Spray Forming And Filming Patents (Class 202/236)
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Patent number: 7597783Abstract: Methods for processing oils and apparatus for carrying out such methods are disclosed herein. One embodiment provides a method for processing a partially processed oil, wherein the oil includes glycerides and a volatilizable impurity fraction. The partially processed oil may be processed by driving off a first volatiles stream having a portion of the glycerides and at least a portion of the volatilizable impurity fraction, leaving a deodorized oil. The first volatiles stream may be introduced into a first condensing chamber and a glyceride-rich, impurity-poor fraction may be condensed from the first volatiles stream, leaving a glyceride-poor, impurity-rich second volatiles stream. The second volatiles stream may be passed into a second condensing chamber and a glyceride-poor, impurity-rich second condensate may be condensed from the second volatiles stream.Type: GrantFiled: November 13, 2001Date of Patent: October 6, 2009Assignee: Cargill, IncorporatedInventor: Marco Kruidenberg
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Patent number: 7591930Abstract: A thin-film evaporator with a vertical drum (1), a supply line (4) that is arranged in the upper region of the drum (1) and is used to supply a medium to be evaporated, a heating jacket (3) arranged on the periphery of the drum and forming vapors, a discharge line (20) for discharging the residue left in the lower end of the drum, and a condenser (11) supplied with a coolant, for increasing the separating capacity and optionally for performing chemical reactions, is characterized in that an inner device (24) influencing the action of the thin-film evaporator is provided in the path of the vapors from the heating jacket (3) to the condenser (11).Type: GrantFiled: March 31, 2006Date of Patent: September 22, 2009Assignee: VTU Holding GmbHInventors: Wolfgang Glasl, Matthaeus Siebenhofer, Michael Koncar
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Patent number: 7435317Abstract: An improved distillation of water. involves distilling significant quantities of water at temperatures well below the boiling point. During distillation, a compound is taken from a liquid-phase to a gas-phase and then condensed to the liquid-phase again to get a pure liquid. The present invention uses water sprayed (105) and absorbed onto a solid surface such as micro-powder (104) made from wood as a starting material. Absorbing water onto such a surface results in rapid evaporation with a relatively low temperature gradient when the water and particles are agitated. The present invention could be characterized as solid-phase distillation.Type: GrantFiled: March 29, 2001Date of Patent: October 14, 2008Assignee: Biomass Conversions, L.L.C.Inventor: Seiji Hata
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Patent number: 7427336Abstract: A blade heat exchanger includes blades that extend axially with respect to an axis of rotation and are elongated in the radial direction. The blades are arranged about the axis such that, when they are disposed in a housing, they form composite condensation and evaporation chambers that are isolated from each other. The interiors of at least some of the blades form the composite condensation chamber. The exteriors of the blades and the inner surface of the housing cooperate to form the composite evaporation chamber.Type: GrantFiled: June 17, 2004Date of Patent: September 23, 2008Assignee: Zanaqua Technologies, Inc.Inventor: William H. Zebuhr
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Patent number: 7422663Abstract: A compact array of vertical rising film evaporators is disclosed in an evacuated multi-effect process, for desalination of seawater, using waste heat of thermal machines. Vapor produced in one stage is the heat source for the next. This invention is based on a concentric disposition of three different evaporators, at which the first stage is a shell and tube evaporator built in a ring format, where is inserted inside the intermediate stage that is a bundle of vertical tubes in a ring format, and the last stage that is a bundle of vertical tubes placed inside the intermediate stage. By this arrangement, vapor pipelines are eliminated, dimensions are reduced, and heat transfer is improved per the rising film evaporators compared to falling film.Type: GrantFiled: August 1, 2003Date of Patent: September 9, 2008Inventor: Sergio Martins Costa
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Patent number: 7300538Abstract: Liquid organic material is controllably delivered to a receptacle located in the center of a heated surface capable of horizontally rotating about its central axis. As the heated surface rotates, material deposited within the central receptacle is forced outwardly and across the rotating surface. As the material moves radially, it evaporates into a vapor which is then transported to one or more nozzles. From the nozzles, the vapor is applied to a substrate and condensed. The spinning disk evaporator enables the evaporation of a wider variety of organic liquids greater reliability in continuous operation, a decrease in maintenance, and a larger and more constant material flow rate.Type: GrantFiled: February 16, 2005Date of Patent: November 27, 2007Assignee: 3M Innovative Properties CompanyInventors: Charles Daniel Lemme, Marc G. Langlois
