Distilling To Separate Or Remove Only Water Patents (Class 203/12)
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Patent number: 11466237Abstract: A fermentation apparatus for preserving the aroma of a fermentable beverage is provided. The fermentation apparatus comprises a flow passage fluidly connectable to the headspace located above a fermentable beverage in a fermentation container. A carbon dioxide scrubber in the flow passage receives a headspace fluid mixture comprising at least carbon dioxide gas and an aromatic fluid originating from the fermenting beverage. When the headspace fluid mixture contacts the carbon dioxide scrubber, the carbon dioxide scrubber retains a modified fluid in the flow passage. The modified fluid has a lower carbon dioxide gas concentration and a higher aromatic fluid concentration than the headspace fluid mixture. The flow passage directs the modified fluid back to the headspace to at least partially retain the aromatic fluid in the fermentable beverage in the fermentation container. A method for preserving the aroma of a fermentable beverage is also provided.Type: GrantFiled: February 6, 2019Date of Patent: October 11, 2022Assignee: AROMALOC INC.Inventor: Richard L. Jones
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Process for generating a mixed multicomponent vapor for preparation of monoalkyl ethers of diphenols
Patent number: 11377410Abstract: This invention comprises a process and a system thereof comprising apparatuses for developing multi-component vapor mixture by heating of solution of reactants comprising one or more of diphenols, or diphenol derivatives, and an organic compound, wherein the organic compound is one which upon reacting in a vapor state in presence of a catalyst with diphenols, or diphenol derivatives, produces a monoalkyl ether of a dihydric phenolic compound; and wherein the entire solution of reactants completely transforms into a super-heated multi-component vapor using heaters without the use of thin film evaporator.Type: GrantFiled: May 19, 2015Date of Patent: July 5, 2022Assignee: CAMLIN FINE SCIENCES LIMITEDInventors: Anil Purushottam Shanbhag, Arjun Sudhakar Dukane -
Patent number: 11203769Abstract: A hydrogen peroxide and gluconic acid production method and system is disclosed that can include receiving an aqueous solution having glucose, water, and glucose oxidase at a reaction chamber. Here, the reaction chamber facilitates an enzymatic reaction between a gas phase and a liquid phase of the aqueous solution, thereby yielding a first solution comprising hydrogen peroxide, gluconic acid, and the glucose oxidase. The method can further include receiving the first solution at a separation chamber, wherein the separation chamber is comprised of a semi-permeable membrane having a pre-defined molecular weight barrier for separating the glucose oxidase, thereby resulting in a combined hydrogen peroxide and gluconic acid solution. The method can further include at least partially converting the gluconic acid into a gluconate salt, and separating and concentrating the hydrogen peroxide from the gluconic acid or gluconate salt via vacuum flash evaporation and vacuum distillation.Type: GrantFiled: February 13, 2017Date of Patent: December 21, 2021Inventors: Gaurab Chakrabarti, Sean T. Hunt
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Patent number: 11028031Abstract: The present invention aims at providing a method for producing a high-concentration alcohol from a water-alcohol mixture, in which the overall process is efficient and the present invention relates to a production method of a high-concentration alcohol, including a water adsorption step of adsorbing water of a water-alcohol mixture on an adsorption column to obtain a first concentrated alcohol, a water desorption step of introducing an alcohol to obtain a hydrous alcohol, and a membrane separation step of introducing the hydrous alcohol into a membrane separation unit provided with a membrane composite containing zeolite having an SiO2/Al2O3 molar ratio of 5 to 15 to obtain a second concentrated alcohol.Type: GrantFiled: May 9, 2019Date of Patent: June 8, 2021Assignee: MITSUBISHI CHEMICAL CORPORATIONInventors: Kazuhide Maeda, Koichi Yamazaki, Hiroyuki Kakiuchi, Takeshi Tahara, Takahiko Takewaki
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Patent number: 11027974Abstract: The present invention generally relates to the field of gas and liquid phase desiccation. In particular, the present invention relates to methods for removing moisture (and hence oxygen precursors) from hydrazine, thereby providing a high purity source gas suitable for use in vapor deposition processes, such as but not limited to, chemical vapor deposition (CVD) or an atomic layer deposition (ALD).Type: GrantFiled: November 8, 2017Date of Patent: June 8, 2021Assignee: Matheson Tri-Gas, Inc.Inventors: Hideharu Shimizu, Mark Raynor, Daniel Tempel, Robin Gardiner, Daniel Alvarez, Jr.
