Diamond Patents (Class 175/434)
  • Patent number: 8936665
    Abstract: The present invention relates to a method for producing diamond-metal composites comprising mixing diamond particles with metal-filler particles forming a diamond/metal-filler mixture, forming a green body of the diamond/metal-filler mixture, optionally green machining the green body to a work piece before or after pre-sintering by heating the green body to a temperature ?500° C., infiltrating the green body or the work piece with one or more wetting elements or infiltrating the green body or the work piece with one or more wetting alloys, which infiltration step being carried out under vacuum or in an inert gas atmosphere at a pressure ?200 Bar. The invention relates further to a green body, a diamond metal composite, and use of the diamond metal composite.
    Type: Grant
    Filed: October 30, 2008
    Date of Patent: January 20, 2015
    Assignee: Alfa Laval Corporate AB
    Inventor: Jie Zheng
  • Patent number: 8925655
    Abstract: In an embodiment, a polycrystalline diamond compacts (“PDC”) includes a substrate and a polycrystalline diamond (“PCD”) table bonded to the substrate. The PCD table defines an upper surface and at least one peripheral surface. The PCD table includes a plurality of bonded diamond grains. The PCD table includes a first region adjacent to the substrate that includes a metallic constituent disposed interstitially between the bonded diamond grains thereof, and a leached second region extending inwardly from the upper surface and the at least one peripheral surface that is depleted of the metallic constituent. The leached second region exhibits a leach depth profile having a maximum leach depth that is measured from the upper surface. A leach depth of the leach depth profile decreases with lateral distance from a central axis of the PCD table and toward the at least one peripheral surface.
    Type: Grant
    Filed: October 22, 2013
    Date of Patent: January 6, 2015
    Assignee: US Synthetic Corporation
    Inventors: Mohammad N. Sani, Andrew E. Dadson
  • Patent number: 8925656
    Abstract: Diamond bonded construction comprise a diamond body attached to a support. In one embodiment, an initial substrate used to sinter the body is interposed between the body and support, and is thinned to less than 5 times the body thickness, or to less than the body thickness, prior to attachment to the support to relieve stress in the body. In another embodiment, the substrate is removed after sintering, and the body is attached to the support. The support has a material construction different from that of the initial substrate, wherein the initial substrate is selected for infiltration and the support for end use properties. The substrate and support include a hard material with a volume content that may be the same or different. Interfaces between the body, substrate, and/or support may be nonplanar. The body may be thermally stable, and may include a replacement material disposed therein.
    Type: Grant
    Filed: October 12, 2010
    Date of Patent: January 6, 2015
    Assignee: Smith International, Inc.
    Inventors: Yuelin Shen, Youhe Zhang
  • Patent number: 8919463
    Abstract: A polycrystalline-diamond cutting element for a drill bit of a downhole tool. The cutting element includes a substrate and a diamond table bonded to the substrate. The diamond table includes a diamond filler with at least one leached polycrystalline diamond segment packed therein along at least one working surface thereof. The cutting element may be formed by positioning the diamond table on the substrate and bonding the diamond table onto the substrate such that the polycrystalline diamond segment is positioned along at least one working surface of the diamond table. A spark plasma sintering or double press operation may be used to bond the diamond table onto the substrate.
    Type: Grant
    Filed: October 24, 2011
    Date of Patent: December 30, 2014
    Assignee: National Oilwell DHT, L.P.
    Inventors: Deepthi Raj Setlur, Michael D. Hughes, Mark Jonathan Francis, Harold A. Sreshta, Guodong Zhan, Russell C. Gilleylen, JiinJen Albert Sue
  • Patent number: 8910730
    Abstract: A cutting element includes a multilayer polycrystalline diamond element bonded to a substrate of a less hard material. The polycrystalline diamond element defines a matrix of interstitial volumes. The interstitial volumes of a first region of the diamond layer are adjacent a working surface thereof being substantially free of a catalyzing material. The interstitial volumes of a second region of the diamond layer are remote from the working surface containing the catalyzing material.
    Type: Grant
    Filed: February 11, 2010
    Date of Patent: December 16, 2014
    Assignee: National Oilwell Varco, L.P.
    Inventors: Nigel D. Griffin, Peter R. Hughes
  • Patent number: 8899358
    Abstract: A method of forming a cutting element is disclosed, wherein the method includes forming a substrate body, forming an intermediate layer on the substrate body, forming a diamond table, and positioning the diamond table on the intermediate layer, such that the intermediate layer is disposed between the substrate body and the diamond table. The intermediate layer has a base portion having a base height and a ring portion having a ring height HR, wherein the intermediate layer has a height HT equal to the sum of the base height and ring height. The diamond table has a cutting layer having a cutting layer diameter D1 and a cutting layer height HE and a protrusion having a protrusion diameter D2 and a protrusion height HP.
    Type: Grant
    Filed: October 27, 2011
    Date of Patent: December 2, 2014
    Assignee: Smith International, Inc.
