With Measuring, Testing Or Inspecting Patents (Class 203/1)
  • Patent number: 11939210
    Abstract: Systems operable to blend at least one finished gasoline from a refined petroleum product comprising at least one neat gasoline with ethanol and optionally butane utilizing a blend model that calculates a volumetric blend ratio comprising at least one neat gasoline, ethanol and optionally, butane. The blend model incorporates estimated values for the octane number and the volatility of the ethanol and butane when calculating the volumetric blend ratio.
    Type: Grant
    Filed: November 10, 2023
    Date of Patent: March 26, 2024
    Assignee: Phillips 66 Company
    Inventors: James C. Moynihan, Paul M. Ryder, Robert L. Schnefke
  • Patent number: 11865473
    Abstract: Methods and apparatus consistent with the present disclosure may provide electrical energy and thermal to extraction or separation equipment. Methods and apparatus consistent with the present disclosure may extract and concentrate essential elements plant matter. An amount of wasted heat energy collected from a engine that powers an electrical generator may be provided to an evaporation or separation process when electrical power is provided to extraction or separation processing equipment. Computers or electronics that control equipment consistent with the present disclosure may be remotely controlled via a mobile electronic device, when desired. Such computers or electronics may receive sensor data related to the operation of plat matter extractors, related separation equipment, or other equipment may be used to manage a production line.
    Type: Grant
    Filed: January 17, 2022
    Date of Patent: January 9, 2024
    Inventors: Andrew David Hospodor, Robert James Rapp
  • Patent number: 11648489
    Abstract: An herbal distillation device includes a herb chamber with perforated holes for holding herbs and a closed heated boiling chamber with openings at the side for a steam outlet. The herbal distillation device further includes an electric air-cooled condensation chamber which connects to the boiling chamber.
    Type: Grant
    Filed: June 22, 2022
    Date of Patent: May 16, 2023
    Inventor: Liang Guo
  • Patent number: 11592379
    Abstract: A method of determining vapor pressure of a fluid is provided. The method includes the steps of providing a meter (5) having meter electronics (20), the meter (5) being at least one of a flowmeter and a densitometer, and flowing a process fluid through the meter (5). A pressure of the process fluid is measured. The pressure of the process fluid is adjusted until a monophasic/biphasic boundary is reached. The flowing vapor pressure of the process fluid is determined at the monophasic/biphasic boundary.
    Type: Grant
    Filed: November 13, 2017
    Date of Patent: February 28, 2023
    Assignee: Micro Motion, Inc.
    Inventors: Justin Craig Hollingsworth, Marc Allan Buttler, Jason Alan Leapley
  • Patent number: 11565529
    Abstract: In one example, a dehumidifier for an inkjet printer includes a condensing unit and a chiller to circulate coolant through the condensing unit. The condensing unit is made of a thermally conductive material forming elongated exterior condensing surfaces and an interior coolant flow passage extending lengthwise between the condensing surfaces.
    Type: Grant
    Filed: June 21, 2017
    Date of Patent: January 31, 2023
    Assignee: Hewlett-Packard Development Company, L.P.
    Inventors: Nicholas J Meisner, Joe Santich, Robert K Saathoff
  • Patent number: 11407655
    Abstract: A system and method for decontaminating a fluid and recovered vapor, particularly processing and recycling water used in an oil zone steam process, utilizing a vaporizer-desalination unit to separate a contaminated water flow into a contaminated disposal flow and a clean water vapor flow. The contaminated water flow is recovered after separation from a combined oil and water flow from an oil well. The clean water vapor flow is preferably passed through a steam generator to produce the steam used in the oil zone steam process. The steam is injected into the oil zone of a designated well and then extracted as the combined oil and water flow. Once primed with sufficient external water, the system and method is designed to operate continuously with minimal replenishment because of the water/vapor/steam cycle.
    Type: Grant
    Filed: July 7, 2020
    Date of Patent: August 9, 2022
    Assignee: Verno Holdings, LLC
    Inventors: John D. Riley, Dana L. Johnson, Harry Patrick Barnum
  • Patent number: 11338219
    Abstract: Embodiments disclosed relate to a debutanizer with a dividing wall. The configuration of the debutanizer includes having a feed section, a top section, a bottom section, and a draw-off section. The debutanizer produces a C4s product, a C5s product and a natural gasoline (NG) product from a C4+s feed. The dividing wall is configured such that an upper portion of the dividing wall is positioned off-set from a vertical centerline and a lower portion of the dividing wall is positioned along the vertical centerline of the debutanizer. A process of use of the debutanizer is also disclosed. A natural gas liquids (NGL) system that includes parallel debutanizers, each with a dividing wall, and a process of use of such system, is also disclosed.