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Patent number: 7153394Abstract: A process to isolate dianhydride from an exchange reaction comprises extracting a bisimide/anhydride exchange reaction aqueous phase with an organic solution comprising an exchange catalyst at a first temperature and pressure to form an extracted aqueous phase comprising water, exchange catalyst and a dianhydride precursor; removing water from the extracted aqueous phase at a second temperature and pressure to form a molten phase, wherein the second pressure is less than the first pressure; removing water and exchange catalyst from the molten phase at a third temperature and pressure to form an isolation mixture; and converting the dianhydride precursor in the isolation mixture to dianhydride at a fourth temperature and pressure, wherein the fourth temperature is greater than the second and third temperatures and the fourth pressure is less than the second and third pressures.Type: GrantFiled: June 19, 2003Date of Patent: December 26, 2006Assignee: General Electric CompanyInventors: Thomas Link Guggenheim, David Anthony Mongilio
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Patent number: 7112262Abstract: A device is disclosed for downward flow evaporation of a liquid substance and subsequent condensation of the vapor formed, which includes a plurality of vertical evaporator tubes housed in a common casing in side-by-side relationship, a distributor tank which is arranged above the evaporator tubes and from which the substance contained therein can be fed to the evaporator tubes with production of a film of the substance running down the tube surface of the evaporator tubes, a heat exchanger arrangement arranged in the casing and having a plurality of vertical condensation tubes having a surface upon which the vapor can be condensed, receiving trays housed below the evaporator tubes and below the condensation tubes in the casing to separately receive unevaporated concentrate of the substance which runs down the tube surface of the evaporator tubes or condensed distillate of the substance which runs down the tube surface of the condensation tubes.Type: GrantFiled: September 9, 2002Date of Patent: September 26, 2006Assignee: GEA Wiegand GmbHInventor: Daniel Bethge
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Patent number: 6998026Abstract: A tert-C4–C8-alkyl (meth)acrylate is prepared by reacting (meth)acrylic acid with an olefin of the formula where R1 and R2, which may be identical or different, are methyl or ethyl and R3 is H, methyl or ethyl, in homogeneous phase in the presence of an acidic catalyst and isolating the tert-C4–C8-alkyl (meth)acrylate from the reaction mixture, by a process in which the catalyst is separated off as residue by a two-stage distillation of the reaction mixture and the tert-C4–C8-alkyl (meth)acrylate is isolated from the distillates. The novel process makes it possible to use acetic acid-containing (meth)acrylic acid. The danger of cleavage of the ester and of polymerization of (meth)acrylic compounds is reduced.Type: GrantFiled: July 27, 2001Date of Patent: February 14, 2006Assignee: BASF AktiengesellschaftInventors: Ruprecht Kroker, Gerhard Nestler, Werner Schmitt, Winfried Schumm
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Patent number: 6911121Abstract: The present application is directed to a continuous contacting apparatus for separating a liquid component from a liquid mixture.Type: GrantFiled: July 26, 2000Date of Patent: June 28, 2005Inventor: James R. Beckman
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Patent number: 6860966Abstract: A method of removing substantially all solvent from a solution containing a polyphenylene ether polymer resin with little by-product formation (less than 250 ppm) is provided. The method employs a wiped thin film evaporator with a cylindrical heating chamber operating under conditions that satisfy the relationships defined by Equations I and II. 5.3*1024RL? exp(?24123/T)/m<C??I 100?(4960AP/Tm)<C??II; Yields are maximized wherein values for feed rate (m) and percent solids (C) are selected to provide a maximum value for the output, Q, determined from the equation m*C=Q and the melt viscosity of the polyphenylene ether product is less than 50,000 centipoise at the operating temperature of the cylindrical heating chamber.Type: GrantFiled: November 12, 2001Date of Patent: March 1, 2005Assignee: General ElectricInventors: David Parrillo, Probjot Singh
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Patent number: 6802941Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.Type: GrantFiled: January 18, 2001Date of Patent: October 12, 2004Assignee: Ovation Products CorporationInventor: William H. Zebuhr
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Publication number: 20040195083Abstract: The solar still has a frame, an evaporator within the frame and a glass sheet supported by the frame and spaced above the evaporator. The evaporator has a peripheral flange in contact with the edge of the glass sheet. The glass sheet and peripheral flange are nested within an inwardly facing channel on the frame, the sealing between the glass and the flange being by surface tension of water between the glass and the flange.Type: ApplicationFiled: April 1, 2003Publication date: October 7, 2004Inventor: John Ward