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Patent number: 10759686Abstract: A method for preparing a thinning ceramic additive using a landfill leachate, comprising the following steps: filtering the landfill leachate; adding aqueous alkali and regulating pH to 7.5-9; adding a coagulant, then stirring and mixing with a blender; taking precipitates to mix with water to prepare a solution, adding a sodium hydroxide solution for alkalization, and regulating the pH to 7-8.5; adding a sulfonating agent, and reacting under an environment of 80-100° C. for 2-4 h; adding acrylic acid and N,N?-methylene bisacrylamide to the solution, then slowly adding the initiator, stirring under the condition of 80-90° C. to react for 1-3.5 h, and after the reaction is completed, drying the solution to obtain a solid matter; crushing the solid matter, and screening through a screen of 16-24 meshes; and uniformly mixing the above screened particulate matter with the montmorillonite and an additive to prepare the thinning ceramic additive.Type: GrantFiled: January 23, 2018Date of Patent: September 1, 2020Assignees: FuZhou University, Fujian BoYi Environmental Protection Technology Co., LTD.Inventors: Minghua Liu, Yuqing Zhang, Yifan Liu, Yuancai Lv, Xiaoquan Li
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Patent number: 10065859Abstract: A system includes an ion separation unit that may receive dilute hydrochloric acid and may generate a concentrated hydrochloric acid and a chamber fluidly coupled to the ion separation unit. The chamber may receive the concentrated hydrochloric acid and may separate the concentrated hydrochloric acid into a liquid concentrated hydrochloric acid and a vapor containing vaporized hydrochloric acid. The system also includes a scrubber fluidly coupled to the chamber. The scrubber may receive the vapor from the chamber, and the scrubber is may remove at least a portion of the vaporized hydrochloric acid from the vapor via a purified condensate to generate a purified vapor and the dilute hydrochloric acid. The system also includes a condenser fluidly coupled to the scrubber The condenser may receive the purified vapor from the scrubber to condense the purified vapor into the purified condensate, and to output the purified condensate to the scrubber.Type: GrantFiled: April 28, 2014Date of Patent: September 4, 2018Assignee: Enviro Water Minerals Company, Inc.Inventor: Paul Steven Wallace
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Patent number: 10005688Abstract: This desalinization system, which obtains industrial-use water and drinking water from seawater and wastewater, is provided with: a purification device that purifies wastewater by removing activated sludge therefrom; a first RO membrane that removes salt from the output of the purification device by transferring said salt to first concentrated water, thereby producing industrial-use water; a UF membrane that seawater passes through and that removes particulates from said seawater; a second RO membrane that removes salt from the treated output of the UF membrane by transferring said salt to second concentrated water, producing drinking water; an agitation device to which the second concentrated water from the second RO membrane and the first concentrated water from the first RO membrane are sent to be agitated; and a third RO membrane removing salt from the liquid mixture agitated by the agitation device by transferring said salt to third concentrated water, producing industrial-use water.Type: GrantFiled: August 16, 2012Date of Patent: June 26, 2018Assignee: HITACHI, LTD.Inventors: Yasunori Sekine, Kazuhiko Noto, Akira Sasaki, Kotaro Kitamura
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Patent number: 9918478Abstract: This invention is about a water soluble antimicrobial polyacrylate silver salt. The molecular chain of the polyacrylate silver salt comprises sodium carboxylic group (—COONa) and silver carboxylic group (—COOAg). It is synthesized by dissolving an polyacrylate polymer comprising sodium carboxylic group (—COONa) in water and then exchanging the sodium carboxylic group of the polyacrylate polymer to silver carboxylic group (—COOAg) using silver salt in aqueous solution. Ultrafiltration membrane is used to remove the sodium salt generated from the metal ion exchanging procedure. An aqueous solution of water soluble antimicrobial polyacrylate silver salt with very few impurity is obtained. The water soluble antimicrobial polyacrylate silver salt is then obtain-ned from the aqueous solution. The molar ratio of —COOAg to —COONa of thus obtained water soluble antimicrobial polyacrylate silver salt can be as high as 66/34.Type: GrantFiled: April 13, 2016Date of Patent: March 20, 2018Inventor: Shyh Yeu Wang
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Patent number: 9884822Abstract: Disclosed herein is a cost effective and environmentally friendly process to prepare 1-hydroxy-6-substituted pyridones from 2,6-dichloropyridine.Type: GrantFiled: February 8, 2013Date of Patent: February 6, 2018Assignee: Arch Chemicals, Inc.Inventors: Rahim Hani, David A. Steele, John Joseph Jardas
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Patent number: 9783427Abstract: A method of recycling mixtures of hydrochloric and hydrofluoric acid. In particular, a method of recycling hydrofluoric acid and boron fluoride mixtures. A process for upgrading mixtures of fluoroboron compounds contaminated with chlorides as an aqueous solution of boron fluoride hydrates, including a step of vacuum distillation. Also, a method of producing gaseous boron trifluoride.Type: GrantFiled: October 1, 2012Date of Patent: October 10, 2017Assignee: ARKEMA FRANCEInventors: Pascal Dufour, Cyrille Le Toullec
