Spray Forming And Filming Patents (Class 202/236)
  • Patent number: 7597783
    Abstract: Methods for processing oils and apparatus for carrying out such methods are disclosed herein. One embodiment provides a method for processing a partially processed oil, wherein the oil includes glycerides and a volatilizable impurity fraction. The partially processed oil may be processed by driving off a first volatiles stream having a portion of the glycerides and at least a portion of the volatilizable impurity fraction, leaving a deodorized oil. The first volatiles stream may be introduced into a first condensing chamber and a glyceride-rich, impurity-poor fraction may be condensed from the first volatiles stream, leaving a glyceride-poor, impurity-rich second volatiles stream. The second volatiles stream may be passed into a second condensing chamber and a glyceride-poor, impurity-rich second condensate may be condensed from the second volatiles stream.
    Type: Grant
    Filed: November 13, 2001
    Date of Patent: October 6, 2009
    Assignee: Cargill, Incorporated
    Inventor: Marco Kruidenberg
  • Patent number: 7591930
    Abstract: A thin-film evaporator with a vertical drum (1), a supply line (4) that is arranged in the upper region of the drum (1) and is used to supply a medium to be evaporated, a heating jacket (3) arranged on the periphery of the drum and forming vapors, a discharge line (20) for discharging the residue left in the lower end of the drum, and a condenser (11) supplied with a coolant, for increasing the separating capacity and optionally for performing chemical reactions, is characterized in that an inner device (24) influencing the action of the thin-film evaporator is provided in the path of the vapors from the heating jacket (3) to the condenser (11).
    Type: Grant
    Filed: March 31, 2006
    Date of Patent: September 22, 2009
    Assignee: VTU Holding GmbH
    Inventors: Wolfgang Glasl, Matthaeus Siebenhofer, Michael Koncar
  • Patent number: 7435317
    Abstract: An improved distillation of water. involves distilling significant quantities of water at temperatures well below the boiling point. During distillation, a compound is taken from a liquid-phase to a gas-phase and then condensed to the liquid-phase again to get a pure liquid. The present invention uses water sprayed (105) and absorbed onto a solid surface such as micro-powder (104) made from wood as a starting material. Absorbing water onto such a surface results in rapid evaporation with a relatively low temperature gradient when the water and particles are agitated. The present invention could be characterized as solid-phase distillation.
    Type: Grant
    Filed: March 29, 2001
    Date of Patent: October 14, 2008
    Assignee: Biomass Conversions, L.L.C.
    Inventor: Seiji Hata
  • Patent number: 7427336
    Abstract: A blade heat exchanger includes blades that extend axially with respect to an axis of rotation and are elongated in the radial direction. The blades are arranged about the axis such that, when they are disposed in a housing, they form composite condensation and evaporation chambers that are isolated from each other. The interiors of at least some of the blades form the composite condensation chamber. The exteriors of the blades and the inner surface of the housing cooperate to form the composite evaporation chamber.
    Type: Grant
    Filed: June 17, 2004
    Date of Patent: September 23, 2008
    Assignee: Zanaqua Technologies, Inc.
    Inventor: William H. Zebuhr
  • Patent number: 7422663
    Abstract: A compact array of vertical rising film evaporators is disclosed in an evacuated multi-effect process, for desalination of seawater, using waste heat of thermal machines. Vapor produced in one stage is the heat source for the next. This invention is based on a concentric disposition of three different evaporators, at which the first stage is a shell and tube evaporator built in a ring format, where is inserted inside the intermediate stage that is a bundle of vertical tubes in a ring format, and the last stage that is a bundle of vertical tubes placed inside the intermediate stage. By this arrangement, vapor pipelines are eliminated, dimensions are reduced, and heat transfer is improved per the rising film evaporators compared to falling film.
    Type: Grant
    Filed: August 1, 2003
    Date of Patent: September 9, 2008
    Inventor: Sergio Martins Costa
  • Patent number: 7300538
    Abstract: Liquid organic material is controllably delivered to a receptacle located in the center of a heated surface capable of horizontally rotating about its central axis. As the heated surface rotates, material deposited within the central receptacle is forced outwardly and across the rotating surface. As the material moves radially, it evaporates into a vapor which is then transported to one or more nozzles. From the nozzles, the vapor is applied to a substrate and condensed. The spinning disk evaporator enables the evaporation of a wider variety of organic liquids greater reliability in continuous operation, a decrease in maintenance, and a larger and more constant material flow rate.