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Publication number: 20040055866Abstract: A sub-atmospheric pressure desalinating still employs a closed top, opened bottom tank filled with seawater, having a height greater than the height of a column of seawater that can be supported by the pressure at the bottom tank so that a vacuum is formed at the top. A compressor draws vapor from the evacuated area, compresses it and passes it through a heat exchanger within the tank volume to condense the vapor in the tank to generate purified water. Replenishing water is drawn in through the bottom of the tank, passes through a heat exchanger, and is pumped through a heat exchanger coil surrounding the compressor, with the outlet feeding a spray head within the vacuum volume. The compressor and the pump for the intake flow are powered by a wind turbine or wave power.Type: ApplicationFiled: September 19, 2003Publication date: March 25, 2004Inventor: Michael R. Levine
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Patent number: 6695951Abstract: The present water reclamation system includes a series of concentric thin shells. The shells mount within a housing that can be maintained under vacuum or low pressure. The shells rotate at high velocity. Contaminated liquid from outside the housing is injected into the space between half the shells. The centrifugal force causes the liquid to form a thin film along the inward facing surface of the shell. A compressor lowers the pressure adjacent the thin film causing the liquid to boil. The compressor carries the vapor to the other side of those shells at a slightly higher temperature. There the vapor encounters the wall, which is cooler because its heat was transferred to boil the contaminated liquid. The vapor condenses, and rotation throws the condensate against the adjacent wall where it is collected. When condensing, the heat of condensation transfers to the shell for boiling the incoming contaminated liquid.Type: GrantFiled: July 18, 2000Date of Patent: February 24, 2004Inventors: Jack G. Bitterly, Steven E. Bitterly
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Publication number: 20040026225Abstract: The invention concerns appliances, one of which uses solar energy as sole source of power. It comprises an accumulation solar water heater (222) and quasi-reversible liquid/vapour heat exchanging alveolar elements, provided with hydrophilic coatings. Elements of types E and C, respectively assigned to water evaporation (224a, b, c) and to vapour condensation (226a-b) are interposed, with narrow free spaces, in a heat-insulated treatment chamber (223), arranged above the boiler (222). Hot water coming from the heater (222) flows in closed circuit, by thermosiphon, from the top downwards of elements E and from the bottom upwards of elements C. A slightly cooling member (242) is interposed between the bottom collectors (240-244) of elements E and C. Hot water spills over slowly from the top of the hydrophilic coatings of elements E and the vapour produced is condensed opposite, on the walls of elements C.Type: ApplicationFiled: June 12, 2003Publication date: February 12, 2004Inventor: Jean-Paul Domen
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Patent number: 6689251Abstract: A distiller (10) that employs a rotary heat exchanger (32) introduces water to be evaporated into evaporation chambers (56). During most of its operation, it collects the water that has passed through the evaporation chamber (56) without evaporating, and it reintroduces the thus-collected liquid back into the evaporation chamber, where it also adds a minor amount of unrecirculated feed liquid to make up for evaporation and concentrate removal. Simultaneously, a minor amount of feed liquid is fed into one side of a transfer pump (116). During this mode of operation, the impurities concentration in the recirculating liquid tends to increase as a result of the evaporation of pure water vapor. Periodically, the erstwhile recirculating liquid is redirected to the other side of the transfer pump (116), where it causes the feed liquid stored in the transfer pump's first side to be fed without accompanying recirculant liquid into the rotary heat exchanger's evaporation chambers.Type: GrantFiled: January 18, 2001Date of Patent: February 10, 2004Assignee: Ovation Products CorporationInventor: William H. Zebuhr
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Publication number: 20040015328Abstract: A process to isolate dianhydride from an exchange reaction comprises extracting a bisimide/anhydride exchange reaction aqueous phase with an organic solution comprising an exchange catalyst at a first temperature and pressure to form an extracted aqueous phase comprising water, exchange catalyst and a dianhydride precursor; removing water from the extracted aqueous phase at a second temperature and pressure to form a molten phase, wherein the second pressure is less than the first pressure; removing water and exchange catalyst from the molten phase at a third temperature and pressure to form an isolation mixture; and converting the dianhydride precursor in the isolation mixture to dianhydride at a fourth temperature and pressure, wherein the fourth temperature is greater than the second and third temperatures and the fourth pressure is less than the second and third pressures.Type: ApplicationFiled: June 19, 2003Publication date: January 22, 2004Applicant: GENERAL ELECTRIC COMPANYInventors: Thomas Link Guggenheim, David Anthony Mongilio
