Abstract: A method of pressure sintering an environmental barrier coating on a surface of a ceramic substrate to form an article is provided. The method includes the steps of etching the surface of the ceramic substrate to texture the surface, disposing an environmental barrier coating on the etched surface of the ceramic substrate. The environmental barrier coating includes a rare earth silicate, and pressure sintering the environmental barrier coating on the etched surface of the ceramic substrate in an inert or nitrogen atmosphere such that at least a portion of the environmental barrier coating is disposed in the texture of the surface of the ceramic substrate thereby forming the article.

Abstract: A method for manufacturing a part made of composite material in which an adhesion promoter is grafted to a coating present on the fibre surface as well as to a ceramic precursor resin. Afterwards, a ceramic matrix phase is formed in the porosity of the fibre preform by pyrolysis of the polymerised resin.

Abstract: A turbine component includes a root and an airfoil extending from the root to a tip opposite the root. The airfoil forms a leading edge and a trailing edge portion extending to a trailing edge. Radial cooling channels in the trailing edge portion of the airfoil permit radial flow of a cooling fluid through the trailing edge portion. Each radial cooling channel has a first end at a lower surface at a root edge of the trailing edge portion or at an upper surface at a tip edge of the trailing edge portion and a second end opposite the first end at the lower surface or the upper surface. A method of making a turbine component and a method of cooling a turbine component are also disclosed.

Abstract: A method of assembling a first part to a second part while applying thermal energy to at least one of the parts. The application of thermal energy is terminated when the first part and second part are in a completed assembly position relative to each other. The thermal energy absorbed by the at least one of: the first part; and the second part is then dissipated until the first part and second part are engaged in an interference fit.

Abstract: A gas turbine engine composite vane assembly and method for making same are disclosed. The method includes providing at least two gas turbine engine airfoil composite preform components. The airfoil composite preform components are interlocked with a first locking component so that mating faces of the airfoil composite preform components face each other. A filler material is inserted between the mating surfaces of the airfoil composite preform components.

Abstract: A method of forming a composite component. The method includes laying up a plurality of composite plies to form a composite ply core. Another step of the method includes partially processing the composite ply core to form a green state core. The method further includes machining a cooling cavity on an exterior surface of the green state core. Additionally, the method includes inserting a filler material within the cooling cavity. A further step includes wrapping composite plies around the green state core and filler material to secure the filler material and form an outer enclosure. In one step, the method includes processing the green state core and outer enclosure to form the composite component.

Abstract: A component for a gas turbine engine including a core and an outer enclosure. The core includes an exterior surface extending along a length between a first end and a second end and at least partially defines a cooling cavity on the exterior surface extending from the first end along at least a portion of the length. The cooling cavity is fluidly coupled to an air supply at the first end. The outer enclosure includes an outer surface. The outer enclosure is positioned outside the core and extends from the first end of the core along at least a portion of the length of the core and at least partially defines the cooling cavity.

Abstract: The present invention provides a ceramic laminate having excellent mechanical properties, heat dissipation property, insulating property, heat resistance and anti-reactivity, and particularly an insulative heat dissipating body having an excellent thermal cycle reliability and a high withstand voltage. The ceramic laminate 1 according to the present invention is a ceramic laminate in which a ceramic film 3 is formed on a metal layer 2, wherein the ceramic film 3 has a minimum film thickness of 1 ?m or more, contains silicon nitride and inevitable impurities, and has silicon nitride crystal grains having an average grain size of 300 nm or less in the film thickness direction and an average grain size of 500 nm or less in the in-plane direction.

Abstract: A protective and abradable coating composition is suitable for application on rolls and more particularly for application on conveyor rolls. The abradable coating is suitable for use in high temperature applications. Rolls incorporating the coating may be produced and used according to disclosed processes and procedures. Application of the composition to rolls reduces corrosion by aluminium melt, and enables the removal of built-up substances by friction. The life time of the roll is thereby increased.

Abstract: Provided is a heat storage including a container including a first container made of ceramics and a second container made of ceramics, the first container and the second container being combined, and a heat storage material housed inside the container. The first container and the second container are bonded via a bonding member. A volume occupied by pores in the first container, in a first contact region including a surface section in contact with the bonding member, is greater than a volume occupied by pores in regions other than the first contact region. A volume occupied by pores in the second container, in a second contact region including a surface section in contact with the bonding member, is greater than a volume occupied by pores in regions other than the second contact region.

