Having A Specified Thermal Property Patents (Class 175/433)
  • Patent number: 11719050
    Abstract: Cutting elements for earth-boring tools may include a rotationally leading end positioned and configured to engage with, and remove, a material of an earth formation. A transition region may extend from proximate to a periphery of the cutting element radially inward and axially toward the rotationally leading end. The transition region may include first faceted surfaces, each first faceted surface extending at a first angle relative to a central geometric axis of the cutting element. The transition region may also include second faceted surfaces, each second faceted surface extending at a second, different angle relative to the central geometric axis of the cutting element. The first faceted surfaces and the second faceted surfaces may intersect one another at edges around a periphery of the transition region.
    Type: Grant
    Filed: June 16, 2021
    Date of Patent: August 8, 2023
    Assignee: Baker Hughes Oilfield Operations LLC
    Inventors: Steven Craig Russell, Stephen Duffy
  • Patent number: 10920826
    Abstract: A radial bearing for transmitting a radial load, including a first radial bearing component having an inner surface defining a bore and a second radial bearing component received within the bore of the first radial bearing component and having an outer surface. The first radial bearing component includes a plurality of first component wear resistant inserts arranged and mounted on the inner surface. The second radial bearing component includes a second component wear resistant coating on at least a portion of the outer surface. The first radial bearing component and the second radial bearing component interact to transmit the radial load between the first radial bearing component and the second radial bearing component.
    Type: Grant
    Filed: March 17, 2017
    Date of Patent: February 16, 2021
    Assignee: HALLIBURTON ENERGY SERVICES, INC.
    Inventor: Philip Park-Hung Leung
  • Patent number: 10704335
    Abstract: Polycrystalline diamond bodies having an annular region of diamond grains and a core region of diamond grains and methods of making the same are disclosed. In one embodiment, a polycrystalline diamond body (120) includes an annular region (142) of inter-bonded diamond grains having a first characteristic property and a core region (140) of inter-bonded diamond grains bonded to the annular region and having a second characteristic property that differs from the first characteristic property. The annular region decreases in thickness from a perimeter surface of the polycrystalline diamond body towards a centerline axis.
    Type: Grant
    Filed: March 16, 2017
    Date of Patent: July 7, 2020
    Assignee: DIAMOND INNOVATIONS, INC.
    Inventors: Andrew Gledhill, Christopher Long, Alexanne Johnson
  • Patent number: 10683705
    Abstract: A MAX-phase material is provided for a cutting tool and other applications.
    Type: Grant
    Filed: December 4, 2017
    Date of Patent: June 16, 2020
    Inventor: L. Pierre de Rochemont
  • Patent number: 10363624
    Abstract: The present disclosure relates to a brazed superabrasive assemblies and method of producing brazed superabrasive assemblies. The brazed superabrasive assemblies may include a plurality of braze alloy layers that are positioned opposite a stress relieving layer. The stress relieving layer may have a solidus temperature that is greater than a solidus temperature of the plurality of braze alloy layers.
    Type: Grant
    Filed: April 3, 2015
    Date of Patent: July 30, 2019
    Assignee: DIAMOND INNOVATIONS, INC.
    Inventor: Thomas Easley
  • Patent number: 10364615
    Abstract: A thermally stable polycrystalline diamond compact is created by (i) preforming an annular thermally stable polycrystalline from a diamond plate, (ii) preforming a substrate with a projection that has an interfacial mating surface that is a negative topology of the annular thermally stable polycrystalline, (iii) and brazing the two components together. The resulting polycrystalline diamond compact can be made thermally stable because cobalt and other catalysts can be leached out of the thermally stable polycrystalline. The thermally stable polycrystalline can be attached to the substrate by brazing, which due to the topology of the thermally stable polycrystalline and the substrate with a projection will unexpectedly have sufficient blaze shear strength to be used in demanding applications.
    Type: Grant
    Filed: November 12, 2014
    Date of Patent: July 30, 2019
    Assignee: Suzhou Superior Industrial Technology Co. Ltd.
    Inventors: Samer Alkhalaileh, Yuming Jiang
  • Patent number: 10358705
    Abstract: A method of forming a polycrystalline diamond cutting element includes assembling a diamond material, a substrate, and a source of catalyst material or infiltrant material distinct from the substrate, the source of catalyst material or infiltrant material being adjacent to the diamond material to form an assembly. The substrate includes an attachment material including a refractory metal. The assembly is subjected to a first high-pressure/high temperature condition to cause the catalyst material or infiltrant material to melt and infiltrate into the diamond material and subjected to a second high-pressure/high temperature condition to cause the attachment material to melt and infiltrate a portion of the infiltrated diamond material to bond the infiltrated diamond material to the substrate.
    Type: Grant
    Filed: November 20, 2015
    Date of Patent: July 23, 2019
    Assignee: SMITH INTERNATIONAL, INC.
