Spray Forming And Filming Patents (Class 202/236)
  • Patent number: 4981554
    Abstract: A thin-layer evaporator particularly suited for treating high-viscosity fluids, including a treating chamber surrounded by a heating or cooling shell, and a rotor equipped with feed and thrust elements. The feed and thrust elements include at least two axial, equidistant and staggered rows of blade members having the same pitch and sloping with respect both to the rotor axis and to the axial plane passing through their connection line; each member being offset, with respect to the members of the adjacent rows, by a space equal to the half pitch of the member.
    Type: Grant
    Filed: October 19, 1989
    Date of Patent: January 1, 1991
    Assignee: Montedipe S.p.A.
    Inventors: Mauro Loconsolo, Claudio Buonerba, Antonio Fucile, Francesco Ferrari
  • Patent number: 4981555
    Abstract: The solutions are concentrated by multiple-effect evaporation in indirectly heated evaporators. The highest concentration of the solution is reached in a final evaporator stage, which is heated with live steam. The final evaporators stage includes two to four falling-film evaporators, all of which are heated with live steam. The falling-film evaporators are consecutively flown through by the solution. Vapor is withdrawn from that falling-film evaporator which is the first to be supplied with the solution and at least part of said vapor is directly contacted with the solution as it flows down through the heating zone of at least one other evaporator of the final stage. From that falling-film evaporator of the final stage which is the first to be supplied with the solution the vapor may be fed to all other evaporators of the final stage.
    Type: Grant
    Filed: September 21, 1989
    Date of Patent: January 1, 1991
    Assignee: Metallgesellschaft AG
    Inventors: Klaus Hohmann, Manfred Mai
  • Patent number: 4959127
    Abstract: A system for desalinating saltwater. The system includes a platform container and a plastic dome covering through which solar ray heat passes to distall the saltwater fed therein and thereby separate therefrom distilled fresh water.
    Type: Grant
    Filed: June 22, 1987
    Date of Patent: September 25, 1990
    Inventor: Claus G. Michna
  • Patent number: 4953694
    Abstract: A distilling apparatus includes an evaporation section which heats raw water and causes the generation of vapor from said raw water, and a hydrophobic porous film through which the thus generated vapor is filtered. Because vapor separated from the raw water is supplied to one surface of the hydrophobic porous film, the proportion of the vapor relative to the fluid supplied to that surface of the film can be increased, thereby enabling the efficient filtering of a large amount of vapor through the film. In addition, because the temperature of condensed water obtained by cooling the vapor can be kept in the vicinity of the boiling point thereof, any gases and volatile substances contained in the raw water are prevented from dissolving in the distilled water, thereby enabling the production of extremely pure distilled water.
    Type: Grant
    Filed: June 17, 1988
    Date of Patent: September 4, 1990
    Assignee: Hitachi, Ltd.
    Inventors: Nobuatsu Hayashi, Sankichi Takahashi, Katsuya Ebara, Hideaki Kurokawa, Akira Yamada, Yasuo Koseki, Harumi Matsuzaki, Hiroaki Yoda
  • Patent number: 4953607
    Abstract: A thermal system includes a plurality of heat exchangers in series and the same number of flash tanks in series is interposed between two subsequent effects of a multiple effect evaporating system for sulfate black liquor. The liquor is indirectly heated in the heat exchangers by vapor produced by step-by-step expansion of the same liquor in the flash tanks and additionally by steam from an external source. To decrease the viscosity of the black liquor it is heated to a temperature of 190.degree.-200.degree. C. and retained in a reactor vessel for 10-20 minutes.Preferably the flash tanks and the heat exchange elements are positioned on top of each other within a shell to form an integral construction in which the vapor compartment of each flash tank is directly connected to the vapor compartment of a corresponding one of the heat exchange elements.
    Type: Grant
    Filed: June 14, 1989
    Date of Patent: September 4, 1990
    Assignee: A. Ahlstrom
    Inventors: Kiiskila Erkki, Ryham Rolf
  • Patent number: 4946559
    Abstract: A method and device for removing, from liquid such as water, dissolved volatile substances and gases when water is being distilled or evaporated. Feed water of a distilling apparatus or evaporator is heated to a sufficiently high temperature, whereby part of the feed water changes into vapor, and is then conducted to a purifying device. The feed water is discharged in the purifying device in the form of a thin film. The gaseous substances present in the feed water or liquid are separated by a separator device provided in the purifying device, and then conducted away through a connector provided on the purifying device.
    Type: Grant
    Filed: November 3, 1988
    Date of Patent: August 7, 1990
    Assignee: Oy Santasalo-Sohlberg AB
    Inventors: Rolf Kroneld, Markku Reunanen, Esko Huhta-Koivisto
  • Patent number: 4944839
    Abstract: A falling film evaporator in which some plate elements have their upper portions surrounded by a hood to prevent feed liquor from contacting hot vapor generated in the evaporator and exchanging heat therewith by direct contact. Other elements are located outside the hood.