    Type: Grant
    Filed: February 16, 2005
    Date of Patent: November 27, 2007
    Assignee: 3M Innovative Properties Company
    Inventors: Charles Daniel Lemme, Marc G. Langlois
  • Patent number: 7153394
    Abstract: A process to isolate dianhydride from an exchange reaction comprises extracting a bisimide/anhydride exchange reaction aqueous phase with an organic solution comprising an exchange catalyst at a first temperature and pressure to form an extracted aqueous phase comprising water, exchange catalyst and a dianhydride precursor; removing water from the extracted aqueous phase at a second temperature and pressure to form a molten phase, wherein the second pressure is less than the first pressure; removing water and exchange catalyst from the molten phase at a third temperature and pressure to form an isolation mixture; and converting the dianhydride precursor in the isolation mixture to dianhydride at a fourth temperature and pressure, wherein the fourth temperature is greater than the second and third temperatures and the fourth pressure is less than the second and third pressures.
    Type: Grant
    Filed: June 19, 2003
    Date of Patent: December 26, 2006
    Assignee: General Electric Company
    Inventors: Thomas Link Guggenheim, David Anthony Mongilio
  • Patent number: 7112262
    Abstract: A device is disclosed for downward flow evaporation of a liquid substance and subsequent condensation of the vapor formed, which includes a plurality of vertical evaporator tubes housed in a common casing in side-by-side relationship, a distributor tank which is arranged above the evaporator tubes and from which the substance contained therein can be fed to the evaporator tubes with production of a film of the substance running down the tube surface of the evaporator tubes, a heat exchanger arrangement arranged in the casing and having a plurality of vertical condensation tubes having a surface upon which the vapor can be condensed, receiving trays housed below the evaporator tubes and below the condensation tubes in the casing to separately receive unevaporated concentrate of the substance which runs down the tube surface of the evaporator tubes or condensed distillate of the substance which runs down the tube surface of the condensation tubes.
    Type: Grant
    Filed: September 9, 2002
    Date of Patent: September 26, 2006
    Assignee: GEA Wiegand GmbH
    Inventor: Daniel Bethge
  • Patent number: 6998026
    Abstract: A tert-C4–C8-alkyl (meth)acrylate is prepared by reacting (meth)acrylic acid with an olefin of the formula where R1 and R2, which may be identical or different, are methyl or ethyl and R3 is H, methyl or ethyl, in homogeneous phase in the presence of an acidic catalyst and isolating the tert-C4–C8-alkyl (meth)acrylate from the reaction mixture, by a process in which the catalyst is separated off as residue by a two-stage distillation of the reaction mixture and the tert-C4–C8-alkyl (meth)acrylate is isolated from the distillates. The novel process makes it possible to use acetic acid-containing (meth)acrylic acid. The danger of cleavage of the ester and of polymerization of (meth)acrylic compounds is reduced.
    Type: Grant
    Filed: July 27, 2001
    Date of Patent: February 14, 2006
    Assignee: BASF Aktiengesellschaft
    Inventors: Ruprecht Kroker, Gerhard Nestler, Werner Schmitt, Winfried Schumm
  • Patent number: 6911121
    Abstract: The present application is directed to a continuous contacting apparatus for separating a liquid component from a liquid mixture.
    Type: Grant
    Filed: July 26, 2000
    Date of Patent: June 28, 2005
    Inventor: James R. Beckman
  • Patent number: 6860966
    Abstract: A method of removing substantially all solvent from a solution containing a polyphenylene ether polymer resin with little by-product formation (less than 250 ppm) is provided. The method employs a wiped thin film evaporator with a cylindrical heating chamber operating under conditions that satisfy the relationships defined by Equations I and II. 5.3*1024RL? exp(?24123/T)/m<C??I 100?(4960AP/Tm)<C??II; Yields are maximized wherein values for feed rate (m) and percent solids (C) are selected to provide a maximum value for the output, Q, determined from the equation m*C=Q and the melt viscosity of the polyphenylene ether product is less than 50,000 centipoise at the operating temperature of the cylindrical heating chamber.
    Type: Grant
    Filed: November 12, 2001
    Date of Patent: March 1, 2005
    Assignee: General Electric
    Inventors: David Parrillo, Probjot Singh
  • Patent number: 6802941
    Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.
    Type: Grant
    Filed: January 18, 2001
    Date of Patent: October 12, 2004
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr
  • Publication number: 20040195083
    Abstract: The solar still has a frame, an evaporator within the frame and a glass sheet supported by the frame and spaced above the evaporator. The evaporator has a peripheral flange in contact with the edge of the glass sheet. The glass sheet and peripheral flange are nested within an inwardly facing channel on the frame, the sealing between the glass and the flange being by surface tension of water between the glass and the flange.
