strength greater than about 700 MPa (100 ksi), and, when being essentially free of molybdenum (<0.3 wt. %), have minimum Pitting Resistance Equivalence (PRE) numbers of 20 and minimum Measure of Alloying for Corrosion Resistance numbers (MARC) of 30 because of the use of both carbon and nitrogen. The ferrous and austenitic alloys are particularly formulated for use in oilfield operations, especially sour oil and gas wells and reservoirs. This abstract allows a searcher or other reader to quickly ascertain the subject matter of the disclosure. It will not be used to interpret or limit the scope or meaning of the claims.Type: GrantFiled: December 18, 2006Date of Patent: February 9, 2010Assignee: Schlumberger Technology CorporationInventors: Manuel Marya, Rashmi Bhavsar
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Patent number: 7485197Abstract: In a martensitic stainless steel tube according to the present invention, the content is determined by each of elements C, Si, Mn and Cr, and the bubble content ratio is further prescribed in accordance with the scale thickness on the outer surface of the steel tube, so that defects can be detected with high precision in the non-destructive inspection, such as ultrasonic test or the like. This allows the non-destructive inspection to be carried out with high efficiency. Moreover, there is another advantage that the weather resistance can be enhanced. The steel tube according to the present invention and the manufacturing method thereof can be suitably used in all of the technical fields in which a martensitic stainless steel tube having equal chemical composition is treated.Type: GrantFiled: March 31, 2006Date of Patent: February 3, 2009Assignee: Sumitomo Metal Industries, Ltd.Inventor: Mutsumi Tanida
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Patent number: 7475478Abstract: A method for making structural automotive components and the like includes providing a blank of air hardenable martensitic stainless steel in the annealed condition. The steel blank has a thickness in the range of 0.5-5.0 mm., and is formed utilizing stamping, forging, pressing, or roller forming techniques or the like into the form of an automotive structural member. The automotive structural member is then hardened by application of heat, preferably to between 950° C. and 1100° C. for standard martensitic stainless steels. Thereafter, the automotive structural member is preferably cooled at a rate greater than 25° C. per minute to achieve a Rockwell C hardness of at least 39. The automotive structural member may undergo additional heat treating processes including high temperature or low temperature tempering processes which may incorporate electro-coating.Type: GrantFiled: September 11, 2006Date of Patent: January 13, 2009Assignee: KVA, Inc.Inventors: Edward J. McCrink, Danny Codd
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Publication number: 20080236710Abstract: A method of reducing the formation of electrically resistive scale on a an article comprising a silicon-containing ferritic stainless subjected to oxidizing conditions in service includes, prior to placing the article in service, subjecting the article to conditions under which silica, which includes silicon derived from the steel, forms on a surface of the steel. Optionally, at least a portion of the silica is removed from the surface to placing the article in service. A ferritic stainless steel alloy having a reduced tendency to form silica on at least a surface thereof also is provided. The steel includes a near-surface region that has been depleted of silicon relative to a remainder of the steel.Type: ApplicationFiled: March 5, 2008Publication date: October 2, 2008Applicant: ATI Properties, Inc.Inventor: James M. Rakowski
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Patent number: 7396421Abstract: A duplex stainless steel containing C, Si, Mn, P, S, Al, Ni, Cr, Mo, N (nitrogen, O (oxygen), Ca, Mg, Cu, B, and W, and the balance Fe and impurities, where a number of oxide-based inclusions, which have a total content of Ca and Mg of 20 to 40% by mass and also have a long diameter of not less than 7 ?m, is not more than a 10 per 1 mm2 of the cross section perpendicular to the working direction, or further, the number of oxide-based inclusions, which have a content of S of not less than 15% by mass and also have a long diameter of not less than 1 ?m, is not more than 10 per 0.1 mm2 of the cross section perpendicular to the working direction. Particularly, the contents of Cu, B and W are desirably 0.2 to 2%, 0.001 to 0.01%, and 0.1 to 4% by mass, respectively.Type: GrantFiled: May 24, 2005Date of Patent: July 8, 2008Assignee: Sumitomo Metal Industries, Ltd.Inventors: Tomohiko Omura, Satoshi Matsumoto
