With Distilland Treating Devices Patents (Class 202/176)
  • Patent number: 5045155
    Abstract: The disclosed invention is an apparatus and process for the distillation of liquids. The apparatus is comprised of a plurality of vertically stacked parallel disks which are rotated in a horizontal plane. The liquid to be distilled is introduced into the center of the disk stack and migrates by centrifugal force as a thin film across the top surface of each disk. During migration, the more volatile portion evaporates from the top surface and condenses on the bottom surface of a top, neighboring disk. The apparatus is multiple-effect in that the heat evolved from condensation is transferred through the thin, heat-conducting disks to provide the heat necessary for vaporization.
    Type: Grant
    Filed: September 11, 1989
    Date of Patent: September 3, 1991
    Inventor: Arnold Ramsland
  • Patent number: 5037510
    Abstract: An integrated system provides combined space heating, water heating and water distillation. The system is adapted for supplying combined services to residential and commercial buildings. The system may be used in retrofitting existing space heating furnaces and/or water heaters to provide an energy and cost efficient combined system. A portable water heating/water distilling unit can be used with an existing portable self-contained heater.
    Type: Grant
    Filed: November 21, 1988
    Date of Patent: August 6, 1991
    Inventor: Nils Nygards
  • Patent number: 5031754
    Abstract: A hydrocarbon material of the starting product is separated in an extractive distillation column in which an N-substituted morpholine whose substituents do not have more than seven carbon atoms is used as a selective solvent. The overhead product comes down as a top product of the extractive distillation and is fed through a coalescer in which the sump product comes down with a solvent content of 20 to 75% by weight at a temperature of 20.degree. to 70.degree. C. and subsequent to that is fed into a separating vessel. There it is separated into a heavier and lighter phase. After that the heavier phase is conducted into an extractive distillation column and the lighter phase into the overhead product distillation column.
    Type: Grant
    Filed: January 19, 1990
    Date of Patent: July 16, 1991
    Assignee: Krupp Koppers GmbH
    Inventors: Gerd Emmrich, Hans-Christoph Schneider, Ulrich Rudel
  • Patent number: 5032230
    Abstract: A vacuum draft submerged combustion system and method for separating combustible hydrocarbons and other components or liquid solutions from their solvents, usually water, includes evaporating volatile components by a submerged combustion burner and condensing the vaporized volatile components under a partial vacuum. The hot gases from the burner are injected under partial vacuum into the first tank. The hot gases bubbled through the solution cause volatile components in the liquid to be evaporated and collected above the level of the liquid. The collected gasses are drawn into a condensing tank where the condensable particulates are condensed and collected.
    Type: Grant
    Filed: August 22, 1988
    Date of Patent: July 16, 1991
    Assignee: Deep Woods, Inc.
    Inventor: Richard C. Shepherd
  • Patent number: 4985122
    Abstract: Method and apparatus for separating volatile contaminants from a liquid to be continuously distilled. A continuous still comprises evaporator (1) having a heating coil (2), and condensor coil (6), and distillate collector (5). An entrainment device (11) removes distillate (13) from collector (5) via line (10) and reduces pressure in evaporator (1). Feed liquid (21) containing volatile contaminants is charged batchwise to a pre-chamber (20) at sub-atmospheric pressure which is then sealed (valve 22) from feed supply (21). Volatile contaminants are extracted from the charge in prechamber (20) via line (26) and entrainment device (32). Pre-chamber (20) is subsequently placed in communication (via valve 25) with evaporator (1) whereby to equilibrate pressure between evaporator (1) and pre-chamber (20).
    Type: Grant
    Filed: December 16, 1988
    Date of Patent: January 15, 1991
    Assignee: Vaqua Limited
    Inventor: Colin W. Spencer
  • Patent number: 4976824
    Abstract: An apparatus for fluid distillation in general, and in particular, or water, adapted for consumer or home use, but capable of being made and operated so that it is suitable for separating solvents and solutes and other industrial use. The apparatus includes a housing having divider structure to form one or more compartments for receiving water to be distilled. The divider structure also presents a fluid passage for receiving water vapor which is formed when the upper portion of the water in the housing is boiled by a heater. An aerator is provided in the housing below the heater and in a location within the water compartment. The aerator operates to direct air under a slight pressure into the water so that air bubbles can be generated in the water. The air bubbles will rise and break the surface of the water as the upper part of the water is being boiled by the heater.