    Inventors: Feng Yu, Yi Fang
  • Patent number: 8899357
    Abstract: Various downhole drilling tools designed and manufactured at least in part on evaluating respective forces acting on respective groups and sets of cutting elements during simulated engagement with the downhole end of a wellbore and drilling from a first downhole formation into a second downhole formation. Simulating forces acting on each cutting element as the cutting element contacts a downhole formation may be used to force balance downhole drilling tools during transition drilling or non-uniform downhole drilling conditions. Multilevel force balanced downhole drilling tools may be designed using five respective simulations, cutter group level, neighbor cutter group level, cutter set level, group of N (N=3 or N=4) consecutive cutters level and all cutters level. Various cutter layout procedures and algorithms may also be used to design multilevel force balanced downhole drilling tools which may drill faster with higher lateral stability, especially during downhole transiting drilling conditions.
    Type: Grant
    Filed: December 9, 2009
    Date of Patent: December 2, 2014
    Assignee: Halliburton Energy Services, Inc.
    Inventor: Shilin Chen
  • Patent number: 8887837
    Abstract: A downhole cutting tool may include a tool body; a plurality of blades extending azimuthally from the tool body; and a plurality of cutting elements disposed on the plurality of blades, the plurality of cutting elements comprising: at least two non-planar cutting elements comprising a substrate and a diamond layer having a non-planar cutting end, wherein at least one of the at least two conical cutting elements has a positive back rake angle or positive side rake angle, and at least one of the at least two non-planar cutting elements has a negative back rake angle or a negative side rake angle.
    Type: Grant
    Filed: March 14, 2013
    Date of Patent: November 18, 2014
    Assignee: Smith International, Inc.
    Inventors: Michael G. Azar, Bala Durairajan, Madapusi K. Keshavan
  • Patent number: 8882869
    Abstract: Methods of forming a polycrystalline element comprise forming a polycrystalline table on a first substrate. Catalyst material may be removed from at least a portion of the polycrystalline table. The polycrystalline table and a portion of a first substrate attached to the polycrystalline table may be removed from a remainder of the first substrate. The portion of the first substrate may be attached to another substrate. Polycrystalline elements comprise a polycrystalline table attached to a portion of a first substrate on which the polycrystalline table was formed another substrate attached to the portion of the first substrate.
    Type: Grant
    Filed: March 4, 2011
    Date of Patent: November 11, 2014
    Assignee: Baker Hughes Incorporated
    Inventors: Anthony A. DiGiovanni, Nicholas J. Lyons, Derek L. Nelms, Danny E. Scott
  • Patent number: 8881851
    Abstract: Thermally-stable polycrystalline diamond materials comprise a first phase including a plurality of bonded together diamond crystals, and a second phase including a reaction product formed between a binder/catalyst material and a material reactive with the binder/catalyst material. The reaction product is disposed within interstitial regions of the polycrystalline diamond material that exists between the bonded diamond crystals. The first and second phases are formed during a single high pressure/high temperature process condition. The reaction product has a coefficient of thermal expansion that is relatively closer to that of the bonded together diamond crystals than that of the binder/catalyst material.
    Type: Grant
    Filed: December 31, 2008
    Date of Patent: November 11, 2014
    Assignee: Smith International, Inc.
    Inventors: John Daniel Belnap, Stewart N. Middlemiss, Anthony Griffo, Thomas W. Oldham, Kumar T. Kembaiyan
  • Patent number: 8875812
    Abstract: A polycrystalline diamond cutting (PDC) element of a drill bit of a downhole drilling tool is provided. The PDC element having a substrate, a diamond table and at least one pattern. The diamond table has an initial cutting edge along a periphery thereof. The pattern integrally formed within the diamond table. The pattern(s) defining at least one discontinuity about the diamond table that, in operation, selectively breaks away upon impact to create new cutting edges in the diamond table whereby a sharp cutting edge is continuously exposed to a material being cut.
    Type: Grant
    Filed: July 22, 2011
    Date of Patent: November 4, 2014
    Assignee: National Oilwell DHT, L.P.
    Inventors: Deepthi Raj Setlur, John Christopher Troncoso, Michael D. Hughes
  • Patent number: 8875814
    Abstract: The disclosure provides a super abrasive element containing a substantially catalyst-free thermally stable polycrystalline diamond (TSP) body having pores and a contact surface, a base adjacent the contact surface of the TSP body; and an infiltrant material infiltrated in the base and in the pores of the TSP body at the contact surface. The disclosure additionally provides earth-boring drill bits and other devices containing such super abrasive elements. The disclosure further provides methods and mold assemblies for forming such super abrasive elements via infiltration and hot press methods.
    Type: Grant
    Filed: April 26, 2012
    Date of Patent: November 4, 2014
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Brian Atkins, Seth G. Anderle, Robert W. Arfele, Ram L. Ladi, Brandon Paul Linford, Jason Keith Wiggins, Kevin Duy Nguyen, Jiang Qian, Kenneth Eugene Bertagnolli, Shawn Casey Scott, Debkumar Mukhopadhyay, Michael Alexander Vail
  • Patent number: 8875813
    Abstract: A sintered body for cutting tools that includes hard particle phase comprising a plurality of hard particles, wherein at least a portion of the hard phase particles comprise a coating deposited by atomic layer deposition disposed thereon; and a binder phase is disclosed. The hard particles that may be included in the sintered bodies may include tungsten carbide, diamond, and boron nitride particles.
    Type: Grant
    Filed: September 21, 2007
    Date of Patent: November 4, 2014
    Assignee: Smith International, Inc.