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Publication number: 20080041504Abstract: A method for reducing surface particle shedding of a material, specifically a suspension mounting arm for a hard disk drive, made of an alloy such as 300 Series stainless steel, by thermally conditioning the mounting arm for a desirable time period sufficient to reduce residual stress in the mounting arm while substantially maintaining its original yield strength characteristics. To ensure fabrication free from oxidation and contamination, the contained heat source can be oxygen depleted by evacuating the interior of the container to a sub-atmospheric pressure or by filling the interior of with an inert gas such as argon or a reducing gas, such as hydrogen. After thermal exposure, the material is cooled to an ambient temperature. The resulting material exhibits adequate stiffness and yield strength for assembly and operation in a hard disk drive.Type: ApplicationFiled: August 16, 2006Publication date: February 21, 2008Inventors: Kevin P. Hanrahan, Ryan J. Schmidt, David D. Dexter
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Patent number: 6921443Abstract: A process for treating a stainless steel strip in an electrolytic tank produces a stainless steel with improved surface properties. The process subjects the stainless steel to a bright annealing process, followed by an electro-chemical treatment stage at current densities of up to 200 A/dm2. The electro-chemical treatment is typically in a sulfate containing electrolyte solution. The current density can range from about 20 A/dm2 to about 200 A/dm2.Type: GrantFiled: November 17, 2000Date of Patent: July 26, 2005Assignee: Andritz AGInventor: Jovan Starcevic
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Patent number: 6793746Abstract: Disclosed are stainless steel parts, particularly, parts of electronic apparatus, with which troubles caused by so-called “sulfide gas” mainly of H2S must be avoided. Release of the sulfide gas from the parts is effectively suppressed. The parts have high hardness and corrosion resistance, and can be produced with high finishing accuracy. The stainless steel parts are produced by processing a ferritic or a martensitic stainless steel of a specific alloy composition by forging and/or machining to the shape of the part followed by quenching and tempering, or quenching and tempering followed by machining to the shape of the part, and applying a solution of oxidative acid to the surface of the part so as to dissolve and remove sulfides existing on the surface of the part.Type: GrantFiled: April 30, 2002Date of Patent: September 21, 2004Assignee: Daido Steel Co., Ltd.Inventors: Tetsuya Shimizu, Michio Okabe
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Patent number: 6780257Abstract: A base plate of a stainless-steel body material formed by pressing is polished and cleared of burrs by means of an abrasive material that consists mainly of Fe2O3 in a polishing process. The polished base plate is heated to a heat treatment temperature for solid solution in a reducing atmosphere in a heat treatment process. In this heat treatment process, an oxide in the constituents of minute fragments of the abrasive material in the surface of the body material of the base plate is reduced to leave iron, which is dispersed into the body material.Type: GrantFiled: January 17, 2002Date of Patent: August 24, 2004Assignees: IBM Japan Ltd., NHK Spring Co., Ltd.Inventors: Tsuyoshi Nagata, Hiroyasu Tsuchida, Yoshio Uematsu, Kiyoshi Satoh, Kosuke Tamaru