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Patent number: 9533940Abstract: Means of preserving 1,5-pentanediamine or a salt thereof without deterioration is provided. 1,5-pentanediamine or a salt thereof is preserved by adjusting any of a water content of 1,5-pentanediamine or a salt thereof purified through a distillation process, a temperature condition, and a material that comes into contact with 1,5-pentanediamine or a salt thereof.Type: GrantFiled: August 6, 2015Date of Patent: January 3, 2017Assignee: AJINOMOTO CO., INC.Inventors: Takehiro Hiura, Masataka Yamamoto, Yasuhiro Maruta
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Patent number: 9254451Abstract: The invention relates to a method and a device with the aid of which hydrogen halide and water are removed from biomass hydrolyzates containing halogen acid. The core of the invention is an evacuated container (B1), which is continuously supplied with a heat-transfer medium and which is completely filled with the heat-transfer medium in a part. In said evaporation chamber, the biomass hydrolyzate is likewise continuously introduced. In the container (B1), heat is transferred from the heat-transfer medium to the hydrolyzate, wherein hydrogen halide and water are continuously evaporated. The remaining hydrolyzate particles are continuously discharged with the cooled heat-transfer medium and continuously removed by means of the heat-transfer medium and continuously separated from said heat-transfer medium. The invention described can also be used to treat other mixtures or solutions for the purpose of evaporation.Type: GrantFiled: July 12, 2011Date of Patent: February 9, 2016Assignee: Green Sugar GmbHInventors: Frank Kose, Matthias Schmidt
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Patent number: 9102604Abstract: A method for cleaning a distilling column includes providing a distilling column including a packing containing nickel and adding hydrochloric acid to the distilling column to wash at least a portion of the packing, thereby cleaning the distilling column.Type: GrantFiled: February 15, 2010Date of Patent: August 11, 2015Assignees: BAXTER INTERNATIONAL INC., BAXTER HEALTHCARE SAInventors: Leonid A. Rozov, Linas Kudzma, Hong-Chang Lee, Ronald Bell
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Patent number: 9028654Abstract: Disclosed herein is a system comprising an evaporation unit comprising a first heat exchanger in fluid communication with a second heat exchanger; where the first heat exchanger is operative to heat an effluent stream comprising an amine solvent and/or amine byproducts and water and to discharge the effluent stream to the second heat exchanger; where the second heat exchanger is operative to convert the effluent stream into a distillate stream and a concentrate stream; and a reverse osmosis unit in fluid communication with the evaporation unit; where the reverse osmosis unit comprises a first reverse osmosis unit that is operative to receive the distillate stream and to separate water from byproducts of the amine solvent such that the water has a purity of greater than 95%, based on the weight of the distillate stream.Type: GrantFiled: February 29, 2012Date of Patent: May 12, 2015Assignee: ALSTOM Technology LtdInventors: Bjoern Ungerer, Christoph Weingaertner, Hans-Peter Dornik
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Publication number: 20140346033Abstract: The present invention relates to a method and system for regeneration of kinetic hydrate inhibitor when it is used without a thermodynamic inhibitor. In that the use of a distillation column or tower is not needed, the present invention enables a more compact system, which also improves the possibility for heat integration of the regeneration process leading to very low energy consumption. Additional improvements over the prior art include reduced cost of buying new chemicals, reduced environmental impact because the chemicals are not discharged with the produced water and the possibility for the use of higher concentrations of kinetic hydrate inhibitor with still reduced cost and environmental impact.Type: ApplicationFiled: September 22, 2011Publication date: November 27, 2014Applicant: Statoil Petroleum ASInventors: Baard Kaasa, Pål Viggo Hemmingsen
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Patent number: 8877016Abstract: Systems and methods for solar steam generation are described. The systems and methods include moving at least one frame mounted optical focusing lens to track the sun in two axes and disposing a water boiler at a focus of each optical focusing lens. Raw water is pumped through an inlet at a bottom of each boiler and solar energy is concentrated, using each optical focusing lens, on each boiler, heating the raw water in each boiler and evaporating steam from the raw water. The steam exits each boiler, via a steam outlet pipe. Remaining salts and solids in each boiler are ground by rotation of salt grinding-cleaning gears. These ground salts and solids are drained and/or pumped out of each boiler from an exit in the bottom of each boiler.Type: GrantFiled: November 6, 2011Date of Patent: November 4, 2014Assignee: King Saud UniversityInventors: Mazen A. Ba-abbad, Hany A. Al-Ansary, Essam A. Al-Ammar
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Patent number: 8801897Abstract: A compact and portable liquid concentrator and contaminant scrubber includes a gas inlet, a gas exit and a flow corridor connecting the gas inlet and the gas exit, wherein the flow corridor includes a narrowed portion that accelerates the gas through the flow corridor. A liquid inlet injects liquid into the gas stream at a point prior to the narrowed portion so that the gas-liquid mixture is thoroughly mixed within the flow corridor, causing a portion of the liquid to be evaporated. A demister or fluid scrubber downstream of the narrowed portion removes entrained liquid droplets from the gas stream and re-circulates the removed liquid to the liquid inlet through a re-circulating circuit. A reagent may be mixed with the liquid to react with contaminants in the liquid.Type: GrantFiled: November 3, 2010Date of Patent: August 12, 2014Assignee: Heartland Technology Partners LLCInventors: Bernard F. Duesel, Jr., Michael J. Rutsch, Craig Clerkin