    Type: Grant
    Filed: May 30, 1989
    Date of Patent: July 31, 1990
    Assignee: Rosenblad Corporation
    Inventor: Axel E. Rosenblad
  • Patent number: 4925558
    Abstract: The residue or residue fraction left behind during vacuum distillation in a crude oil refinery is further processed, in that it undergoes thin-film short-path distillation at a higher temperature and under a fine vacuum. Raising the temperature leads to a rise in the feed rate and to an improvement in the distillate/residue ratio.
    Type: Grant
    Filed: July 16, 1987
    Date of Patent: May 15, 1990
    Assignee: Buss A.G.
    Inventor: Peter Kappenberger
  • Patent number: 4925526
    Abstract: A falling film evaporator having vertical outer tubes with closed upper ends connected to an upper tube plate disposed in the lower region of the evaporator. Other parallel tubes are disposed inside the outer tubes and are connected to a lower tube plate under the upper tube plate. The evaporator also has a mechanism for distributing the material to be evaporated onto the upper ends of the outer tubes in such a way that the material flows down along the tubes and forms a film on the external surface of the tubes. The space between the tube plates, in which the ends of the outer pipes are located, is divided by an intermediate wall into an inlet and an outlet compartments. Heating steam is fed to the inlet compartment. Clean condensate is recovered from the inlet compartment and contaminated condensate from the outlet compartment.
    Type: Grant
    Filed: October 3, 1988
    Date of Patent: May 15, 1990
    Assignee: A. Ahlstrom Corporation
    Inventor: Reino I. Havukainen
  • Patent number: 4917770
    Abstract: A vertically extending distillation cylinder has a closed top and an open bottom having an electric heating element disposed therein to form a closure. Adjacent to the top of the distillation cylinder is connected a condensing tube. The condensing tube extends down through a condenser having a cooling water inlet at the bottom and a water discharge at the top. A throttle valve regulates the flow of cooling water. From the water discharge, a trough carries the water to impinge on the distillation cylinder causing pollutants to vaporize. The water collects below in a basin surrounding the distillation cylinder. A feed tube carries water from the basin to the bottom of the distillation cylinder. A discharge tube also connected to the bottom of the distillation cylinder carries water up to where it makes a U-turn. This regulates water height in the distillation cylinder. The discharge tube and an over flow tube from the basin discharge into a funnel from which water is conveyed to a sewer.
    Type: Grant
    Filed: August 7, 1989
    Date of Patent: April 17, 1990
    Inventors: Charles T. Asbury, Genevieve J. Asbury
  • Patent number: 4913777
    Abstract: A rotary evaporator for laboratory scale solvent evaporative procedures is described. A magnetically driven fluorocarbon coated rotor, being open at its base and closed at its top, operating within a container for solvents, creates a thin film for rapid solvent evaporation without the usual requirement for rotating the entire solvent assembly. Rotary seals are eliminated, increased control over bubbling and foaming at higher vacuum is obtained, and continuous solvent addition is simplified.
    Type: Grant
    Filed: December 2, 1988
    Date of Patent: April 3, 1990
    Inventor: Martin Parkinson
  • Patent number: 4906338
    Abstract: A method for removing the volatile constituents from gasoline and volatile organic chemicals from contaminated potable water when a fluid including gasoline-water mixture and when contaminated potable water is introduced into a vertical tower includes the steps of flowing the gasoline-water fluid and the water downward in a tower over and in contact with media trays stacked in courses in the tower. The media trays, either circular or square, fit closely within the tower inner wall, such trays are aluminum or molded plastic frames one inch by one inch angles one-eighth inch thick, with a plurality of one and one-half inch wide slats one-quarter of an inch thick on the top of the frame; the slats being spaced apart not less than one-half inch nor more than three-quarters of an inch.
    Type: Grant
    Filed: October 8, 1987
    Date of Patent: March 6, 1990
    Inventor: Walter W. DeLoach
  • Patent number: 4882009
    Abstract: A brine concentrator utilizing two separate concentrating devices in combination wherein a first concentrating device comprises a plurality of serpentine pipes interposed within a concentrator tank containing a dilute brine solution and a second concentrating device, including a venturi, is attached to the upper end of the concentrator tank and connected to receive exhaust gases from an exterior source. The brine solution which has been concentrated by the first concentrating device exit the tank through an output opening and is introduced into the venturi via a plurality of nozzles where it is mixed with the exhaust gases.A venting stack is also attached to the upper end of the tank for venting the exhaust gases emitted from the venturi and pre-heating dilute brine solution, which is introduced into the tank through the venting stack. As the solution travels down the stack and into the tank, it comes into contact with the exhaust gases exiting the tank from the venturi.
    Type: Grant
    Filed: July 13, 1987
    Date of Patent: November 21, 1989
    Assignee: Four Nines, Inc.