    Inventors: Guodong Zhan, Youhe Zhang, Feng Yu, Xian Yao, J. Daniel Belnap, Yuelin Shen, Madapusi K. Keshavan
  • Publication number: 20140311810
    Abstract: A polycrystalline diamond composite compact element comprises a body of polycrystalline diamond material and a cemented carbide substrate bonded to the body of polycrystalline material. The cemented carbide substrate has tungsten carbide particles bonded together by a binder material comprising an alloy of Co, Ni and Cr. The tungsten carbide particles form between 70 weight percent and 95 weight percent of the substrate. The binder material comprises between about 10 to 50 wt. % Ni, between about 0.1 to 10 wt. % Cr, and the remainder weight percent comprising Co. The size distribution of the tungsten carbide particles in the substrate has fewer than 17 percent of the carbide particles with a grain size of equal to or less than about 0.3 microns, between about 20 to 28 percent of the tungsten carbide particles having a grain size of between about 0.3 to 0.5 microns; between about 42 to 56 percent of the tungsten carbide particles having a grain size of between about 0.
    Type: Application
    Filed: December 13, 2012
    Publication date: October 23, 2014
    Inventors: Igor Yurievich Konyashin, Bernd Heinrich Ries, Frank Friedrich Lachmann
  • Patent number: 8857541
    Abstract: An insert for a drill bit may include a metallic carbide body; an outer layer of polycrystalline diamond material on the outermost end of the insert, the polycrystalline diamond material comprising a plurality of interconnected first diamond grains and a first binder material in interstitial regions between the interconnected first diamond grains; and at least two transition layers between the metallic carbide body and the outer layer, the at least two transition layers comprising: an outermost transition layer comprising a composite of second diamond grains, first metal carbide or carbonitride particles, and a second binder material; and an innermost transition layer comprising a composite of third diamond grains, second metal carbide or carbonitride particles, and a third binder material wherein a thickness of the outer layer is lesser than that of each of the at least two transition layers.
    Type: Grant
    Filed: August 6, 2010
    Date of Patent: October 14, 2014
    Assignee: Smith International, Inc.
    Inventors: Nephi M. Mourik, Peter T. Cariveau, Michael Stewart, Frederico Bellin, Yi Fang
  • Patent number: 8852546
    Abstract: PCD materials comprise a diamond body having bonded diamond crystals and interstitial regions disposed among the crystals. The diamond body is formed from diamond grains and a catalyst material at high pressure/high temperature conditions. The diamond grains have an average particle size of about 0.03 mm or greater. At least a portion of the diamond body has a high diamond volume content of greater than about 93 percent by volume. The entire diamond body can comprise high volume content diamond or a region of the diamond body can comprise the high volume content diamond. The diamond body includes a working surface, a first region substantially free of the catalyst material, and a second region that includes the catalyst material. At least a portion of the first region extends from the working surface to depth of from about 0.01 to about 0.1 mm.
    Type: Grant
    Filed: November 13, 2012
    Date of Patent: October 7, 2014
    Assignee: Smith International, Inc.
    Inventors: Madapusi K. Keshavan, Youhe Zhang, Yuelin Shen, Anthony Griffo, Michael Janssen
  • Patent number: 8851206
    Abstract: A superabrasive cutter including a superabrasive table having a cutting face in non-perpendicular orientation with respect to a longitudinal axis of the cutter. A superabrasive cutter having a cutting face of a superabrasive table in non-parallel orientation to a back surface thereof.
    Type: Grant
    Filed: December 4, 2012
    Date of Patent: October 7, 2014
    Assignee: Baker Hughes Incorporated
    Inventor: Suresh G. Patel
  • Patent number: 8851208
    Abstract: A cutting element for an earth-boring drill bit may include a thermally stable cutting table comprising a polycrystalline diamond material. The polycrystalline diamond material may consist essentially of a matrix of diamond particles bonded to one another and a silicon, silicon carbide, or silicon and silicon carbide material located within interstitial spaces among interbonded diamond particles of the matrix of diamond particles. The cutting table may be at least substantially free of Group VIII metal or alloy catalyst material. The cutting element may further include a substrate and an adhesion material between and bonded to the cutting table and the substrate. The adhesion material may include diamond particles bonded to one another and to the cutting table and the substrate after formation of the preformed cutting table.
    Type: Grant
    Filed: October 24, 2013
    Date of Patent: October 7, 2014
    Assignee: Baker Hughes Incorporated
    Inventor: Danny E. Scott
  • Patent number: 8839889
    Abstract: Methods of forming a polycrystalline diamond compact for use in an earth-boring tool include forming a body of polycrystalline diamond material including a first material disposed in interstitial spaces between inter-bonded diamond crystals in the body, removing the first material from interstitial spaces in a portion of the body, selecting a second material promoting a higher rate of degradation of the polycrystalline diamond compact than the first material under similar elevated temperature conditions and providing the second material in interstitial spaces in the portion of the body. Methods of drilling include engaging at least one cutter with a formation and wearing a second region of polycrystalline diamond material comprising a second material faster than the first region of polycrystalline diamond material comprising a first material. Polycrystalline diamond compacts and earth-boring tools including such compacts are also disclosed.