    Type: Grant
    Filed: December 22, 1989
    Date of Patent: December 11, 1990
    Inventor: Naisin Lee
  • Patent number: 4975154
    Abstract: A distillation type of water purification system has a raw water inlet valve for admitting raw water continuously to a boiling tank at a rate greater than the rate at which raw water is converted to treated water. A drain valve located at the bottom of the boiling tank is energized by a raw water level sensing means whenever the raw water level reaches a predetermined level, to discharge water from the boiling tank. Treated water is stored in a storage tank having a pump for discharging treated water to the user upon demand. A single conductivity sensor in the storage tank controls the pump to allow it to operate only if the sensed conductivity is above a first predetermined value but not at or above a second predetermined value greater than the first value. An improved condenser has two sets of tubes, each set is arranged in a pair of planes oriented transverse the flow of cooling air with the tubes parallel. The internal cross-sectional area of one set is about twice that of the other.
    Type: Grant
    Filed: November 16, 1987
    Date of Patent: December 4, 1990
    Assignee: Pure Water, Inc.
    Inventors: David G. Palmer, David J. Shannon, Keith L. Vacha
  • Patent number: 4963231
    Abstract: Process for the evaporative concentration of liquids. Vaporization is carried out by indirect heat exchange with a heating fluid in an evaporator. The vapor produced in the evaporator is thereafter condensed in a condenser by indirect heat exchange with a cooling liquid which is mainly composed of the liquid to be concentrated or the liquid which has already been concentrated in the evaporator. The vapor pressure over the cooling liquid in the condenser may be lowered by causing gas to flow in contact with the cooling liquid.
    Type: Grant
    Filed: June 13, 1988
    Date of Patent: October 16, 1990
    Assignee: Ahlstromforetagen Svenska AB
    Inventor: Rolf Ryham
  • Patent number: 4954222
    Abstract: A dry cleaning solvent recovery and filtering system includes a dry cleaning solvent tank containing solvent for use in a dry cleaning machine. A filtration path from the tank includes a centrifugal separator for removing coarse debris and a filter element for removing fine debris from the solvent fluid. The filter element includes a perforated metal cylinder, having an open mouth, with a Teflon.RTM. coated screen forming the interior debris collection surface. A rinsing spray nozzle situated at the mouth of the filter element directs a fluid spray under pressure against the collection surface in the same direction that debris contaminated solvent fluid flows therethrough. The pressure of the fluid spray is sufficient to dislodge fine debris adhered to the collection surface without forcing the debris into the perforations of the filter element.
    Type: Grant
    Filed: November 18, 1988
    Date of Patent: September 4, 1990
    Inventors: Larry L. Durr, B. Jan Clay, Larry J. Durr
  • Patent number: 4950363
    Abstract: A flashing feed inlet device is used in a vapor/liquid contacting column, such as a distillation column, to decrease the amount of liquid entrainment and maldistribution of vapor occurring when the liquid feed stream is introduced into the column at a temperature and/or pressure conditions higher than those existing in the column. The entrainment of the liquid and the maldistribution of the vapor are decreased by substantially decreasing the linear velocity of the vapor produced by the flashing of the liquid feed stream.
    Type: Grant
    Filed: July 19, 1989
    Date of Patent: August 21, 1990
    Assignee: Mobil Oil Corporation
    Inventor: Frank C. Silvey
  • Patent number: 4946558
    Abstract: A water distiller is provided which is used in conjunction with a hot water heater where normally wasted energy is used to preheat the hot water heater inlet. The distiller includes a heat storage tank, an evaporator tank having a water inlet, a heater and a steam outlet, and a first and second heat exchanger located within the heat storage tank. Steam generated in the evaporator tank passes through the first heat exchanger and condenses, forming distilled water. The heat rejected during condensation is absorbed within the heat storage tank. The second heat exchanger is used to preheat the water flowing to the hot water heater inlet by passing the water through the second heat exchanger on an as needed basis where it absorbs heat from the heat storage tank.
    Type: Grant
    Filed: December 9, 1988
    Date of Patent: August 7, 1990
    Assignee: Terrill Designs, Inc.
    Inventor: Michael E. Salmon
  • Patent number: 4938868
    Abstract: The vacuum column system distills liquid under partial vacuum conditions. The system rigorously splashes and boils liquid in a boiler chamber so as to form vapor and a rising mist from the splashing liquid. The vapor and mist rise in a circularly converging path through a mist collector. The heavier mist strikes the surfaces of the mist collector and deposits on those surfaces, thereby separating itself from the vapor. The vapor is then drawn to a condensor chamber where droplets of treated liquid are sprayed through it and fall into a shallow pool of treated liquid. The droplets seed condensation of the vapor directly onto the droplets. Also, the droplets assist in encapsulating bubbles of vapor in the pool as the droplets fall into the pool. The bubbles are then entrained with other treated liquid of the pool as the treated liquid is drawn from the pool down an entrainment conduit.
    Type: Grant
    Filed: May 2, 1988
    Date of Patent: July 3, 1990
    Inventor: Thomas R. Nelson
  • Patent number: 4936955
    Abstract: A two-step distillation process provides semiconductor purity, concentrated hydrofluoric acid. Further, the distillation process, occurring under reduced pressures eliminates essentially pure water after the first distillation step. The product output of the second distillation process provides an acid of weight percent greater than 27 weight percent. The product acid is carefully diluted to the required concentrations during the dilution step.