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Patent number: 6467148Abstract: A producing method of a metal band of a metal belt for a belt-type continuously variable transmission includes the following steps of: superposing a predetermined number of blank rings concentrically on one another to constitute a laminated blank rings; fitting the laminated blank rings to an outer periphery of a circle jig made of material having higher thermal expansivity than that of the blank ring; heating the laminated blank rings together with the circle jig; and deforming the laminated blank rings plastically by thermal expansion of the circle jig.Type: GrantFiled: December 10, 1998Date of Patent: October 22, 2002Assignee: Nissan Motor Co., Ltd.Inventors: Masayuki Suzuki, Akira Maruyama
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Patent number: 6436202Abstract: Heat resistant stainless steel may be treated in a low oxidizing atmosphere in a heat/soak-heat/soak sequence to deplete its surface of Ni and Cr which tend to catalyze coking of hydrocarbons in contact with the surface of the stainless steel, and enrich it with elements which are inert to coke formation. Parts made of stainless steel, such as furnace tubes or coils, treated in accordance with the present invention when used have a significantly reduced rate of catalytic coking.Type: GrantFiled: September 12, 2000Date of Patent: August 20, 2002Assignee: Nova Chemicals (International) S.A.Inventors: Leslie Wilfred Benum, Michael C. Oballa
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Patent number: 6290790Abstract: A method for reducing the electrical resistance caused by a corrosion oxide coating at the current-carrying transition of a chromium steel component includes annealing the chromium steel component a temperature of at least 950° C. and removing any oxide coating that develops during said annealing before the component carries current.Type: GrantFiled: July 12, 2000Date of Patent: September 18, 2001Assignee: MTU Motoren- und Turbinen-Union Friedrichshafen GmbHInventors: Jörg Wind, Felix Nitschke
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Patent number: 6231698Abstract: A swage mount including a base plate having a first side and a second side. A hub extends from the first side of said base plate with the hub having an aperture therethrough. The second side of the base plate is mounted on either the actuator arm or the load beam so that the aperture of the hub is in registration with a swage opening disposed in the actuator arm or the load beam. The hub is inserted in the swage opening of the other of the actuator arm or load beam thereby forming an interference fit therebetween. The swage mount is surface hardened by gas carburizing, bead blasting or tumbling thereby increasing the torque retention value of the interference fit.Type: GrantFiled: May 19, 1998Date of Patent: May 15, 2001Inventors: Stephen Thomas Braunheim, Ernest Edward Swayney
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Patent number: 6217679Abstract: The invention provides hot-rolled steel strips which, after having been acid-pickled, can be directly used. The strips have no Cr-decreasing layer and no shot blasted marks on their surface and have good corrosion resistance. The invention also provides a technique of efficiently producing the hot-rolled steel strips. A steel slab having a Cr content of from 6.0 to 25.0 wt. % is hot-rolled, then coiled at a temperature not higher than 700° C., then optionally quenched in water immediately after the coiling, then annealing in a reducing atmosphere, and thereafter acid-pickled in a solution of nitric acid/hydrochloric acid.Type: GrantFiled: November 23, 1998Date of Patent: April 17, 2001Assignee: Kawasaki Steel CorporationInventors: Masaaki Kohno, Kunio Fukuda, Kazuhide Ishii, Susumu Satoh, Hiroshi Yaginuma, Takumi Ujiro
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Patent number: 6156440Abstract: A treated stainless steel is used as the material of construction for parts of an apparatus exposed to an organic amine. The stainless steel is treated by cleaning the stainless steel, forming a colored oxide film on the surface of the cleaned stainless steel by heating the cleaned stainless steel in an oxidizing atmosphere, and removing a portion of the colored oxide film to expose a passivating oxide film.Type: GrantFiled: July 7, 1997Date of Patent: December 5, 2000Assignee: Shinko Pantec Co., Ltd.Inventors: Takeshi Suwa, Mitsuru Shinkoda