    Type: Grant
    Filed: August 13, 2020
    Date of Patent: May 24, 2022
    Assignee: SAUDI ARABIAN OIL COMPANY
    Inventor: Hae Yong Noh
  • Patent number: 11224823
    Abstract: Methods and apparatus consistent with the present disclosure may provide electrical energy and thermal to extraction or separation equipment. Methods and apparatus consistent with the present disclosure may extract and concentrate essential elements plant matter. An amount of wasted heat energy collected from an engine that powers an electrical generator may be provided to an evaporation or separation process when electrical power is provided to extraction or separation processing equipment. Computers or electronics that control equipment consistent with the present disclosure may be remotely controlled via a mobile electronic device, when desired. Such computers or electronics may receive sensor data related to the operation of plant matter extractors, related separation equipment, or other equipment may be used to manage a production line.
    Type: Grant
    Filed: June 22, 2020
    Date of Patent: January 18, 2022
    Inventors: Andrew David Hospodor, Robert James Rapp
  • Patent number: 11040294
    Abstract: A laboratory device, in particular a rotary evaporator, serves for evaporating a substance, preferably under reduced pressure, and comprises an evaporation flask for receiving the substance to be evaporated, a condenser for condensing the evaporated substance and a vapor passage for passing through the evaporated substance, which vapor passage is arranged in a vapor path between the evaporation flask and the condenser. The laboratory device further comprises a detection unit for foam detection, which detection unit is provided outside of the vapor passage and/or the evaporation flask.
    Type: Grant
    Filed: June 26, 2018
    Date of Patent: June 22, 2021
    Assignee: Hans Heidolph GmbH
    Inventors: Lea Lindner, Robert Loschel
  • Patent number: 11034631
    Abstract: Process for isolating pure 1,3-butadiene from a crude C4 fraction by extractive distillation using a selective solvent, wherein (a) the crude C4 fraction is introduced into a predistillation column, a first low boiler fraction comprising C3-hydrocarbons is taken off as overhead stream, a gaseous C4 fraction is taken off as side stream and a first high boiler fraction is taken off as bottom stream, (b) the gaseous C4 fraction is brought into contact with a selective solvent in at least one extraction column, giving an overhead fraction comprising butanes and butenes and a bottom fraction comprising 1,3-butadiene and selective solvent, (c) crude 1,3-butadiene is desorbed from the bottom fraction in at least one stripping column, with a stripped selective solvent being obtained and the stripped selective solvent being recirculated to the extraction column, and (d) at least part of the crude 1-3-butadiene is fed to a pure distillation column and a second high boiler fraction is separated off and a gaseous purge s
    Type: Grant
    Filed: January 24, 2018
    Date of Patent: June 15, 2021
    Assignee: BASF SE
    Inventors: Bernd Heida, Tobias Keller, Jan-Oliver Weidert
  • Patent number: 10968152
    Abstract: A process for isolating pure 1,3-butadiene from a crude C4 fraction, which produces pure 1,3-butadiene having a prescribed maximum content of at least one low boiler and a prescribed maximum content of 1,2-butadiene, in each case based on 1,3-butadiene, wherein (a) a low boiler fraction and a high boiler fraction are separated off by distillation from the crude C4 fraction, giving a purified C4 fraction whose content of the at least one low boiler, based on 1,3-butadiene, is equal to or lower than the prescribed maximum content of the at least one low boiler and whose content of 1,2-butadiene, based on 1,3-butadiene, is equal to or lower than the prescribed maximum content of 1,2-butadiene; (b) the purified C4 fraction is subjected to at least one extractive distillation using a selective solvent, giving at least a fraction comprising butanes and butenes and a pure 1,3-butadiene fraction, is described. The process makes a pure distillation column dispensable.
    Type: Grant
    Filed: March 12, 2018
    Date of Patent: April 6, 2021
    Assignee: BASF SE
    Inventors: Bernd Heida, Tobias Keller
  • Patent number: 10918968
    Abstract: The present application relates to a selective distillation apparatus and a distillation method, which provides a distillation apparatus capable of switching between a serial connection mode and a parallel connection mode on the situation, thereby enabling selective operation of high-efficiency operation and high-capacity operation.
    Type: Grant
    Filed: September 6, 2017
    Date of Patent: February 16, 2021
    Assignee: LG CHEM, LTD.