    Type: Grant
    Filed: August 12, 1988
    Date of Patent: June 26, 1990
    Assignee: Alameda Instruments, Inc.
    Inventors: Jesse Dobson, Marshall McCormick
  • Patent number: 4936954
    Abstract: A liquid mixture is separated by pervaporation in an apparatus formed by a unitary stack of upright rectangular plates, diaphragms, and seals held together by tie rods. Each of the plates is formed with two upper and two lower corners formed with respective holes and each plate is formed inward of the respective holes with a corrugated central portion and the holes of the plates are aligned horizontally. Each diaphragm is sandwiched between two plates to form a cell having a pair of compartments separated by the respective diaphragm. The seals are arranged in the upstream region of the stack such that the liquid mixture enters one of the lower holes, passes downstream along the upstream portion into one of the compartments of each cell, and its lighter fraction passes as vapor through the diaphragms into the other compartments of these cells while its heavier fraction passes back upstream and exits the apparatus from one of the upper holes.
    Type: Grant
    Filed: August 29, 1988
    Date of Patent: June 26, 1990
    Assignee: Metallgesellschaft AG
    Inventor: Ulrich Sander
  • Patent number: 4935104
    Abstract: The invention provides a process for producing essential oils by plant hydro-distillation including the following steps:(a) loading the plants continuously into a still where they are processed counterflow wise with steam,(b) continuous unloading of the exhausted plants,(c) recovery of the latent heat of distillation and condensation of the steam by means of a gas in a condenser,(d) drying of the exhausted plants by contacting with the gas, in a drying installation,(e) combustion of at least a part of the dried exhausted plants in a boiler and use of the combustion heat for producing steam.
    Type: Grant
    Filed: November 13, 1987
    Date of Patent: June 19, 1990
    Assignee: Biolandes
    Inventor: Dominique Coutiere
  • Patent number: 4929312
    Abstract: A solvent recovery system is provided which is characterized by improved efficiency and safety. The system includes an evaporator unit having a heat source for vaporizing contaminated solvent. The resulting vapors are subsequently liquified in a condensing unit. During evaporation and condensation of the solvent, a negative pressure is maintained within the system using a vacuum generator. After condensation, the liquid solvent passes into at least one accumulator which is periodically drained. The accumulator and vacuum generator operate in synchronization so that a vacuum is maintained in the system while drainage of the accumulator occurs. Since the evaporation and condensation systems of the invention are maintained at a negative pressure, any leaks therein do not result in the escape of flammable vapors.
    Type: Grant
    Filed: January 27, 1988
    Date of Patent: May 29, 1990
    Inventor: Robert D. Westcott
  • Patent number: 4917770
    Abstract: A vertically extending distillation cylinder has a closed top and an open bottom having an electric heating element disposed therein to form a closure. Adjacent to the top of the distillation cylinder is connected a condensing tube. The condensing tube extends down through a condenser having a cooling water inlet at the bottom and a water discharge at the top. A throttle valve regulates the flow of cooling water. From the water discharge, a trough carries the water to impinge on the distillation cylinder causing pollutants to vaporize. The water collects below in a basin surrounding the distillation cylinder. A feed tube carries water from the basin to the bottom of the distillation cylinder. A discharge tube also connected to the bottom of the distillation cylinder carries water up to where it makes a U-turn. This regulates water height in the distillation cylinder. The discharge tube and an over flow tube from the basin discharge into a funnel from which water is conveyed to a sewer.
    Type: Grant
    Filed: August 7, 1989
    Date of Patent: April 17, 1990
    Inventors: Charles T. Asbury, Genevieve J. Asbury
  • Patent number: 4917773
    Abstract: The process and the device according to the invention relate to the introduction, at a stable, known flow rate, of sublimable tetrachloride into a column for continuous extractive distillation under pressure of the chlorides. The sublimable tetrachloride is dissolved in a hot dissolver in a liquid solvent such as KAlCl.sub.4, and is then recirculated by pump at a stable, known flow rate into an evaporator connected to the column. The solution is then heated in an evaporator in order to sublime the majority of the product which it contains, the sublimed vapors thus passing into the column at a stable, known flow rate. The process according to the invention is adapted, in particular, to a plant for the production of ArCl.sub.4 of nulear purity and of HfCl.sub.4.