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Patent number: 6656327Abstract: An evaporation product discharged from a lower end a falling-film evaporator enters a downpipe (7), makes a 180° turn at a bottom of the downpipe, and moves upward through an annular rising channel (9) defined between the downpipe and an intermediate housing (10). As the evaporation product moves along a spiral path (12) defined by the spiral fins, centrifugal forces urges water droplets and impurities to a radial outward periphery where they pass through openings (13) in the intermediate shell as pure steam continues through the spiral path and out a pure steam outlet (21). A cooling jacket (15) chills a peripheral wall of an outer shell (14) adjacent the holes such that the discharged water droplets condense on the outer shell and flow down a reject water return path to a reject water reservoir at the bottom of the outer shell.Type: GrantFiled: September 21, 2001Date of Patent: December 2, 2003Assignee: Steris Europe, Inc. Suomen SivuliikeInventor: Mauri J. Salmisuo
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Patent number: 6635150Abstract: A method for distilling a fluid which is useful, for instance, in eliminating salt from brackish and/or sea water includes percolating films on plates with multiple effects having several evaporating zones and condensation zones. The evaporation zones (EVAP) and the condensation zones (COND) are vertically arranged. The liquid to be distilled emerges in the top part of the evaporation zone (EVAP). The vapors produced in the evaporation zone (EVAP) are horizontally transferred into the condensation zone (COND) through a communicating connection. The condensed liquid percolates vertically along the walls of the condensation zone and is evacuated from the lower part of the condensation zone. A distilling plant is also provided for implementing the distilling method, and includes plural cascades made up of elementary cells alternatingly assembled in thermal series.Type: GrantFiled: January 23, 2001Date of Patent: October 21, 2003Assignee: Centre International de l'Eau de Nancy - NancieInventors: Pierre Le Goff, Jean-Marie Hornut, Viviane Renaudin
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Publication number: 20030127315Abstract: A tert-C4-C8-alkyl (meth)acrylate is prepared by reacting (meth)acrylic acid with an olefin of the formula 1Type: ApplicationFiled: January 27, 2003Publication date: July 10, 2003Inventors: Ruprecht Kroker, Gerhard Nestler, Werner Schmitt, Winfried Schumm
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Publication number: 20020130029Abstract: An apparatus for and method of distillation uses a high temperature thermoelectric device to heat a liquid, such as water to vapor (steam) and cool the vapor to a purified, distilled liquid. Distillation system has no moving parts, thereby increasing reliability while reducing noise and maintenance. Liquid in a container has a heating section on the container extending into it to boil it into a vapor that is fed to a condenser section disposed on the container adjacent to the heating section. A thermoelectric section provided with a Peltier effect device is interposed between the heating section and condenser section. The Peltier effect device has one side in contiguous contact with the condenser to transfer heat from it and another side is in contiguous contact with the heating section to transfer heat to it to boil the liquid into the vapor and feed the vapor through the condenser that condenses it into distilled liquid.Type: ApplicationFiled: March 19, 2001Publication date: September 19, 2002Inventors: Brian Stout, Robert Peebles
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Patent number: 6423187Abstract: A thin film distiller is provided which applies distilland to an evaporative side by the use of wicks which work by capillary action. The evaporated vapor is transferred to the condensate side after being compressed to a higher pressure where it is condensed and removed by similar wicks. The condensing and evaporating surfaces are formed on opposing sides of a bellows-like sheet of heat conducting material. The sheet would preferably be formed into a cylindrical shape with the evaporative stage on the outside and the condensing stage on the inside of the cylinder. Either the wicks or the heat conducting material are moved with respect to the other such that the wicks place a thin film of distilland on the evaporative surface. Removal of condensate is performed in a similar manner by the wicks in the condensate stage.Type: GrantFiled: December 11, 1998Date of Patent: July 23, 2002Assignee: Ovation Products CorporationInventor: William H. Zebuhr