    Inventors: Tae Woo Kim, Sung Kyu Lee, Sung Kyun Kim, Joon Ho Shin, Yeon Uk Choo
  • Patent number: 10807883
    Abstract: A fluid vapor distillation system. The system includes a control system for controlling a fluid vapor distillation apparatus including a blow down controller for controlling a blow down valve, a source flow controller for controlling a source flow valve, and a blow down level sensor in communication with a blow down controller and a source flow controller, the blow down level sensor sends signals related to the blow down level to the blow down controller and the source flow controller indicative of the blow down level, wherein the source flow controller actuates the source flow valve based at least on the blow down level sensor signals, and wherein the blow down controller actuates the blow down valve based at least on the blow down level sensor signals, whereby the blow down level and the source flow level are maintained using the blow down level sensor signals as input.
    Type: Grant
    Filed: April 3, 2017
    Date of Patent: October 20, 2020
    Assignee: DEKA Products Limited Partnership
    Inventors: Dean Kamen, Ryan K. LaRocque, Chris C. Langenfeld, Stephen M. Ent, Andrew A. Schnellinger, Prashant Bhat, Stanley B. Smith, Otis L. Clapp
  • Patent number: 10800668
    Abstract: A system for obtaining purified water includes a heat exchanger fluidly coupled to the heat source for receiving a thermal management fluid from the heat source, and a reservoir fluidly coupled with the heat exchanger to supply water, at an ambient temperature, for receiving heat from the thermal management fluid at the heat exchanger. A pump provides a pre-defined flow rate of the water from the reservoir to the heat exchanger based on a temperature gradient of the thermal management fluid across the heat exchanger. A purification device has a cold side chamber in fluid communication with the pump and the heat exchanger while a hot side chamber is in fluid communication with the heat exchanger and the reservoir. The cold and hot side chambers of the purification device thermally co-operate with each other to develop condensate therebetween from moisture present in the ambient air for forming water.
    Type: Grant
    Filed: September 10, 2018
    Date of Patent: October 13, 2020
    Assignee: Caterpillar Inc.
    Inventors: Umakanth Sakaray, Dhanasekar Murugan, Curtis Allen Danielson
  • Patent number: 10759676
    Abstract: A fluid vapor distillation system. The system includes a control system for controlling a fluid vapor distillation apparatus including a blow down controller for controlling a blow down valve, a source flow controller for controlling a source flow valve, and a blow down level sensor in communication with a blow down controller and a source flow controller, the blow down level sensor sends signals related to the blow down level to the blow down controller and the source flow controller indicative of the blow down level, wherein the source flow controller actuates the source flow valve based at least on the blow down level sensor signals, and wherein the blow down controller actuates the blow down valve based at least on the blow down level sensor signals, whereby the blow down level and the source flow level are maintained using the blow down level sensor signals as input.
    Type: Grant
    Filed: March 24, 2017
    Date of Patent: September 1, 2020
    Assignee: DEKA Products Limited Partnership
    Inventors: Dean Kamen, Ryan K. LaRocque, Christopher C. Langenfeld, Andrew Schnellinger, Prashant Bhat, Otis L. Clapp, Stanley B. Smith, III, Stephen M. Ent
  • Patent number: 10493375
    Abstract: The present application relates to a distillation device and a distillation method, and according to the distillation device of the present application, it is possible to minimize the energy losses that occur in the refining process of the raw material containing the monomer and the solvent used in the polymerization process of the thermoplastic elastomer and to reduce the installation cost of the distillation device more than the case of refinement with two distillation columns, and thus the process economics may be improved.
    Type: Grant
    Filed: June 7, 2016
    Date of Patent: December 3, 2019
    Assignee: LG CHEM, LTD.
    Inventors: Sung Kyu Lee, Joon Ho Shin
  • Patent number: 10323201
    Abstract: A system including a fluid processing system including an absorber configured to remove a component from an untreated first fluid using a lean second fluid, output a treated first fluid, and output a rich second fluid, a stripper configured to strip the component from the rich second fluid, output the lean second fluid, and output the component, a first pump configured to pump the lean second fluid into the absorber, and a hydraulic turbocharger configured to pump the lean second fluid by transferring pressure from the rich second fluid to the lean second fluid.
    Type: Grant
    Filed: April 21, 2016
    Date of Patent: June 18, 2019
    Assignee: ENERGY RECOVERY, INC.
    Inventors: Prem Krish, Jeremy Grant Martin, John Sienkiewicz
  • Patent number: 10173956
    Abstract: This disclosure relates to a method for continuous recovery of (meth)acrylic acid and an apparatus used for the recovery method. The method of continuous recovery of (meth)acrylic acid according to the present invention may minimize loss of (meth)acrylic acid particularly in the distillation process, and yet enables stable operation of the distillation process and energy reduction.