    Type: Grant
    Filed: April 26, 2011
    Date of Patent: September 23, 2014
    Assignees: Baker Hughes Incorporated, Element Six Ltd
    Inventors: Anthony A. DiGiovanni, Iain P. Goudemond
  • Patent number: 8840831
    Abstract: A method of producing a PCD body includes the step of providing a region of coarser diamond particles between a source of binder phase and a region of fine grained diamond particles having a particle size less than 2 ?m. The binder phase is caused to infiltrate the diamond mass through the region of coarser diamond particles under elevated temperature and pressure conditions suitable to produce PCD. The invention further provides for a PCD diamond composite manufactured by the method of the invention wherein the PCD body is substantially free of abnormal diamond growth.
    Type: Grant
    Filed: May 6, 2008
    Date of Patent: September 23, 2014
    Inventors: Geoffrey John Davies, Gerrard Peters
  • Patent number: 8820442
    Abstract: In various embodiments, a polycrystalline diamond compact (“PDC”) comprises a substrate including an interfacial surface having a raised region. In an embodiment, a PDC comprises a substrate including an interfacial surface having a generally cylindrical raised region and a peripheral region extending about the generally cylindrical raised region. The generally cylindrical raised region extends to a height above the peripheral region of about 450 ?m or less. The PDC includes a PCD table bonded to the interfacial surface of the substrate. The PCD table includes an upper surface and at least one peripheral surface, and includes a plurality of bonded diamond grains defining interstitial regions. At least a portion of the interstitial regions includes a metallic constituent therein. In another embodiment, instead of employing a generally cylindrical raised region, the interfacial surface may include a plurality of raised arms extending above the face. Each raised arm extends radially and circumferentially.
    Type: Grant
    Filed: March 1, 2011
    Date of Patent: September 2, 2014
    Assignee: US Synthetic Corporation
    Inventors: Jair J. Gonzalez, Neil D. Haddock
  • Patent number: 8814966
    Abstract: In an embodiment, a polycrystalline diamond compact includes a substrate and a preformed polycrystalline diamond body bonded to the substrate. The preformed polycrystalline diamond body includes a plurality of bonded diamond grains. The preformed polycrystalline diamond body further includes an infiltrant comprising at least one interstitial carbide phase. Rotary drill bits for drilling a subterranean formation including such polycrystalline diamond compacts and methods of fabricating such polycrystalline diamond compacts are also disclosed.
    Type: Grant
    Filed: June 29, 2011
    Date of Patent: August 26, 2014
    Assignee: US Synthetic Corporation
    Inventors: Kenneth E. Bertagnolli, David P. Miess
  • Patent number: 8813878
    Abstract: Embodiments relate to PDCs, methods of fabricating PDCs, and applications for such PDCs. In an embodiment, a PDC includes a substrate and a pre-sintered PCD table including an interfacial surface that is bonded to the substrate. The pre-sintered PCD table may be substantially free of leaching by-products in a region at least proximate to the interfacial surface. In an embodiment, a method of fabricating a PDC includes providing an at least partially leached PCD including an interfacial surface. The method includes removing at least some leaching by-products from the at least partially leached PCD table. After removing the at least some leaching by-products, the method includes bonding the interfacial surface of the at least partially leached PCD table to a substrate to form a PDC.
    Type: Grant
    Filed: November 1, 2010
    Date of Patent: August 26, 2014
    Assignee: US Synthetic Corporation
    Inventors: Michael A. Vail, Kenneth E. Bertagnolli
  • Patent number: 8800692
    Abstract: Cutting elements for earth-boring tools may generate a shear lip at a wear scar thereon during cutting. A diamond table may exhibit a relatively high wear resistance, and an edge of the diamond table may be chamfered, the combination of which may result in the formation of a shear lip. Cutting elements may comprise multi-layer diamond tables that result in the formation of a shear lip during cutting. Earth-boring tools include such cutting elements. Methods of forming cutting elements may include selectively designing and configuring the cutting elements to form a shear lip. Methods of cutting a formation using an earth-boring tool include cutting the formation with a cutting element on the tool, and generating a shear lip at a wear scar on the cutting element. The cutting element may be configured such that the shear lip comprises diamond material of the cutting element.
    Type: Grant
    Filed: October 1, 2010
    Date of Patent: August 12, 2014
    Assignees: Baker Hughes Incorporated, Element Six Ltd
    Inventors: Danny E. Scott, Marcus R. Skeem, Jeffrey B. Lund, John H. Liversage, Moosa Mahomed Adia
  • Patent number: 8800693
    Abstract: Polycrystalline compacts include non-catalytic, non-carbide-forming particles in interstitial spaces between interbonded grains of hard material in a polycrystalline hard material. Cutting elements and earth-boring tools include such polycrystalline compacts. Methods of forming polycrystalline compacts include forming a polycrystalline material including a hard material and a plurality of particles comprising a non-catalytic, non-carbide-forming material. Methods of forming cutting elements include infiltrating interstitial spaces between interbonded grains of hard material in a polycrystalline material with a plurality of non-catalytic, non-carbide-forming particles.