Abstract: A method of forming a ceramic matrix composite component is provided. The method includes applying a first amount of adhesive across a surface of a release film, providing a first ceramic foam panel including a plurality of channels formed on a first side of the first ceramic foam panel, contacting the first ceramic foam panel and the release film such that adhesive transfers to the first side of the first ceramic foam panel, and coupling the first ceramic foam panel to a second ceramic foam panel.

Abstract: A method of forming a component for use in a gas turbine engine includes the steps of forming an airfoil/root assembly; creating a platform assembly structure having an opening; inserting the airfoil/root assembly into the opening; and bonding the platform assembly structure to the airfoil/root assembly to form the component.

Abstract: An improved method of preparing ceramic matrix composites includes blending one or more ceramic powders with one or more paraffinic binders to form a slurry; introducing a ceramic fiber preform into a die or mold; heating the slurry to a temperature above the melting point of the one or more paraffinic binders to form a heated slurry; introducing the heated slurry into the die or mold, the heated slurry infiltrating the ceramic fiber preform to form a slurry infiltrated preform; cooling the die or mold below the solidification temperature of the paraffinic binder, thereby forming a solid component from the slurry infiltrated preform; removing the solid component from the die or mold; heating the solid component to a temperature whereby the paraffinic binder is removed; and densifying the solid component after removing the paraffinic binder, thereby forming the ceramic matrix composite.

Abstract: A method of forming an improved sealed joint between two or more shaped ceramic structures includes providing at least first and second ceramic structures joined together by a joint comprising one or more of silicon, a silicon alloy and a silicon compound, the joint including an exposed portion interior of the joined structures, then converting at least a portion of the one or more of silicon, a silicon alloy, and a silicon compound of the joint to silicon nitride and/or silicon carbide, desirably at least at an interior exposed portion of the joint, so as to provide increased chemical resistance for the joint when aggressive chemicals are used within device formed from the sealed-together ceramic structures. The ceramic structures desirably comprise silicon carbide.

Abstract: A composite article includes a substrate and a powder-derived composite coating on the substrate. The composite coating includes discrete regions of a first material and discrete regions of a second material. At least one of the first material or the second material is a chemical precursor.

Abstract: A coating of atactic polypropylene over a transparent armor substrate improves resistance to penetration while allowing convenient repair of minor abrasions and scratches.

Abstract: A bonded, boron carbide-containing ceramic body includes ceramic members. These ceramic members each contain boron carbide at 2 mass % or higher, and are integrated together via a bonding layer bonded with a bonding material containing at least one metal selected from the group consisting of aluminum, copper, gold and zirconium or integrated together via a bonding layer formed from one of aluminum metal and an aluminum compound and a titanium compound as bonding materials, wherein a bonded part has a strength of 100 MPa or higher. According to this technology, the boron carbide-containing ceramic members can be bonded together with a high strength of 100 MPa or more by a simple process, and further, the bonding is feasible with excellent chemical resistance at the bonded part as needed.

Abstract: A turbine engine turbine blade of ceramic matrix composite. The root of the blade includes a single densified fiber preform including at least one recess made by machining, each point of the root of the blade being situated at a distance from a free surface of the root that is no greater than twice the maximum penetration distance into the preform of densification gas for densifying the preform, and the distal portion of the root of the blade includes a distal wall that is continuous and in a single piece.

Abstract: A method of providing an end-capped tubular ceramic composite for containing nuclear fuel (34) in a nuclear reactor involves the steps of providing a tubular ceramic composite (40), providing at least one end plug (14, 46, 48), applying (42) the at least one end plug material to the ends of the tubular ceramic composite, applying electrodes to the end plug and tubular ceramic composite and applying current in a plasma sintering means (10, 50) to provide a hermetically sealed tube (52). The invention also provides a sealed tube made by this method.

Abstract: A method for making a treated super-hard structure, the method including providing a super-hard structure comprising super-hard material selected from polycrystalline cubic boron nitride (PCBN) material or thermally stable polycrystalline diamond (PCD) material; subjecting the super-hard structure to heat treatment at a treatment temperature of greater than 700 degrees centigrade at a treatment pressure at which the super-hard material is not thermodynamically stable, for a treatment period of at least about 5 minutes to produce the treated super-hard structure.