    Type: Application
    Filed: April 1, 2003
    Publication date: October 7, 2004
    Inventor: John Ward
  • Publication number: 20040055866
    Abstract: A sub-atmospheric pressure desalinating still employs a closed top, opened bottom tank filled with seawater, having a height greater than the height of a column of seawater that can be supported by the pressure at the bottom tank so that a vacuum is formed at the top. A compressor draws vapor from the evacuated area, compresses it and passes it through a heat exchanger within the tank volume to condense the vapor in the tank to generate purified water. Replenishing water is drawn in through the bottom of the tank, passes through a heat exchanger, and is pumped through a heat exchanger coil surrounding the compressor, with the outlet feeding a spray head within the vacuum volume. The compressor and the pump for the intake flow are powered by a wind turbine or wave power.
    Type: Application
    Filed: September 19, 2003
    Publication date: March 25, 2004
    Inventor: Michael R. Levine
  • Patent number: 6695951
    Abstract: The present water reclamation system includes a series of concentric thin shells. The shells mount within a housing that can be maintained under vacuum or low pressure. The shells rotate at high velocity. Contaminated liquid from outside the housing is injected into the space between half the shells. The centrifugal force causes the liquid to form a thin film along the inward facing surface of the shell. A compressor lowers the pressure adjacent the thin film causing the liquid to boil. The compressor carries the vapor to the other side of those shells at a slightly higher temperature. There the vapor encounters the wall, which is cooler because its heat was transferred to boil the contaminated liquid. The vapor condenses, and rotation throws the condensate against the adjacent wall where it is collected. When condensing, the heat of condensation transfers to the shell for boiling the incoming contaminated liquid.
    Type: Grant
    Filed: July 18, 2000
    Date of Patent: February 24, 2004
    Inventors: Jack G. Bitterly, Steven E. Bitterly
  • Publication number: 20040026225
    Abstract: The invention concerns appliances, one of which uses solar energy as sole source of power. It comprises an accumulation solar water heater (222) and quasi-reversible liquid/vapour heat exchanging alveolar elements, provided with hydrophilic coatings. Elements of types E and C, respectively assigned to water evaporation (224a, b, c) and to vapour condensation (226a-b) are interposed, with narrow free spaces, in a heat-insulated treatment chamber (223), arranged above the boiler (222). Hot water coming from the heater (222) flows in closed circuit, by thermosiphon, from the top downwards of elements E and from the bottom upwards of elements C. A slightly cooling member (242) is interposed between the bottom collectors (240-244) of elements E and C. Hot water spills over slowly from the top of the hydrophilic coatings of elements E and the vapour produced is condensed opposite, on the walls of elements C.
    Type: Application
    Filed: June 12, 2003
    Publication date: February 12, 2004
    Inventor: Jean-Paul Domen
  • Patent number: 6689251
    Abstract: A distiller (10) that employs a rotary heat exchanger (32) introduces water to be evaporated into evaporation chambers (56). During most of its operation, it collects the water that has passed through the evaporation chamber (56) without evaporating, and it reintroduces the thus-collected liquid back into the evaporation chamber, where it also adds a minor amount of unrecirculated feed liquid to make up for evaporation and concentrate removal. Simultaneously, a minor amount of feed liquid is fed into one side of a transfer pump (116). During this mode of operation, the impurities concentration in the recirculating liquid tends to increase as a result of the evaporation of pure water vapor. Periodically, the erstwhile recirculating liquid is redirected to the other side of the transfer pump (116), where it causes the feed liquid stored in the transfer pump's first side to be fed without accompanying recirculant liquid into the rotary heat exchanger's evaporation chambers.
    Type: Grant
    Filed: January 18, 2001
    Date of Patent: February 10, 2004
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr
  • Publication number: 20040015328
    Abstract: A process to isolate dianhydride from an exchange reaction comprises extracting a bisimide/anhydride exchange reaction aqueous phase with an organic solution comprising an exchange catalyst at a first temperature and pressure to form an extracted aqueous phase comprising water, exchange catalyst and a dianhydride precursor; removing water from the extracted aqueous phase at a second temperature and pressure to form a molten phase, wherein the second pressure is less than the first pressure; removing water and exchange catalyst from the molten phase at a third temperature and pressure to form an isolation mixture; and converting the dianhydride precursor in the isolation mixture to dianhydride at a fourth temperature and pressure, wherein the fourth temperature is greater than the second and third temperatures and the fourth pressure is less than the second and third pressures.