    Type: Grant
    Filed: September 6, 2011
    Date of Patent: August 12, 2014
    Assignee: Baker Hughes Incorporated
    Inventor: Anthony A. DiGiovanni
  • Patent number: 8789626
    Abstract: The invention provides for an ultra hard or hard composite material comprising a primary ultra hard or hard particulate material and at least one secondary ultra hard or hard particulate material dispersed in a matrix material. The primary ultra hard or hard particulate material has a thermal expansion coefficient lower than that of the matrix material and the at least one secondary ultra hard or hard particulate material has a thermal expansion coefficient greater than that of the matrix material.
    Type: Grant
    Filed: December 18, 2009
    Date of Patent: July 29, 2014
    Inventors: Antionette Can, Geoffrey John Davies, Johannes Lodewikus Myburgh
  • Patent number: 8790430
    Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) comprising a preformed polycrystalline diamond (“PCD”) table including a thermally-stable region having a copper-containing material disposed interstitially between bonded diamond grains thereof, and methods of fabricating such PDCs. In an embodiment, a PDC includes a substrate, and a preformed PCD table having an interfacial surface bonded to the substrate and a generally opposing upper surface. The PCD table includes a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween and defining a plurality of interstitial regions. The preformed PCD table further includes a first region extending inwardly from the upper surface that includes a copper-containing material disposed therein and a second region extending inwardly from the interfacial surface that includes a nickel-containing material disposed therein.
    Type: Grant
    Filed: November 30, 2012
    Date of Patent: July 29, 2014
    Assignee: US Synthetic Corporation
    Inventors: David P. Miess, Michael A. Vail, Kenneth E. Bertagnolli, C. Eugene McMurray, Paul Douglas Jones
  • Patent number: 8789627
    Abstract: Disclosed are a high impact/high abrasion cutter and a method for manufacture. The high impact/high abrasion cutter includes a plurality of preformed polycrystalline abrasive bodies sintered under high temperature/high pressure conditions to form an abrasive cutting table. The impact and abrasion resistance of a cutter can simultaneously be improved through forming a cutting table from larger preformed polycrystalline sintered particles formed from finer grain particles. Such a cutter can be manufactured through the steps of preforming the polycrystalline abrasive bodies, forming a mixture of said polycrystalline abrasive bodies and sintering said mixture under high temperature/high pressure conditions.
    Type: Grant
    Filed: July 17, 2005
    Date of Patent: July 29, 2014
    Assignee: US Synthetic Corporation
    Inventors: Mohammad Sani, Ken Bertagnolli, Eric Pope
  • Patent number: 8783389
    Abstract: A method for facilitating infiltration of an infiltrant material into a TSP material during re-bonding of the TSP material to a substrate, by enhancing the porosity of the TSP material near the interface with the substrate is provided. Cutting elements formed by such method and downhole tools including such cutting elements are also provided.
    Type: Grant
    Filed: June 18, 2010
    Date of Patent: July 22, 2014
    Assignee: Smith International, Inc.
    Inventors: Guojiang Fan, Feng Yu, Yi Fang, J. Daniel Belnap, Peter T. Cariveau
  • Patent number: 8763731
    Abstract: Polycrystalline compacts include a hard polycrystalline material comprising first and second regions. The first region comprises a first plurality of grains of hard material having a first average grain size, and a second plurality of grains of hard material having a second average grain size smaller than the first average grain size. The first region comprises catalyst material disposed in interstitial spaces between inter-bonded grains of hard material. Such interstitial spaces between grains of the hard material in the second region are at least substantially free of catalyst material. In some embodiments, the first region comprises a plurality of nanograins of the hard material. Cutting elements and earth-boring tools include such polycrystalline compacts.
    Type: Grant
    Filed: June 17, 2011
    Date of Patent: July 1, 2014
    Assignee: Baker Hughes Incorporated
    Inventors: Danny E. Scott, Anthony A. DiGiovanni
  • Patent number: 8763730
    Abstract: Diamond bonded constructions comprise a body comprising a plurality of bonded together diamond grains with interstitial regions disposed between the grains that are substantially free of the catalyst material used to initially sinter the body. A metallic substrate is attached to the body, and a braze joint is interposed between the body and the substrate. The body is metallized to include a metallic material disposed along a substrate attachment surface in contact with the braze joint, wherein the metallic material is different from the braze joint material. The metallic material may exist within a region of the body extending fully or partially into the body, and/or may exist as a layer extending away from the substrate attachment surface. The body includes a working surface characterized by empty interstitial regions or by interstitial regions filled with an infiltrant material, wherein the infiltrant material is different from the metallizing material.
    Type: Grant
    Filed: May 28, 2009
    Date of Patent: July 1, 2014
    Assignee: Smith International, Inc.
    Inventors: Peter Cariveau, Georgiy Voronin, J. Daniel Belnap
  • Patent number: 8764862
    Abstract: The disclosure provides a super abrasive element containing a substantially catalyst-free thermally stable polycrystalline diamond (TSP) body having pores and a contact surface, a base adjacent the contact surface of the TSP body; and an infiltrant material infiltrated in the base and in the pores of the TSP body at the contact surface. The disclosure additionally provides earth-boring drill bits and other devices containing such super abrasive elements. The disclosure further provides methods and mold assemblies for forming such super abrasive elements via infiltration and hot press methods.