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Publication number: 20020092624Abstract: In a distillation unit (10) a rotary heat exchanger (32) receives from a radially inward position feed liquid to be purified and collects on the inner surface of a rotating exterior shell (36) liquid that has passed through its evaporation chambers (56). Stationary scoop tubes (122 and 124) scoop liquid from the resultant liquid layer that forms on the shell (36)'s inner surface, and the kinetic energy of the liquid scooped from the thus-spinning layer drives it radially inward through the scoop tubes (122 and 124) into spray arms (58) for reintroduction into the rotary heat exchanger's evaporation chambers (56).Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Publication number: 20020092759Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Publication number: 20020092758Abstract: A distillation unit (10) employs counterflow-heat-exchanger modules (102, 104, 106, 108, and 110) to use the heat from water that has come from a rotary heat exchanger (32) to heat feed water that is being sent to it for distillation. In one of the modules the feed water is heated only by concentrate that results from the distillation process, whereas only condensate heats the feed water in the other modules. By thus employing four different flows in two sets of heat-exchanger modules rather than three flows in a single set, the distillation unit can employ relatively simple counterflow-heat-exchanger modules and easily adjust flows to achieve a desired output concentration in response to different expected feed concentrations while maintaining optimum feed flows.Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Publication number: 20020040844Abstract: A thin film distiller is provided which applies distilland to an evaporative side by the use of wicks which work by capillary action. The evaporated vapor is transferred to the condensate side after being compressed to a higher pressure where it is condensed and removed by similar wicks. The condensing and evaporating surfaces are formed on opposing sides of a bellows-like sheet of heat conducting material. The sheet would preferably be formed into a cylindrical shape with the evaporative stage on the outside and the condensing stage on the inside of the cylinder. Either the wicks or the heat conducting material are moved with respect to the other such that the wicks place a thin film of distilland on the evaporative surface. Removal of condensate is performed in a similar manner by the wicks in the condensate stage.Type: ApplicationFiled: December 11, 1998Publication date: April 11, 2002Inventor: WILLIAM H. ZEBUHR
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Liquid distributor for non-vertical distillation columns, and distillation column including the same
Patent number: 6338774Abstract: A liquid distributor includes a principal container with a perforated bottom, as well as transport members to transmit, by gravity, the liquid from at least one opening in the perforated bottom, to a supply point not in vertical alignment with this opening.Type: GrantFiled: November 17, 1998Date of Patent: January 15, 2002Assignee: L'Air Liquide Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges ClaudeInventor: Jean-Yves Lehman -
Patent number: 6309508Abstract: Liquid organic material is controllably delivered to a receptacle located in the center of a heated surface capable of horizontally rotating about its central axis. As the heated surface rotates, material deposited within the central receptacle is forced outwardly and across the rotating surface. As the material moves radially, it evaporates into a vapor which is then transported to one or more nozzles. From the nozzles, the vapor is applied to a substrate and condensed. Relative to existing devices and methods, the present invention enables the evaporation of a wider variety of organic liquids, greater reliability in continuous operation, a decrease in maintenance, and a larger and more constant material flow rate.Type: GrantFiled: January 15, 1998Date of Patent: October 30, 2001Assignee: 3M Innovative Properties CompanyInventors: Charles Daniel Lemme, Marc G. Langlois
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Patent number: 6294056Abstract: In a method for distilling (meth)acrylic acid and/or (meth)acrylic ester, the method has the step of uniformly distributing a supply liquid in a distillation tower over an entirety of a horizontal cross sectional area in the distillation tower. A distillation apparatus for distilling (meth)acrylic acid and/or (meth)acrylic ester in a distillation tower has a supply element for supplying the supply liquid into the distillation tower. The supply element is formed with at least two supply ports through which the liquid is supplied into the distillation tower.Type: GrantFiled: February 19, 1999Date of Patent: September 25, 2001Assignee: Nippon Shokubai Co., Ltd.Inventors: Yukihiro Matsumoto, Kazukiyo Arakawa, Osamu Dodo, Hiroo Iwato, Mamoru Takamura
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Patent number: 6200428Abstract: Wastewater treatment apparatus having a fluid receiving vessel for collecting and heating wastewater to a temperature below boiling, a superheated vaporizing chamber and at least one spray head to spray wastewater into the vaporizing chamber for conversion of the wastewater to vapor to be withdrawn from the apparatus, with the contaminants in the wastewater collected in the apparatus for separate removal.Type: GrantFiled: March 31, 1998Date of Patent: March 13, 2001Inventor: Raymond E. VanKouwenberg