Abstract: The invention relates to a method for the manufacture of double-sided metallized ceramic substrates according to the direct-bonding process. The method enables a ceramic substrate to be bonded to a metal plate or foil on the upper side and the underside in only one process sequence. The composite to be bonded is located on a specially designed carrier structured on the upper side with a plurality of contact points. After the bonding process the composite of metal plates and ceramic substrate can be detached from the carrier free of any residue.

Abstract: Disclosed herein is a method of manufacturing inorganic hollow yarns, such as cermets, oxide-non oxide composites, poorly sinterable non-oxides, and the like, at low costs. The method includes preparing a composition comprising a self-propagating high temperature reactant, a polymer and a dispersant, wet-spinning the composition through a spinneret to form wet-spun yarns, washing and drying the wet-spun yarns to form polymer-self propagating high temperature reactant hollow yarns, and heat-treating the polymer-self propagating high temperature reactant hollow yarns to remove a polymeric component from the polymer-self propagating high temperature reactant hollow yarns while inducing self-propagating high temperature reaction of the self-propagating high temperature reactant to form inorganic hollow yarns. The composition comprises 45˜60 wt % of the self-propagating high temperature reactant, 6˜17 wt % of the polymer, 0.1˜4 wt % of the dispersant, and the balance of an organic solvent.

Abstract: A method for making a treated super-hard structure, the method including providing a super-hard structure comprising super-hard material selected from polycrystalline cubic boron nitride (PCBN) material or thermally stable polycrystalline diamond (PCD) material; subjecting the super-hard structure to heat treatment at a treatment temperature of greater than 700 degrees centigrade at a treatment pressure at which the super-hard material is not thermodynamically stable, for a treatment period of at least about 5 minutes to produce the treated super-hard structure.

Abstract: Disclosed herein is a method of manufacturing inorganic hollow yarns, such as cermets, oxide-non oxide composites, poorly sinterable non-oxides, and the like, at low costs. The method includes preparing a composition comprising a self-propagating high temperature reactant, a polymer and a dispersant, wet-spinning the composition through a spinneret to form wet-spun yarns, washing and drying the wet-spun yarns to form polymer-self propagating high temperature reactant hollow yarns, and heat-treating the polymer-self propagating high temperature reactant hollow yarns to remove a polymeric component from the polymer-self propagating high temperature reactant hollow yarns while inducing self-propagating high temperature reaction of the self-propagating high temperature reactant to form inorganic hollow yarns. The composition comprises 45˜60 wt % of the self-propagating high temperature reactant, 6˜17 wt % of the polymer, 0.1˜4 wt % of the dispersant, and the balance of an organic solvent.

Abstract: A bonding agent is provided which includes a flux containing either calcium aluminate or calcium oxide and aluminum oxide and aluminum nitride powder.

Abstract: In the case of a metal-ceramic substrate with a multilayered ceramic material in sheet form, and with at least one metallization that is provided on one surface side of the ceramic material and is joined to be ceramic material by direct bonding or active soldering, the ceramic material has at least one inner layer or base layer of a silicon nitride ceramic. The surface side of the ceramic material that is provided with the at least one metallization is formed by an intermediate layer of an oxidic ceramic applied to the base layer.

Abstract: A method of manufacturing a ceramic matrix composite article comprising the steps of: — a) forming a slurry consisting of water, polyvinyl alcohol, nitric acid, polyethylene glycol and alumina particles only, b) providing a length of fabric, the fabric comprising a plurality of ceramic fibres, c) applying slurry to at least one of the sides of the length of fabric such that the slurry adheres and impregnates the length of fabric, d) drying the slurry impregnated length of fabric, e) cutting the slurry impregnated length of fabric into a plurality of pieces of slurry impregnated laminates of fabric, f) applying water to each of the pieces of slurry impregnated laminates of fabric to reactivate the slurry, g) stacking the plurality of pieces of slurry impregnated laminates of fabric on a first mould part, h) consolidating the plurality of pieces of slurry impregnated laminates of fabric on the mould part, and i) sintering the stack of the plurality of pieces of slurry impregnated laminates of fabric to form an

Abstract: The invention relates to a slip for producing a durable, firmly adhering release layer on a substrate, comprising a suspension of solid particles, wherein the solid particles comprise 67-95% by weight of silicon nitride and 5-33% by weight of an SiO2-based high-temperature binder and the SiO2-based high-temperature binder is derived from SiO2 precursors and has been pretreated by heat treatment in a temperature range of 300-1300° C. The invention further provides shaped bodies comprising a substrate having a durable, firmly adhering release layer and also processes for producing them. The shaped bodies of the invention are suitable for use in the field of corrosive nonferrous metal melts.