    Inventors: Yahua Bao, Fulong Wang, J. Daniel Belnap, Ronald K. Eyre, Yi Fang
  • Patent number: 10259101
    Abstract: Polycrystalline compacts include an interface between first and second volumes of a body of inter-bonded grains of hard material. The first volume is at least substantially free of interstitial material, and the second volume includes interstitial material in interstitial spaces between surfaces of the inter-bonded grains of hard material. The interface between the first and second volumes is configured, located and oriented such that cracks originating in the compact during use of the compacts and propagating along the interface generally toward a central axis of the compacts will propagate generally toward a back surface and away from a front cutting face of the compacts at an acute angle or angles. Methods of forming polycrystalline compacts involve the formation of such an interface within the compacts.
    Type: Grant
    Filed: December 21, 2016
    Date of Patent: April 16, 2019
    Assignee: Baker Hughes Incorporated
    Inventor: Xiaomin Chris Cheng
  • Patent number: 10221628
    Abstract: Methods of repairing earth-boring tools may involve providing wear-resistant material over a temporary displacement member to repair a cutting element pocket in a body and a depth-of-cut control feature using the wear-resistant material. In some embodiments, the wear-resistant material may comprise a particle-matrix composite material. For example, a hardfacing material may be built up over a temporary displacement member to form or repair a cutting element pocket and provide a depth-of-cut control feature. Earth-boring tools may include a depth-of-cut control feature comprising a wear-resistant material. The depth-of-cut control feature may be configured to limit a depth-of-cut of a cutting element secured within a cutting element pocket partially defined by at least one surface of the depth-of-cut control feature. Intermediate structures formed during fabrication of earth-boring tools may include a depth-of-cut control feature extending over a temporary displacement member.
    Type: Grant
    Filed: February 23, 2016
    Date of Patent: March 5, 2019
    Assignee: Baker Hughes Incorporated
    Inventors: James L. Overstreet, Kenneth E. Gilmore, Travis E. Puzz
  • Patent number: 10119334
    Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDC”) exhibiting enhanced diamond-to-diamond bonding. In an embodiment, PDC includes a sintered substantially single-phase polycrystalline diamond (“PCD”) body consisting essentially of bonded-together diamond grains exhibiting a morphology different than that of a PCD body formed by sintering diamond crystals. A substrate is bonded to the sintered substantially single-phase PCD body. Other embodiments are directed to methods of forming such PDCs, and various applications for such PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.
    Type: Grant
    Filed: January 4, 2016
    Date of Patent: November 6, 2018
    Assignee: US SYNTHETIC CORPORATION
    Inventors: Kenneth E. Bertagnolli, C. Eugene McMurray
  • Patent number: 10099346
    Abstract: Embodiments relate to PDCs, methods of fabricating PDCs, and applications for such PDCs. In an embodiment, a PDC includes a substrate and a pre-sintered PCD table including an interfacial surface that is bonded to the substrate. The pre-sintered PCD table may be substantially free of leaching by-products in a region at least proximate to the interfacial surface. In an embodiment, a method of fabricating a PDC includes providing an at least partially leached PCD including an interfacial surface. The method includes removing at least some leaching by-products from the at least partially leached PCD table. After removing the at least some leaching by-products, the method includes bonding the interfacial surface of the at least partially leached PCD table to a substrate to form a PDC.
    Type: Grant
    Filed: August 29, 2016
    Date of Patent: October 16, 2018
    Assignee: US SYNTHETIC CORPORATION
    Inventors: Michael A. Vail, Kenneth E. Bertagnolli
  • Patent number: 9790746
    Abstract: Polycrystalline compacts include a polycrystalline material comprising a plurality of inter-bonded grains of hard material, and a metallic material disposed in interstitial spaces between the inter-bonded grains of hard material. At least a portion of the metallic material comprises a metal alloy that includes two or more elements. A first element of the two or more elements comprises at least one of cobalt, iron, and nickel. A second element of the two or more elements comprises at least one of dysprosium, yttrium, terbium, gadolinium, germanium, samarium, neodymium, and praseodymium. The metal alloys may comprise eutectic or near-eutectic compositions, and may have relatively low melting points. Cutting elements and earth-boring tools include such polycrystalline compacts. Methods include the formation of such polycrystalline compacts, cutting elements, and earth-boring tools.
    Type: Grant
    Filed: January 16, 2014
    Date of Patent: October 17, 2017
    Assignee: Baker Hughes Incorporated
    Inventor: Anthony A. DiGiovanni
  • Patent number: 9682460
    Abstract: A method of treating a polycrystalline diamond (PCD) compact including a substrate and a layer of diamond material mixture of diamond particles and binder-catalyst disposed on the substrate. A leaching agent is applied to at least the layer of diamond material of the PCD compact. The leaching agent and a surface of the layer of diamond material are heated to a first temperature. The substrate is cooled to a second temperature. A first temperature gradient is established within the PCD compact to cause an inward diffusion of the leaching agent into at least the layer of diamond material. The cooling of the substrate is stopped and energy is applied directly to the PCD compact to heat the same to a third temperature. A second temperature gradient is established within the PCD compact to cause an outward diffusion of the binder-catalyst to remove the same from the layer of diamond material.