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Patent number: 6080273Abstract: A process and a device for treating a liquid by separating out constituents contained in the liquid. Pollutants are removed or the liquid is sterilized by partial evaporization. The liquid is introduced into a vacuum tank in which a portion thereof is evaporated. The remaining liquid phase is discharged from the vacuum tank. The liquid in the vacuum tank flows under the effect of gravity on a fixed inclined or horizontal surface on which it forms a liquid film. The vapor phase emerges from the liquid film as a function of the vapor pressure defined relative to the prevailing temperature. The flow surface slopes downwardly away from the inflow of the liquid, it rises slightly or it extends horizontally.Type: GrantFiled: July 23, 1997Date of Patent: June 27, 2000Inventor: Martin Schrems
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Patent number: 6066232Abstract: The invention relates to a process for evaporating a liquid containing vaporizable oxidation-sensitive compounds in an evaporator in which the liquid is brought into contact with a heated solid surface for evaporation, by a process in which direct contact between the resulting vapor phase and the heated solid surface is substantially avoided. It also directed to an evaporator composed of a heatable solid surface (16), an apparatus (2, 3) for heating the solid surface and an apparatus (10) for feeding a liquid containing vaporizable compounds to the heatable solid surface, wherein the apparatus for feeding the liquid is designed and arranged in the evaporator in such a way (12, 14, 18) that direct contact between a resulting vapor phase and the heatable solid surface is substantially avoided.Type: GrantFiled: July 24, 1998Date of Patent: May 23, 2000Assignee: BASF AktiengesellschaftInventors: Jurgen Mohr, Frans Vansant, Axel Werner Polt, Stephan Scholl, Siegfried Kruger, Hartmut Staatz
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Patent number: 5980694Abstract: An installation for cleaning oil-polluted water, in particular at oil and gas production plants, is provided with a distillation column having a polluted water feed and at least one contact packing above which the outlet of the polluted water feed is located, a vapor discharge, a clean water outlet and a measuring device for the analysis of the water from the clean water outlet.Type: GrantFiled: July 25, 1997Date of Patent: November 9, 1999Assignee: EMSYS Separation Technology B.V.Inventors: Adrianus P. Apeldoorn, Jachebus W. Bos, Johannes J. Dozy, Johannes J. Elling, Leonardus C. Gordijn, Pieter Ottens, Wayne S. Penny, Cornelis Spel, Aatje J. Spel-van der Linde, Tom M. Vader, Theodorus J. De Wit
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Patent number: 5928469Abstract: Materials which are not themselves storage-stable at room temperature are made suitable for storage by mixing them with a carrier substance and spray drying the resulting mixture so as to form particles containing both the material and the carrier substance in which the carrier substance is in an amorphous, i.e. glassy or rubbery, state. Formation of such a composition greatly enhances stability. The material stored may be a biological material such as an enzyme, the components of a chemical reaction such as reagents for carrying out an assay, or even viable biological cells.Type: GrantFiled: May 11, 1994Date of Patent: July 27, 1999Assignee: Inhale Therapeutic SystemsInventors: Felix Franks, Ross Henry Hatley, Sheila Frances Mathias
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Patent number: 5902457Abstract: An apparatus for generating a liquid spray from two jets of fluid which issue from a pair of opposing nozzles and interact, wherein the fluid is supplied to the nozzles under fully turbulent conditions such that random variations in the momentum of the fluid as it leaves the nozzles occur which results in random variations in the orientation of the resultant spray of liquid drops.Type: GrantFiled: August 18, 1994Date of Patent: May 11, 1999Assignee: AEA Technology PLCInventors: Lionel Houston Ford, John William Stairmand
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Patent number: 5820748Abstract: Gasses, water and solvents, major contaminants in used lubricating oils, can be removed from used lubricating oils at mild temperature conditions under vacuum. Apparatus in which the removal can take place includes a hollow vacuum separator vessel with a spray nozzle to spray an ultra fine spray of warm, used lubricating oil onto an angularly disposed thin film separator plate. In conjunction with the plate is a cooling device within the vacuum chamber. Cleaned oil can be passed from the bottom back into a holding tank, while water and solvents are drained out into a separate tank for safe disposal.Type: GrantFiled: April 25, 1997Date of Patent: October 13, 1998Inventor: Tajwar Shadikhan