    Inventors: Joseph J. Santoleri, Richard D. Ross
  • Patent number: 4879004
    Abstract: In order to dissolve oil or PCB which exists in the electrical insulation of parts to be cleaned, a solvent is evaporated during a heating phase by an evaporator located with the parts in an autoclave. The solvent vapor condenses on the parts and penetrates into the electrical insulation to form an oil or PCB-solvent mixture. In the heating phase, a plurality of intermediate pressure reductions are carried out in the autoclave, and during each intermediate pressure reduction the solvent is simultaneously distilled out of the oil or PCB-solvent mixture, directly from the autoclave. That is, during each of the pressure reductions, the solvent supply is discontinued and the mixture circulated through a circulating line. Following the completion of each intermediate pressure reduction, the pure oil or PCB present in a condensate vessel is pumped out by an intermediately located feed pump through a connecting line and into a reservoir.
    Type: Grant
    Filed: May 4, 1988
    Date of Patent: November 7, 1989
    Assignee: Micafil AG
    Inventors: Gustav Oesch, Paul Gmeiner, Urs Hofer
  • Patent number: 4878535
    Abstract: Heating elements formed by joining a pair of plates around most of their peripheries are provided with an internal partition which separates upper and lower internal spaces within the element so that separate streams of condensate are discharged from the element. A plurality of such plate elements can be used in a falling film condenser.
    Type: Grant
    Filed: April 27, 1988
    Date of Patent: November 7, 1989
    Assignee: Rosenblad Corporation
    Inventor: Axel E. Rosenblad
  • Patent number: 4865689
    Abstract: A device for removing the volatile components of a polymer in a polymer train includes a hollow pipe which defines an interior chamber, a pair of flanges mounted on opposite axial ends of the pipe, a heat jacket mounted on the pipe and disposed to surround the pipe, a plurality of band heating elements mounted on the outer peripheral surface of the heat jacket, and an arrangement of fin elements disposed in the interior chamber of the pipe to contact the polymer flowing through the pipe. Heat from the heating elements is distributed by the heat jacket over the axial length of the pipe and is transferred to the fin elements to heat the polymer flowing through the pipe. The fin elements may be in a cruciform arrangement within the interior chamber of the pipe. A method of removing the volatile components includes forming a thin film of polymer and heating and distributing the heat evenly on the thin film of polymer so that the volatile components may be vaporized.
    Type: Grant
    Filed: January 27, 1988
    Date of Patent: September 12, 1989
    Assignee: Mobil Oil Corporation
    Inventor: Clarence C. Hon
  • Patent number: 4863570
    Abstract: Process for the fractional distillation of a liquid under vacuum comprising preheating a liquid to be distilled, forming under vacuum the preheated liquid into a first series of thin sheets of falling liquid to be distilled, and a cooling liquid into a second series of thin sheets of falling cooling liquid, the thin sheets of the first series being alternately arranged with the thin sheets of the second series, in close proximity to one another. Part of the liquid to be distilled is vaporized and passed to the thin sheets of cooling liquid to form liquid distillate and separately recovering the liquid distillate with the cooling liquid and the non-vaporized part of the liquid.
    Type: Grant
    Filed: August 31, 1987
    Date of Patent: September 5, 1989
    Assignee: Shell Oil Company
    Inventor: Enno F. Wijn
  • Patent number: 4863568
    Abstract: An apparatus for the fractional distillation of a liquid under vacuum is disclosed in which first and second inlets are disposed in the upper portion of a normally vertically closed vessel for the entrance of a liquid to be distilled and a cooling liquid, respectively and outlets are provided in the bottom portion of the vessel for the residue for the liquid being distilled and for the cooling liquid. First and second distribution means are provided for establishing thin sheets of liquid to be distilled and cooling liquid wherein each thin sheet falls freely absent both support and guiding means. Means are also provided for separately collecting the liquid distillate with the cooling liquid in the residue of the liquid to be distilled.
    Type: Grant
    Filed: May 29, 1987
    Date of Patent: September 5, 1989
    Assignee: Shell Oil Company
    Inventor: Enno F. Wijn
  • Patent number: 4857279
    Abstract: Edible fats and oils are extracted from oil-bearing materials by loading the raw materials onto an inlet end of a flat and fixed conveying surface having elongate slits therein. The materials are conveyed from the inlet end to the outlet end of the conveying surface by scrapers moved by endless chains. Oil extracting solvent is sprayed onto the material on the conveying surface, to produce miscella, which flows through the slits in the surface and into hoppers beneath the surface. The miscella is circulated back to additional sprayers located upstream of the solvent sprayers for spraying the miscella onto the upstream end of the conveying surface. The resulting concentrated miscella is collected in hoppers beneath the surface and delivered to a further use.
    Type: Grant
    Filed: December 24, 1986
    Date of Patent: August 15, 1989
    Assignee: Showa Sangyo Co., Ltd.