    Type: Application
    Filed: June 19, 2003
    Publication date: January 22, 2004
    Applicant: GENERAL ELECTRIC COMPANY
    Inventors: Thomas Link Guggenheim, David Anthony Mongilio
  • Patent number: 6656327
    Abstract: An evaporation product discharged from a lower end a falling-film evaporator enters a downpipe (7), makes a 180° turn at a bottom of the downpipe, and moves upward through an annular rising channel (9) defined between the downpipe and an intermediate housing (10). As the evaporation product moves along a spiral path (12) defined by the spiral fins, centrifugal forces urges water droplets and impurities to a radial outward periphery where they pass through openings (13) in the intermediate shell as pure steam continues through the spiral path and out a pure steam outlet (21). A cooling jacket (15) chills a peripheral wall of an outer shell (14) adjacent the holes such that the discharged water droplets condense on the outer shell and flow down a reject water return path to a reject water reservoir at the bottom of the outer shell.
    Type: Grant
    Filed: September 21, 2001
    Date of Patent: December 2, 2003
    Assignee: Steris Europe, Inc. Suomen Sivuliike
    Inventor: Mauri J. Salmisuo
  • Patent number: 6635150
    Abstract: A method for distilling a fluid which is useful, for instance, in eliminating salt from brackish and/or sea water includes percolating films on plates with multiple effects having several evaporating zones and condensation zones. The evaporation zones (EVAP) and the condensation zones (COND) are vertically arranged. The liquid to be distilled emerges in the top part of the evaporation zone (EVAP). The vapors produced in the evaporation zone (EVAP) are horizontally transferred into the condensation zone (COND) through a communicating connection. The condensed liquid percolates vertically along the walls of the condensation zone and is evacuated from the lower part of the condensation zone. A distilling plant is also provided for implementing the distilling method, and includes plural cascades made up of elementary cells alternatingly assembled in thermal series.
    Type: Grant
    Filed: January 23, 2001
    Date of Patent: October 21, 2003
    Assignee: Centre International de l'Eau de Nancy - Nancie
    Inventors: Pierre Le Goff, Jean-Marie Hornut, Viviane Renaudin
  • Publication number: 20030127315
    Abstract: A tert-C4-C8-alkyl (meth)acrylate is prepared by reacting (meth)acrylic acid with an olefin of the formula 1
    Type: Application
    Filed: January 27, 2003
    Publication date: July 10, 2003
    Inventors: Ruprecht Kroker, Gerhard Nestler, Werner Schmitt, Winfried Schumm
  • Publication number: 20020130029
    Abstract: An apparatus for and method of distillation uses a high temperature thermoelectric device to heat a liquid, such as water to vapor (steam) and cool the vapor to a purified, distilled liquid. Distillation system has no moving parts, thereby increasing reliability while reducing noise and maintenance. Liquid in a container has a heating section on the container extending into it to boil it into a vapor that is fed to a condenser section disposed on the container adjacent to the heating section. A thermoelectric section provided with a Peltier effect device is interposed between the heating section and condenser section. The Peltier effect device has one side in contiguous contact with the condenser to transfer heat from it and another side is in contiguous contact with the heating section to transfer heat to it to boil the liquid into the vapor and feed the vapor through the condenser that condenses it into distilled liquid.
    Type: Application
    Filed: March 19, 2001
    Publication date: September 19, 2002
    Inventors: Brian Stout, Robert Peebles
  • Patent number: 6423187
    Abstract: A thin film distiller is provided which applies distilland to an evaporative side by the use of wicks which work by capillary action. The evaporated vapor is transferred to the condensate side after being compressed to a higher pressure where it is condensed and removed by similar wicks. The condensing and evaporating surfaces are formed on opposing sides of a bellows-like sheet of heat conducting material. The sheet would preferably be formed into a cylindrical shape with the evaporative stage on the outside and the condensing stage on the inside of the cylinder. Either the wicks or the heat conducting material are moved with respect to the other such that the wicks place a thin film of distilland on the evaporative surface. Removal of condensate is performed in a similar manner by the wicks in the condensate stage.
    Type: Grant
    Filed: December 11, 1998
    Date of Patent: July 23, 2002
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr
  • Publication number: 20020092624
    Abstract: In a distillation unit (10) a rotary heat exchanger (32) receives from a radially inward position feed liquid to be purified and collects on the inner surface of a rotating exterior shell (36) liquid that has passed through its evaporation chambers (56). Stationary scoop tubes (122 and 124) scoop liquid from the resultant liquid layer that forms on the shell (36)'s inner surface, and the kinetic energy of the liquid scooped from the thus-spinning layer drives it radially inward through the scoop tubes (122 and 124) into spray arms (58) for reintroduction into the rotary heat exchanger's evaporation chambers (56).