    Type: Grant
    Filed: June 9, 2015
    Date of Patent: June 20, 2017
    Assignee: DIAMOND INNOVATIONS, INC
    Inventors: Ramamoorthy Ramasamy, Thomas R Dugan
  • Patent number: 9435159
    Abstract: A polycrystalline diamond compact comprising a diamond table is formed in a high-pressure, high-temperature process using a catalyst, the catalyst being substantially removed from the entirety of the diamond table, and the diamond table attached to a supporting substrate in a subsequent high-pressure, high-temperature process using a binder material differing at least in part from a material of the catalyst. The binder material is permitted to penetrate substantially completely throughout the diamond table from an interface with the substrate to and including a cutting surface, and the binder material is selectively removed from a region or regions of the diamond table by a conventional technique (e.g., acid leaching). Cutting elements so formed and drill bits equipped with such cutting elements are also disclosed.
    Type: Grant
    Filed: October 28, 2013
    Date of Patent: September 6, 2016
    Assignee: Baker Hughes Incorporated
    Inventor: Danny E. Scott
  • Patent number: 8997900
    Abstract: A polycrystalline diamond compact formed in an in-situ boron-doped process. The in-situ boron-doped process includes consolidating a mixture of diamond crystals and boron-containing alloy via liquid diffusion of boron into diamond crystals at a pressure greater than 5 Gpa and at a temperature greater than the melting temperature of the boron-containing alloy, typically less than about 1450° C.
    Type: Grant
    Filed: December 15, 2010
    Date of Patent: April 7, 2015
    Assignee: National Oilwell DHT, L.P.
    Inventors: Jiinjen Albert Sue, Harold Sreshta
  • Publication number: 20150075877
    Abstract: A polycrystalline-diamond cutting element for a drill bit of a downhole tool. The cutting element includes a substrate and a diamond table bonded to the substrate. The diamond table includes a diamond filler with at least one leached polycrystalline diamond segment packed therein along at least one working surface thereof. The cutting element may be formed by positioning the diamond table on the substrate and bonding the diamond table onto the substrate such that the polycrystalline diamond segment is positioned along at least one working surface of the diamond table. A spark plasma sintering or double press operation may be used to bond the diamond table onto the substrate.
    Type: Application
    Filed: November 25, 2014
    Publication date: March 19, 2015
    Inventors: Deepthi Raj Setlur, Michael D. Hughes, Mark Jonathan Francis, Harold A. Sreshta, Guodong Zhan, Russell C. Gilleylen, JiinJen Albert Sue
  • Patent number: 8978789
    Abstract: In an embodiment, a polycrystalline diamond compact (“PDC”) includes a substrate and a polycrystalline diamond (“PCD”) table bonded to the substrate. The PCD table includes an upper surface. The PCD table includes a first PCD region including bonded-together diamond grains and exhibits a first diamond density. At least a portion of the first PCD region extending inwardly from the working surface is substantially free of metal-solvent catalyst. The PCD table includes an intermediate second PCD region bonded to the substrate, which is disposed between the first PCD region and the substrate. The second PCD region includes bonded-together diamond grains defining interstitial regions, with at least a portion of the interstitial regions including metal-solvent catalyst disposed therein. The second PCD region exhibits a second diamond density that is greater than that of the first diamond density of the first PCD region.
    Type: Grant
    Filed: July 28, 2010
    Date of Patent: March 17, 2015
    Assignee: US Synthetic Corporation
    Inventors: Mohammad N. Sani, Alberto Castillo
  • Patent number: 8939238
    Abstract: A sintered cutting element including a superabrasive layer supported on a substrate. The superabrasive layer includes superabrasive material and secondary phase, and the substrate includes a binder phase. The sintered cutting element is formed by a high temperature high pressure sintering process in which separate source elements melt and sweep first through the superabrasive layer, and then to the substrate to form the secondary phase and binder phase. The superabrasive layer is substantially free of or free of eta-phase, Co3W3C. Further, the portion of the substrate nearest the interface between the superabrasive layer and the substrate has equal or more binder phase than portions of the substrate further from the interface. In certain embodiments, the superabrasive material includes polycrystalline diamond, and the substrate includes cobalt tungsten carbide.
    Type: Grant
    Filed: September 6, 2011
    Date of Patent: January 27, 2015
    Assignee: Diamond Innovations, Inc.
    Inventors: Malin Martensson, Yuanbo Lin, Andreas Markstrom, Susanne Norgren
  • Patent number: 8936114
    Abstract: A composite may generally include a substantially continuous binder phase and a first reinforcing agent cluster infiltrated by the binder phase, the first reinforcing agent cluster comprising a plurality of first reinforcing agent particles. A drill bit may include at least one cutting element for engaging a formation and a bit body, at least a portion of said drill bit being a composite that includes a substantially continuous binder phase and a first reinforcing agent cluster infiltrated by the binder phase.
    Type: Grant
    Filed: January 13, 2012
    Date of Patent: January 20, 2015
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Jeffrey Gerard Thomas, Brian Atkins
  • Patent number: 8931854
    Abstract: In one aspect of the present invention, a high impact wear resistant tool has a superhard material bonded to a cemented metal carbide substrate at a non-planar interface. The superhard material has a thickness of at least 0.100 inch and forms an included angle of 35 to 55 degrees. The superhard material has a plurality of substantially distinct diamond layers. Each layer of the plurality of layers has a different catalyzing material concentration. A diamond layer adjacent the substrate of the superhard material has a higher catalyzing material concentration than a diamond layer at a distal end of the superhard material.