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Patent number: 8790496Abstract: A compact and portable liquid concentrator includes a gas inlet, a gas exit and a flow corridor connecting the gas inlet and the gas exit, wherein the flow corridor includes a narrowed portion that accelerates the gas through the flow corridor. A liquid inlet injects liquid into the gas stream at a point prior to the narrowed portion so that the gas-liquid mixture is thoroughly mixed within the flow corridor, causing a portion of the liquid to be evaporated. A demister or fluid scrubber downstream of the narrowed portion removes entrained liquid droplets from the gas stream and re-circulates the removed liquid to the liquid inlet through a re-circulating circuit. Fresh liquid to be concentrated is also introduced into the re-circulating circuit at a rate sufficient to offset the amount of liquid evaporated in the flow corridor.Type: GrantFiled: July 29, 2010Date of Patent: July 29, 2014Assignee: Heartland Technology Partners LLCInventors: Bernard F. Duesel, Jr., Michael J. Rutsch, Craig Clerkin
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Patent number: 8776879Abstract: Embodiments presented herein provide an evaporation based zero liquid discharge method for generation of up to 100% quality high pressure steam from produced water in the heavy oil production industry. De-oiled water is processed in an evaporation system producing a distillate that allows steam to be generated with either drum-type boilers operating at higher pressures or once-through steam generators (OTSGs) operating at higher vaporization rates. Evaporator blowdown is treated in a forced-circulation evaporator to provide a zero liquid discharge system that could recycle >98% of the deoiled water for industrial use. Exemplary embodiments of the invention provide at least one “straight sump” evaporator and at least one hybrid external mist eliminator. Embodiments of the evaporation method operate at a higher overall efficiency than those of the prior art by producing distillate at a higher enthalpy which minimizes the high pressure boiler preheating requirement.Type: GrantFiled: June 4, 2013Date of Patent: July 15, 2014Assignee: Aquatech International CorporationInventors: Daniel P. Bjorklund, Gregory J. Mandigo, Richard M. Schoen, James Michael Marlett, Chandrakant Tiwari
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Publication number: 20140157846Abstract: Methods and systems for treating bioreactor wastewater streams are provided. In some embodiments, the methods and systems involve producing a composition, for example in the form of a solution, comprising ammonia or ammonium from the bioreactor wastewater stream. In some cases, the bioreactor is an anaerobic digester.Type: ApplicationFiled: December 12, 2012Publication date: June 12, 2014Applicant: ThermoEnergy CorporationInventors: Sam S. Jeppson, Mark M. Simon, Thomas Karl Bisson
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Patent number: 8652333Abstract: A process for removing a solvent from a source solution, said process comprising a) contacting the source solution with one side of a selectively permeable membrane, b) contacting a draw solution having a higher osmotic pressure (higher solute concentration) than the source solution with the opposite side of the membrane, such that solvent from the source solution passes across the membrane to dilute the draw solution by direct osmosis, c) removing solvent from the diluted draw solution to regenerate the draw solution, and d) recycling the regenerated draw solution to step a), characterized in that a portion of the draw solution is discarded or treated before and/or after the draw solution is regenerated in step c) so as to reduce the concentration of any solute species present in the draw solution from the source solution.Type: GrantFiled: December 8, 2009Date of Patent: February 18, 2014Assignee: Surrey Aquatechnology LimitedInventor: Peter Nicoll
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Publication number: 20140021032Abstract: Systems and methods are provided for heating and manipulating a fluid to heat the fluid, evaporate water from the fluid, concentrate the fluid, separate the fluid into fractions; and/or pasteurize the fluid, comprising a closed-loop heating subsystem coupled to a primary fluid-to-fluid heat exchanger, and one or more fluid manipulation subsystems also coupled to the primary fluid-to-fluid heat exchanger.Type: ApplicationFiled: July 21, 2013Publication date: January 23, 2014Inventor: FRANKLIN ALAN FRICK
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Publication number: 20140021033Abstract: Systems and methods are provided for heating and manipulating a fluid to heat the fluid, evaporate water from the fluid, concentrate the fluid, separate the fluid into fractions; and/or pasteurize the fluid, comprising a closed-loop heating subsystem coupled to a primary fluid-to-fluid heat exchanger, and one or more fluid manipulation subsystems also coupled to the primary fluid-to-fluid heat exchanger.Type: ApplicationFiled: September 13, 2013Publication date: January 23, 2014Inventor: FRANKLIN ALAN FRICK
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Patent number: 8623174Abstract: A liquid evaporation system for evaporating clean water from a reservoir of wastewater includes a liquid evaporator to evaporate and separate water vapor from the wastewater in a confined space, an air blower to supply air to the liquid evaporator, and a wastewater heating system arranged to collect heat to heat the wastewater in the reservoir.Type: GrantFiled: December 14, 2012Date of Patent: January 7, 2014Assignee: Heartland Technology Partners LLCInventors: Bernard F. Duesel, Jr., Craig Clerkin
