Shaping Or Treating Of Multilayered, Impregnated, Or Composite-structured Article Patents (Class 264/642)
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Publication number: 20040207134Abstract: Unfired first ceramic layers 11 and at least one unfired second ceramic layer 12 having a different color from the unfired first ceramic layers 11 are laminated to prepare an unfired ceramic laminate 13. Notches 14 are then formed on a surface of the unfired ceramic laminate 13 using the second ceramic layer 12 as a reference. The unfired ceramic laminate 13 is fired to provide a fired ceramic laminate 13a, which is then divided along the notches 14 into ceramic composites 13b. In this process, notches having the proper depth can be formed on the unfired ceramic laminate 13.Type: ApplicationFiled: December 22, 2003Publication date: October 21, 2004Inventor: Kazuo Kishida
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Patent number: 6800241Abstract: A description is given of a filling level measuring device operating with microwaves, having a housing and an insert composed of a dielectric, and of a process for producing the dielectric, in which the dielectric constant of the insert is adjustable and in which the insert has a high chemical resistance and a mechanical strength adequate for industrial applications. The dielectric is a composite material composed of a fluoroplastic, in particular polytetrafluoroethylene, and ceramic and is produced by mixing powdered ceramic and powdered fluoroplastic, drying the mixture, pressing the mixture and sintering the pressed mixture.Type: GrantFiled: April 19, 2002Date of Patent: October 5, 2004Assignee: Endress + Hauser GmbH + Co.Inventors: Sergej Lopatin, Rolf Schwald, Alexander Hardell
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Patent number: 6800242Abstract: A process for making an alkaline resistant material comprises the steps of grinding together 0-40% light magnesia, 0-80% roasted magnesia, 10-54% ceramic clay, 0-9% limestone, 1-4% water glass, 0-1.5% carboxymethyl cellusolve, 0-27% talc, 0-3% calcium or barium carbonate to a particle size of less than 50 microns, mixing the ground mixture with water to produce a paste containing <23% wt. water, shaping the paste to a desired shape, drying the shaped product at a temperature of 110 degrees Centigrade, and firing the dried shaped product in a kiln at 1350 degrees Centigrade. The resulting alkali resistant ceramic contains 25-76 wt % MgO, 13-47% SiO2, 5-20 wt % Al2O3, and 1-10 wt % Fe2O3, CaO, K2O, and/or Na2O, with forsterite and spinel being the dominant crystalline phases.Type: GrantFiled: April 14, 2003Date of Patent: October 5, 2004Inventor: Xueren Cao
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Patent number: 6800182Abstract: A sputtering target is provided that includes SiC and metallic Si and has an atomic ratio of C to Si of from 0.5 to 0.95 and a density of from 2.75×103 kg/m3 to 3.1×103 kg/m3. The sputtering target is capable of forming at high speed a film that contains SiO2 as the main component and has a low refractive index. The sputtering target can be produced by a process in which a molded product of SiC is impregnated with molten Si.Type: GrantFiled: April 15, 2002Date of Patent: October 5, 2004Assignee: Asahi Glass Company, LimitedInventors: Akira Mitsui, Hiroshi Ueda, Kouichi Kanda, Susumu Nakagama
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Patent number: 6800229Abstract: Method for forming large-dimension ceramic tiles comprising the following operative stages: feeding a determined quantity of powders into the mould cavity of a first pressing station; pressing said quantity of powders to obtain a slab of congruent material the thickness of which is reduced by a quantity between 20 and 40%; feeding said slab to at least one decorating station which deposits in a controlled manner at least a second layer of powders; feeding said decorated slab to a second pressing station; pressing the decorated slab.Type: GrantFiled: November 26, 2001Date of Patent: October 5, 2004Assignee: Sacmi-Cooperativa Meccanici Imola-Soc. Coop. A R.L.Inventors: Pier Ugo Acerbi, Paolo Mongardi
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Patent number: 6797220Abstract: Processes for mechanically fabricating two and three-dimensional fibrous monolith composites include preparing a fibrous monolith filament from a core composition of a first powder material and a boundary material of a second powder material. The filament includes a first portion of the core composition surrounded by a second portion of the boundary composition. One or more filaments are extruded through a mechanically-controlled deposition nozzle onto a working surface to create a fibrous monolith composite object. The objects may be formed directly from computer models and have complex geometries.Type: GrantFiled: December 4, 2001Date of Patent: September 28, 2004Assignee: Advanced Ceramics Research, Inc.Inventors: Anthony C. Mulligan, Mark J. Rigali, Manish P. Sutaria, Gregory J. Artz, Felix H. Gafner, K. Ranji Vaidyanathan
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Patent number: 6790806Abstract: The core/jacket catalyst molding with a core made from an inorganic support material and with a jacket made from a catalytically active material can be prepared by coextruding an aqueous molding composition which comprises the support material or a precursor thereof, with an aqueous molding composition which comprises the catalytically active material or a precursor thereof, then drying the coextrudate, and then calcining the dried coextrudate.Type: GrantFiled: January 17, 2002Date of Patent: September 14, 2004Assignee: BASF AktiengesellschaftInventors: Michael Hesse, Rainer Anderlik, Hans-Gerhard Fritz, Jochen Hammer