    Type: Grant
    Filed: September 6, 2013
    Date of Patent: January 13, 2015
    Assignee: Schlumberger Technology Corporation
    Inventor: David R. Hall
  • Patent number: 8925656
    Abstract: Diamond bonded construction comprise a diamond body attached to a support. In one embodiment, an initial substrate used to sinter the body is interposed between the body and support, and is thinned to less than 5 times the body thickness, or to less than the body thickness, prior to attachment to the support to relieve stress in the body. In another embodiment, the substrate is removed after sintering, and the body is attached to the support. The support has a material construction different from that of the initial substrate, wherein the initial substrate is selected for infiltration and the support for end use properties. The substrate and support include a hard material with a volume content that may be the same or different. Interfaces between the body, substrate, and/or support may be nonplanar. The body may be thermally stable, and may include a replacement material disposed therein.
    Type: Grant
    Filed: October 12, 2010
    Date of Patent: January 6, 2015
    Assignee: Smith International, Inc.
    Inventors: Yuelin Shen, Youhe Zhang
  • Patent number: 8919463
    Abstract: A polycrystalline-diamond cutting element for a drill bit of a downhole tool. The cutting element includes a substrate and a diamond table bonded to the substrate. The diamond table includes a diamond filler with at least one leached polycrystalline diamond segment packed therein along at least one working surface thereof. The cutting element may be formed by positioning the diamond table on the substrate and bonding the diamond table onto the substrate such that the polycrystalline diamond segment is positioned along at least one working surface of the diamond table. A spark plasma sintering or double press operation may be used to bond the diamond table onto the substrate.
    Type: Grant
    Filed: October 24, 2011
    Date of Patent: December 30, 2014
    Assignee: National Oilwell DHT, L.P.
    Inventors: Deepthi Raj Setlur, Michael D. Hughes, Mark Jonathan Francis, Harold A. Sreshta, Guodong Zhan, Russell C. Gilleylen, JiinJen Albert Sue
  • Patent number: 8893829
    Abstract: A polycrystalline compact comprises a plurality of grains of hard material and a plurality of nanoparticles disposed in interstitial spaces between the plurality of grains of hard material. The plurality of nanoparticles has a thermal conductivity less than a thermal conductivity of the plurality of grains of hard material. An earth-boring tool comprises such a polycrystalline compact. A method of forming a polycrystalline compact comprises combining a plurality of hard particles and a plurality of nanoparticles to form a mixture and sintering the mixture to form a polycrystalline hard material comprising a plurality of interbonded grains of hard material. A method of forming a cutting element comprises infiltrating interstitial spaces between interbonded grains of hard material in a polycrystalline material with a plurality of nanoparticles. The plurality of nanoparticles have a lower thermal conductivity than the interbonded grains of hard material.
    Type: Grant
    Filed: October 19, 2011
    Date of Patent: November 25, 2014
    Assignee: Baker Hughes Incorporated
    Inventor: Anthony A. DiGiovanni
  • Patent number: 8893828
    Abstract: A drill bit may include a bit body having a plurality of blades extending radially therefrom and at least one cutting element for engaging a formation disposed on at least one of the plurality of blades. The bit body has a continuous infiltration binder and a plurality of carbide particles dispersed in the continuous infiltration binder, wherein at least a portion of the plurality of carbide particles and at least a portion of the continuous infiltration binder form a first carbide matrix region, and wherein the plurality of carbide particles forming the first carbide matrix region have an average grain sizes of less than about 44 microns.
    Type: Grant
    Filed: November 18, 2010
    Date of Patent: November 25, 2014
    Assignee: Smith International, Inc.
    Inventors: Gregory T. Lockwood, Madapusi K. Keshavan, Anthony Griffo
  • Patent number: 8869920
    Abstract: Methods, systems, and compositions for manufacturing downhole tools and downhole tool parts for drilling subterranean material are disclosed. A model having an external peripheral shape of a downhole tool or tool part is fabricated. Mold material is applied to the external periphery of the model. The mold material is permitted to harden to form a mold about the model. The model is eliminated and a composite matrix material is cast within the mold to form a finished downhole tool or tool part.
    Type: Grant
    Filed: June 17, 2013
    Date of Patent: October 28, 2014
    Assignee: Baker Hughes Incorporated
    Inventors: John H. Stevens, Jimmy W. Eason
  • Patent number: 8839889
    Abstract: Methods of forming a polycrystalline diamond compact for use in an earth-boring tool include forming a body of polycrystalline diamond material including a first material disposed in interstitial spaces between inter-bonded diamond crystals in the body, removing the first material from interstitial spaces in a portion of the body, selecting a second material promoting a higher rate of degradation of the polycrystalline diamond compact than the first material under similar elevated temperature conditions and providing the second material in interstitial spaces in the portion of the body. Methods of drilling include engaging at least one cutter with a formation and wearing a second region of polycrystalline diamond material comprising a second material faster than the first region of polycrystalline diamond material comprising a first material. Polycrystalline diamond compacts and earth-boring tools including such compacts are also disclosed.