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Patent number: 8608966Abstract: The invention relates to a method and an apparatus for dewatering mixture of ethanol and water. The method comprises steps for feeding mixture of ethanol and water (1) into an evaporator (2), evaporating said mixture of ethanol and water (1) and feeding a stream of vaporized mixture of ethanol and water (3) to a vapor recompression unit (4), pressurizing vaporized mixture of ethanol and water (3) in the vapor recompression unit (4) and feeding a stream of pressurized vaporized mixture of ethanol and water (5) to a membrane unit (6), and dividing said stream of pressurized mixture of ethanol and water (5) in to a stream of mixture of ethanol and water (8) and into a stream of dewatered mixture of ethanol and water (7).Type: GrantFiled: November 7, 2008Date of Patent: December 17, 2013Assignee: ST1 Biofuels OyInventors: Antti Pasanen, Mikko Ahokas
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Patent number: 8603301Abstract: A method and apparatus for producing high purity distillate in evaporators. is useful for evaporation of waters where volatile silica or organic compounds are encountered such as in production of hydrocarbons from geological formations. An evaporator having a contaminant reduction system is provided. The contaminant reduction system includes an upflow first mist eliminator portion to remove entrained liquid droplets and produce an intermediate purity water vapor stream. A continuous spray system provides a spray of dilute caustic solution in a selected spray configuration for mass transfer contact with the passing intermediate purity water vapor stream, to remove volatile silica compounds therefrom, and produce a partially decontaminated steam stream having mist particles therein. An upflow second mist eliminator portion is provided to remove the residual mist particles, and produce a high purity water vapor stream. The high purity water vapor stream is condensed to provide a high purity distillate stream.Type: GrantFiled: September 29, 2010Date of Patent: December 10, 2013Assignee: General Electric CompanyInventors: William F. Heins, Gregg L. Wilson
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Patent number: 8603223Abstract: A water desalination system including at least one pair of evaporators, said pair including a high pressure and a low pressure evaporator, each for evaporating saline water to produce water vapor; at least three adsorption beds in selective vapor communication with each evaporator, said adsorption beds arranged to reversibly adsorb the water vapor from the corresponding evaporator; said adsorption beds in selective vapor communication with a condenser, and in heat transfer communication with a heat source for selectively desorbing the adsorbed water vapor; said condenser arranged to condense the water vapor to desalinated water; wherein said system is arranged to sequentially connect, for a pre-determined period, each evaporator to a corresponding adsorption bed, and the heat source to the third bed.Type: GrantFiled: July 20, 2010Date of Patent: December 10, 2013Assignee: National University of SingaporeInventors: Bidyut Baran Saha, Kim Choon Ng, Anutosh Chakraborty, Kyaw Thu
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Patent number: 8591704Abstract: A fractionation process for producing at least two concentration fractions of a fluid including a solute, suspended or dissolved content using at least two fluidly connected evaporator units is provided. The process includes the steps of: feeding a feed fluid including a solute, suspended or dissolved content into at least a first evaporator unit; evaporating a first amount of fluid from the feed fluid in at least the first evaporator unit to produce a first concentrated fluid; feeding at least a portion of the first concentrated fluid into at least a second evaporator unit; and evaporating a second amount of fluid from the first concentrated fluid in at least the second evaporator unit to produce a second concentrated fluid.Type: GrantFiled: March 20, 2009Date of Patent: November 26, 2013Assignee: Creative Water Technology Ltd.Inventor: Stephen Shelley
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Patent number: 8586779Abstract: The present invention relates in general terms to a process for preparing alkyl methacrylates, comprising as steps: providing an acetone cyanohydrin by a process according to one of the preceding claims; contacting the acetone cyanohydrin with an inorganic acid to obtain a methacrylamide; contacting the methacrylamide with an alcohol in the presence of an inorganic acid in a reactor to obtain an alkyl methacrylate; continuously discharging at least a portion of the alkyl methacrylate from the reactor into a distillation column as a vapor stream; the discharge being effected by feeding a discharge stream comprising steam into the reactor, to an apparatus for preparing alkyl methacrylates, to a process for preparing polymers based at least partly on alkyl methacrylates, to the use of the alkyl methacrylates obtainable by the process according to the invention in chemical products, and to chemical products based on alkyl methacrylates obtainable by the process according to the invention.Type: GrantFiled: August 31, 2007Date of Patent: November 19, 2013Assignee: Evonik Röhm GmbHInventors: Udo Gropp, Robert Weber, Thomas Schaefer, Andreas Perl, Rudolf Sing, Thomas Mertz
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Patent number: 8585869Abstract: Methods, systems, and/or apparatuses for treating wastewater produced at a thermoelectric power plant, other industrial plants, and/or other industrial sources are disclosed. The wastewater is directed through a wastewater concentrator including a direct contact adiabatic concentration system. A stream of hot feed gases is directed through the wastewater concentrator. The wastewater concentrator mixes the hot feed gases directly with the wastewater and evaporates water vapor from the wastewater. The wastewater concentrator separates the water vapor from remaining concentrated wastewater. A contained air-water interface liquid evaporator may be arranged to pre-process the wastewater before being treated by the wastewater concentrator.Type: GrantFiled: February 7, 2013Date of Patent: November 19, 2013Assignee: Heartland Technology Partners LLCInventors: Bernard F. Duesel, Jr., Craig Clerkin