    Type: Grant
    Filed: March 6, 1989
    Date of Patent: April 17, 1990
    Assignee: Compagnie Europeenne Du Zirconium Cezus
    Inventors: Pierre Brun, Jean Guerin
  • Patent number: 4915793
    Abstract: A potable water dispenser includes a first reservoir for storing raw water, a second reservoir for storing boiled hot water, and a third reservoir for storing boiled warm water. The second reservoir is surrounded by the raw water in the first reservoir so as to effect a heat exchange therebetween. A condenser is disposed on the top end of the second reservoir. A heating device is interposed between the first and second reservoirs so as to vaporize the raw water from the first reservoir. Then, the vapor flows into the condenser so as to form boiled hot water which falls into the second reservoir. The boiled hot water will flow from the second reserovir into the third reservoir through a water duct so as to form boiled warm water. Two water tap units are respectively communicated with the second and third reservoirs so as to supply hot and warm water.
    Type: Grant
    Filed: October 7, 1988
    Date of Patent: April 10, 1990
    Inventor: Tien-Fu Chou
  • Patent number: 4904347
    Abstract: A liquid product (4) leaving a furnace (2) is introduced into a series of cyclone separators (5, 6, 7). The liquid product to be vaporized is introduced tangentially into the top portion (5a, 6a, 7a) of each cyclone to place the product into contact with a side wall (5b, 6b, 7b) of the cyclone. A gaseous phase (11, 12, 13) formed in each cyclone is collected in the central zone (8, 9, 10) of the cyclone and is then introduced into a vacuum distillation column (3). The liquid phase obtained in each cyclone is collected at the bottom (5c, 6c, 7c) of the cyclone and then is introduced tangentially into the top (6a, 7a) of the following cyclone or, in the case of the last cyclone, is introduced directly into the vacuum distillation column (3). The side wall (5b, 6b, 7b) of each cyclone (5, 6, 7) is heated to a temperature near the maximum temperature allowable for avoiding all thermal deterioration of the product.
    Type: Grant
    Filed: December 17, 1987
    Date of Patent: February 27, 1990
    Assignees: Spie Batignolles, Electricite de France
    Inventors: Pierre Cros, Christian Daumas
  • Patent number: 4894123
    Abstract: A highly efficient distillation unit is provided for heating water and condensing the generated steam to remove the contaminants from the water. Efficiency is enhanced by providing a compact air cooled fin-and-tube heat exchanger which removes heat from the steam, with a powered blower passing air by the fins. A removable bowl which houses the evaporating water is suspended from a rod biased toward its upper position. Mechanical linkage interconnects the rod and a valve which controls incoming water flow to the bowl. The valve closure member is incrementally moved from an opened position to a closed position as a function of the weight of the water in the heating bowl. A low density electrical heating element is powered with from 40 to 55 watts per square inch of submerged heating element exterior surface. The bowl is configured to have a large surface area of heated water to heater input power, thereby further maximizing efficiency.
    Type: Grant
    Filed: November 1, 1988
    Date of Patent: January 16, 1990
    Inventor: Arthur R. Helmich
  • Patent number: 4888097
    Abstract: A distillation type of water purification system has a raw water inlet valve for admitting raw water continuously to a boiling tank at a rate greater than the rate at which raw water is converted to treated water. A drain valve located at the bottom of the boiling tank is energized by a raw water level sensing device whenever the raw water level reaches a predetermined level, to discharge water from the boiling tank. Treated water is stored in a storage tank having a pump for discharging treated water to the user upon demand. A single conductivity sensor in the storage tank controls the pump to allow it to operate only if the sensed conductivity is above a first predetermined value but not at or above a second predetermined value greater than the first value. An improved condenser has two sets of tubes, each set is arranged in a pair of planes oriented transverse the flow of cooling air with the tubes parallel. The internal cross-sectional area of one set is about twice that of the other.
    Type: Grant
    Filed: November 16, 1987
    Date of Patent: December 19, 1989
    Assignee: Pure Water, Inc.
    Inventors: David G. Palmer, David J. Shannon, Keith L. Vacha
  • Patent number: 4886574
    Abstract: A citrus juice concentrate processor homogenizes a mixture of citrus juice and pulp within or after a multi-effect, multi-stage evaporator. The homogenizer employs a positive displacement pump for pumping the citrus juice mixture through an orifice with a high pressure differential across the orifice. The homogenizer reduces viscosity of the citrus juice mixture. Inter-stage placement of the homogenizer further enables final citrus juice concentrate Brix levels of 65.degree.Brix and greater to be achieved.
    Type: Grant
    Filed: May 10, 1987
    Date of Patent: December 12, 1989
    Assignee: APV Gaulin, Inc.
    Inventor: Philip M. Grant
  • Patent number: 4882012
    Abstract: A water distiller includes an inner vessel in which source water is heated, an outer dome or housing on the inner surface of which the vapor from the inner vessel is condensed and a reservoir for receiving the condensate. The inner vessel includes a closure which directs vapor radially of the inner vessel to the dome or housing and which may include a vapor filtration element. A variety of domes or housings are shown including those of double wall construction with ports or vents to direct heat transfer fluid or air between the walls thereof, and those having lower portions which downwardly converge to direct the condensate to a central mouth of a reservoir.