    Type: Application
    Filed: January 18, 2001
    Publication date: July 18, 2002
    Inventor: William H. Zebuhr
  • Publication number: 20020092759
    Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.
    Type: Application
    Filed: January 18, 2001
    Publication date: July 18, 2002
    Inventor: William H. Zebuhr
  • Publication number: 20020092758
    Abstract: A distillation unit (10) employs counterflow-heat-exchanger modules (102, 104, 106, 108, and 110) to use the heat from water that has come from a rotary heat exchanger (32) to heat feed water that is being sent to it for distillation. In one of the modules the feed water is heated only by concentrate that results from the distillation process, whereas only condensate heats the feed water in the other modules. By thus employing four different flows in two sets of heat-exchanger modules rather than three flows in a single set, the distillation unit can employ relatively simple counterflow-heat-exchanger modules and easily adjust flows to achieve a desired output concentration in response to different expected feed concentrations while maintaining optimum feed flows.
    Type: Application
    Filed: January 18, 2001
    Publication date: July 18, 2002
    Inventor: William H. Zebuhr
  • Publication number: 20020040844
    Abstract: A thin film distiller is provided which applies distilland to an evaporative side by the use of wicks which work by capillary action. The evaporated vapor is transferred to the condensate side after being compressed to a higher pressure where it is condensed and removed by similar wicks. The condensing and evaporating surfaces are formed on opposing sides of a bellows-like sheet of heat conducting material. The sheet would preferably be formed into a cylindrical shape with the evaporative stage on the outside and the condensing stage on the inside of the cylinder. Either the wicks or the heat conducting material are moved with respect to the other such that the wicks place a thin film of distilland on the evaporative surface. Removal of condensate is performed in a similar manner by the wicks in the condensate stage.
    Type: Application
    Filed: December 11, 1998
    Publication date: April 11, 2002
    Inventor: WILLIAM H. ZEBUHR
  • Patent number: 6338774
    Abstract: A liquid distributor includes a principal container with a perforated bottom, as well as transport members to transmit, by gravity, the liquid from at least one opening in the perforated bottom, to a supply point not in vertical alignment with this opening.
    Type: Grant
    Filed: November 17, 1998
    Date of Patent: January 15, 2002
    Assignee: L'Air Liquide Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges Claude
    Inventor: Jean-Yves Lehman
  • Patent number: 6309508
    Abstract: Liquid organic material is controllably delivered to a receptacle located in the center of a heated surface capable of horizontally rotating about its central axis. As the heated surface rotates, material deposited within the central receptacle is forced outwardly and across the rotating surface. As the material moves radially, it evaporates into a vapor which is then transported to one or more nozzles. From the nozzles, the vapor is applied to a substrate and condensed. Relative to existing devices and methods, the present invention enables the evaporation of a wider variety of organic liquids, greater reliability in continuous operation, a decrease in maintenance, and a larger and more constant material flow rate.
    Type: Grant
    Filed: January 15, 1998
    Date of Patent: October 30, 2001
    Assignee: 3M Innovative Properties Company
    Inventors: Charles Daniel Lemme, Marc G. Langlois
  • Patent number: 6294056
    Abstract: In a method for distilling (meth)acrylic acid and/or (meth)acrylic ester, the method has the step of uniformly distributing a supply liquid in a distillation tower over an entirety of a horizontal cross sectional area in the distillation tower. A distillation apparatus for distilling (meth)acrylic acid and/or (meth)acrylic ester in a distillation tower has a supply element for supplying the supply liquid into the distillation tower. The supply element is formed with at least two supply ports through which the liquid is supplied into the distillation tower.
    Type: Grant
    Filed: February 19, 1999
    Date of Patent: September 25, 2001
    Assignee: Nippon Shokubai Co., Ltd.
    Inventors: Yukihiro Matsumoto, Kazukiyo Arakawa, Osamu Dodo, Hiroo Iwato, Mamoru Takamura
  • Patent number: 6200428
    Abstract: Wastewater treatment apparatus having a fluid receiving vessel for collecting and heating wastewater to a temperature below boiling, a superheated vaporizing chamber and at least one spray head to spray wastewater into the vaporizing chamber for conversion of the wastewater to vapor to be withdrawn from the apparatus, with the contaminants in the wastewater collected in the apparatus for separate removal.