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Patent number: 6767662Abstract: A process of making an electrochemical device comprising providing a trilayer structure comprising an electrode/electrolyte/electrode and simultaneously sintering the trilayer structure.Type: GrantFiled: October 10, 2001Date of Patent: July 27, 2004Assignee: The Regents of the University of CaliforniaInventors: Craig P. Jacobson, Steven J. Visco, Lutgard C. De Jonghe
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Patent number: 6764619Abstract: A method of making an EUV lithography stage structure includes depositing a layer of a Ti doped SiO2 glass powder in a confined region to provide an underlying layer; applying a binder to form a primitive with the binder bonding the glass powder together at one or more selected regions; depositing an above layer of the glass powder above the deposited layer; applying the binder to the above layer with the binder bonding the glass powder together at one or more selected regions; repeating the deposition and binding steps to produce a number of successive layers with the binder bonding the successive layers together; and removing the unbonded glass powder to provide a bonded glass powder lithography stage structure which is then sintered and densified into a densified nonpowder glass lithography stage.Type: GrantFiled: October 31, 2001Date of Patent: July 20, 2004Assignee: Corning IncorporatedInventors: James J. Bernas, Bradley F. Bowden, Kenneth E. Hrdina, John F. Wight, Jr.
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Patent number: 6764620Abstract: A method for reaction forming refractory metal carbides. The method involves the fabrication of a glassy carbon preform by casting an organic, resin-based liquid mixture into a mold and subsequently heat treating it in two steps, which cures and pyrolizes the resin resulting in a porous carbon preform. By varying the amounts of the constituents in the organic, resin-based liquid mixture, control over the density of the carbon preform is obtained. Control of the density and microstructure of the carbon preform allows for determination of the microstructure and properties of the refractory metal carbide material produced. The glassy carbon preform is placed on a bed of refractory metal or refractory metal—silicon alloy. The pieces are heated above the melting point of the metal or alloy. The molten metal wicks inside the porous carbon preform and reacts, forming the refractory metal carbide or refractory metal carbide plus a minor secondary phase.Type: GrantFiled: November 28, 2001Date of Patent: July 20, 2004Assignee: The United States of America as represented by the United States Department of EnergyInventors: Marc N. Palmisiano, Kevin J. Jakubenas, Rita Baranwal
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Patent number: 6759117Abstract: A multilayer ceramic composite is described which contains at least one supporting zone having oxidation-sensitive reinforcing fibers as well as a matrix. The matrix optionally contains oxidation-sensitive components. The composite further contains at least one surface layer, as well as at least one additional protective layer disposed between the supporting zone and surface layer, and whose matrix is composed substantially of at least one component of the matrix of the supporting zone or cover layer. The protective layer further contains additives that form self-healing layers.Type: GrantFiled: July 8, 2002Date of Patent: July 6, 2004Assignee: SGL Carbon AGInventors: Moritz Bauer, Martin Christ, Udo Gruber, Michael Heine, Andreas Kienzle, Jens Rosenlöcher, Rainer Zimmermann-Chopin
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Publication number: 20040113332Abstract: A powdery mixture of fine SiC powder with one or more oxide sintering additives of Al2O3, Y2O3, SiO2 and CaO is blended and uniformly dispersed in a polymeric SiC precursor to prepare a matrix-forming polymeric slurry. A preform of SiC fiber, which has quasi-stoichiometric composition with high crystallinity, is impregnated with the polymeric slurry and then hot-pressed at a temperature of 1600° C. or higher in presence of a liquid phase. Since the heat-resistant SiC fiber is used as strengthening fiber, the prepreg is sintered to a dense SiC composite excellent in mechanical properties by one-step hot-pressing.Type: ApplicationFiled: October 2, 2003Publication date: June 17, 2004Inventors: Akira Kohyama, Yutai Katoh
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Publication number: 20040108629Abstract: The method for fabricating a ceramic substrate comprises the step of screen-printing a first dielectric material in a first region of a resin film 30 and screen-printing a second dielectric material of a dielectric constant different from that of the first dielectric material in a second region of the resin film 30 to form a layer including on the resin film 30 a high dielectric layer 20a of the first dielectric material and a base dielectric layer 24a of the second dielectric material, the step of releasing the layer from the resin film 30, and the step of sintering the layer released form the resin film 30.Type: ApplicationFiled: December 2, 2003Publication date: June 10, 2004Applicant: FUJITSU LIMITEDInventors: Yoshihiko Imanaka, Masatoshi Takenouchi