    Type: Grant
    Filed: December 10, 1987
    Date of Patent: November 21, 1989
    Inventor: Kurt Wasserman
  • Patent number: 4882009
    Abstract: A brine concentrator utilizing two separate concentrating devices in combination wherein a first concentrating device comprises a plurality of serpentine pipes interposed within a concentrator tank containing a dilute brine solution and a second concentrating device, including a venturi, is attached to the upper end of the concentrator tank and connected to receive exhaust gases from an exterior source. The brine solution which has been concentrated by the first concentrating device exit the tank through an output opening and is introduced into the venturi via a plurality of nozzles where it is mixed with the exhaust gases.A venting stack is also attached to the upper end of the tank for venting the exhaust gases emitted from the venturi and pre-heating dilute brine solution, which is introduced into the tank through the venting stack. As the solution travels down the stack and into the tank, it comes into contact with the exhaust gases exiting the tank from the venturi.
    Type: Grant
    Filed: July 13, 1987
    Date of Patent: November 21, 1989
    Assignee: Four Nines, Inc.
    Inventors: Joseph J. Santoleri, Richard D. Ross
  • Patent number: 4872949
    Abstract: Used drilling muds containing substantial quantities of organic liquids and water-soluble salts are treated to render them environmentally acceptable for disposal purposes, by drying the muds to evaporate all liquids, aqueous and non-aqueous, preferably in a shell-and-tube type heat exchanger through which they are conveyed and held in suspension by screw conveyors, and preferably with the vapors thus generated flowing in a direction counter-current to the mud. Water-soluble salts are removed from the dried mud components by dissolving with water, and the vapors are condensed and phase separated for further purification and re-use if desired.
    Type: Grant
    Filed: January 18, 1989
    Date of Patent: October 10, 1989
    Inventor: Carl M. Wilwerding
  • Patent number: 4869785
    Abstract: A steam distillation apparatus is provided which has a column body, a head connected to one end of the column body which has a diameter larger than the column body, a sump connected to the other end of the column body and contact elements disposed within the column body which are positioned and arranged to avoid formation of preferential pathways for the steam passing through the column body while providing for ready flow of the material being steam distilled through the column body. The connection of the head and column body may be frustoconical in shape such that its diameter diminishes from a diameter corresponding with that of the head at its connection with the head to a diameter corresponding with that of the column body at its connection with the column body. A collar is positioned at the connection of the neck and column body and extends into the head to define an annular space between the neck and collar.
    Type: Grant
    Filed: May 31, 1988
    Date of Patent: September 26, 1989
    Assignee: Nestec S. A.
    Inventors: Roland Fasi, Giancarlo Werner, Ursula Wolfensberger
  • Patent number: 4865697
    Abstract: A flashing feed inlet device is used in a vapor/liquid contacting column, such as a distillation column, to decrease the amount of liquid entrainment and maldistribution of vapor occurring when the liquid feed stream is introduced into the column at a temperature and/or pressure conditions higher than those existing in the column. The entrainment of the liquid and the maldistribution of the vapor are decreased by substantially decreasing the linear velocity of the vapor produced by the flashing of the liquid feed stream.
    Type: Grant
    Filed: October 15, 1987
    Date of Patent: September 12, 1989
    Assignee: Mobil Oil Corp.
    Inventor: Frank C. Silvey
  • Patent number: 4853088
    Abstract: A process and apparatus for separating volatile components from a volatile-containing liquid by a stripping gas flowing countercurrent to the liquid. Separation of the volatile components is enhanced by heating the liquid with radiant solar energy and agitating the liquid as it flows.
    Type: Grant
    Filed: April 12, 1988
    Date of Patent: August 1, 1989
    Assignee: Marathon Oil Company
    Inventor: David D. Conway
  • Patent number: 4842693
    Abstract: A method and apparatus for removing water from a liquid mixture of water and ethanol contacts it with liquid carbon dioxide so that the ethanol is preferentially transferred into solution, dries the solution using an adsorbent, and then recovers dry ethanol by distilling off the carbon dioxide. This process is particularly energy efficient especially when it includes a fermentation process to generate the ethanol and uses the carbon dioxide generated during the fermentation as the source of liquid carbon dioxide. In this case the method and apparatus provide an additional product of dry carbon dioxide.
    Type: Grant
    Filed: August 25, 1987
    Date of Patent: June 27, 1989
    Assignee: The Distillers Company PLC
    Inventor: Alfred G. Wheldon
  • Patent number: 4834840
    Abstract: Processes for managing toxic and hazardous waste materials containing distillable solvents or chemicals in which the waste materials are collected and introduced into solar dryers wherein the more volatile solvent or chemical components thereof are distilled and recaptured as pure byproducts which may be recycled for future use and wherein the residue is retained within the solar dryers until such time as the residue is substantially free of all of the contaminant solvents or chemicals and after which such residue may be removed as a non-toxic and non-hazardous byproduct which may be prepared for future use or disposed of in a conventional manner.