    Inventors: Yoshio Kawamata, Kiyoshi Iwai
  • Patent number: 4822455
    Abstract: A distilling and desalination apparatus comprising an evaporation chamber and a condensing chamber in which the evaporation chamber through a cooling circuit communicates by way of heat exchange with the condensing chamber and rotates in relation thereto. The evaporation chamber is constructed to form a thin fluid film on the inner surface of the evaporation chamber during rotation, surplus water being slung out along the edge and into channels and led tangentially to the rear by blades. The cooling circuit comprises a condensing portion and an evaporation portion, the fluid being evaporated along the inner surface of the coolant condensing portion, and fluid vapors being condensed along the outer surface of the coolant condensing portion, whereupon the drops of fluid are slung outwards and collected.
    Type: Grant
    Filed: January 7, 1987
    Date of Patent: April 18, 1989
    Assignee: Chas. Hude
    Inventor: Henrik-Gerner Olrik
  • Patent number: 4812203
    Abstract: An evaporator which is formed, in combination, of a first evaporator of a centrifugal falling-film type; and a second evaporator having a shape formed of a heating side wall portion of a downward-pointing conical configuration, a cover portion defining at least one opening, through which a liquid to be treated is charged and resulting volatile components are discharged, and a bottom portion defining at least one opening permitting discharge of an evaporation residue. A scraping agitator is built in the second evaporator. The side wall portion is externally wrapped with a pipe or the like, whereby a heating medium is caused to pass therethrough for heating the side wall portion. The evaporation residue discharge opening of the first evaporator is connected to the opening of the cover portion of the second evaporator.The above evaporator is suitable to recover a volatile component from a high-viscosity liquid containing tar-like substances. It can achieve a high recovery rate.
    Type: Grant
    Filed: June 23, 1987
    Date of Patent: March 14, 1989
    Assignee: Mitsui Toatsu Chemicals, Incorporated
    Inventors: Kenji Obata, Nobuhiko Yoneda, Masabumi Kataita, Yoshihiro I, Hironori Yamashita
  • Patent number: 4810327
    Abstract: In a falling film evaporator of the vertical-tube type in which liquid to be evaporated is supplied at the top on the outer surface of vertical heat exchanger tubes and the heat medium is supplied to the heat exchanger tubes at the bottom for flow inside the same, at least one larger tube element than the heat exchanger tubes is disposed between and fixed to tube plates at the both ends of the group of tubes to stabilize the group of tubes against tension and especially compression stresses.
    Type: Grant
    Filed: April 18, 1985
    Date of Patent: March 7, 1989
    Assignee: Ahlstromforetagen Svenska AB
    Inventor: Kjell Norrmen
  • Patent number: 4790904
    Abstract: An atmospheric evaporator for reducing the water content of various chemical solutions, more particularly useful in the electroplating industry, wherein the evaporator includes a solution-secure molded tank in which a removable blower sleeve is mounted having a blower inlet duct and support strut members formed at the opposite end thereof to support a multiplicity of finned evaporator members over which the solution is sprayed. When a large-volume, low RPM blower is mounted to the inlet duct, a straight-line downdraft of both air and solution is created, allowing the air and evaporated water to exhaust through an up-facing outlet duct, thus defining a substantially "U" shaped duct arrangement from the inlet side to the exhaust side of the tank with the heavy chemical particles returning to the process tank from the bottom of the evaporator tank.
    Type: Grant
    Filed: May 19, 1987
    Date of Patent: December 13, 1988
    Inventor: William Yates
  • Patent number: 4790911
    Abstract: A rotary evaporator for laboratory scale solvent evaporative procedures is described. A magnetically driven fluorocarbon coated rotor, operating within a container for solvents, creates a thin film for rapid solvent evaporation without the usual requirement for rotating the entire solvent container assembly. Rotary seals are eliminated, increased control over bubbling and foaming at higher vacuum is obtained, and continuous solvent addition is simplified.
    Type: Grant
    Filed: December 11, 1987
    Date of Patent: December 13, 1988
    Inventor: Martin Parkinson
  • Patent number: 4786363
    Abstract: An evaporator includes heating elements which are part of a thin skin providing the evaporator vessel wall, supporting the skin for internal and external pressure, and a top portion of the vessel. A liquor distributing plate is supported on the heating elements, with a liquor inlet donut-shaped conduit disposed above the liquor distributing plate. The heating elements are radially disposed within the vessel, and are supported at the bottom by a ring which engages the bottoms of the heating elements, and a vertical axis tube extending from the vessel bottom to the ring, the tube having a plurality of through-extending openings formed in it. The vapor outlet for the vessel is concentric with the heating elements and the liquor distributing perforated plate. Heating fluid (e.g. steam) is introduced into the interior volumes of the heating elements adjacent the tops thereof, and a vent is provided adjacent the bottoms.
    Type: Grant
    Filed: February 20, 1987
    Date of Patent: November 22, 1988
    Assignee: Kamyr, Inc.