    Type: Grant
    Filed: April 26, 2011
    Date of Patent: September 23, 2014
    Assignees: Baker Hughes Incorporated, Element Six Ltd
    Inventors: Anthony A. DiGiovanni, Iain P. Goudemond
  • Patent number: 8813878
    Abstract: Embodiments relate to PDCs, methods of fabricating PDCs, and applications for such PDCs. In an embodiment, a PDC includes a substrate and a pre-sintered PCD table including an interfacial surface that is bonded to the substrate. The pre-sintered PCD table may be substantially free of leaching by-products in a region at least proximate to the interfacial surface. In an embodiment, a method of fabricating a PDC includes providing an at least partially leached PCD including an interfacial surface. The method includes removing at least some leaching by-products from the at least partially leached PCD table. After removing the at least some leaching by-products, the method includes bonding the interfacial surface of the at least partially leached PCD table to a substrate to form a PDC.
    Type: Grant
    Filed: November 1, 2010
    Date of Patent: August 26, 2014
    Assignee: US Synthetic Corporation
    Inventors: Michael A. Vail, Kenneth E. Bertagnolli
  • Patent number: 8800693
    Abstract: Polycrystalline compacts include non-catalytic, non-carbide-forming particles in interstitial spaces between interbonded grains of hard material in a polycrystalline hard material. Cutting elements and earth-boring tools include such polycrystalline compacts. Methods of forming polycrystalline compacts include forming a polycrystalline material including a hard material and a plurality of particles comprising a non-catalytic, non-carbide-forming material. Methods of forming cutting elements include infiltrating interstitial spaces between interbonded grains of hard material in a polycrystalline material with a plurality of non-catalytic, non-carbide-forming particles.
    Type: Grant
    Filed: September 6, 2011
    Date of Patent: August 12, 2014
    Assignee: Baker Hughes Incorporated
    Inventor: Anthony A. DiGiovanni
  • Patent number: 8783389
    Abstract: A method for facilitating infiltration of an infiltrant material into a TSP material during re-bonding of the TSP material to a substrate, by enhancing the porosity of the TSP material near the interface with the substrate is provided. Cutting elements formed by such method and downhole tools including such cutting elements are also provided.
    Type: Grant
    Filed: June 18, 2010
    Date of Patent: July 22, 2014
    Assignee: Smith International, Inc.
    Inventors: Guojiang Fan, Feng Yu, Yi Fang, J. Daniel Belnap, Peter T. Cariveau
  • Patent number: 8763731
    Abstract: Polycrystalline compacts include a hard polycrystalline material comprising first and second regions. The first region comprises a first plurality of grains of hard material having a first average grain size, and a second plurality of grains of hard material having a second average grain size smaller than the first average grain size. The first region comprises catalyst material disposed in interstitial spaces between inter-bonded grains of hard material. Such interstitial spaces between grains of the hard material in the second region are at least substantially free of catalyst material. In some embodiments, the first region comprises a plurality of nanograins of the hard material. Cutting elements and earth-boring tools include such polycrystalline compacts.
    Type: Grant
    Filed: June 17, 2011
    Date of Patent: July 1, 2014
    Assignee: Baker Hughes Incorporated
    Inventors: Danny E. Scott, Anthony A. DiGiovanni
  • Patent number: 8757299
    Abstract: A cutting element for use in a drilling bit and/or milling bit having a cutter body made of a substrate having an upper surface, and a superabrasive layer overlying the upper surface of the substrate. The cutting element further including a sleeve extending around a portion of a side surface of the superabrasive layer and a side surface of the substrate, wherein the sleeve exerts a radially compressive force on the superabrasive layer.
    Type: Grant
    Filed: July 8, 2010
    Date of Patent: June 24, 2014
    Assignees: Baker Hughes Incorporated, Element Six (Production) (Pty) Ltd., Element Six Limited
    Inventors: Anthony A. DiGiovanni, Nicholas J. Lyons, Matthew S. Hale, Konstantin E. Morozov, John H. Liversage, Danny E. Scott, Allen Sinor
  • Patent number: 8752656
    Abstract: A bottom hole assembly containing a drill bit. The drill bit additionally has a plurality of primary cutter elements mounted thereto. The plurality of cutter elements comprise one or more first cutter elements and one or more second cutter elements. The second cutter element differs from the first cutter element in at least one cutter element property. The first cutter element has a diamond body containing a first region comprising an infiltrant material disposed within the interstitial regions. The first region is located remote from the working surface of the diamond body. The first cutter element also contains a second region comprising interstitial regions that are substantially free of the infiltrant material. The second region is located along at least the working surface of the diamond body. Also included are a cutter element, method of designing a bottom hole assembly as well as method of designing a drill bit.
    Type: Grant
    Filed: December 17, 2009
    Date of Patent: June 17, 2014
    Assignee: Smith International, Inc.
    Inventors: Youhe Zhang, Yuelin Shen, Madapusi K Keshavan, Peter T Cariveau
  • Patent number: 8727044
    Abstract: In an embodiment, a polycrystalline diamond compact (“PDC”) includes a substrate and a pre-sintered polycrystalline diamond (“PCD”) table bonded to the substrate. The pre-sintered PCD table includes an upper surface, a back surface bonded to the substrate, and at least one lateral surface extending between the upper surface and the back surface. The pre-sintered PCD table includes a region including at least a residual amount of at least one interstitial constituent disposed in at least a portion of the interstitial regions thereof, and a bonding region. The at least one interstitial constituent includes at least one metal carbonate and/or at least one metal oxide. The region extends inwardly from the upper surface and the at least one lateral surface.