    Type: Grant
    Filed: March 16, 1987
    Date of Patent: May 30, 1989
    Assignee: Matrix Recovery Systems
    Inventor: Joseph A. Capella
  • Patent number: 4834841
    Abstract: The improved method and apparatus treats the stack gases from a commercial bakery oven to remove and recover pollutants, specifically ethyl alcohol. The method includes the steps of cooling the stack gases and passing the cooled gases through a packed column to condense the water and ethyl alcohol and if the ethyl alcohol is to be recovered drying the ethyl alcohol by distillation and by absorption of the water therefrom by a molecular sieve. The apparatus includes blowers and controls to maintain the normal flow of gases from the oven so that the removal and recovery of the ethyl alcohol from the stack gases does not interfere or change the baking conditions of the oven. This may be accomplished by a system of dampers or by controlling the discharge rate of the blowers used.
    Type: Grant
    Filed: October 1, 1987
    Date of Patent: May 30, 1989
    Inventor: Kenneth W. Peck
  • Patent number: 4830710
    Abstract: A portable apparatus for on-site clean-up of dirty solvents. An open top liner for receiving dirty solvent is provided in a still housing. A head sits down over the top of the liner to form an enclosed space. Hot heating oil is provided beneath the liner and in the annular space between the liner and the housing. Dirty solvent is placed in the liner and is heated. The solvent vapors are fed to condensation coils for recovery. The heating oil is next removed and then the cap or head is removed and the contaminants are removed from the liner.
    Type: Grant
    Filed: September 24, 1987
    Date of Patent: May 16, 1989
    Inventor: Ronald D. Thompson
  • Patent number: 4828660
    Abstract: A continuous process and apparatus for the repurification of ultrapure liquids. An oxidant solution comprising ultrapure sulfuric acid, peroxydisulfuric acid, and ultrapure water is continuously withdrawn from a process after use. The withdrawn oxidant is reprocessed continuously by contacting with alumina to remove fluoride ions. Water is continuously separated or stripped from the oxidant solution by heating the solution and bubbling an inert gas therethrough causing the water to vaporize from the solution. The separated oxidant is continuously distilled and condensed to form a purified stream of sulfuric acid. The major portion of this stream is continuously returned to the process. The remaining minor portion is continuously cooled, subjected to analysis for purity, and diluted with ultrapure water. The diluted sulfuric acid is further cooled prior to electrochemical treatment in the anode compartment of an electrochemical cell.
    Type: Grant
    Filed: October 6, 1986
    Date of Patent: May 9, 1989
    Assignee: Athens Corporation
    Inventors: R. Scot Clark, Joe G. Hoffman, John B. Davison, Alan W. Jones, Allen H. Jones, Jr., David W. Persichini, Wallace I. Yuan, Bruce A. Lipisko
  • Patent number: 4826575
    Abstract: A laboratory apparatus for continuously producing high purity distilled water includes a distillation flask, a carboy and condenser unit. A double walled microwave oven with a spacing between the walls, large enough to accommodate piping and valving means for controlling the flow of water to the distillation flask. The microwave oven supplies the heat to the system.
    Type: Grant
    Filed: July 27, 1987
    Date of Patent: May 2, 1989
    Inventor: Narbik A. Karamian
  • Patent number: 4818344
    Abstract: A portable water distiller comprising a vaporization chamber containing an electric coil heating element, a finned tube condenser coil, and an electric fan motor for cooling the condenser coil's outer surface. In a preferred embodiment, the vaporization chamber includes an upper vertical tube having an open bottom and closed top communication with the condenser, and a raw water receptacle with its rim surrounding the tube at a distance and with its bottom near the bottom end of the tube. The receptacle of the portable water distiller is automatically kept full with water up to a predetermined level, and is readily removable from the distiller for cleaning of residue, the lower portion of the tube is similarly removable for access to the heating element. The condenser coil is designed to offer low flow resistance resulting in only a small over-pressure in the vaporization chamber thus affecting only a small depression of the water level therein.
    Type: Grant
    Filed: December 17, 1987
    Date of Patent: April 4, 1989
    Inventor: Dov Z. Glucksman
  • Patent number: 4814044
    Abstract: In a technique for recovering hydrocarbon values from a heavy hydrocarbon-water mixture, the mixture is first delivered through a sub-assembly to remove solid particulates. Then the mixture is delivered through a series of heat exchanger--kettle arrangements in which the mixture is heated above the boiling point of water. Some of the steam formed is allowed to escape through steam removal devices in the heat exchanger. The inside of the heat exchanger includes a plurality of discrete baffles which are unconnected to the heat exchanger and which can be readily removed therefrom. Heating of the mixture continues in the kettles where the bulk of the water is boiled off the mixture. A heavy hydrocarbon oil is recovered in the liquid outlet from the last kettle. The vapors boiled off are recovered and condensed to recover a light hydrocarbon oil and quite pure water.