    Inventors: Carl L. Elmore, Charles W. Dier
  • Patent number: 4781797
    Abstract: An apparatus and process for separating a more volatile substance from a liquid in which it is dissolved by vacuum means. The apparatus has a perforated inner casing having a plurality of sub-stages which contain packing material to provide a tortuous path of interstices for the liquid to flow through; an outer casing surrounds the inner casing to define an evacuating space between the outer and inner casing and vacuum means to create a vacuum in the evacuating space which communicates with the sub-stages through the perforations in the inner casing. The vacuum means also acts to pull off the more volatile substance.
    Type: Grant
    Filed: September 11, 1987
    Date of Patent: November 1, 1988
    Assignee: Energy Conservation Partnership, Ltd.
    Inventor: Arthur F. Johnson
  • Patent number: 4778535
    Abstract: An apparatus for vaporizing and recovering, by condensation, a composite mixture of at least two components, at least one of which is a liquid. The apparatus includes at least one chamber in which the mixture is brought to boiling and includes means to condense the vaporized portion of the mixtures. A liquid of the mixture in the vaporizing chamber is vaporized by heating coils and subjected to circulation to uniformly disperse the mixture. The apparatus may further include a system for continuously filtering the mixture in the vaporizing chamber to remove undesirable particulates, a mixture spray device for spraying the mixture into the vaporizing chamber, and an ultrasonic vibrating means.
    Type: Grant
    Filed: September 28, 1982
    Date of Patent: October 18, 1988
    Inventor: James W. McCord
  • Patent number: 4767498
    Abstract: Photographic waste solution is treated by a method which comprises contacting the waste solution with air, in an especially designed treatment vessel, at a solution temperature of from about 120.degree. F. to about 140.degree. F. The air thus becomes supersaturated with the liquid in the waste, and the waste solution is thus concentrated to form a waste slurry which is transferred out into a waste storage vessel. The supersaturated air which is virtually free from waste is discharged to the atmosphere. The method is carried out in an especially constructed apparatus comprising a uniquely designed treatment vessel.
    Type: Grant
    Filed: August 20, 1987
    Date of Patent: August 30, 1988
    Inventor: Lawrence M. Kreisler
  • Patent number: 4762592
    Abstract: A wobbling-type evaporator mounts a container 1 holding at least one vertically oriented heat transfer tube 30 fed by a liquid inlet 35 to the container 1. The container 1 is supported with respect to a base 10 so that it wobbles in response to the rotation of an orbiting counterweight 2,2' the counterweight and container wobble as a two body system about common axis. In one form a set of struts 6 located around the container are part of the support system. The invention also includes inlet water distribution systems, compatible with this orbital drive.
    Type: Grant
    Filed: October 20, 1986
    Date of Patent: August 9, 1988
    Inventor: Yao T. Li
  • Patent number: 4756797
    Abstract: A multiple effect evaporator system and a process for concentrating a process liquid wherein evaporated process liquid from one effect serves as heating fluid in an adjacent effect. Low energy heating fluid in vapor form is fed to an evaporative surface condenser where it is condensed and collected as clean and foul condensate. Coolant for the evaporative surface condenser is provided in the form of process liquid from one of the effects. Prior to passage into the evaporative surface condenser, the process liquid is cooled. In the cooling circuit of the evaporative surface condenser, the process liquid absorbs the heat of condensation of the heating fluid and subsequently rejects the heat into a counter flowing air stream. The process liquid is thereafter heated and returned to another of the multiple evaporator effects.
    Type: Grant
    Filed: October 20, 1986
    Date of Patent: July 12, 1988
    Assignee: Kamyr, Inc.
    Inventors: Carl Elmore, Timothy Carter
  • Patent number: 4747915
    Abstract: A falling-film process and apparatus for the cocurrent evaporation of a solution is disclosed. The process utilizes a tube-bundle heat exchanger in which the upper ends of the individual tubes of the tube-bundle are closed. Apertures, preferably in the form of slots, are formed adjacent the closed-end of the individual tubes. A liquid heel is maintained above the highest of said apertures and flows into the interior of the tubes through said apertures. Upon entering the tubes the liquid and any vapor released therefrom flows cocurrently in a downward direction. The vapors released from the liquid are recycled to a point above the liquid heel through conduit means separate from the individual tubes.
    Type: Grant
    Filed: March 6, 1986
    Date of Patent: May 31, 1988
    Assignee: Montedison S.p.A.
    Inventor: Giorgio Pagani
  • Patent number: 4741803
    Abstract: A spray dryer consisting of a tower-like drying container with spraying elements for introducing therein the material to be dried, pipelines and heater for injecting a heated drying gas, and a separator for separating dry fine material and gas. The dry fine material is agglomerated inside the drying tower. The separator consists of porous filter tubes, on which a dust-laden gas stream impinges, which covers the entire flow cross-section of the drying tower. Fine product material deposited on the filter tubes is shaken off by surges of compressed air and drops into a drying zone, a spraying zone, and finally, into a collecting hopper.