    Type: Grant
    Filed: June 28, 2018
    Date of Patent: January 8, 2019
    Assignee: LG CHEM, LTD.
    Inventors: Jong Hun Song, Se Won Baek, Sul Hee Yoo, Yoon Jae Min
  • Patent number: 10035751
    Abstract: This disclosure relates to a method for continuous recovery of (meth)acrylic acid and an apparatus used for the recovery method. The method of continuous recovery of (meth)acrylic acid according to the present invention may minimize loss of (meth)acrylic acid particularly in the distillation process, and yet enables stable operation of the distillation process and energy reduction.
    Type: Grant
    Filed: August 26, 2014
    Date of Patent: July 31, 2018
    Assignee: LG CHEM, LTD.
    Inventors: Jong Hun Song, Se Won Baek, Sul Hee Yoo, Yoon Jae Min
  • Patent number: 9168468
    Abstract: In a system for recycling a high-boiling-point waste photoresist stripper generated in processes of manufacturing LCDs or semiconductor devices, wherein an expensive high-boiling-point stripper solvent can be easily recycled at high yield and high-purity electronic grade. This system includes a first distillation device for removing low-boiling-point impurities, a second distillation device for recycling a stripper solvent composition while removing high-boiling-point impurities, a third distillation device for removing trace water, thus recovering the stripper solvent composition, a fourth distillation device for additionally recycling a stripper solvent, thus additionally recovering a high-boiling-point stripper solvent, and a fifth distillation device for sequentially and separately recovering the stripper solvent composition recovered by the second distillation device and the high-boiling-point stripper solvent additionally recovered by the fourth distillation device.
    Type: Grant
    Filed: January 21, 2015
    Date of Patent: October 27, 2015
    Assignee: KOREX CORPORATION
    Inventors: Ho Kyung Lee, In Gyoo Lee, Myung Jun Park, Kee-Kahb Koo, Jae-Kyeong Kim
  • Patent number: 9095785
    Abstract: A product output rate for a packed column is optimized by setting a desired product output rate from the distillation column, calculating a fraction of flood point of the distillation column at a reflux ratio, and determining a pressure drop value within the distillation column at the fraction of flood point. The step of determining the pressure drop employs the method of producing a plot of pressure drop as a function of fraction of flood point at any liquid flow rate, or producing a mathematical expression thereof.
    Type: Grant
    Filed: April 30, 2013
    Date of Patent: August 4, 2015
    Assignee: Aspen Technology, Inc.
    Inventor: Brian Hanley
  • Patent number: 9057557
    Abstract: An apparatus and system to produce purified drinking water from humid air is provided. The apparatus includes a condenser and evaporator coil assembly with a source of germicidal activity. A method to provide purified drinking water from humid air using a stand along apparatus is provided. The apparatus can also dehumidify, improve air-quality and provide air-conditioning.
    Type: Grant
    Filed: March 15, 2013
    Date of Patent: June 16, 2015
    Assignee: Water Technologies International, LLC
    Inventor: William Scott Tudor
  • Publication number: 20150122631
    Abstract: A closed loop contaminant control system for an evaporative water purification process at an oil recovery facility includes an evaporator having a water inlet, a distilled water discharge, and an oil and brine water discharge. A sump in the evaporator is divided by an oil skimming weir into a main sump and a blowdown sump, with the oil and brine water discharge located proximate the blowdown sump and the steam discharge located above the oil and brine discharge. A distillate tank receives distilled water from the evaporator and discharges the distilled water. The distillate tank has a level controller, other controllers provided for the system include a distilled water flow meter, a blowdown flow meter, a cycle controller, a total flow controller, a hardness controller, and a silica controller.
    Type: Application
    Filed: January 12, 2015
    Publication date: May 7, 2015
    Applicant: 1NSITE TECHNOLOGIES LTD.
    Inventors: Kenneth James, Bob Nabata
  • Publication number: 20150083576
    Abstract: A processes is for purifying an amine compound from a feed solvent which includes an amine salt of the amine compound. The process includes heating the feed solvent in a single stage evaporator of a reclaimer at a reduced operating pressure by feeding the evaporator with a constant amount of thermal energy; and evaporating the amine compound to purity the amine compound from the feed solvent.
    Type: Application
    Filed: March 28, 2013
    Publication date: March 26, 2015
    Applicant: HTC Purenergy Inc.