    Type: Grant
    Filed: September 14, 1987
    Date of Patent: March 21, 1989
    Inventor: Franz A. Hitt
  • Patent number: 4795532
    Abstract: A method and apparatus for treating the distilled water obtained from an evaporation process sea water desalination plant is provided wherein carbon dioxide is extracted from sea water in the high temperature stages of the desalination plant and where the carbon dioxide thus extracted is dissolved into the water, along with calcium, thereby converting the distilled water into the quality suited for city tap water.
    Type: Grant
    Filed: February 13, 1987
    Date of Patent: January 3, 1989
    Assignee: Sasakura Engineering Co. Ltd.
    Inventors: Junji Mizutani, Kozo Fujita
  • Patent number: 4790904
    Abstract: An atmospheric evaporator for reducing the water content of various chemical solutions, more particularly useful in the electroplating industry, wherein the evaporator includes a solution-secure molded tank in which a removable blower sleeve is mounted having a blower inlet duct and support strut members formed at the opposite end thereof to support a multiplicity of finned evaporator members over which the solution is sprayed. When a large-volume, low RPM blower is mounted to the inlet duct, a straight-line downdraft of both air and solution is created, allowing the air and evaporated water to exhaust through an up-facing outlet duct, thus defining a substantially "U" shaped duct arrangement from the inlet side to the exhaust side of the tank with the heavy chemical particles returning to the process tank from the bottom of the evaporator tank.
    Type: Grant
    Filed: May 19, 1987
    Date of Patent: December 13, 1988
    Inventor: William Yates
  • Patent number: 4783242
    Abstract: A distillation system and process for removing vaporizable components from an aqueous medium including a distillation column for receiving an aqueous medium containing vaporizable components and passing steam through the column such that the steam directly contacts the aqueous medium to vaporize at least a portion of the components, a condenser in a communication with the column to condense at least a portion of the vapor in the column, a separator in communication with the condenser to separate flash vapor from liquid condensate in the separator and a thermal compressor in communication with the separator and the column to remove vapor from the separator and to inject exhaust steam from the thermal compressor into the column.
    Type: Grant
    Filed: May 22, 1986
    Date of Patent: November 8, 1988
    Assignee: The Dow Chemical Company
    Inventor: Lanny A. Robbins
  • Patent number: 4778535
    Abstract: An apparatus for vaporizing and recovering, by condensation, a composite mixture of at least two components, at least one of which is a liquid. The apparatus includes at least one chamber in which the mixture is brought to boiling and includes means to condense the vaporized portion of the mixtures. A liquid of the mixture in the vaporizing chamber is vaporized by heating coils and subjected to circulation to uniformly disperse the mixture. The apparatus may further include a system for continuously filtering the mixture in the vaporizing chamber to remove undesirable particulates, a mixture spray device for spraying the mixture into the vaporizing chamber, and an ultrasonic vibrating means.
    Type: Grant
    Filed: September 28, 1982
    Date of Patent: October 18, 1988
    Inventor: James W. McCord
  • Patent number: 4770747
    Abstract: An inlet horn for reducing liquid entrainment of liquid in vapor products in distillation towers. The inlet horn has a tangential entry for the vapor-liquid feed which opens into a peripheral open bottomed horn with a number of deflector vanes angularly disposed horizontally and vertically along the length of the horn to deflect liquid components of the feed radially outwards and vapor components downwards so as to improve their separation. The horn may be used in atmospheric and vacuum crude distillation and other vapor-liquid separation units.
    Type: Grant
    Filed: October 21, 1987
    Date of Patent: September 13, 1988
    Assignee: Mobil Oil Corporation
    Inventor: Herbert M. Muller
  • Patent number: 4762592
    Abstract: A wobbling-type evaporator mounts a container 1 holding at least one vertically oriented heat transfer tube 30 fed by a liquid inlet 35 to the container 1. The container 1 is supported with respect to a base 10 so that it wobbles in response to the rotation of an orbiting counterweight 2,2' the counterweight and container wobble as a two body system about common axis. In one form a set of struts 6 located around the container are part of the support system. The invention also includes inlet water distribution systems, compatible with this orbital drive.
    Type: Grant
    Filed: October 20, 1986
    Date of Patent: August 9, 1988
    Inventor: Yao T. Li
  • Patent number: 4755261
    Abstract: An apparatus for vaporizing a liquid and condensing the vapor includes at least one chamber in which the liquid is vaporized and in which the vaporized liquid is condensed. The vaporizing chamber contains a heat emitting device providing a surface temperature above the vapor temperature for substantially instantaneously vaporizing the liquid condensate maintaining a predetermined vapor level in the vaporizing chamber, and a heat absorbing device for condensing the vaporized liquid.