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Patent number: 8535486Abstract: A water desalination system includes an evaporator for evaporating saline water to produce water vapor and an adsorption means in selective vapor communication with the evaporator for reversibly adsorbing the water vapor from the evaporator. The adsorption means is in selective vapor communication with a condenser, and desorbing means for desorbing the adsorbed water vapor from the adsorption means for collection by the condenser. The condenser is adapted to condense the water vapor to desalinated water.Type: GrantFiled: May 11, 2006Date of Patent: September 17, 2013Assignees: National University of Singapore, Kyushu UniversityInventors: Kim Choon Ng, Xiao-Lin Wang, Lizhen Gao, Anutosh Chakraborty, Bidyut Baran Saha, Shigeru Koyama, Atsushi Akisawa, Takao Kashiwagi
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Patent number: 8524047Abstract: A method of dehydrating tolylenediamine which includes subjecting tolylenediamine having a water content of 5-40 wt. % to first-stage distillation at a vacuum of 13-101.3 kPa and subjecting the bottoms from the first-stage distillation to second-stage distillation at a vacuum lower than 13kPa.Type: GrantFiled: November 25, 2008Date of Patent: September 3, 2013Assignee: Mitsui Chemicals Inc.Inventors: Toshiyuki Ogawa, Mitsunaga Dohzaki, Masaaki Sasaki
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Patent number: 8523980Abstract: An apparatus for water reclamation includes an inlet head for admitting warm humid ambient air, a buried pipe coupled at a first end to the inlet head and sloping downward in the ground from the first end. Water condenses as the air is cooled in the buried pipe and collects in a cistern coupled at a second end of the buried pipe. A tube coupled at a lower end near the second end of the buried pipe includes a heated element extending at least partially into the tube from an upper end of the tube. Cooled air is heated by the heated element and is expelled at the top of the tube. A heater is coupled to an upper end of the heated element. The heater may be a solar collector with a Bernoulli aperture.Type: GrantFiled: January 7, 2011Date of Patent: September 3, 2013Inventor: Javier Fernandez-Han
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Patent number: 8512567Abstract: A desalination system wherein a latent heat of condensation produced by the temperature gradient across a membrane distillation (MD) module is transferred directly to a latent heat of vaporization during desalination of a liquid flow stream. The desalination system comprises the MD module disposed within an object and configured to receive an input feed stream for desalination and produce an output flow stream of a product. The system also comprises a vapor compressor in fluidic communication with the MD module and configured to introduce a hot steam to a high temperature side of the MD module and extract a cool steam, having a temperature less than the hot steam, from a low temperature side of the MD module, thereby creating a temperature gradient across of the MD module. A desalination method is also presented.Type: GrantFiled: August 31, 2010Date of Patent: August 20, 2013Assignee: General Electric CompanyInventor: Andrew Philip Shapiro
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Patent number: 8469091Abstract: Embodiments presented herein provide an evaporation based zero liquid discharge method for generation of up to 100% quality high pressure steam from produced water in the heavy oil production industry. De-oiled water is processed in an evaporation system producing a distillate that allows steam to be generated with either drum-type boilers operating at higher pressures or once-through steam generators (OTSGs) operating at higher vaporization rates. Evaporator blowdown is treated in a forced-circulation evaporator to provide a zero liquid discharge system that could recycle >98% of the deoiled water for industrial use. Exemplary embodiments of the invention provide at least one “straight sump” evaporator and at least one hybrid external mist eliminator. Embodiments of the evaporation method operate at a higher overall efficiency than those of the prior art by producing distillate at a higher enthalpy which minimizes the high pressure boiler preheating requirement.Type: GrantFiled: August 5, 2010Date of Patent: June 25, 2013Assignee: Aquatech International CorporationInventors: Daniel P. Bjorklund, Gregory J. Mandigo, Richard M. Schoen, James Michael Marlett, Chandrakant Tiwari
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Publication number: 20130118889Abstract: A method of producing one or more precipitable substances such as salt (NaCl) from a feed liquid source (such as sea water) in a precipitation apparatus, the method involving steps of providing a first solar energy treatment arrangement having at least one treatment panel construction having an upper solar energy transmission wall capable of passing solar energy to a treatment member located beneath the upper solar energy transmission wall, the or each treatment panel construction being arranged to receive liquid from the feed liquid source, the solar radiation energy concentrating the precipitable substance or substances in the treatment liquid within the or each said treatment panel construction, the method further sensing via a sensor the density of the treatment liquid discharged from the first solar energy treatment arrangement, returning the liquid discharged from the first solar energy treatment apparatus to an inlet region of the first solar energy treatment apparatus if the sensed density is below aType: ApplicationFiled: April 7, 2011Publication date: May 16, 2013Applicant: FIRST GREEN PARK PTY LTDInventor: Peter Johnstone