    Type: Grant
    Filed: March 31, 1998
    Date of Patent: March 13, 2001
    Inventor: Raymond E. VanKouwenberg
  • Patent number: 6080273
    Abstract: A process and a device for treating a liquid by separating out constituents contained in the liquid. Pollutants are removed or the liquid is sterilized by partial evaporization. The liquid is introduced into a vacuum tank in which a portion thereof is evaporated. The remaining liquid phase is discharged from the vacuum tank. The liquid in the vacuum tank flows under the effect of gravity on a fixed inclined or horizontal surface on which it forms a liquid film. The vapor phase emerges from the liquid film as a function of the vapor pressure defined relative to the prevailing temperature. The flow surface slopes downwardly away from the inflow of the liquid, it rises slightly or it extends horizontally.
    Type: Grant
    Filed: July 23, 1997
    Date of Patent: June 27, 2000
    Inventor: Martin Schrems
  • Patent number: 6066232
    Abstract: The invention relates to a process for evaporating a liquid containing vaporizable oxidation-sensitive compounds in an evaporator in which the liquid is brought into contact with a heated solid surface for evaporation, by a process in which direct contact between the resulting vapor phase and the heated solid surface is substantially avoided. It also directed to an evaporator composed of a heatable solid surface (16), an apparatus (2, 3) for heating the solid surface and an apparatus (10) for feeding a liquid containing vaporizable compounds to the heatable solid surface, wherein the apparatus for feeding the liquid is designed and arranged in the evaporator in such a way (12, 14, 18) that direct contact between a resulting vapor phase and the heatable solid surface is substantially avoided.
    Type: Grant
    Filed: July 24, 1998
    Date of Patent: May 23, 2000
    Assignee: BASF Aktiengesellschaft
    Inventors: Jurgen Mohr, Frans Vansant, Axel Werner Polt, Stephan Scholl, Siegfried Kruger, Hartmut Staatz
  • Patent number: 5980694
    Abstract: An installation for cleaning oil-polluted water, in particular at oil and gas production plants, is provided with a distillation column having a polluted water feed and at least one contact packing above which the outlet of the polluted water feed is located, a vapor discharge, a clean water outlet and a measuring device for the analysis of the water from the clean water outlet.
    Type: Grant
    Filed: July 25, 1997
    Date of Patent: November 9, 1999
    Assignee: EMSYS Separation Technology B.V.
    Inventors: Adrianus P. Apeldoorn, Jachebus W. Bos, Johannes J. Dozy, Johannes J. Elling, Leonardus C. Gordijn, Pieter Ottens, Wayne S. Penny, Cornelis Spel, Aatje J. Spel-van der Linde, Tom M. Vader, Theodorus J. De Wit
  • Patent number: 5928469
    Abstract: Materials which are not themselves storage-stable at room temperature are made suitable for storage by mixing them with a carrier substance and spray drying the resulting mixture so as to form particles containing both the material and the carrier substance in which the carrier substance is in an amorphous, i.e. glassy or rubbery, state. Formation of such a composition greatly enhances stability. The material stored may be a biological material such as an enzyme, the components of a chemical reaction such as reagents for carrying out an assay, or even viable biological cells.
    Type: Grant
    Filed: May 11, 1994
    Date of Patent: July 27, 1999
    Assignee: Inhale Therapeutic Systems
    Inventors: Felix Franks, Ross Henry Hatley, Sheila Frances Mathias
  • Patent number: 5902457
    Abstract: An apparatus for generating a liquid spray from two jets of fluid which issue from a pair of opposing nozzles and interact, wherein the fluid is supplied to the nozzles under fully turbulent conditions such that random variations in the momentum of the fluid as it leaves the nozzles occur which results in random variations in the orientation of the resultant spray of liquid drops.
    Type: Grant
    Filed: August 18, 1994
    Date of Patent: May 11, 1999
    Assignee: AEA Technology PLC
    Inventors: Lionel Houston Ford, John William Stairmand
  • Patent number: 5820748
    Abstract: Gasses, water and solvents, major contaminants in used lubricating oils, can be removed from used lubricating oils at mild temperature conditions under vacuum. Apparatus in which the removal can take place includes a hollow vacuum separator vessel with a spray nozzle to spray an ultra fine spray of warm, used lubricating oil onto an angularly disposed thin film separator plate. In conjunction with the plate is a cooling device within the vacuum chamber. Cleaned oil can be passed from the bottom back into a holding tank, while water and solvents are drained out into a separate tank for safe disposal.