    Inventors: Ahmed A. Aboudheir, Walid H. Elmoudir
  • Patent number: 8951392
    Abstract: A modular portable evaporator system for use in a Steam Assisted Gravity Drainage (SAGD) systems having an evaporator, with a sump including an oil skimming weir, a short tube vertical falling film heat exchanger including an outer shell containing short tubes provided for lower water circulation rate. The system further having external to the evaporator, a compressor for compressing evaporated steam from the tube side of the heat exchanger and routing to the shell side of the same exchanger, a distillate tank to collect hot distilled water, a recirculation pump to introduce liquids from the sump into the heat exchanger and an external suction drum protecting the compressor from liquid impurities. The evaporator system receives produced water from the SAGD process into the sump and provides cleaned hot water to a boiler.
    Type: Grant
    Filed: April 15, 2011
    Date of Patent: February 10, 2015
    Assignee: 1nSite Technologies Ltd.
    Inventor: Kenneth James
  • Patent number: 8951391
    Abstract: A solar distillation apparatus utilizing a substantially vertical reactor assembly is disclosed. The reactor includes a tubular outer shell, a base, a cap, and a central tension member. The annular space between the outer tube and the central tension member forms the reactor chamber. Seawater or other feed liquid enters the reactor chamber through the base plate. Reflected or direct solar energy heats the feed liquid, generating low pressure vapor. The vapor exits the reactor through the cap structure or the base. The concentrate left behind settles by gravity to the bottom region of the reactor's liquid column. Extension tubes on the feed openings allow feed liquid to enter the liquid column above the concentrate layer and avoid excessive mixing of the feed liquid and the concentrate. The concentrate exits the reactor through one or more openings in the base.
    Type: Grant
    Filed: May 2, 2011
    Date of Patent: February 10, 2015
    Inventor: Miles McClure
  • Publication number: 20150014145
    Abstract: In a desalination system, a water-repellent particle layer is provided at a lower portion of a water tank and composed of water-repellent particles. A devolatilizing layer is provided below the layer. Liquid is provided in the tank and is heated for evaporation, and obtained vapor passes through the particle layer and is liquefied at the devolatilizing layer, so that freshwater is obtained from the liquid. The particle layer includes a first and a second particle layers composed of discriminable first and second particles. A particle measuring unit measures an amount of the second water-repellent particles. A decision unit decides whether or not the measured amount of the second water-repellent particles is equal to or more than a predetermined value. A controller alerts when the decision unit decides that the amount of the second particles is equal to or more than the predetermined value.
    Type: Application
    Filed: September 29, 2014
    Publication date: January 15, 2015
    Inventors: Yumi WAKITA, Norihisa MINO, Hiroki TAKEUCHI, Mikiya NAKATA
  • Publication number: 20150014146
    Abstract: A desalination system includes a water tank, a water-repellent particle layer located at a lower portion of the tank and composed of water-repellent particles, and a devolatilizing layer located below the water-repellent particle layer. Liquid is introduced to the tank, the introduced liquid is heated to be evaporated into water vapor, and the water vapor passes through the water-repellent particle layer and is liquefied at the devolatilizing layer, so that fresh water is obtained from the liquid. The desalination system further includes a liquid level controller for determining a level of the liquid introduced to the tank in accordance with information on relationship between information corresponding to an amount of the liquid introduced to the tank and a surface level of the liquid in the tank, and an introduced amount controller for adjusting the amount of the liquid introduced to the tank in accordance with the determined liquid surface level.
    Type: Application
    Filed: September 29, 2014
    Publication date: January 15, 2015
    Inventors: Yumi WAKITA, Norihisa MINO, Hiroki TAKEUCHI, Mikiya NAKATA
  • Publication number: 20140374235
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.
    Type: Application
    Filed: September 8, 2014
    Publication date: December 25, 2014
    Inventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
  • Patent number: 8871062
    Abstract: An apparatus and method are disclosed for controlling the thickness of a flowing, laminar fluid film. The film flow may be gravity-induced or the result of an alternative force. The fluid is deposited on an upper end of a flow surface where a relatively thick layer of the film forms. The film flows over a fluid dispersal region where the surface area is rapidly expanding, which results in rapid thinning of the film thickness. The fluid then flows over an active region where the surface area is designed to control the fluid film thickness. For example, in some applications, it may be desirable to maintain an approximately constant film thickness as the fluid flows over the active region of the surface. The geometry of the flow surface is used to obtain the desired control over the fluid film thickness. The flow surface is the outer surface of a solid with a closed upper end and a lower end that may be open or closed.
    Type: Grant
    Filed: November 23, 2010
    Date of Patent: October 28, 2014
    Inventors: Charles David Gilliam, Stefanie Renee Gilliam
  • Patent number: 8828192
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.