Abstract: A ceramic matrix composite structure has a reinforced core for carrying loads. The core includes a web connected between the facesheets by edge bonded joints for transmitting compressive, tensile and shear loads. The edge bonded joints are laterally reinforced by bridging members bonded to the facesheets, on opposite sides of the webs The bridging members may comprise low density, high temperature rigid foam.

Abstract: The invention relates to a method for the manufacture of double-sided metallized ceramic substrates according to the direct-bonding process. The method enables a ceramic substrate to be bonded to a metal plate or foil on the upper side and the underside in only one process sequence. The composite to be bonded is located on a specially designed carrier structured on the upper side with a plurality of contact points. After the bonding process the composite of metal plates and ceramic substrate can be detached from the carrier free of any residue.

Abstract: A method of manufacturing a ceramic matrix composite article comprising the steps of: — a) forming a slurry consisting of water, polyvinyl alcohol, nitric acid, polyethylene glycol and alumina particles only, b) providing a length of fabric, the fabric comprising a plurality of ceramic fibres, c) applying slurry to at least one of the sides of the length of fabric such that the slurry adheres and impregnates the length of fabric, d) drying the slurry impregnated length of fabric, e) cutting the slurry impregnated length of fabric into a plurality of pieces of slurry impregnated laminates of fabric, f) applying water to each of the pieces of slurry impregnated laminates of fabric to reactivate the slurry, g) stacking the plurality of pieces of slurry impregnated laminates of fabric on a first mould part, h) consolidating the plurality of pieces of slurry impregnated laminates of fabric on the mould part, and i) sintering the stack of the plurality of pieces of slurry impregnated laminates of fabric to form an

Abstract: In the case of a metal-ceramic substrate with a multilayered ceramic material in sheet form, and with at least one metallization that is provided on one surface side of the ceramic material and is joined to be ceramic material by direct bonding or active soldering, the ceramic material has at least one inner layer or base layer of a silicon nitride ceramic. The surface side of the ceramic material that is provided with the at least one metallization is formed by an intermediate layer of an oxidic ceramic applied to the base layer.

Abstract: A method for producing a high temperature-resistant article comprises an assembling step of foaming an assembly of a first substrate and a second substrate with an adhesive layer interposed therebetween and comprising paste of powder of at least one carbide of niobium carbide, hafnium carbide, tantalum carbide and tungsten carbide; and a bonding step of heating the assembly to bond the first substrate and the second substrate by sintering, thereby obtaining a high temperature-resistant article comprising the assembly after sintering.

Abstract: In a method for the material bonding of two metallic components (11a and 11b), a joining adjuvant (19) is applied to corresponding joining surfaces (12a, 12b), wherein the adjuvant has precursors for a ceramic. After joining the components, a heat treatment step is conducted, transforming the precursors of the ceramic into an intermediate layer, which firmly adheres to both of the joining areas (12a, 12b), thus creating a comparatively strong composite bond, particularly also between different types of metals. Other additives in the form of particles may advantageously be introduced into the joining adjuvant (19), allowing for an adaptation to the requirement profile.

Abstract: A process for producing integrated bodies from an aluminum nitride sintered body and a high-melting point metal member includes the steps of: (I) forming an aluminum nitride porous layer on a planned joint surface of the aluminum nitride sintered body; and (II) causing a mixture paste including aluminum nitride and a high-melting point metal to be present between the aluminum nitride porous layer and a planned joint surface of the high-melting point metal member while impregnating the porous layer with the mixture paste, and sintering the aluminum nitride and high-melting point metal in the mixture paste.