    Type: Grant
    Filed: April 26, 2012
    Date of Patent: July 1, 2014
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Brian Atkins, Seth G. Anderle, Robert W. Arfele, Ram L. Ladi, Brandon Paul Linford, Jason Keith Wiggins, Kevin Duy Nguyen, Jiang Qian, Kenneth Eugene Bertagnolli, Shawn Casey Scott, Debkumar Mukhopadhyay, Michael Alexander Vail
  • Patent number: 8757299
    Abstract: A cutting element for use in a drilling bit and/or milling bit having a cutter body made of a substrate having an upper surface, and a superabrasive layer overlying the upper surface of the substrate. The cutting element further including a sleeve extending around a portion of a side surface of the superabrasive layer and a side surface of the substrate, wherein the sleeve exerts a radially compressive force on the superabrasive layer.
    Type: Grant
    Filed: July 8, 2010
    Date of Patent: June 24, 2014
    Assignees: Baker Hughes Incorporated, Element Six (Production) (Pty) Ltd., Element Six Limited
    Inventors: Anthony A. DiGiovanni, Nicholas J. Lyons, Matthew S. Hale, Konstantin E. Morozov, John H. Liversage, Danny E. Scott, Allen Sinor
  • Publication number: 20140165476
    Abstract: A polycrystalline diamond construction comprising a body of polycrystalline diamond material is formed of a mass of diamond grains exhibiting inter-granular bonding and defining a plurality of interstitial regions therebetween, and a non-diamond phase at least partially filling a plurality of the interstitial regions to form non-diamond phase pools, the non-diamond phase pools each having an individual cross-sectional area. The percentage of non-diamond phase in the total area of a cross-section of the body of polycrystalline diamond material and the mean of the individual cross-sectional areas of the non-diamond phase pools in the image analysed using an image analysis technique at a selected magnification is less than 0.7, or less than 0.340 microns squared, or between around 0.005 to 0.340 microns squared depending on the percentage of non-diamond phase in the total area of the cross-section of the polycrystalline diamond construction. There is also disclosed a method of making such a construction.
    Type: Application
    Filed: August 1, 2012
    Publication date: June 19, 2014
    Applicants: ELEMENT SIX LIMITED, ELEMENT SIX ABRASIVES S.A.
    Inventors: Nedret Can, Michael Lester Fish
  • Patent number: 8752656
    Abstract: A bottom hole assembly containing a drill bit. The drill bit additionally has a plurality of primary cutter elements mounted thereto. The plurality of cutter elements comprise one or more first cutter elements and one or more second cutter elements. The second cutter element differs from the first cutter element in at least one cutter element property. The first cutter element has a diamond body containing a first region comprising an infiltrant material disposed within the interstitial regions. The first region is located remote from the working surface of the diamond body. The first cutter element also contains a second region comprising interstitial regions that are substantially free of the infiltrant material. The second region is located along at least the working surface of the diamond body. Also included are a cutter element, method of designing a bottom hole assembly as well as method of designing a drill bit.
    Type: Grant
    Filed: December 17, 2009
    Date of Patent: June 17, 2014
    Assignee: Smith International, Inc.
    Inventors: Youhe Zhang, Yuelin Shen, Madapusi K Keshavan, Peter T Cariveau
  • Patent number: 8746376
    Abstract: Embodiments relate to methods of fabricating PCD materials by subjecting a mixture that exhibits a broad diamond particle size distribution to an HPHT process, PCD materials so-formed, and PDCs including a polycrystalline diamond table comprising such PCD materials. In an embodiment, a PCD material includes a plurality of bonded diamond grains that exhibit a substantially unimodal diamond grain size distribution characterized, at least in part, by a parameter ? that is less than about 1.0. ? = x 6 · ? , where x is the average grain size of the substantially unimodal diamond grain size distribution, and ? is the standard deviation of the substantially unimodal diamond grain size distribution.
    Type: Grant
    Filed: December 20, 2012
    Date of Patent: June 10, 2014
    Assignee: US Synthetic Corporation
    Inventors: Michael A. Vail, Kenneth E. Bertagnolli, Jason Wiggins, Jiang Qian, David P. Miess
  • Patent number: 8740048
    Abstract: Thermally stable polycrystalline constructions comprise a body having a polycrystalline ultra-hard phase and a plurality of empty voids. A population of the voids can be filled with a reaction product. The body is substantially free of a catalyst material. The construction comprises a first support member attached to the body by a first braze material. A second support member is attached to the body and the first support member by a second braze material. The construction may include a third support member attached to the body that is integral or separate from one of the other support members. The braze materials used to attached the support members can be the same or different, as can be the materials used to form the different support members.
    Type: Grant
    Filed: June 29, 2010
    Date of Patent: June 3, 2014
    Assignee: Smith International, Inc.
    Inventors: Georgiy Voronin, J. Daniel Belnap
  • Patent number: 8741007
    Abstract: Embodiments of the invention relate to thermally-stable polycrystalline diamond (“PCD”) elements, polycrystalline diamond compacts (“PDCs”), and methods of fabricating such PCD elements and PDCs. In an embodiment, a method of fabricating a thermally-stable PCD element includes providing an at least partially leached PCD body including a plurality of interstitial regions, and infiltrating at least a portion of the interstitial regions of the at least partially leached PCD body with at least a portion of an infiltrant material. The infiltrant material may include at least one member chosen from the group of glass, silicone, and a ceramic having a negative coefficient of thermal expansion.