    Type: Grant
    Filed: October 5, 2012
    Date of Patent: September 9, 2014
    Assignee: DEKA Products Limited Partnership
    Inventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
  • Publication number: 20140224638
    Abstract: Methods and apparatus for desolvating flowing liquid streams while retaining temporal resolution of dissolved substrates are disclosed. A novel small-scale self-regulating spray dryer preserves temporal resolution while desolvating a liquid chromatography eluent stream and depositing the solute onto an optical surface for infrared spectrographic analysis. The liquid eluent is pumped through a heated nebulizer to create a high-speed jet of solute containing liquid and solvent vapor. This jet is directed circumferentially inside a hot cylindrical cavity. Centrifugal force causes the larger liquid droplets to travel along the outer diameter of the cavity. The cavity surface is heated to cause the droplets to film boil. Film boiling reduces droplet contact with the cavity surface thereby retaining the solute in the droplets. The solute temperature is limited by controlling the pressure into which the solvent evaporates from the droplets.
    Type: Application
    Filed: February 21, 2014
    Publication date: August 14, 2014
    Applicant: SPECTRA ANALYSIS INSTRUMENTS, INC.
    Inventors: William W. CARSON, Sidney BOURNE
  • Patent number: 8741109
    Abstract: A method for purifying a crude acetone raw material containing low molecular weight impurities using two columns is disclosed. Crude acetone raw material is fed into a first column; adding an alkaline reagent and an oxidative agent into the first column to form high molecular weight impurities; removing a top fraction from the first column by distillation to form bottom fraction containing an acetone mixture containing high molecular weight impurities; feeding the bottom fraction containing the acetone mixture obtained to a second rectification column at a charge point on the column; adding an alkaline reagent to the second column above the charge point of the bottom fraction fed; and separating a purified acetone from the high molecular weight impurities and removing the purified acetone as a top fraction by distillation in the second column, wherein the second rectification column is operated at atmospheric pressure.
    Type: Grant
    Filed: December 8, 2009
    Date of Patent: June 3, 2014
    Assignee: Sabic Innovative Plastics IP B.V.
    Inventors: Mark Erik Nelson, Andrey Yurievich Sokolov, Ilya Yurievich Krupenko, Valery Yurievich Aristovich
  • Patent number: 8715467
    Abstract: This invention provides a method for purifying a chlorine supply that includes a chlorine component, a bromine component, and nitrogen trichloride. The method includes the steps of introducing the chlorine supply into a vaporizer, heating the chlorine supply in the vaporizer to form a vapor, and introducing the vapor into a distillation system to provide purified chlorine gas, a distillate that includes liquid chlorine and the bromine component, and a bottoms component including the nitrogen trichloride. The method also includes the steps of condensing the vapor in a reflux condenser, heating the condensate in a reboiler, removing the purified chlorine gas from the distillation system, and removing the distillate from the distillation system.
    Type: Grant
    Filed: July 11, 2013
    Date of Patent: May 6, 2014
    Assignee: BASF SE
    Inventors: Robert A. Doerr, Steven D. Gagnon, Kenneth K. Bordelon, Johannes D. Jacobs, Thomas A. Grzanka
  • Publication number: 20140021029
    Abstract: A system for distributed utilities including electrical power and water. A generation device is provided for converting an available resource to a desired utility; the resource may be water, in which case the generator is a purifier for purifying untreated water, or, alternatively, the generator may convert a fuel to electrical power. In either case, an input sensor is provided for measuring input to the generation device, while an output sensor is provided for measuring consumption of output from the generation device. The monitoring system has a controller for concatenating measured input and consumption of output on the basis of the input and output sensors. Measured parameters are telemetered to a remote site where utility generation and use are monitored and may also be controlled.
    Type: Application
    Filed: September 12, 2013
    Publication date: January 23, 2014
    Applicant: DEKA Products Limited Partnership
    Inventors: Dean Kamen, Jason A. Demers, Kingston Owens
  • Publication number: 20140008208
    Abstract: A continuous thermal process for treating oilfield produced water and generating steam from the same is provided. Raw water in is passed in direct counterflow heat exchange with produced steam to heat the raw water to a temperature at which a substantial portion of dissolved calcium and magnesium ions in the raw water are precipitated as insoluble salts. The raw water is further passed into a reaction zone for completion of reactions. A strong base is added to the raw water prior to passing the raw water in direct counterflow heat exchange with the produced steam in amount such that pH of the reaction zone is at least 10.5 as measured by a pH sensor to promote silica soluability. Other embodiments are also disclosed.