    Type: Grant
    Filed: March 24, 2011
    Date of Patent: May 20, 2014
    Assignee: US Synthetic Corporation
    Inventors: Jiang Qian, Kenneth E. Bertagnolli, Jair J. Gonzalez, Craig H. Cooley
  • Patent number: 8727046
    Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”) that are less susceptible to liquid metal embrittlement damage due to the use of at least one transition layer between a polycrystalline diamond (“PCD”) layer and a substrate. In an embodiment, a PDC includes a PCD layer, a cemented carbide substrate, and at least one transition layer bonded to the substrate and the PCD layer. The at least one transition layer is formulated with a coefficient of thermal expansion (“CTE”) that is less than a CTE of the substrate and greater than a CTE of the PCD layer. At least a portion of the PCD layer includes diamond grains defining interstitial regions and a metal-solvent catalyst occupying at least a portion of the interstitial regions. The diamond grains and the catalyst collectively exhibit a coercivity of about 115 Oersteds or more and a specific magnetic saturation of about 15 Gauss·cm3/grams or less.
    Type: Grant
    Filed: April 15, 2011
    Date of Patent: May 20, 2014
    Assignee: US Synthetic Corporation
    Inventors: David P. Miess, Kenneth E. Bertagnolli, Damon B. Crockett, Arnold D. Cooper
  • Patent number: 8721752
    Abstract: A PCD cutting element for use in earth boring drill bits where die interstices remote from the working surface are filled with a catalyzing material and the interstices adjacent to the working surface are substantially free of the catalyzing material is described. An intermediate region between the substantially free portion and filled portion has a plurality of generally conically sectioned catalyst-free projections which taper down, extending to a second depth from the planar working surface, preferably about 0.5 times or more of the first depth.
    Type: Grant
    Filed: August 14, 2008
    Date of Patent: May 13, 2014
    Assignee: Reedhycalog UK Limited
    Inventors: John Michael Fuller, Douglas Caraway, Graham Richard Watson
  • Patent number: 8720612
    Abstract: The present disclosure relates in one aspect to a cutting element comprising a substrate and a cutting layer disposed on a surface of the substrate. The cutting layer comprises an ultra hard material. The substrate comprises tungsten carbide and a metal binder. The substrate has a magnetic saturation value in the range of from 80% to less than 85%. In another aspect, the magnetic saturation value may increase within the substrate along a gradient, wherein proximal to the interface with the cutting layer, the substrate has a magnetic saturation value in the range of from 80% to less than 85%. Also included are drill bits incorporating such cutting elements. Additionally, the present disclosure relates to methods of manufacturing cutting elements.
    Type: Grant
    Filed: November 23, 2009
    Date of Patent: May 13, 2014
    Assignee: Smith International, Inc.
    Inventors: Loel G Corbett, Daniel J Belnap
  • Publication number: 20140116791
    Abstract: Diamond bonded constructions comprise a polycrystalline diamond body having a matrix phase of bonded-together diamond grains and a plurality of interstitial regions between the diamond grains including a catalyst material used to form the diamond body disposed within the interstitial regions. A sintered thermally stable diamond element is disposed within and bonded to the diamond body, and is configured and positioned to form part of a working surface. The thermally stable diamond element is bonded to the polycrystalline diamond body, and a substrate is bonded to the polycrystalline diamond body. The thermally stable diamond element comprises a plurality of bonded-together diamond grains and interstitial regions, wherein the interstitial regions are substantially free of a catalyst material used to make or sinter the thermally stable diamond element. A barrier material may be disposed over or infiltrated into one or more surfaces of the thermally stable diamond element.
    Type: Application
    Filed: January 6, 2014
    Publication date: May 1, 2014
    Applicant: Smith International, Inc.
    Inventors: Georgiy Voronin, J. Daniel Belnap, Feng Yu, Benjamin Randall
  • Patent number: 8695733
    Abstract: PCD inserts comprise a PCD body having multiple FG-PCD regions with decreasing diamond content moving from a body outer surface to a metallic substrate. The diamond content changes in gradient fashion by changing metal binder content. A region adjacent the outer surface comprises 5 to 20 percent by weight metal binder, and a region remote from the surface comprises 15 to 40 percent by weight metal binder. One or more transition regions are interposed between the PCD body and substrate. The transition region comprises PCD, binder metal, and a carbide, comprises a metal binder content less than that present in the PCD body region positioned next to it.
    Type: Grant
    Filed: August 6, 2010
    Date of Patent: April 15, 2014
    Assignee: Smith International, Inc.
    Inventors: Yi Fang, Federico Bellin, Michael Stewart, Nephi A Mourik, Peter T Cariveau
  • Patent number: 8689912
    Abstract: Diamond bonded constructions include a diamond body comprising intercrystalline bonded diamond and interstitial regions. The body has a working surface and an interface surface, and may be joined to a metallic substrate. The body has a gradient diamond volume content greater about 1.5 percent, wherein the diamond content at the interface surface is less than 94 percent, and increases moving toward the working surface. The body may include a region that is substantially free of a catalyst material otherwise disposed within the body and present in a gradient amount. An additional material may be included within the body and be present in a changing amount. The body may be formed by high-pressure HPHT processing, e.g., from 6,200 MPa to 10,000 MPa, to produce a sintered body having a characteristic diamond volume fraction v. average grain size relationship distinguishable from that of diamond bonded constructions form by conventional-pressure HPHT processing.