Abstract: A precursor of a ceramic adhesive suitable for use in a vacuum, thermal, and microgravity environment. The precursor of the ceramic adhesive includes a silicon-based, preceramic polymer and at least one ceramic powder selected from the group consisting of aluminum oxide, aluminum nitride, boron carbide, boron oxide, boron nitride, hafnium boride, hafnium carbide, hafnium oxide, lithium aluminate, molybdenum silicide, niobium carbide, niobium nitride, silicon boride, silicon carbide, silicon oxide, silicon nitride, tin oxide, tantalum boride, tantalum carbide, tantalum oxide, tantalum nitride, titanium boride, titanium carbide, titanium oxide, titanium nitride, yttrium oxide, zirconium, diboride, zirconium carbide, zirconium oxide, and zirconium silicate. Methods of forming the ceramic adhesive and of repairing a substrate in a vacuum and microgravity environment are also disclosed, as is a substrate repaired with the ceramic adhesive.

Abstract: A bonding agent is provided which includes a flux containing either calcium aluminate or calcium oxide and aluminum oxide and aluminum nitride powder.

Abstract: [Problem] It is an object to provide a joining method that enables to join aluminum nitride sinters together efficiently and tightly. [Means for solution] A method of joining an aluminum nitride sinter includes placing an inclusion including a sintering aid between a surface to be joined of one aluminum nitride sinter and a surface to be joined of the other aluminum nitride sinter, and heating the inclusion by electromagnetic wave irradiation, thereby joining the aluminum nitride sinters together.

Abstract: The invention relates to a slip for producing a durable, firmly adhering release layer on a substrate, comprising a suspension of solid particles, wherein the solid particles comprise 67-95% by weight of silicon nitride and 5-33% by weight of an SiO2-based high-temperature binder and the SiO2-based high-temperature binder is derived from SiO2 precursors and has been pretreated by heat treatment in a temperature range of 300-1300° C. The invention further provides shaped bodies comprising a substrate having a durable, firmly adhering release layer and also processes for producing them. The shaped bodies of the invention are suitable for use in the field of corrosive nonferrous metal melts.

Abstract: An aluminum nitride joined body comprising two pieces of aluminum nitride sintered body plates joined together without using adhesive, and a metal layer formed on a portion of the junction interface thereof, wherein, as viewed on a side section passing through the center of the joined body, a plurality of voids are existing in the directly joined region where the sintered body plates are directly facing each other on the junction interface, the voids having an average length L of 0.5 to 4 ?m along the junction interface, thereby forming non-joined portions due to the voids, and a non-joined ratio Q on the side section as calculated by the following formula (1), Non-joined ratio Q=(X/Y)×100??(1) where X is a length of the non-joined portion in the direction of junction interface expressed by the sum of lengths L of the voids existing in the directly joined region, and Y is a length of the directly joined region where the voids are existing, is in a range of from 0.1 to 0.5% on average.

Abstract: High-volume, fully dense, multi-component monoliths with microstructurally indistinguishable joints that can be used as refractory, corrosion and wear resistant components in the non-ferrous metal industry. The Si3N4 monoliths according to the invention comprise at least 90% by weight ?-type Si3N4 and up to 10% by weight of a predominantly amorphous binder phase, said binder phase being formed from compositions of the rare earth metal —Al—Si—O—N, rare earth metal —Mg—Si—O—N or Mg—Si—O—N systems. Preferably the rare earth metal is yttrium (Y). The monoliths have a volume of greater than 250 cm3. A method of making the multi-component monoliths is achieved by simultaneously joining and uniaxially hot pressing an assembly of reaction bonded silicon nitride bodies (RBSN bodies). RBSN bodies are placed in contact with each other in the substantial absence of any interlayer or ceramic paste in between.

Abstract: The invention includes methods of forming an aluminum oxynitride-comprising body. For example, a mixture is formed which comprises A:B:C in a respective molar ratio in the range of 9:3.6-6.2:0.1-1.1, where “A” is Al2O3, “B” is AlN, and “C” is a total of one or more of B2O3, SiO2, Si—Al—O—N, and TiO2. The mixture is sintered at a temperature of at least 1,600° C. at a pressure of no greater than 500 psia effective to form an aluminum oxynitride-comprising body which is at least internally transparent and has at least 99% maximum theoretical density.

Abstract: Refractory coatings comprising unstabilized zirconia, silica, and, optionally, zircon and/or mullite are disclosed herein. The unstabilized zirconia, silica, and optional zircon and/or mullite are applied as a slurry onto ceramic substrates such as silicon carbide and fired. The refractory coatings of the present invention maintained good edge definition and color when applied to ceramic substrates and subjected to temperatures over 1100° C.