    Type: Grant
    Filed: April 25, 1997
    Date of Patent: October 13, 1998
    Inventor: Tajwar Shadikhan
  • Patent number: 5770020
    Abstract: The invention relates to a distillation apparatus (1) which is suitable in particular for the distillation of sea water into fresh water. The apparatus includes a plurality of flat, bag-like elements (3) formed from a thin film material such as plastic film and placed one against the other, the elements serving as heat exchangers between a vaporizing liquid flowing along the exterior surfaces of the element and a condensing vapor directed to the inside of the element, and a compressor (15) for increasing the pressure and temperature of the generated vapor before it is directed to the inside of the elements. The essential idea of the invention is that at the upper end of each bag-like element (3) there is a honeycomb-structured end strip (4) having substantially the width of the element, the strip containing parallel feeding ducts (26) separated from each other by partition walls, the ducts distributing the liquid to be evaporated over the entire width of the element surface.
    Type: Grant
    Filed: November 18, 1996
    Date of Patent: June 23, 1998
    Assignee: Keeran Corporation N.V.
    Inventors: Peter Koistinen, Reijo Rantala
  • Patent number: 5755924
    Abstract: An apparatus, e.g. centrifugal evaporator, has at least one rotary treatment surface, e.g. a heated evaporating surface, which rises outwards from the rotation axis, a liquid feed in the vicinity of the lowest point of the treatment surface close to the rotation axis and a product removal on the periphery of the treatment surface. Such an apparatus is characterized in that the treatment surface over at least part of its axial length has a stepped construction and each step has a step angle of approximately 90.degree.. Thus, as desired, a laminar or turbulent flow is possible. Through the construction of the steps it is possible to widely vary the nature of the flow and consequently the heat and material exchange, as well as the residence time of the liquid.
    Type: Grant
    Filed: August 23, 1996
    Date of Patent: May 26, 1998
    Inventor: Vaclav Feres
  • Patent number: 5728273
    Abstract: Method for bringing a gas and a liquid into contact with one another, the liquid being passed in the form of a film over an evaporator surface (1) provided with small openings and the gas being fed through the openings in the evaporator surface, which gas mixes with the liquid on the surface and absorbs vapor from the liquid, a liquid subsequently being passed in the form of a film over a condenser surface (11) provided with small openings and the gas which has absorbed vapors from the liquid film on the evaporator surface being fed through the openings in the condenser surface, at least some of the absorbed vapor condensing and being carried along with the liquid film on the condenser surface and removed.
    Type: Grant
    Filed: January 19, 1996
    Date of Patent: March 17, 1998
    Inventor: Leendert Aandewiel
  • Patent number: 5684125
    Abstract: The invention relates to a method for purifying liquid polysiloxane containing impurities as a low-molecular-weight fraction, by evaporating the low-molecular-weight fraction, in which method a liquid stream of impure liquid material in the form of a bundle of a multiplicity of streams or jets is brought into contact with a flowing gas phase, after which the gas stream, which contains the impurities, is removed and purified liquid material is collected; a device for performing this method and also the use of purified liquid material.
    Type: Grant
    Filed: May 26, 1995
    Date of Patent: November 4, 1997
    Assignee: Bayer Aktiengesellschaft
    Inventor: Franciscus Petrus Marie Nooren
  • Patent number: 5676802
    Abstract: An improved apparatus for treating waste water containing volatile and corrosive substances by steam-stripping to remove the volatile and corrosive substances from the waste water. The apparatus has a liquid pooling zone installed at a part over the waste water supplying part of a stripper tower and liquid distributor at the top of the tower, and pipe arrangement is prepared to recycle liquid drawn from the liquid pooling zone to the liquid distributor. In the pipe arrangement, a cooler for the recycling liquid is installed. Serious corrosion can be avoided utilizing this apparatus.
    Type: Grant
    Filed: April 10, 1995
    Date of Patent: October 14, 1997
    Assignee: JGC Corporation
    Inventors: Kenji Satoh, Naohiko Kagawa, Sei Tange, Shun-ichi Ohya
  • Patent number: 5658433
    Abstract: An integral system and method for the separation and purification in a single operation of a heat or oxygen-sensitive liquid feed, such as a plant derived liquid feed mixture of fatty acids, tocopherol compounds and sterols, into a low boiling point purified fraction of Vitamin E tocopherol compounds and a high boiling point concentrate fraction of triglycerides, which system can be maintained in the presence of an inert gas to provide reduced degradation and increased purity of the Vitamin E fraction. The system includes a pre-evaporator, a vapor-liquid separator, a packed bed distillation column, a rotary thin film evaporator and an evaporator-stripper.
    Type: Grant
    Filed: March 26, 1996
    Date of Patent: August 19, 1997
    Assignee: Artisan Industries Inc.