    Type: Grant
    Filed: December 20, 1985
    Date of Patent: May 3, 1988
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventor: Rudolf Loeffelmann
  • Patent number: 4731159
    Abstract: An evaporator comprises a plurality of substantially parallel plates mounted for rotation about a common axis and in which provision is made for a condensible vapor to flow across a first face of each of said plates and for a liquid, at least a portion of which is to be evaporated, to flow across the second face of each of said plate, which plates are arranged to be rotatable at such a mean acceleration, measured in a radial direction with respect to said axis of rotation, greater than the acceleration due to gravity, said first face of each of said plates has a surface designed to discourage formation of a continuous liquid film thereon. The evaporator may be used to concentrate solutions, e.g. of depleted brine or aqueous caustic soda.
    Type: Grant
    Filed: December 19, 1985
    Date of Patent: March 15, 1988
    Assignee: Imperial Chemical Industries plc
    Inventors: John E. Porter, Colin Ramshaw
  • Patent number: 4707220
    Abstract: A thin film evaporator consists of an enclosure defining a vapor space, a level drive shaft running into the enclosure and a rotor fixed to the shaft and having an axis of rotation disposed horizontally when in operative position, the rotor being made up of spaced coaxial conical evaporator elements, whose evaporation space communicates with the vapor space. The feed to be evaporated is supplied at one end of the rotor at the inner circumference of one or more conical evaporator elements thereof. Such evaporator elements are placed together in pairs so that they taper outwards with the evaporating faces thereof facing each other, so as to form a collection trough at their outer edges for the concentrate. The feed spreads out in the form of a film from the inner edge or edges for the elements and is taken up in the respective collection trough as a preconcentrate.
    Type: Grant
    Filed: March 14, 1986
    Date of Patent: November 17, 1987
    Inventor: Vaclav Feres
  • Patent number: 4706741
    Abstract: In a heat exchanger of falling film type comprising heat exchange plates with area enlarging corrugation forming ridges and valleys extending in the falling film direction, repeated redistribution of the falling film is brought about by having the ridges and the valleys extending continuously within each of a number of zones formed one after the other in the falling direction, whereas the ridges and the valleys with regard to two consecutive zones are laterally displaced in relation to each other such that the ridges and the valleys, respectively, in one zone extend in alignment with the valleys and the ridges, respectively, in a consecutive zone.
    Type: Grant
    Filed: November 29, 1985
    Date of Patent: November 17, 1987
    Assignee: Alfa-Laval Food & Dairy Engineering AB
    Inventors: Ulf Bolmstedt, Bengt Lundblad
  • Patent number: 4702799
    Abstract: A finely atomized liquid is projected in a stream and dried by contact with drying gas. The drying gas is projected in turbulent flow from opposite sides of the stream such flow being distributed along the length of the stream. The material may be atomized and projected by a jet of gas issuing from a nozzle, and the drying gas may be projected around the jet so that the drying gas meets the entrainment demand of the jet, thereby preventing recirculation of gases outside the jet.
    Type: Grant
    Filed: September 3, 1985
    Date of Patent: October 27, 1987
    Assignee: Nestec S.A.
    Inventor: James Tuot
  • Patent number: 4698136
    Abstract: A process for the continuous production of boiler feed water from process waters in the oil extraction industry during which salts and hydrocarbons are removed from the water, without Fe.sup.++ precipitating. The heavy hydrocarbons are mechanically separated, the volatile hydrocarbons are separated from the water, by means of a thermal degassing, and the low boiling and the non-condensable hydrocarbons are separated in a shower evaporation step with downstream vapor compression, wherein the low boiling non-condensable hydrocarbons are evaporated with the waste water within the shower evaporator and the non-condensable hydrocarbons then are drawn off from a downstream separator. A salt-free oxygen-free pure water is removed from a separator.
    Type: Grant
    Filed: May 23, 1985
    Date of Patent: October 6, 1987
    Assignee: Fried Krupp GmbH
    Inventor: Mohammed El-Allawy
  • Patent number: 4687547
    Abstract: The present invention provides a process for the separation of materials obtained by means of high pressure extraction from an extraction agent, wherein extraction agent loaded with extracted material is passed from below into a separator comprising a head (2), a bottom (3), a runback pipe (4) and a heat exchanger (1) in the form of one or more pipes and extract recycled in a forced circulation via the head (2) and the runback pipe (4) to the bottom (3) and there either discharged and/or returned to the heat exchanger (1), the extraction agent evaporated in the heat exchanger being removed via a filter (11) on the head (2).