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Patent number: 5770020Abstract: The invention relates to a distillation apparatus (1) which is suitable in particular for the distillation of sea water into fresh water. The apparatus includes a plurality of flat, bag-like elements (3) formed from a thin film material such as plastic film and placed one against the other, the elements serving as heat exchangers between a vaporizing liquid flowing along the exterior surfaces of the element and a condensing vapor directed to the inside of the element, and a compressor (15) for increasing the pressure and temperature of the generated vapor before it is directed to the inside of the elements. The essential idea of the invention is that at the upper end of each bag-like element (3) there is a honeycomb-structured end strip (4) having substantially the width of the element, the strip containing parallel feeding ducts (26) separated from each other by partition walls, the ducts distributing the liquid to be evaporated over the entire width of the element surface.Type: GrantFiled: November 18, 1996Date of Patent: June 23, 1998Assignee: Keeran Corporation N.V.Inventors: Peter Koistinen, Reijo Rantala
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Patent number: 5755924Abstract: An apparatus, e.g. centrifugal evaporator, has at least one rotary treatment surface, e.g. a heated evaporating surface, which rises outwards from the rotation axis, a liquid feed in the vicinity of the lowest point of the treatment surface close to the rotation axis and a product removal on the periphery of the treatment surface. Such an apparatus is characterized in that the treatment surface over at least part of its axial length has a stepped construction and each step has a step angle of approximately 90.degree.. Thus, as desired, a laminar or turbulent flow is possible. Through the construction of the steps it is possible to widely vary the nature of the flow and consequently the heat and material exchange, as well as the residence time of the liquid.Type: GrantFiled: August 23, 1996Date of Patent: May 26, 1998Inventor: Vaclav Feres
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Patent number: 5728273Abstract: Method for bringing a gas and a liquid into contact with one another, the liquid being passed in the form of a film over an evaporator surface (1) provided with small openings and the gas being fed through the openings in the evaporator surface, which gas mixes with the liquid on the surface and absorbs vapor from the liquid, a liquid subsequently being passed in the form of a film over a condenser surface (11) provided with small openings and the gas which has absorbed vapors from the liquid film on the evaporator surface being fed through the openings in the condenser surface, at least some of the absorbed vapor condensing and being carried along with the liquid film on the condenser surface and removed.Type: GrantFiled: January 19, 1996Date of Patent: March 17, 1998Inventor: Leendert Aandewiel
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Patent number: 5684125Abstract: The invention relates to a method for purifying liquid polysiloxane containing impurities as a low-molecular-weight fraction, by evaporating the low-molecular-weight fraction, in which method a liquid stream of impure liquid material in the form of a bundle of a multiplicity of streams or jets is brought into contact with a flowing gas phase, after which the gas stream, which contains the impurities, is removed and purified liquid material is collected; a device for performing this method and also the use of purified liquid material.Type: GrantFiled: May 26, 1995Date of Patent: November 4, 1997Assignee: Bayer AktiengesellschaftInventor: Franciscus Petrus Marie Nooren
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Patent number: 5676802Abstract: An improved apparatus for treating waste water containing volatile and corrosive substances by steam-stripping to remove the volatile and corrosive substances from the waste water. The apparatus has a liquid pooling zone installed at a part over the waste water supplying part of a stripper tower and liquid distributor at the top of the tower, and pipe arrangement is prepared to recycle liquid drawn from the liquid pooling zone to the liquid distributor. In the pipe arrangement, a cooler for the recycling liquid is installed. Serious corrosion can be avoided utilizing this apparatus.Type: GrantFiled: April 10, 1995Date of Patent: October 14, 1997Assignee: JGC CorporationInventors: Kenji Satoh, Naohiko Kagawa, Sei Tange, Shun-ichi Ohya
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Patent number: 5658433Abstract: An integral system and method for the separation and purification in a single operation of a heat or oxygen-sensitive liquid feed, such as a plant derived liquid feed mixture of fatty acids, tocopherol compounds and sterols, into a low boiling point purified fraction of Vitamin E tocopherol compounds and a high boiling point concentrate fraction of triglycerides, which system can be maintained in the presence of an inert gas to provide reduced degradation and increased purity of the Vitamin E fraction. The system includes a pre-evaporator, a vapor-liquid separator, a packed bed distillation column, a rotary thin film evaporator and an evaporator-stripper.Type: GrantFiled: March 26, 1996Date of Patent: August 19, 1997Assignee: Artisan Industries Inc.Inventor: James L. Baird