Abstract: A process for continuous composite coextrusion comprising: (a) forming first a material-laden composition comprising a thermoplastic polymer and at least about 40 volume % of a ceramic or metallic particulate in a manner such that the composition has a substantially cylindrical geometry and thus can be used as a substantially cylindrical feed rod; (b) forming a hole down the symmetrical axis of the feed rod; (c) inserting the start of a continuous spool of ceramic fiber, metal fiber or carbon fiber through the hole in the feed rod; (d) extruding the feed rod and spool simultaneously to form a continuous filament consisting of a green matrix material completely surrounding a dense fiber reinforcement and said filament having an average diameter that is less than the average diameter of the feed rod; and (e) depositing the continuous filament into a desired architecture which preferably is determined from specific loading conditions of the desired object and CAD design of the object to provide a green fiber rei

Abstract: A turbomachine component includes a silicon nitride substrate and a protective coating on the substrate. The protective coating includes a porous silicon nitride matrix and a noble metal infiltrated in the porous silicon nitride matrix.

Abstract: A novel method for joining aluminum nitride-series substrates to each other is provided in the substantial absence of an intervening third layer at the joining interface between the substrates. In the method, the aluminum nitride-series substrates are joined to each other by interposing a joining agent between the substrates heating the substrates and the joining agent to a first temperature range of at least the melting point of the joining agent to melt the joining agent and liquefy particles of the aluminum nitride at the neighborhood of the interfaces between the melted joining agent and the substrates, and then heating the joining agent and the substrates to a temperature range higher than the temperature range of the first process but lower than the melting point of the substrates to exhaust the joining agent from between the substrates.

Abstract: A resistance element comprising at least a resistance element body comprised of a ceramic including &bgr;-SIALON of a composition expressed by Si6−zAlzOzN8−z (where, in the formula, z=0.3 to 1.0) and an internal conductor embedded inside the resistance element body, wherein the internal conductor includes a conductor material containing tungsten and carbon and having an atomic ratio of carbon to tungsten of 0.4 to 1.1 and an insulator material and the volume ratio of the insulator material to the conductor material is 0.25 to 1.5. Such a resistance element can be used over a long time under a high temperature environment, has little fluctuation in resistance even with repeated rises and falls between room temperature and a high temperature, can withstand oxidation at a high temperature, and is otherwise superior in durability.

Abstract: A process for producing bodies made of fiber-reinforced composites from fiber-reinforced precursor bodies having a porous carbon matrix, in particular from C/C bodies, includes (1) mixing fibers, fiber bundles or fiber agglomerates based on carbon, nitrogen, boron and/or silicon with at least one carbonizable binder to give a pressing composition, and (2) pressing the pressing composition to form a green body. At least one metal- or silicon-containing core is added to the green body. The green body is subsequently pyrolysed to convert the binder or binders into a porous carbon matrix, and the resulting fiber-reinforced precursor body is infiltrated with molten metal or silicon from the metal- or silicon-containing core.

Abstract: A fibrous ceramics fabrication method using a room extrusion process and a fibrous monolithic ceramics fabrication method using thereof is disclosed. The method includes the steps of obtaining a extrusion-purpose slurry by evenly mixing a hydrophilic cellulose bonding agent 3 to 7 and a hydrophilic organic plasticizer 5 to 20 for improving a formation property by softening the cellulose bonding agent with a distilled water 45 to 55, with regard to a weight percent 100 of a ceramic powders selected from a group of silicon nitride, silicon carbide and alumina, carrying out a room temperature extrusion from the extrusion-purpose slurry, and coating the fiber by passing through a mixedly dispersed coating-purpose slurry a ceramic powders 20 to 45 selected from a group of boron nitride and graphite, an organic dispersant 0.

Abstract: Refractory coatings comprising unstabilized zirconia, silica, and, optionally, zircon and/or mullite are disclosed herein. The unstabilized zirconia, silica, and optional zircon and/or mullite are applied as a slurry onto ceramic substrates such as silicon carbide and fired. The refractory coatings of the present invention maintained good edge definition and color when applied to ceramic substrates and subjected to temperatures over 1100° C.