    Type: Grant
    Filed: November 24, 2010
    Date of Patent: April 8, 2014
    Assignee: Smith International, Inc.
    Inventors: J. Daniel Belnap, Georgiy Voronin, Feng Yu, Peter Cariveau
  • Publication number: 20140069727
    Abstract: Ultra-hard constructions comprise a sintered diamond-bonded body comprising a matrix of bonded-together diamond grains and a plurality of interstitial regions substantially free of a catalyst material. A metal material comprising a carbide constituent is disposed on a substrate interface surface of the diamond body. A substrate is attached to the diamond-bonded body through a braze joint interposed between the metal material and the substrate. The braze joint is formed from a non-active braze material that reacts with the substrate and metal material. The braze joint is formed at the melting temperature of the non-active braze material in the absence of high-pressure conditions. In an example embodiment, the non-active braze material reacts with the carbide constituent in the metal material. Example materials useful for forming the non-active braze material include those selected from Cu, Ni, Mn, Au, Pd, and combinations and alloys thereof.
    Type: Application
    Filed: September 5, 2013
    Publication date: March 13, 2014
    Applicant: SMITH INTERNATIONAL, INC.
    Inventor: J. DANIEL BELNAP
  • Patent number: 8662207
    Abstract: Rotary drag bits comprise a body comprising a face at a leading end of the body. An abrasive-impregnated cutting structure is located at the face of the bit body. The abrasive-impregnated cutting structure comprises abrasive particles dispersed within a matrix material. The abrasive-impregnated cutting structure exhibits an anisotropic wear resistance. The wear resistance varies at least substantially continuously within the abrasive-impregnated cutting structure.
    Type: Grant
    Filed: December 18, 2012
    Date of Patent: March 4, 2014
    Assignee: Baker Hughes Incorporated
    Inventors: Van J. Brackin, Jeffrey B. Lund, Danny E. Scott, Marcus R. Skeem, Matthew R. Isbell
  • Patent number: 8662209
    Abstract: A front face of a diamond table mounted to a substrate is processed, for example through an acid leach, to remove interstitial catalyst binder and form a thermal channel. A material is then introduced to the front face of the diamond table, the introduced material backfilling the front face of the diamond table to fill interstitial voids left by removal of the catalyst binder in the thermal channel to a desired depth. The material is selected to be less thermally expandable than the catalyst binder and/or more thermally conductive than the catalyst binder and/or having a lower heat capacity than the catalyst binder.
    Type: Grant
    Filed: March 2, 2010
    Date of Patent: March 4, 2014
    Assignee: Varel International, Ind., L.P.
    Inventors: Alfazazi Dourfaye, William W. King, Michael R. Reese
  • Patent number: 8616306
    Abstract: Embodiments of the invention relate to a polycrystalline diamond compact. In an embodiment, the polycrystalline diamond compact includes a substrate and a polycrystalline diamond table including a first polycrystalline diamond layer bonded to the substrate and at least a second polycrystalline diamond layer. At least an un-leached portion of the polycrystalline diamond table includes a plurality of diamond grains defining a plurality of interstitial regions and a metal-solvent catalyst occupying at least a portion of the plurality of interstitial regions. The plurality of diamond grains and the metal-solvent catalyst collectively exhibit a coercivity of about 115 Oe or more and a specific magnetic saturation of about 15 G·cm3/g or less. The second polycrystalline diamond layer exhibits a second average diamond grain size that is less than a first average diamond grain size of the first polycrystalline diamond layer and/or the first polycrystalline diamond layer includes a tungsten-containing material therein.
    Type: Grant
    Filed: September 20, 2012
    Date of Patent: December 31, 2013
    Assignee: US Synthetic Corporation
    Inventors: Kenneth E. Bertagnolli, Michael A. Vail, Jason K. Wiggins, Jiang Qian, David P. Miess, Debkumar Mukhopadhyay
  • Patent number: 8616307
    Abstract: Thermally stable diamond bonded construction comprise a diamond bonded body including a thermally stable region, comprising a plurality of diamond grains bonded together by a reaction product of the diamond grains with a reactant such as Si, and a polycrystalline diamond region, comprising intercrystalline bonded diamond and a catalyst material. The body further comprises a ceramic compound formed by reaction of an Nb, Zr, Ti, or Mo getter material with a gaseous element generated during HPHT sintering of the diamond bonded body. The diamond bonded body may comprise from 0.1 to 15 percent by weight of the ceramic compound. The diamond bonded body can be formed during a single HPHT process operated at different temperatures when the reactant has a melting temperature above the catalyst material. The construction may include a metallic substrate attached to the diamond bonded body to facilitate use as a wear or cutting element.
    Type: Grant
    Filed: December 16, 2010
    Date of Patent: December 31, 2013
    Assignee: Smith International, Inc.