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Patent number: 5653852Abstract: A distilling device has an undistilled water tank to contain undistilled water, a cover covering the tank, a water heating area communicating with the tank, a high-frequency oscillator disposed under the water heating area, a heater disposed above the water heating area, a cooling area beside the heater, and a water collecting can disposed under the cooling area. The cooling area and the water heating area are separated by a separating plate.Type: GrantFiled: November 8, 1995Date of Patent: August 5, 1997Inventor: Ching Ping Meng
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Patent number: 5628901Abstract: A single vessel with no moving parts is constructed to perform the functions of coalescing, vacuum dehydration, and thin film evaporation.Type: GrantFiled: April 30, 1993Date of Patent: May 13, 1997Assignee: Castrol Industrial North America Inc.Inventors: William L. Lawrence, Robert D. Coyle
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Patent number: 5624534Abstract: An apparatus and method for stripping volatiles from a feed stream and concentrating the volatiles in the overhead vapors forming a condensate product and simultaneously producing a low percent volatiles outlet stream as a concentrate product. The volatiles separator and concentrator, ("VSC"), unit has many applications in the reduction and the concentration of voiatiles in the beverage, fuel, and industrial alcohol industries, as well as in chemical applications for removing or stripping volatiles from heat sensitive feed substrates which require low temperatures and a short residence time to prevent degradation of the product. For heat sensitive applications, the VSC unit utilizes a short feed stream preheat contact time in combination with turbulent high velocity flow to separate and concentrate volatile and nonvolatile components at temperatures below 100.degree. F. utilizing flash vaporization for volatiles separation with reboil capability to adjust volatiles concentration in the residue and product.Type: GrantFiled: June 7, 1995Date of Patent: April 29, 1997Inventors: Armand R. Boucher, Philip N. Hambrick
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Patent number: 5624530Abstract: Spray drying system for drying a liquid feed which is made up of a solution or suspension of particles in a fluid medium. The system enables the spray drying of wet material and converting the material into powder by evaporation of a liquid medium at reduced pressure or at a vacuum. The system includes a heating chamber and an evacuation device, communicating with the interior of the heating chamber. This provision enables creation of reduced pressure within the chamber, accompanied by evaporation of the fluid medium at temperatures lower than needed for evaporation at normal pressure, and evacuation of the moisture vapor generated during evaporation.Type: GrantFiled: April 21, 1994Date of Patent: April 29, 1997Assignee: Ultrasonic Dryer, Ltd.Inventors: Akper Sadykhov, Raphael Semiat
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Patent number: 5624531Abstract: An evaporator operating on falling film principle, has a shell (1) with a system (2) of evaporating tubes therein, whereby a liquid to be concentrated is fed on the outer surface of the evaporating tube system (2) and vapor is led to flow inside the tubes of the evaporating tube system (2). The evaporating tube system (2) is formed of evaporating elements, each evaporating element being formed of evaporating tubes (9) substantially on the same level. The upper ends of the tubes are connected to a common collecting chamber (8) and the lower end, respectively, to a common collecting chamber (10) in such a manner that there is a connection between both collecting chambers (8, 10) through each tube (9) between them, due to which the collecting chambers (8) of the upper end of the evaporating elements are interconnected through the upper connecting chamber (12), and respectively, the collecting chambers (10) of the lower end are interconnected through the connecting chamber (13) of the lower end.Type: GrantFiled: March 23, 1994Date of Patent: April 29, 1997Assignee: Tampella Power OyInventors: Matti Knuutila, Kalevi Nurminen, Jukka Vaistomaa, Anssi Makela
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Patent number: 5601688Abstract: The horizontal distance traveled by droplets of starting solution sprayed into a gaseous medium above a catch basin, where the gaseous medium has a horizontal velocity component is controlled by controlling the size of the droplets as a function of the horizontal velocity component.Type: GrantFiled: October 30, 1992Date of Patent: February 11, 1997Assignee: Ormat Industries Ltd.Inventors: Gad Assaf, Joseph Weinberg
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Patent number: 5573635Abstract: A thin film evaporating device includes a housing defining a space for receiving a plurality of elongated tubular evaporators. An inlet is associated with the housing for feeding a flowable heating medium to the space for heating the plurality of elongated tubular evaporators.Type: GrantFiled: June 3, 1994Date of Patent: November 12, 1996Assignee: Buss AGInventor: Rolf Van Der Piepen