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Patent number: 5976282Abstract: An austenite stainless steel plate having both excellent surface brightness and superior corrosion resistance, without polishing after finish annealing and pickling for descaling of the strip. The steel plate contains Si 0.02 to 0.2 wt % together with Si oxides at 1.0 wt % or less in the surface layer part in the 10 .mu.m depth from the surface. The depth of the intergranular groove in the surface layer part is 0.1 .mu.m or more to 0.5 .mu.m or less. Furthermore, the steel plate contains Al of 0.005 wt % or less and 0 of 0.006 wt % or less. The Al oxides are contained at 0.1 wt % or less in the surface layer part in the 10 .mu.m depth from the surface.Type: GrantFiled: September 18, 1998Date of Patent: November 2, 1999Assignee: Kawasaki Steel CorporationInventors: Kunio Fukuda, Yoshikazu Kawabata, Kazuhide Ishii, Susumu Sato
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Patent number: 5830291Abstract: A method for producing bright stainless steel whereby a hot mill band having a dull oxide-free surface is first formed. The hot mill band is cold reduced to form a full hard coil having a shiny surface. The coil is subjected to continuous annealing at a temperature of 1500.degree.-1950.degree. F. in an oxygen-containing atmosphere sufficient to form a protective FeCr.sub.2 O.sub.3 scale. The annealed coil is subjected to a mild non-etching pickling process to remove the black scale. The coil is then rolled on a temper mill having specially finished rolls to impart a surface pattern that replicates an abrasively polished surface.Type: GrantFiled: October 8, 1996Date of Patent: November 3, 1998Assignee: J&L Specialty Steel, Inc.Inventors: Michael F. McGuire, Kelley L. Senzarin-Kulik, Anthony J. Denoi
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Patent number: 5814166Abstract: A continuous process for heat treating and cleaning and tempering martensitic stainless steel surgical needles is disclosed. The method comprises exposing the surgical needles to a partial vacuum at a temperature less than the heat treating temperature to remove volatile surface contaminant. Then the needles are heat treated in an argon gas environment at a pressure equal to or greater than 1.0 Torr. Next the temperature of the oven is lowered to temper the needles.Type: GrantFiled: November 14, 1996Date of Patent: September 29, 1998Assignee: Ethicon, Inc.Inventors: Douglas Warren Ackerman, Timothy Sardelis, William McJames
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Patent number: 5783000Abstract: A method for heat-treating steel, primarily strip-like or rod-like steel material, such as steel strip, steel sheet, steel rod or steel wire which have been rolled and heated in an oven or furnace to a surface temperature above about 900 degrees C. and thereafter cooled and optionally treated in an electrolyte bath and/or acid bath. The oven burners are fired with a liquid or a gaseous fuel which is burned with the aid of a gas that contains at least 85 percent by volume oxygen and at most 10 percent by volume nitrogen.Type: GrantFiled: September 6, 1996Date of Patent: July 21, 1998Assignees: AGA Aktiebolag, Avesta Sheffield AktiebolagInventors: Carl-Lennart Axelsson, Sten Ljungars, Lars Folke Saltin, Sven-Eric Lunner, Sten-.ANG.ke Brannvall
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Patent number: 5626689Abstract: This invention relates to a catalytic fuel composition capable of reducing pollutants in the combustion gasses generated upon combustion of the same. A catalytic material is combined with a liquid, petroleum-based fuel, mixed and solid particles are separated out to give the catalytic fuel product. The catalytic material predominantly comprises a plagioclase feldspar belonging mainly to the albiteanorthite series, and contains small amount of mica, kaolinite and serpentine, and optionally contains magnetite. An alloy material is also disclosed, comprising a mixture of the above-described catalytic material and a metal. The alloy material exhibits unique properties relative to the metal component alone, such as increased tensile strength, improved heat resistance, improved acid resistance, improved corrosion resistance, as well as exhibiting unusual conductive properties.Type: GrantFiled: September 29, 1995Date of Patent: May 6, 1997Inventor: Jack H. Taylor, Jr.