    Inventors: Georgiy Voronin, J. Daniel Belnap
  • Patent number: 8602131
    Abstract: A block of dense material is made up of hard particles, of the same or different nature, dispersed in a binder phase. The material has a solidus temperature Ts above which the binder phase is liquid. There is deposited on at least a portion of the surface of the block of dense material an active coating composed of a material capable of reacting chemically with the dense material when the assembly is heated to beyond a minimum reaction temperature Tr. The block coated with the active coating is subjected to a heat treatment comprising heating, then maintenance for a time tm at a maintenance temperature Tm greater than or equal to the minimum reaction temperature Tr, followed by cooling to ambient temperature.
    Type: Grant
    Filed: October 7, 2009
    Date of Patent: December 10, 2013
    Assignee: Varel International, Ind., L.P.
    Inventors: Christophe Colin, Elodie Sorlier, Alfazazi Dourfaye
  • Patent number: 8596387
    Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”) including a non-uniformly leached polycrystalline diamond (“PCD”) table, and methods of fabricating such PDCs. In an embodiment, a PDC includes a substrate and a PCD table integrally formed with and bonded to the substrate. The PCD table defines an upper surface and at least one peripheral surface. The PCD table includes a plurality of bonded diamond grains. The PCD table includes a first region adjacent to the substrate that includes metal-solvent catalyst disposed interstitially between the bonded diamond grains thereof, and a leached second region extending inwardly from the upper surface and the at least one peripheral surface that is depleted of the metal-solvent catalyst. The leached second region exhibits a leach depth profile having a maximum leach depth that is measured from the upper surface.
    Type: Grant
    Filed: October 5, 2010
    Date of Patent: December 3, 2013
    Assignee: US Synthetic Corporation
    Inventors: Mohammad N. Sani, Andrew E. Dadson
  • Patent number: 8590643
    Abstract: A PCD structure comprising a first region, in a state of residual compressive stress, and a second region in a state of residual tensile stress adjacent the first region; the first and second regions each formed of respective PCD grades and directly bonded to each other by intergrowth of diamond grains, the PCD grades having transverse rupture strength (TRS) of at least 1,200 MPa. A third region in a state of residual compressive stress may also be provided such that the second region is disposed between the first and third regions and is bonded to the first and third regions by intergrowth of diamond grains.
    Type: Grant
    Filed: December 7, 2010
    Date of Patent: November 26, 2013
    Assignees: Element Six Limited, Element Six Abrasives S.A.
    Inventors: Clint Guy Smallman, Moosa Mahomed Adia, Lai Hong Lai Sang
  • Patent number: 8579052
    Abstract: Polycrystalline compacts include hard polycrystalline materials comprising in situ nucleated smaller grains of hard material interspersed and inter-bonded with larger grains of hard material. The average size of the larger grains may be at least about 250 times greater than the average size of the in situ nucleated smaller grains. Methods of forming polycrystalline compacts include nucleating and catalyzing the formation of smaller grains of hard material in the presence of larger grains of hard material, and catalyzing the formation of inter-granular bonds between the grains of hard material. For example, nucleation particles may be mixed with larger diamond grains, a carbon source, and a catalyst. The mixture may be subjected to high temperature and high pressure to form smaller diamond grains using the nucleation particles, the carbon source, and the catalyst, and to catalyze formation of diamond-to-diamond bonds between the smaller and larger diamond grains.
    Type: Grant
    Filed: August 6, 2010
    Date of Patent: November 12, 2013
    Assignee: Baker Hughes Incorporated
    Inventors: Anthony A. DiGiovanni, Danny E. Scott
  • Patent number: 8573332
    Abstract: A polycrystalline diamond compact comprising a diamond table is formed in a high-pressure, high-temperature process using a catalyst, the catalyst being substantially removed from the entirety of the diamond table, and the diamond table attached to a supporting substrate in a subsequent high-pressure, high-temperature process using a binder material differing at least in part from a material of the catalyst. The binder material is permitted to penetrate substantially completely throughout the diamond table from an interface with the substrate to and including a cutting surface, and the binder material is selectively removed from a region or regions of the diamond table by a conventional technique (e.g., acid leaching). Cutting elements so formed and drill bits equipped with such cutting elements are also disclosed.
    Type: Grant
    Filed: January 15, 2010
    Date of Patent: November 5, 2013
    Assignee: Baker Hughes Incorporated
    Inventor: Danny E. Scott
  • Patent number: 8567531
    Abstract: The present disclosure relates to cutting elements incorporating polycrystalline diamond bodies used for subterranean drilling applications, and more particularly, to polycrystalline diamond bodies having a high diamond content which are configured to provide improved properties of thermal stability and wear resistance, while maintaining a desired degree of impact resistance, when compared to prior polycrystalline diamond bodies. In various embodiments disclosed herein, a cutting element with high diamond content includes a modified PCD structure and/or a modified interface (between the PCD body and a substrate), to provide superior performance.
    Type: Grant
    Filed: May 20, 2010
    Date of Patent: October 29, 2013
    Assignee: Smith International, Inc.
    Inventors: J. Daniel Belnap, Georgiy Voronin, Feng Yu, Peter T. Cariveau, Youhe Zhang, Yuelin Shen, Guodong Zhan