    Type: Application
    Filed: July 5, 2012
    Publication date: January 9, 2014
    Inventor: Garry Pichach
  • Patent number: 8623179
    Abstract: A seawater desalinization device includes a container portion, a guiding pipe, a plug, a heat conduction cover, a switch, and a connecting pipe. The container portion defines a receiving chamber, a slot, and a through hole communicating with the receiving chamber. The guiding pipe is fixed on the container portion to communicating with the slot. The plug is detachably inserted into the guiding pipe. The heat conduction cover covers on the container portion and sealing the receiving chamber and the slot. The switch is assembled in the container portion to control open or close the through hole upon a seawater level in the container portion. The connecting pipe is inserted into the through hole and a seawater source.
    Type: Grant
    Filed: December 30, 2010
    Date of Patent: January 7, 2014
    Assignees: Shenzhen Futaihong Precision Industry Co., Ltd., FIH (Hong Kong) Limited
    Inventors: Zheng Shi, Jiang-Feng Liu
  • Publication number: 20140001027
    Abstract: The present invention is directed to a modular distillation system incorporating a removable capsule for containing source material for extraction. Through the action of the invention, the steam distillation process described herein produces a substantially larger amount of volatile oil than a distillation system that does not use an enclosed, modular system. The present invention provides for an apparatus that allows for greater contact between the steam and plant matter during the distillation process through the use of a closed removable capsule containing relatively small amount of plant matter. Additionally, the present invention is directed to a system that allows the generation of higher quality distillate and considerably higher quantity of volatile oil extracts by forcing the steam to evenly disperse through a removable capsule, and by preventing the condensed liquid to return back to the boiling water within the vessel.
    Type: Application
    Filed: June 20, 2013
    Publication date: January 2, 2014
    Applicant: Aromator LLC
    Inventor: Moshe Balass
  • Patent number: 8608912
    Abstract: Embodiments of extraction unit and an analysis method are provided. In one embodiment, the analysis method includes the steps of providing a feed stream and a species-selective solvent to the distillation column, drawing a vapor sample from the distillation column, condensing the vapor sample, and analyzing at least a portion of the condensed vapor sample.
    Type: Grant
    Filed: September 29, 2010
    Date of Patent: December 17, 2013
    Assignee: UOP LLC
    Inventors: Jason L. Noe, Ian Horn, Lars Sullivan, Bruce R. Beadle, Edward M. Casey, James W. Harris
  • Patent number: 8586788
    Abstract: A method for producing of ultra-clean and high-purity electronic acetic acid is disclosed. The method including following steps: Step 1, industrial acetic acid is fast distilled; Step 2, filtering the fraction by membrane of 0.05˜0.3 ?m aperture; Step 3, rectification; Step 4, membrane filtration again. Due to the adoption of the technical scheme above, the ultra-clean and high-purity electronic grade acetic acid which purity is 99.8% is produced. The content of single metal ion is lower than 1 ppb and the content of particulates which is ?0.5 ?m is lower than 5 pcs/ml. The method of the invention will help to reduce energy consumption, to simplify the operation, and to achieve the high security.
    Type: Grant
    Filed: October 28, 2010
    Date of Patent: November 19, 2013
    Assignee: Asia Union Electronic Chemical Corporation Shanghai
    Inventors: Jiarong Zhan, Curtis Dove, I-Hsing Lin
  • Patent number: 8562791
    Abstract: A system and method for decontaminating water and generating water vapor includes introducing contaminated water in to a vessel. The water is moved through a series of rotating trays alternately separated by stationary baffles so as to swirl and heat the water to effect the vaporization thereof to produce a vapor having at least some of the contaminants separated therefrom. The vapor is removed from the vessel for condensing apart from the separated contaminants and the remaining water. The vapor may be passed through a turbine connected to an electric generator. Sensors in a controller may be employed to adjust the speed of rotation of the trays or water input into the vessel in response to the sensed conditions. The treated water may be recirculated and reprocessed through the vessel to increase the purification thereof.
    Type: Grant
    Filed: June 22, 2009
    Date of Patent: October 22, 2013
    Assignee: Verno Holdings, LLC
    Inventors: John D. Riley, Dana L. Johnson
  • Patent number: 8557087
    Abstract: The present invention relates to a process for the separation by distillation of a hydrocarbon-containing feed stream containing olefin monomer, co-monomer and hydrocarbon diluent. The present invention also relates to a distillation system including a distillation column for carrying out the process according to the invention.
    Type: Grant
    Filed: July 15, 2008
    Date of Patent: October 15, 2013
    Assignee: Total Petrochemicals Research Feluy
    Inventor: Denis Mignon
  • Publication number: 20130240345
    Abstract: A process for producing high-purity liquids, in particular liquid chemicals, by distillation, includes the steps of: providing a liquid to be purified from a storage vessel in a sample container arranged in a sample chamber, heating and evaporating the uppermost layers of the liquid to be purified, condensing the sample vapor produced of the liquid to be purified in a condensation device outside the sample chamber, and collecting the distillate in a collecting container. The collecting container being connectable to the storage vessel via a return line for the non-condensed sample vapor and forming a space that is closed off from the surroundings between the space above the liquid surface of the liquid to be purified in the sample chamber and the storage vessel.