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Patent number: 5614039Abstract: Method for heat treating a metal in which argon gas is selectively injected into the cooling zone of a heat treating apparatus when the temperature therein is above the level at which significant nitriding will occur.Type: GrantFiled: September 29, 1995Date of Patent: March 25, 1997Assignee: The BOC Group, Inc.Inventors: Harbhajan S. Nayar, John J. Dwyer, Jr., Neeraj Saxena
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Patent number: 5605587Abstract: Martensitic steel components of apparatus for magnetic conditioning of liquids which are subjected to cathodic reaction and degradation are treated prior to use to form a barrier of iron-chromium oxide and a uniform level of hardness throughout by heating the steel to a temperature near the grain boundary temperature of the steel, maintaining that temperature for a specified period and then rapidly quenching the steel.Type: GrantFiled: April 7, 1995Date of Patent: February 25, 1997Assignee: Hydrodynamics CorporationInventor: John H. Meckling
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Patent number: 5591277Abstract: A method for thermally conditioning a disc drive swage mount to enhance torque retention capability and plate stiffness wherein the swage mount is baked in an oxygen depleted environment to an elevated temperature within a predetermined range of temperatures which activates inherent frictional properties therein and controllably cooled non-linearly through a series of thermal cycles then instantaneously quenched to alter the material grain structure forming the swage mount. After the component is quenched, it is returned to ambient conditions for assembly into such disc drives.Type: GrantFiled: June 28, 1995Date of Patent: January 7, 1997Assignee: Intri-Plex Technologies, Inc.Inventor: Stephen T. Braunheim
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Patent number: 5575867Abstract: A method of preventing corrosion damage at weld joints, in the heat affected zones of weld joints, and in heat-treated zones of components made of stainless steels having chromium contents .gtoreq.12% by weight, which comprises exposing weld joints and the heat affected zones of the weld joints, or the heat-treated zones, to a water vapor atmosphere at temperatures of 100.degree. to 250.degree. C. for five to sixty minutes.Type: GrantFiled: August 17, 1995Date of Patent: November 19, 1996Assignee: Bayer AktiengesellschaftInventor: Michael Renner
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Patent number: 5557704Abstract: A kettle which includes a vessel that provides a chamber for holding water, a pouring spout for dispensing water from the chamber, and a handle for lifting and tilting the vessel during pouring, also includes an electric heating element in the form of a conductive track of a thick film printed circuit on a metal substrate that forms a heated portion of the vessel, the electric heating element being located externally of the chamber.Type: GrantFiled: December 2, 1994Date of Patent: September 17, 1996Assignee: Pifco LimitedInventors: Michael E. Dennis, David Huddart
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Patent number: 5505786Abstract: A system for descaling a strip of metal includes a nozzle assembly mounted within a spray box for spraying descaling product on the strip. The nozzle assembly includes a spray chamber; nozzles mounted directly to the spray chamber; and a heater for heating the chamber, the descaling product in the chamber, and the nozzles by conduction through the chamber. The nozzles are oriented to direct the descaling product in a spray against the upper and lower surfaces of the metal strip for an amount and a time sufficient to descale the metal strip. The nozzle assembly is attached to the spray box and can be easily removed therefrom for inspection.Type: GrantFiled: October 31, 1994Date of Patent: April 9, 1996Assignee: Kolene CorporationInventors: John M. Cole, Charles M. Bessey
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Patent number: 5476554Abstract: Fe--Cr--Al alloy foil having high oxidation resistance for a substrate catalytic converter. The alloy foil contains about: C: 0.02 wt. % or less, N: 0.02 wt. % or less, Si: 1.0 wt. % or less, Mn: 1.0 wt. % or less, Cr: from 15 to 26 wt. %, Al: from 4.5 to 8.0 wt. %, Sm: from 0.05 to 0.30 wt. %, Zr: from 0.01 to 0.10 wt. %, and Hf: 0.005 wt. % to 0.10 wt. %, the balance consisting of Fe and incidental impurities.Type: GrantFiled: May 20, 1994Date of Patent: December 19, 1995Assignee: Kawasaki Steel CorporationInventors: Kazuhide Ishii, Masaaki Kohno