    Type: Grant
    Filed: October 18, 2012
    Date of Patent: June 3, 2014
    Assignee: US Synthetic Corporation
    Inventors: David P. Miess, Craig H. Cooley
  • Patent number: 8727046
    Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”) that are less susceptible to liquid metal embrittlement damage due to the use of at least one transition layer between a polycrystalline diamond (“PCD”) layer and a substrate. In an embodiment, a PDC includes a PCD layer, a cemented carbide substrate, and at least one transition layer bonded to the substrate and the PCD layer. The at least one transition layer is formulated with a coefficient of thermal expansion (“CTE”) that is less than a CTE of the substrate and greater than a CTE of the PCD layer. At least a portion of the PCD layer includes diamond grains defining interstitial regions and a metal-solvent catalyst occupying at least a portion of the interstitial regions. The diamond grains and the catalyst collectively exhibit a coercivity of about 115 Oersteds or more and a specific magnetic saturation of about 15 Gauss·cm3/grams or less.
    Type: Grant
    Filed: April 15, 2011
    Date of Patent: May 20, 2014
    Assignee: US Synthetic Corporation
    Inventors: David P. Miess, Kenneth E. Bertagnolli, Damon B. Crockett, Arnold D. Cooper
  • Patent number: 8727045
    Abstract: Embodiments of the invention relate to polycrystalline diamond compact (“PDC”) including a polycrystalline diamond (“PCD”) table that bonded to a cobalt-nickel alloy cemented carbide substrate. The cobalt-nickel alloy cemented carbide substrate provides both erosion resistance and corrosion resistance to the cemented carbide substrate. In an embodiment, a PDC includes a cemented carbide substrate including cobalt-nickel alloy cementing constituent. The PDC further includes a PCD table bonded to the cemented carbide substrate.
    Type: Grant
    Filed: February 23, 2011
    Date of Patent: May 20, 2014
    Assignee: US Synthetic Corporation
    Inventors: Debkumar Mukhopadhyay, Kenneth E. Bertagnolli
  • Patent number: 8727042
    Abstract: Polycrystalline compacts include smaller and larger hard grains that are interbonded to form a polycrystalline hard material. The larger grains may be at least about 150 times larger than the smaller grains. An interstitial material comprising one or more of a boride, a carbide, a nitride, a metal carbonate, a metal bicarbonate, and a non-catalytic metal may be disposed between the grains. The compacts may be used as cutting elements for earth-boring tools such as drill bits, and may be disposed on a substrate.
    Type: Grant
    Filed: September 11, 2009
    Date of Patent: May 20, 2014
    Assignee: Baker Hughes Incorporated
    Inventor: Anthony A. DiGiovanni
  • Patent number: 8727044
    Abstract: In an embodiment, a polycrystalline diamond compact (“PDC”) includes a substrate and a pre-sintered polycrystalline diamond (“PCD”) table bonded to the substrate. The pre-sintered PCD table includes an upper surface, a back surface bonded to the substrate, and at least one lateral surface extending between the upper surface and the back surface. The pre-sintered PCD table includes a region including at least a residual amount of at least one interstitial constituent disposed in at least a portion of the interstitial regions thereof, and a bonding region. The at least one interstitial constituent includes at least one metal carbonate and/or at least one metal oxide. The region extends inwardly from the upper surface and the at least one lateral surface.
    Type: Grant
    Filed: March 24, 2011
    Date of Patent: May 20, 2014
    Assignee: US Synthetic Corporation
    Inventors: Jiang Qian, Kenneth E. Bertagnolli, Jair J. Gonzalez, Craig H. Cooley
  • Patent number: 8720609
    Abstract: A method of optimizing drill bit design and an optimized drill bit for drilling a well into an earth formation comprising a bit body; a number of blades spaced around the bit body, each blade having a curved outer edge and a forward face; a first row of cutter pockets recessed into the face along the outer edge of each blade; a second group of cutter pockets recessed into the face of each blade offset from the first row; and a plurality of cutting elements, each cutting element being brazed into a different one of the cutter pockets.
    Type: Grant
    Filed: October 13, 2008
    Date of Patent: May 13, 2014
    Assignee: Baker Hughes Incorporated
    Inventors: Robert M. Welch, Eric E. McClain, L. Allen Sinor
  • Patent number: 8695733
    Abstract: PCD inserts comprise a PCD body having multiple FG-PCD regions with decreasing diamond content moving from a body outer surface to a metallic substrate. The diamond content changes in gradient fashion by changing metal binder content. A region adjacent the outer surface comprises 5 to 20 percent by weight metal binder, and a region remote from the surface comprises 15 to 40 percent by weight metal binder. One or more transition regions are interposed between the PCD body and substrate. The transition region comprises PCD, binder metal, and a carbide, comprises a metal binder content less than that present in the PCD body region positioned next to it.
    Type: Grant
    Filed: August 6, 2010
    Date of Patent: April 15, 2014
    Assignee: Smith International, Inc.