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Patent number: 8428753Abstract: The disclosure relates to a system and a method for planning the operation of, monitoring processes in, simulating, and/or optimizing a technical installation comprising several units that can be combined with each other. Said system comprises at least one process planning module, at least one process simulation module, and at least one process optimization module. Components for modeling, simulating, and optimizing the technical installation are stored in said modules. The interrelated modules cooperate with a data management layer via at least one interface, said data management layer making available actual measured and/or historical process data for determining parameters and/or operational data for the modules in order to plan operations as well as simulate and optimize processes. The parameters and/or operational data determined in the modules can be fed to the data management layer for further processing by taking into account the stored components.Type: GrantFiled: January 20, 2006Date of Patent: April 23, 2013Assignee: ABB Technology AGInventors: Markus Gauder, Rolf Schmitt, Stefan Lauxtermann
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Patent number: 8343316Abstract: A vacuum dehydrator for processing an oil containing entrained contaminants such as water, air, and particulates comprises a tower enclosing upper and lower chambers. A random packing is contained in the upper chamber. The oil is preheated to a temperature above the boiling point of water and is introduced into the upper chamber for downward flow through the random packing into the lower chamber. Entrained air and water is retained as water vapor in the upper chamber, and particulates are retained in the random packing. Heated ambient air is introduced into the lower chamber for upward flow through the random packing into the upper chamber, and the upper chamber is cooled to condense the water vapor. Oil and condensed water are pumped respectively from the lower and upper chambers.Type: GrantFiled: November 10, 2009Date of Patent: January 1, 2013Assignee: Siemens Industry, Inc.Inventors: Mortimer Daniel Williams, John G. Donnelly, Eric M. Laliberte, J. Rafael Lazo, Juan Alejandro Segrelles Sacristan, Anselmo Garcia Gracia
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Publication number: 20120279847Abstract: The invention disclosed and claimed herein relates to treatment of water contaminated with glycol to be recycled for further effective use of the cleaned water resulting therefrom, especially at airports. More specifically, this invention relates to improved techniques for efficiently and reliably generating continuous flows of cleaned water as well as a continuous flow of recyclable glycol water of controlled concentration.Type: ApplicationFiled: July 20, 2012Publication date: November 8, 2012Inventor: Brad Michael MALATESTA
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Patent number: 8273156Abstract: Contaminated water stored in an equalization basin is distributed to one or more flash vessels and a desired vacuum is pulled in a filled flash vessel, reducing the boiling point of the contained contaminated water. The suction force is preferably created by passing the contaminated water under pressure through a differential pressure injector. The contaminated water in the flash vessel completes an electrical circuit between conductive plates and a heating element that are submerged therein. An alternating electrical current is applied, some of which is conducted by the contaminated water to a heating element that heats the water, and the rest of which dissipates as thermal energy, heating the contaminated water. The alternating current is preferably generated by passing the contaminated water under pressure through a hydroelectric power generator. Little thermal energy is needed to evaporate the contaminated water, which condenses at the top of the flash vessel and is collected from a collection trough.Type: GrantFiled: July 1, 2009Date of Patent: September 25, 2012Inventor: Eric John Dole
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Patent number: 8257557Abstract: A dehydration method for removing water from a hydrolysis reaction mixture containing unreacted water generated when monochlorobenzene is hydrolyzed to produce phenol, the method for dehydrating the hydrolysis reaction mixture includes supplying a hydrolysis reaction mixture to a distillation tower, supplying a liquid containing monochlorobenzene to the tower top portion of the distillation tower, and removing the substantially whole amount of the water in the hydrolysis reaction mixture together with monochlorobenzene from the tower top portion by distillation.Type: GrantFiled: August 29, 2006Date of Patent: September 4, 2012Assignee: Sumitomo Chemical Company, LimitedInventors: Tateo Seo, Tetsuya Suzuta, Toshiaki Ui
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Patent number: 8216351Abstract: An Apparatus for purifying a feed stream containing carbon dioxide in which the feed stream, after having been compressed and dried, is partly cooled and then used to reboil a stripping column. Thereafter, the feed stream is further cooled and expanded to a lower operational temperature of the stripping column. A carbon dioxide product stream composed of the liquid column bottoms of the stripping column is expanded at one or more pressures to generate refrigeration, then fully vaporized within the main heat exchanger and compressed by a compressor to produce a compressed carbon dioxide product. Refrigeration is recovered in the main heat exchanger from a column overhead stream extracted from the stripping column within the main heat exchanger either directly or indirectly by auxiliary processing in which carbon dioxide is further separated and optionally recycled back to the main compressor used in compressing the feed stream.Type: GrantFiled: December 7, 2009Date of Patent: July 10, 2012Assignee: Praxair TechnologyInventors: Minish Mahendra Shah, Henry Edward Howard