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Publication number: 20040089985Abstract: Electronically tunable dielectric materials having favorable properties are disclosed. The electronically tunable materials include an electronically tunable dielectric phase such as barium strontium titanate in combination with at least two additional metal oxide phases. The additional metal oxide phases may include, for example, oxides of Mg, Si, Ca, Zr, Ti and Al. The electronically tunable materials may be provided in bulk, thin film and thick film forms for use in devices such as phased array antennas, tunable filters and the like. The materials are useful in many applications, including the area of radio frequency engineering and design.Type: ApplicationFiled: October 16, 2003Publication date: May 13, 2004Inventors: Louise C. Sengupta, Xubai Zhang, Luna H. Chiu
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Publication number: 20040079190Abstract: A die (20) comprises metal-rich sections (40a, 40b) which form an inner wall and an outer wall of the die (20), respectively. Gradient sections (42a, 42b) are disposed adjacent to the metal-rich sections (40a, 40b), respectively. Further, a ceramics-rich section (44) is disposed between the gradient sections (42a, 42b). A punch (30) comprises an inner ceramics-rich section (46), a gradient section (50), and an outer metal-rich section (48). In the die (20), the composition ratio of metal gradually decreases from the metal-rich sections (40a, 40b) to the ceramics-rich section (44). Similarly, in the punch (30), the composition ratio of the metal gradually decreases from the metal-rich section (48) to the ceramics-rich section (46).Type: ApplicationFiled: June 17, 2003Publication date: April 29, 2004Inventors: Mitsuo Kuwabara, Masanori Ohtsuka
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Patent number: 6716376Abstract: The invention relates to a process for producing a fiber composite material containing fibers with a high hot strength, in particular based on carbon, silicon, boron and/or nitrogen, a pressing compound being produced from fibers, a binder and, if appropriate, fillers and/or additives, which is then pressed in a press mold to form a green body. Various pressing compounds are produced, which contain fibers of different qualities and/or in different proportions, and the press mold is filled with the various pressing compounds in a number of successive steps. The invention also relates to a fiber composite material of this nature.Type: GrantFiled: November 1, 2000Date of Patent: April 6, 2004Assignee: DaimlerChrysler AGInventors: Tilmann Haug, Kolja Rebstock, Christian Schwarz
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Publication number: 20040061443Abstract: A ceramic arc tube assembly and a method for making a ceramic arc tube are described which simplify the manufacture of ceramic arc tubes by reducing the number of handling and heat treatments required to assemble arc tubes prior to the final sintering operation. In particular, the invention uses transient assembly buttons during intermediate assembly steps which are removed prior to the final sintering operation.Type: ApplicationFiled: September 30, 2003Publication date: April 1, 2004Inventors: Jeffrey T. Neil, Matthew A. Stough
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Publication number: 20040062911Abstract: A combinatorial library includes a gelcast substrate defining a plurality of cavities in at least one surface thereof; and a plurality of gelcast test materials in the cavities, at least two of the test materials differing from the substrate in at least one compositional characteristic, the two test materials differing from each other in at least one compositional characteristic.Type: ApplicationFiled: September 27, 2002Publication date: April 1, 2004Inventors: Robert J. Lauf, Claudia A. Walls, Lynn A. Boatner
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Patent number: 6709627Abstract: A method of making a product which is generally impervious to water including the steps of making a generally homogenous mixture of slate particles and clay, wetting the mixture as necessary to produce a formable composition, forming the wet mixture to a desired configuration, at least partially drying the formed mixture and subjecting the dried formed mixture to a temperature of at least 1100° C. for a time sufficient for at least some of the clay to convert into a binder to bind together the slate particles.Type: GrantFiled: March 8, 2002Date of Patent: March 23, 2004Assignee: Digive LimitedInventor: John Dutton
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Publication number: 20040053030Abstract: A method for producing composite ceramic material is provided wherein a core ceramic structure is produced and simultaneously enveloped with a sleeve of similar material.Type: ApplicationFiled: October 3, 2003Publication date: March 18, 2004Inventors: Kenneth C. Goretta, Dileep Singh, Bryant J. Polzin, Terry Cruse, John J. Picciolo