    Inventors: Yi Fang, Federico Bellin, Michael Stewart, Nephi A Mourik, Peter T Cariveau
  • Patent number: 8689912
    Abstract: Diamond bonded constructions include a diamond body comprising intercrystalline bonded diamond and interstitial regions. The body has a working surface and an interface surface, and may be joined to a metallic substrate. The body has a gradient diamond volume content greater about 1.5 percent, wherein the diamond content at the interface surface is less than 94 percent, and increases moving toward the working surface. The body may include a region that is substantially free of a catalyst material otherwise disposed within the body and present in a gradient amount. An additional material may be included within the body and be present in a changing amount. The body may be formed by high-pressure HPHT processing, e.g., from 6,200 MPa to 10,000 MPa, to produce a sintered body having a characteristic diamond volume fraction v. average grain size relationship distinguishable from that of diamond bonded constructions form by conventional-pressure HPHT processing.
    Type: Grant
    Filed: November 24, 2010
    Date of Patent: April 8, 2014
    Assignee: Smith International, Inc.
    Inventors: J. Daniel Belnap, Georgiy Voronin, Feng Yu, Peter Cariveau
  • Patent number: 8689909
    Abstract: An insert for an earth-boring tool includes a body and a coating disposed over at least a portion of the body. The coating comprises a ceramic comprising boron, aluminum, and magnesium. Polycrystalline diamond compact cutting elements may include a hard polycrystalline material, a supporting substrate, and a coating disposed over at least a portion of the hard polycrystalline material. An earth-boring drill bit may include a bit body and at least one polycrystalline diamond compact cutting element secured to the bit body. The polycrystalline diamond compact cutting element may have a coating comprising a ceramic of boron, aluminum, and magnesium, and may be disposed over at least a portion of a hard polycrystalline material. A method of forming an insert for an earth-boring tool may include forming a protective coating including a ceramic of boron, aluminum, and magnesium over a cutting element.
    Type: Grant
    Filed: October 17, 2011
    Date of Patent: April 8, 2014
    Assignee: Baker Hughes Incorporated
    Inventor: Anthony A. DiGiovanni
  • Patent number: 8672061
    Abstract: Polycrystalline ultra-hard compact constructions comprise a polycrystalline ultra-hard compact having a polycrystalline ultra-hard body attached to a substrate. A support member is attached to the compact by a braze material. The support member can have a one-piece construction including one or more support sections. The support member has a first section extending axially along a wall surface of the compact, and extending circumferentially along a portion of the compact. The support member can include a second section extending radially along a backside surface of the compact, and/or a third section extending radially along a front side surface of the compact. In one embodiment, the support member includes a second and/or third section and the compact disposed therein is in an axially compressed state. The support member is interposed between the compact and an end-use device to improve the compact attachment strength with respect to the end-use device.
    Type: Grant
    Filed: February 10, 2011
    Date of Patent: March 18, 2014
    Assignee: Smith International, Inc.
    Inventors: Georgiy Voronin, Nephi A Mourik, J. Daniel Belnap
  • Patent number: 8662209
    Abstract: A front face of a diamond table mounted to a substrate is processed, for example through an acid leach, to remove interstitial catalyst binder and form a thermal channel. A material is then introduced to the front face of the diamond table, the introduced material backfilling the front face of the diamond table to fill interstitial voids left by removal of the catalyst binder in the thermal channel to a desired depth. The material is selected to be less thermally expandable than the catalyst binder and/or more thermally conductive than the catalyst binder and/or having a lower heat capacity than the catalyst binder.
    Type: Grant
    Filed: March 2, 2010
    Date of Patent: March 4, 2014
    Assignee: Varel International, Ind., L.P.
    Inventors: Alfazazi Dourfaye, William W. King, Michael R. Reese
  • Patent number: 8662207
    Abstract: Rotary drag bits comprise a body comprising a face at a leading end of the body. An abrasive-impregnated cutting structure is located at the face of the bit body. The abrasive-impregnated cutting structure comprises abrasive particles dispersed within a matrix material. The abrasive-impregnated cutting structure exhibits an anisotropic wear resistance. The wear resistance varies at least substantially continuously within the abrasive-impregnated cutting structure.
    Type: Grant
    Filed: December 18, 2012
    Date of Patent: March 4, 2014
    Assignee: Baker Hughes Incorporated
    Inventors: Van J. Brackin, Jeffrey B. Lund, Danny E. Scott, Marcus R. Skeem, Matthew R. Isbell
  • Patent number: 8662210
    Abstract: In an embodiment, a rotary drill bit includes a bit body having a leading end structure configured to facilitate drilling a subterranean formation, and a plurality of cutting elements mounted to the bit body. At least one of the plurality of cutting elements includes a polycrystalline diamond compact (“PDC”) comprising a cemented carbide substrate including a first cemented carbide portion and a second cemented carbide portion bonded to the first cemented carbide portion and exhibiting an erosion resistance that is greater than the first cemented carbide portion. The PDC further comprises a polycrystalline diamond (“PCD”) table bonded to the first cemented carbide portion. The PCD table includes a plurality of bonded diamond grains exhibiting diamond-to-diamond bonding therebetween, with the plurality of bonded diamond grains defining a plurality of interstitial regions.
    Type: Grant
    Filed: April 10, 2013
    Date of Patent: March 4, 2014
    Assignee: US Synthetic Corporation
    Inventors: Debkumar Mukhopadhyay, Kenneth E. Bertagnolli, Jair J. Gonzalez