    Type: Grant
    Filed: March 22, 1985
    Date of Patent: August 18, 1987
    Assignee: SKW Trostberg Aktiengesellschaft
    Inventors: Herbert Jekat, Erwin Schutz, Kurt Stork
  • Patent number: 4683026
    Abstract: A thin layer evaporator comprises a container forming a body, a container cover on the one side, a drive shaft projecting into the container from the opposite side, a rotor fixed to the drive shaft and which has one or more conically outwardly widening evaporator areas and whose evaporator chamber is connected to the body, as well as a heating chamber separated from the body. The starting product is fed to the inner periphery of the evaporator areas, spreads outwards therefrom in a thin film and the concentrate is removed on the outer periphery by means of a draw-off pipe. In order to be able to absorb dynamic forces in a vibration free manner, the drive shaft is partly constructed as a hollow shaft and is mounted on a fixed spindle projecting into the container and rotor.
    Type: Grant
    Filed: May 8, 1985
    Date of Patent: July 28, 1987
    Inventor: Vaclav Feres
  • Patent number: 4683025
    Abstract: A method and apparatus for converting a long tube vertical evaporator to a falling film evaporator in a manner which permits salvaging most of the long tube vertical evaporator structure. The bottom chamber of the existing evaporator is extended to define a flash chamber intermediate the existing heat exchanger chamber and the bottom chamber. A vapor riser conduit is provided for directing vapor from the flash chamber to the vapor separation chamber positioned above the heat exchanger chamber. A recirculation conduit is provided for directing liquid from the bottom chamber therethrough into a distribution chamber which is provided above and in communication with the upper ends of the heat exchange tubes positioned in the heat exchanger chamber. The distribution chamber is preferably provided with a plurality of spray nozzles which communicate with the recirculation conduit to evenly distribute a film of liquid downwardly through the heat exchange tubes.
    Type: Grant
    Filed: February 10, 1986
    Date of Patent: July 28, 1987
    Assignee: The Graver Company
    Inventor: A. Roland Flores
  • Patent number: 4673459
    Abstract: A free flow evaporator of the falling film type has the heating elements disposed in a circular configuration so that each extends radially a distance less than the interior radius of the evaporator cylindrical vessel. Heating vapor is introduced concentrically into the top of the vessel and passes into the tops of the heating elements, and condensate is withdrawn from the bottoms of the heating elements in the vessel. Excess vapor passes through a vapor vent in the bottom of the vessel. The boiling liquid, such as black liquor from paper pulp processing, is introduced through a header above an annular channel with a perforated plate bottom, the perforated plate being disposed on top of the heating elements. The evaporated liquid vapor passes radially outwardly in the vessel, and then upwardly, and is discharged from the top of the vessel and passes to the top of another vessel (providing another effect), to provide heating vapor to the other vessel.
    Type: Grant
    Filed: June 18, 1985
    Date of Patent: June 16, 1987
    Assignee: Kamyr, Inc.
    Inventors: Carl L. Elmore, Paul Sherman, Daniel A. McGrath
  • Patent number: 4668345
    Abstract: Desalination apparatus comprising a vessel, an evaporation surface for receiving saline water in the vessel, a condensation chamber arranged in the vessel beneath the evaporation surface, an evaporation chamber arranged in the vessel above the evaporation surface, a fresh water tank for containing a reservoir of fresh water and fresh water vapor thereabove, a first conduit connecting the fresh water tank and the condensation chamber, a pump for compressing in the condensation chamber fresh water and fresh water vapor to maintain a pressure-temperature differential between the condensation chamber and the evaporation chamber at the evaporation surface, a second conduit connecting the evaporation chamber and the fresh water tank for removal of fresh water vapor from the evaporation chamber and its delivery to the reservoir of fresh water, and valves and conduits for conveying saline water to the evaporation surface and for taking off fresh water accumulated in the fresh water tank.
    Type: Grant
    Filed: February 26, 1985
    Date of Patent: May 26, 1987
    Inventor: Thomas B. Warren
  • Patent number: 4664752
    Abstract: An aqueous saline vapor is passed through a porous mass having a temperature no less than that of the vapor and subsequently condensed to provide substantially salt-free water.
    Type: Grant
    Filed: November 26, 1982
    Date of Patent: May 12, 1987
    Assignee: Industrial Filter & Pump Mfg. Co.
    Inventors: James F. Zievers, Paul Eggerstedt
  • Patent number: 4659433
    Abstract: Apparatus for concentrating and dehydrating maleic acid to form maleic anhydride, comprising: at least a first and a second vertical, independent and distinct, falling thin-film, multitubular evaporators of the static type arranged in series, wherein the first thin-film multitubular evaporator of the static type has an upper part and a lower part and includes a feedpipe at the upper part and a discharge pipe at the lower part; a separator connected by its sidewall to the discharge pipe from the first evaporator and including a first discharge pipe at the upper portion thereof and a second discharge pipe at the lower part; the second thin-film multitubular evaporator of the static type having a feedpipe having an upper part and a lower part connected to the second discharge pipe from the separator and including a discharge pipe only at the lower part thereof; a boiler having an upper part and a lower part, said upper part of said boiler being connected to and in open communication with the lower portion of the
    Type: Grant
    Filed: August 12, 1983
    Date of Patent: April 21, 1987
    Assignee: Societe Chimiques des Charbonnages
    Inventor: Roland Kotwica
  • Patent number: 4655879
    Abstract: An improved process for purification of glycerol obtained from natural sources comprising alkalizing a glycerol-containing crude mixture in the presence of air for oxidation, evaporating the mixture in a thin-layer evaporator with redistillation of the residue, rectification and reevaporation in a packed column characterized by low-pressure-loss plates with a falling-film evaporator designed for internal and external partial condensation and to separate off unwanted constituents of the mixture, bleaching the product with activated carbon and separating the bleach in known manner.