    Inventor: James L. Baird
  • Patent number: 5653852
    Abstract: A distilling device has an undistilled water tank to contain undistilled water, a cover covering the tank, a water heating area communicating with the tank, a high-frequency oscillator disposed under the water heating area, a heater disposed above the water heating area, a cooling area beside the heater, and a water collecting can disposed under the cooling area. The cooling area and the water heating area are separated by a separating plate.
    Type: Grant
    Filed: November 8, 1995
    Date of Patent: August 5, 1997
    Inventor: Ching Ping Meng
  • Patent number: 5628901
    Abstract: A single vessel with no moving parts is constructed to perform the functions of coalescing, vacuum dehydration, and thin film evaporation.
    Type: Grant
    Filed: April 30, 1993
    Date of Patent: May 13, 1997
    Assignee: Castrol Industrial North America Inc.
    Inventors: William L. Lawrence, Robert D. Coyle
  • Patent number: 5624534
    Abstract: An apparatus and method for stripping volatiles from a feed stream and concentrating the volatiles in the overhead vapors forming a condensate product and simultaneously producing a low percent volatiles outlet stream as a concentrate product. The volatiles separator and concentrator, ("VSC"), unit has many applications in the reduction and the concentration of voiatiles in the beverage, fuel, and industrial alcohol industries, as well as in chemical applications for removing or stripping volatiles from heat sensitive feed substrates which require low temperatures and a short residence time to prevent degradation of the product. For heat sensitive applications, the VSC unit utilizes a short feed stream preheat contact time in combination with turbulent high velocity flow to separate and concentrate volatile and nonvolatile components at temperatures below 100.degree. F. utilizing flash vaporization for volatiles separation with reboil capability to adjust volatiles concentration in the residue and product.
    Type: Grant
    Filed: June 7, 1995
    Date of Patent: April 29, 1997
    Inventors: Armand R. Boucher, Philip N. Hambrick
  • Patent number: 5624530
    Abstract: Spray drying system for drying a liquid feed which is made up of a solution or suspension of particles in a fluid medium. The system enables the spray drying of wet material and converting the material into powder by evaporation of a liquid medium at reduced pressure or at a vacuum. The system includes a heating chamber and an evacuation device, communicating with the interior of the heating chamber. This provision enables creation of reduced pressure within the chamber, accompanied by evaporation of the fluid medium at temperatures lower than needed for evaporation at normal pressure, and evacuation of the moisture vapor generated during evaporation.
    Type: Grant
    Filed: April 21, 1994
    Date of Patent: April 29, 1997
    Assignee: Ultrasonic Dryer, Ltd.
    Inventors: Akper Sadykhov, Raphael Semiat
  • Patent number: 5624531
    Abstract: An evaporator operating on falling film principle, has a shell (1) with a system (2) of evaporating tubes therein, whereby a liquid to be concentrated is fed on the outer surface of the evaporating tube system (2) and vapor is led to flow inside the tubes of the evaporating tube system (2). The evaporating tube system (2) is formed of evaporating elements, each evaporating element being formed of evaporating tubes (9) substantially on the same level. The upper ends of the tubes are connected to a common collecting chamber (8) and the lower end, respectively, to a common collecting chamber (10) in such a manner that there is a connection between both collecting chambers (8, 10) through each tube (9) between them, due to which the collecting chambers (8) of the upper end of the evaporating elements are interconnected through the upper connecting chamber (12), and respectively, the collecting chambers (10) of the lower end are interconnected through the connecting chamber (13) of the lower end.
    Type: Grant
    Filed: March 23, 1994
    Date of Patent: April 29, 1997
    Assignee: Tampella Power Oy
    Inventors: Matti Knuutila, Kalevi Nurminen, Jukka Vaistomaa, Anssi Makela
  • Patent number: 5601688
    Abstract: The horizontal distance traveled by droplets of starting solution sprayed into a gaseous medium above a catch basin, where the gaseous medium has a horizontal velocity component is controlled by controlling the size of the droplets as a function of the horizontal velocity component.
    Type: Grant
    Filed: October 30, 1992
    Date of Patent: February 11, 1997
    Assignee: Ormat Industries Ltd.
    Inventors: Gad Assaf, Joseph Weinberg
  • Patent number: 5573635
    Abstract: A thin film evaporating device includes a housing defining a space for receiving a plurality of elongated tubular evaporators. An inlet is associated with the housing for feeding a flowable heating medium to the space for heating the plurality of elongated tubular evaporators.
    Type: Grant
    Filed: June 3, 1994
    Date of Patent: November 12, 1996
    Assignee: Buss AG
    Inventor: Rolf Van Der Piepen