    Type: Application
    Filed: May 2, 2013
    Publication date: September 19, 2013
    Inventor: Werner LAUTENSCHLAEGER
  • Publication number: 20130233695
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.
    Type: Application
    Filed: October 5, 2012
    Publication date: September 12, 2013
    Applicant: DEKA Products Limited Partnership
    Inventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
  • Patent number: 8524046
    Abstract: Methods and systems for controlling the pressure of distillation columns, for example those operating under vacuum pressure and conventionally equipped with a steam ejector system, are described. Representative distillation columns are used in the separation of thermally unstable components, such as the physical solvent sulfolane, having relatively low volatility. Such columns are employed in aromatic hydrocarbon extraction processes for the recovery of purified C6-C8 aromatic hydrocarbons from a hydrocarbon feed stream (e.g., obtained from the catalytic reforming of naphtha).
    Type: Grant
    Filed: March 30, 2010
    Date of Patent: September 3, 2013
    Assignee: UOP LLC
    Inventors: Bruce R. Beadle, Jason L. Noe, Sara A. Williams
  • Patent number: 8506762
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.
    Type: Grant
    Filed: October 30, 2007
    Date of Patent: August 13, 2013
    Assignee: DEKA Products Limited Partnership
    Inventors: David F. Bednarek, Jason A. Demers, Timothy P. Duggan, James L. Jackson, Scott A. Leonard, David W. McGill, Kingston Owens
  • Patent number: 8486223
    Abstract: A falling film evaporator having a shell pass, multiple tubes parallel to each other, a condensed steam outlet, an inlet for an aqueous solution on the top of the tube pass, an outlet for the aqueous solution at the bottom of the tube pass, a distributing assembly having a plurality of distributing trays arranged vertically from top to bottom in incremental diameters and each having multiple holes, and a plate for collecting the aqueous solution below the distributing assembly. The tubes are straight and installed vertically in the evaporator; inner wall of the tubes is smooth, and the top portion of the tubes is protruded above a horizontal plane of the plate. The evaporator is particularly useful for concentrating an aqueous solution containing thermosensitive materials.
    Type: Grant
    Filed: October 7, 2010
    Date of Patent: July 16, 2013
    Assignee: Jiangsu Sinorgchem Technology Co., Ltd.
    Inventors: Xiaogen Feng, Nongyue Wang, Xiaohui Mao, Ruibiao Yu, Qianwen Cheng
  • Patent number: 8480860
    Abstract: A divided exchange column includes a shell column having a first longitudinal axis, a cylindrical wall spaced apart from and surrounding the first longitudinal axis and defining a first interior space, a first divided wall column having a second longitudinal axis substantially parallel to the first longitudinal axis, and a second divided wall column having a third longitudinal axis substantially parallel to the first and the second longitudinal axes, where the first divided wall column and the second divided wall column are positioned in the first interior space of the shell column.
    Type: Grant
    Filed: October 22, 2008
    Date of Patent: July 9, 2013
    Assignee: Air Products and Chemicals, Inc.
    Inventor: Kenneth William Kovak
  • Patent number: 8475632
    Abstract: A method for recycling cutting fluid includes preparing and processing a cutting fluid of silicon including a silicon mixture and a cutting fluid at an anoxic circumstance of 150° C. to 350° C. in a container, to obtain a vaporized cutting fluid and a silicon slurry; and condensing the vaporized cutting fluid to obtain a recycling cutting fluid.
    Type: Grant
    Filed: November 10, 2010
    Date of Patent: July 2, 2013
    Assignee: Hong Jing Environment Company
    Inventors: Yu-Lung Sun, Yung-Hao Liu, Ming-Zhe Tsai
  • Patent number: 8470138
    Abstract: A distillation assembly that reduces malodors resulting from a process of recycling a solvent from a contaminated solvent solution that includes a distillation chamber defined by a top wall, a side wall and a bottom wall, a heating element disposed in the distillation chamber including an active portion and an inactive portion. The contaminated solvent solution disposed at a level within the distillation chamber such that the active portion always disposed below the level.
    Type: Grant
    Filed: February 2, 2010
    Date of Patent: June 25, 2013
    Assignee: Safety-Kleen Systems, Inc.
    Inventors: Rudy Publ, David Kisela, Gary Myers