    Type: Grant
    Filed: January 2, 1987
    Date of Patent: July 5, 1988
    Inventors: James W. McCord, Lamont I. Hoppestad, Michael J. Ruckriegel
  • Patent number: 4734167
    Abstract: A compact and energy efficient water distillation unit is disclosed including a housing divided by shared interior walls into deaerator, heater and evaporator chambers. A deaerator is mounted in the deaerator chamber. An evaporator is mounted in the evaporator chamber and a vapor compressor is provided for drawing water vapor produced by the evaporator through a demister and outputting the vapor into a duct open to the evaporator. The duct is at least partially located above the heater chamber and open thereto. A heater is mounted in the heater chamber. A duct interconnects the evaporator with the deaerator chamber and a vertical standpipe connects the deaerator and evaporator chambers.
    Type: Grant
    Filed: June 11, 1986
    Date of Patent: March 29, 1988
    Assignee: Mechanical Equipment Company, Inc.
    Inventor: Richard W. Goeldner
  • Patent number: 4724048
    Abstract: A water distiller apparatus for purifying and degassing domestic water supplies is provided which is constructed for easy cleaning of all parts and in which inflowing water is preheated by condensing steam within a condenser which preheating allows dissolved gases to dissipate through a vent before the inlet water reaches an evaporator portion. The rate of inflowing water is controlled by a temperature responsive valve that is in thermal communication with the condenser to maximize heat transfer and minimize heat and water loss.
    Type: Grant
    Filed: September 4, 1985
    Date of Patent: February 9, 1988
    Inventor: Arthur R. Helmich
  • Patent number: 4708775
    Abstract: Volatile matter especially solvents is recovered from waste material using a hot granular material such as sand, as a heat carrier to drive off the solvents, and as a carrier for the non-volatile resin content of the waste; the resins are thermally decomposed in reactions which provide heat to maintain the granular material hot and the granular material is continuously circulated; the exhaust gases from the thermal decomposition of the resins can be used as a source of heat outside the system.
    Type: Grant
    Filed: July 8, 1985
    Date of Patent: November 24, 1987
    Assignee: Anachemia Solvents Limited
    Inventors: Ian R. McGregor, D. Keith Jackson, Walter F. M. Brown, Kenneth Burrell
  • Patent number: 4698136
    Abstract: A process for the continuous production of boiler feed water from process waters in the oil extraction industry during which salts and hydrocarbons are removed from the water, without Fe.sup.++ precipitating. The heavy hydrocarbons are mechanically separated, the volatile hydrocarbons are separated from the water, by means of a thermal degassing, and the low boiling and the non-condensable hydrocarbons are separated in a shower evaporation step with downstream vapor compression, wherein the low boiling non-condensable hydrocarbons are evaporated with the waste water within the shower evaporator and the non-condensable hydrocarbons then are drawn off from a downstream separator. A salt-free oxygen-free pure water is removed from a separator.
    Type: Grant
    Filed: May 23, 1985
    Date of Patent: October 6, 1987
    Assignee: Fried Krupp GmbH
    Inventor: Mohammed El-Allawy
  • Patent number: 4696718
    Abstract: A highly efficient water purification device includes a degasification apparatus, a distillation apparatus and an ion removal device to purify contaminated water. When a partial vacuum is applied to the degasification apparatus, dissolved gases leave the water, and a heat exchange process occurs which heats the gases and cools the degassed water. A gas exhaust channel transfers the warmed gases to a heating coil in the distillation apparatus to preheat water for evaporation therein while the cooled, degassed water is transferred to a condenser to condense vapor and steam. The degasification apparatus may include one or more towers in which a vacuum is formed by first filling the towers with water, sealing the tower top, and then draining water from the tower bottom; this vacuum may be applied to the distillation apparatus and a reservoir by transferring the vacuum from the towers through a depressurization conduit to thereby achieve boiling in the distillation apparatus at reduced temperatures.
    Type: Grant
    Filed: February 4, 1986
    Date of Patent: September 29, 1987
    Inventor: Henry C. Lasater
  • Patent number: 4687546
    Abstract: A beneficiated kaolin clay slurry is concentrated from a solids content of about 50% to 60% by weight to a solids content of at least 65% by weight by evaporating water therefrom by passing the aqueous clay slurry through one or more non-contact evaporated heat exchangers. The kaolin clay slurry is passed in indirect heat exchange relationship with a heating vapor, with the heating vapor comprising water vapor previously evaporated from the aqueous clay slurry.
    Type: Grant
    Filed: July 19, 1985
    Date of Patent: August 18, 1987
    Assignee: Georgia Kaolin Company, Inc.
    Inventor: Mark S. Willis