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Patent number: 5411613Abstract: Surgical needles are produced from martensitic precipitation-hardening stainless steel and then vacuum heat treated and vacuum cooled to increase its tensile strength while retaining the polished surface of the needle. A needle made by this process is also disclosed.Type: GrantFiled: October 5, 1993Date of Patent: May 2, 1995Assignee: United States Surgical CorporationInventors: Said Rizk, William O. Powers, W. Scott Samsel
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Patent number: 5407492Abstract: A process for a passivated film which is far reduced in the amount of gas discharge and can desorb an adsorbed gas more readily, which process comprises heating a stainless member with a surface roughness, Rmax, of 1.0 .mu.m or less in an atmosphere of a mixture comprising oxygen gas and an inert gas and having a dew point of -95.degree. C. or below, an impurity concentration of 10 ppb or less and an oxygen content 5 ppm 25 vol % at 300.degree. to 420.degree. C.Type: GrantFiled: June 23, 1993Date of Patent: April 18, 1995Assignee: Osaka Sanso Kogyo Ltd.Inventors: Tadahiro Ohmi, Yoshiyuki Nakahara, Takashi Sakanaka, Eiji Ohta, Satoshi Mizokami
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Patent number: 5380378Abstract: Method and apparatus is disclosed for heat treating coiled, metal strip in bell shaped annealing furnaces employing an annealing stand upon which coils of strip are vertically stacked. An inner cover removably sealed to the stand surrounds the coil and an outer cover surrounds the inner cover. A vacuum is drawn within the inner cover while the work is being preheated to volatize oil on the coil into hydrocarbon vapors and permit the hydrocarbons to be drawn off prior to annealing so that carbon soot formation does not occur. A unique concentric, two seal arrangement is disclosed which provides for drawing a vacuum between the seals to positively seal the inner cover to the base while providing a fail safe mechanism for monitoring the process thus permitting a potentially explosive reducing atmosphere, such as pure hydrogen, to be used in the annealing furnace in a safe manner.Type: GrantFiled: April 23, 1993Date of Patent: January 10, 1995Assignee: Gas Research InstituteInventor: Klaus H. Hemsath
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Patent number: 5306354Abstract: A blackening treating furnace includes a soot generation burner for blowing an incomplete combustion flame toward a surface of a cold-rolled stainless steel strip moving continuously through the furnace. A pair of secondary air nozzles installed at positions enclosing the incomplete combustion flame blow secondary air toward the surface of the stainless steel strip in directions perpendicular thereto or in directions slightly inclined toward the middle of the incomplete combustion flame. A flame guide air nozzle is installed between the pair of secondary air nozzles and an exhaust duct for drawing and discharging the combustion reaction flame of the incomplete combustion flame and secondary air along the direction of movement of the stainless steel strip. The flame guide air nozzle injects flame guide air toward the combustion reaction flame in a direction perpendicular to the direction of movement of the stainless steel strip or in a direction inclined thereto.Type: GrantFiled: June 23, 1992Date of Patent: April 26, 1994Assignees: Nisshin Steel Co., Ltd., Chugai Ro Co., Ltd.Inventor: Takakatsu Adachi