    Type: Grant
    Filed: October 26, 1984
    Date of Patent: April 7, 1987
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Rolf Brockmann, Lutz Jeromin, Wilhelm Johannisbauer, Helmut Meyer, Otto Michel, Juergen Plachenka
  • Patent number: 4636283
    Abstract: In the distillation of fresh water from sea water, the sea water is passed ownwardly in a falling film evaporator through a multiplicity of vertical tube evaporator (VTE) stages and multiple stage flash (MSF) evaporators. After the sea water passes through the first VTE stage where it forms a liquid component and a steam component, the liquid component is distributed evenly into the next VTE stage while the steam component enters an adjoining MSF stage. Condensed fresh water flows downwardly from one MSF stage to the next and experiences flash evaporation. The sea water or brine component and the fresh water distillate flow downwardly through the VTE and MSF stages so that the brine component can be removed from the final VTE stage and the fresh water distillate from the final MSF stage.
    Type: Grant
    Filed: March 6, 1984
    Date of Patent: January 13, 1987
    Assignee: D.V.T. Buro fur Anwendung Deutscher Verfahrenstechnik H. Morsy
    Inventor: Gamal E. D. Nasser
  • Patent number: 4627890
    Abstract: In a centrifugal mass transfer device comprising a rotary annular permeable element, annular plates are mounted adjacent the radially inner or outer face of the permeable element and gaseous or liquid material flowing from the permeable element across one surface of the annular plates is cooled or heated by a heat exchange fluid on the opposite surface of the plates. In this way condensed or vaporized material is returned to the permeable element.
    Type: Grant
    Filed: November 22, 1982
    Date of Patent: December 9, 1986
    Assignee: Imperial Chemical Industries PLC
    Inventors: John E. Porter, Colin Ramshaw
  • Patent number: 4618399
    Abstract: An evaporation or distillation apparatus uses one or more tubes driven to wobble about a vertical wobble axis that is aligned with the tube. A fluid distributor supplies a fluid to the inner surface of the wobbling tube at its upper end. A flexible whip rod located at least in part within the tube slides around over the inner surface as the tube wobbles. The pressure generated between the wobbling whip rod and the tube spreads the incoming fluid stream into a very thin film having a uniform thickness over the entire length of the tube. In the preferred form the whip rod is anchored at its lower end to a stationary base and is restrained against rotation about its own longitudinal axis, but is sufficiently flexible at its lower end to act as a universal joint. In this preferred form the whip rod has a flexible core surrounded by at least one length of tubular sheathing.
    Type: Grant
    Filed: April 9, 1984
    Date of Patent: October 21, 1986
    Inventor: Yao T. Li
  • Patent number: 4613410
    Abstract: A method and apparatus for distilling, especially vacuum refining and deodorizing edible oils and fats utilizing sheets of oil driven downwardly in a distiller with a vacuum source at its top. A nozzle includes pressure equalization chambers, cantilever adjustment screws, and a central drag sheet to produce longer lasting and more uniform thin oil sheets to be driven in the distiller. A continuous process deaerates, dehydrates, degums, bleaches, refines, removes tocopherol, deodorizes, and strips peroxides and hydroperoxides from raw oil in a series of isothermal stages utilizing driven sheet distillers. No stripping steam is used except in the stage which strips peroxides and hydroperoxides. The method produces valuable, pure products such as tocopherol and fractionated fatty acids. It is especially efficient in heat exchange and low in waste and pollution producing products.
    Type: Grant
    Filed: October 7, 1983
    Date of Patent: September 23, 1986
    Inventor: Jacob B. Rivers, Jr.
  • Patent number: 4608119
    Abstract: An apparatus for concentrating aqueous solutions of hygroscopic organic liquid having boiling points higher than the normal boiling point of water is disclosed. The apparatus includes an airtight evacuated chamber, means for injecting a preheated temperature adjusted solution into the chamber to vaporize water from the solution and produce a concentrated aerosol of organic liquid, and means for coalescing the concentrated aerosol. Also included is a system for recovery of organic vapor leaving the chamber along with the vaporized water.
    Type: Grant
    Filed: May 14, 1984
    Date of Patent: August 26, 1986
    Assignee: Niagara Blower Company
    Inventor: Jack T. Rowland