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Patent number: 8128787Abstract: Processes for removing water from organic solvents, such as ethanol. The processes include distillation in two columns operated at sequentially higher pressure, followed by treatment of the overhead vapor by one or two membrane separation steps.Type: GrantFiled: August 27, 2008Date of Patent: March 6, 2012Assignee: Nitto Denko CorporationInventors: Nicholas P. Wynn, Yu Huang, Masakatsu Urairi, Richard W Baker
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Patent number: 8114255Abstract: Processes for removing water from organic solvents, such as ethanol. The processes include distillation in two columns operated at sequentially higher pressure, followed by treatment of the overhead vapor by one or two membrane separation steps.Type: GrantFiled: August 27, 2008Date of Patent: February 14, 2012Assignee: Membrane Technology & Research, Inc.Inventors: Leland M Vane, Franklin R Alvarez, Yu Huang, Richard W Baker
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Publication number: 20120018293Abstract: The invention provides a process for the production of a lean liquid hydrate inhibitor composition from a rich liquid hydrate inhibitor composition in which the liquid hydrate inhibitor has a boiling point above that of water, which process comprises: (a) feeding said rich liquid hydrate inhibitor composition to a first distillation vessel; (b) withdrawing a water and inhibitor containing vapour from said first distillation vessel and feeding it to a second distillation vessel; (c) withdrawing water vapour from said second distillation vessel; (d) withdrawing a lean hydrate inhibitor composition from said second distillation vessel in liquid form; (e) withdrawing a lean hydrate inhibitor composition from said first distillation vessel in liquid form; (f) withdrawing liquid from said first distillation vessel and removing solids therefrom; wherein the withdrawal of steps (e) and (f) may be of a single liquid stream and wherein at least a portion of the lean hydrate inhibitor composition withdrawn from said firType: ApplicationFiled: January 22, 2010Publication date: January 26, 2012Applicant: STATOIL PETROLEUM ASInventors: Baard Kaasa, Per Halvard Billington
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Patent number: 8101048Abstract: This invention relates to methods of removing impurities from compounds having similar volatilities to form ultra high purity compounds.Type: GrantFiled: June 30, 2008Date of Patent: January 24, 2012Assignee: Rohm and Haas CompanyInventors: Francis Joseph Lipiecki, Stephen G Maroldo, Deodatta Vinayak Shenai-Khatkhate, Robert A. Ware
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Patent number: 8092656Abstract: A process for treatment of an aqueous stream to produce a low solute containing distillate stream and a high solute/solids containing blowdown stream utilizing a method to increase the efficiency of an evaporator while providing an essentially scale free environment for the heat transfer surface. Multi-valent ions and non-hydroxide alkalinity are removed from aqueous feed streams to very low levels and then the pH is increased preferably to about 9 or higher to increase the ionization of low ionizable constituents in the aqueous solution. In this manner, species such as silica and boron become highly ionized, and their solubility in the concentrated solution that is present in the evaporation equipment is significantly increased. The result of this is high allowable concentration factors and a corresponding increase in the recovery of high quality reusable water with essentially no scaling.Type: GrantFiled: October 17, 2003Date of Patent: January 10, 2012Assignee: Aquatech International CorporationInventors: Keith R. Minnich, Ramkumar Karlupudi, Richard M. Schoen
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Publication number: 20110278151Abstract: A method for recovering base oil from waste lubricating oil by separating base oil range constituents from a waste lubricating oil mixture, thereafter separating higher quality base oil constituents and lower quality base oil constituents from the base oil recovered from the waste lubricating oil mixture and thereafter treating the lower quality base oil constituents to produce marketable base oil. The total base oil produced from a waste lubricating oil mixture by this process is greater than the quantity producible by previous processes using only base oil separation from the waste lubricating oil mixture or processes which use only treatment of the base oil recovered from the waste lubricating oil mixture to produce the product base oil.Type: ApplicationFiled: May 16, 2011Publication date: November 17, 2011Inventor: Martin R. MacDonald
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Patent number: 8048309Abstract: A method for disposing of carbon dioxide is provided. According to the invention, CO2 is dissolved in seawater and the salinity of the seawater is increased to produce CO2-containing brine. The CO2-containing brine is denser than the seawater from which it is made. Therefore, when it is released into the ocean, the CO2-containing brine sinks to depth and sequesters the carbon dioxide. The brine may be produced by forming CO2 hydrate, which extracts fresh water from the seawater. Alternatively, the brine may be produced by forming water ice from the seawater and injecting CO2 into the seawater either before or, more preferably, after the water ice has been formed.Type: GrantFiled: August 28, 2008Date of Patent: November 1, 2011Assignee: Water Generating Systems, LLCInventors: John P. Osegovic, Michael D. Max, Shelli R. Tatro