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Patent number: 5288347Abstract: A high strength, high toughness stainless steel consisting, by weight, of C more than 0.16% but less than 0.25%, Si not more than 2.0%, Mn not more than 1.0%, Ni not more than 2.0%, Cr from 11 to 15%, Mo not less than 0.5% but less than 3.0%, Co from 12 to 21%, at least one kind selected from the group consisting of V from 0.1 to 0.5% and Nb less than 0.1% which at least one kind is added as occasion demands, and the balance Fe and incidental impurities. This steel is produced by a method comprising the steps of: preparing a stainless steel having the composition of any one of the claims 1 to 4; subjecting the stainless steel to a solution heat treatment at a temperature of 950.degree. to 1150.degree. C.; quenching the steel; subjecting the steel to a sub zero treatment at a temperature of -50 to -100.degree. C.; and subjecting the steel to a tempering at a temperature of 120.degree. to 450.degree. C.Type: GrantFiled: June 4, 1992Date of Patent: February 22, 1994Assignees: Hitachi Metals, Ltd., Society of Japanese Aerospace Companies, Inc., Sumitomo Precision Products Co., Ltd.Inventors: Toshihiro Uehara, Rikizo Watanabe, Nobuhito Nakama
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Patent number: 5259935Abstract: The present invention provides a method for surface passivating stainless steel articles against the effects of corrosive materials having activities anywhere from aqueous salt solutions to corrosive gases such as hydrogen chloride and silane. Additionally, after the treatment and exposure of the article to moisture, when the article is subsequently flushed with a dry gaseous fluid, the time that the article takes to exhibit an acceptable moisture outgassing rate is reduced over an untreated article. In accordance with the present invention, the surface to be passivated is flushed with a dry gaseous fluid, chemically non-reactive with the stainless steel and containing essentially no oxygen. During such flushing, the articles is baked and cooled. The baking is accomplished at a predetermined temperature and time (preferably between about 250.0.degree. C. and about 500.0.degree. C. for about 4.Type: GrantFiled: April 29, 1992Date of Patent: November 9, 1993Assignee: The BOC Group, Inc.Inventors: Jeffrey Davidson, Robert Sherman, Richard Paciej, Takashi Sakanaka, Shigeki Hayashi, Yoshiyuki Nakahara
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Patent number: 5226984Abstract: Fe-Cr-Ni-Al ferritic alloy capable of forming hot oxidation/corrosion resistive aluminum oxide scale in the surface thereof by exposure to oxidation environments at elevated temperatures. Due to the ferritic structure, the aluminum oxide scale is formed uniformly and densely to improve scale adherence, or prevent scale flaking. The mechanical properties of the ferritic alloy is considerably improved by incorporation of controlled amounts of Cr, Ni, and Al relative to each other, which are added to precipitate minute Ni-Al intermetallic compounds in the alloy matrix while retaining the ferritic structure. Such minute Ni-Al intermetallic compounds are thought to be responsible for improved mechanical properties, including high temperature strength, tensile strength, hardness and the like. Whereby, the alloy combine excellent hot oxidation/corrosion resistance and improved mechanical properties.Type: GrantFiled: January 8, 1992Date of Patent: July 13, 1993Assignee: Matsushita Electric Works, Ltd.Inventors: Tadashi Hamada, Shuji Yamada, Eiji Tsuji, Tomoyuki Mizukoshi
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Patent number: 5188681Abstract: A process for manufacturing a thin sheet of a Cr-Ni-base stainless steel having an excellent surface quality and material quality, which comprises casting a cast strip having a thickness of 6 mm or less from a Cr-Ni-base stainless steel including 18% Cr-8% Ni steel by a continuous casting wherein a casting mold is moved synchronously with the cast strip, and subjecting the cast strip to cold rolling to form a thin sheet product, wherein the cast strip immediately after the casting is coiled at a temperature of 800.degree. to 1200.degree. C. and subjected to cold rolling and final annealing to form a thin sheet product.Type: GrantFiled: September 12, 1991Date of Patent: February 23, 1993Assignee: Nippon Steel CorporationInventors: Shinichi Teraoka, Masanori Ueda, Toshiyuki Suehiro
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Patent number: 5167735Abstract: For the annealing of steel in continuously operating units, the formation of so-called white dust is almost completely eliminated by subjecting the steel to a deoxidizing pretreatment before the annealing sequence so as to at least largely remove the oxygen adsorbed on the surface of the steel, as well as any oxygen compounds also present on the surface.Type: GrantFiled: March 28, 1991Date of Patent: December 1, 1992Assignee: Linde AktiengesellschaftInventor: Alexander Jurmann