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Patent number: 6699429Abstract: A process for forming a silicon nitride-bonded silicon carbide honeycomb monolith by a) forming a plasticizable mixture which includes (1) about 60% to 85% by weight, powdered silicon carbide with a median particle size of about 10-40 micrometers; (2) about 15% to 40% by weight, powdered silicon metal with a median particle size of about 5-20 micrometers; and, (3) organic components; b) extruding the plasticizable mixture to form a green honeycomb monolith; c) drying the green honeycomb monolith; and, d) heating the honeycomb monolith to 1450° C. with a hold of 1 hour in an atmosphere of argon; and, e) nitriding the honeycomb monolith between 1450° C. to 1600° C. for a time sufficient to obtain a silicon nitride-bonded silicon carbide body.Type: GrantFiled: August 1, 2002Date of Patent: March 2, 2004Assignee: Corning IncorporatedInventors: Yanxia Lu, Dale R. Wexell, Elizabeth M. Wheeler
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Patent number: 6689308Abstract: Methods of forming plasma addressed liquid crystal display ribs are disclosed. An exemplary method includes introducing a glass paste which includes a curable medium into cavities formed in an intaglio collector to define rib structures, which are from the collector to a surface of the substrate, and removing the curable medium from the rib structures on the substrate surface to generate pores in the rib structures. The substrate having rib structures is then dipped into a solution containing an opaque pigment which is absorbed into the rib structure.Type: GrantFiled: June 27, 2002Date of Patent: February 10, 2004Assignee: Corning IncorporatedInventors: Pascale Laborde, Jean-Pierre Themont
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Publication number: 20040007800Abstract: A method for manufacturing an electrostatic chuck is disclosed wherein a sintered ceramic body having a dielectric layer made from Alumina (Al2O2) and Titanium Nitride (TiN) having a specific range of particle size is heat treated in an oxygen-rich environment in order to produce a uniform dielectric layer having no pores or micro-cracks.Type: ApplicationFiled: July 10, 2002Publication date: January 15, 2004Inventors: Hongy Lin, Jason Eugene Smith, Thomas Michael Laskowski
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Patent number: 6669893Abstract: A neutron absorbent material and a process for manufacturing said material, the neutron absorbent material having great resistance to mechanical damage and more particularly great resistance to crack propagation, which material contains boron carbide and hafnium in the form of powders of fine grain size, and with the manufacturing process it is possible, by reactive sintering of the two powders, to obtain a boron carbide based material having hafnium boride strata, which process comprises a step consisting of mixing boron carbide and hafnium and a reactive sintering step of the mixture obtained.Type: GrantFiled: September 28, 2001Date of Patent: December 30, 2003Assignee: Commissariat a l'Energie AtomiqueInventors: Bruno Provot, Xavier Deschanels, Philippe Bry
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Patent number: 6670021Abstract: 12A high temperature gas turbine component includes an inner core made of a monolithic ceramic material embedded within an outer CMC shell. The inner core may be formed with a through hole, blind hole, wear pads and the like. A method of making the bushing includes the steps of a) forming an inner core of silicon nitride or silicon carbide; and b) applying a ceramic matrix composite material over substantially all of the inner core.Type: GrantFiled: November 14, 2001Date of Patent: December 30, 2003Assignee: General Electric CompanyInventors: Mark Stewart Schroder, Paul Stephen DiMascio, Randall Richard Good
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Patent number: 6660115Abstract: A method of manufacturing a ceramic matrix composite comprises forming a slurry comprising a ceramic sol, filler particles and a solvent and forming laminates of fibers (12). The laminates of fibers (12) are impregnated with the slurry and are stacked (14) on a mold (10). The stack (14) of laminates of fibers (12) is covered by a porous membrane (16), a breather fabric (18) and a vacuum bag (20). The vacuum bag (20) is evacuated and is heated to a temperature of 60° C. for 10 hours to produce a ceramic matrix composite. The ceramic matrix composite is then heated to a temperature of 1200° C. at atmospheric pressure to sinter the ceramic matrix composite.Type: GrantFiled: September 18, 2002Date of Patent: December 9, 2003Assignee: Rolls-Royce plcInventors: Edwin G Butler, Anthony G Razzell, John Dominy, Paul A Doleman, Ihsan A H Al-Dawery
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Patent number: 6656336Abstract: A hydrocarbon sensor is formed with an electrolyte body having a first electrolyte surface with a reference electrode depending therefrom and a metal oxide electrode body contained within the electrolyte body and having a first electrode surface coplanar with the first electrolyte surface. The sensor was formed by forming a sintered metal-oxide electrode body and placing the metal-oxide electrode body within an electrolyte powder. The electrolyte powder with the metal-oxide electrode body was pressed to form a pressed electrolyte body containing the metal-oxide electrode body. The electrolyte was removed from an electrolyte surface above the metal-oxide electrode body to expose a metal-oxide electrode surface that is coplanar with the electrolyte surface. The electrolyte body and the metal-oxide electrode body were then sintered to form the hydrocarbon sensor.Type: GrantFiled: May 30, 2002Date of Patent: December 2, 2003Assignee: The Regents of the University of CaliforniaInventors: Rangachary Mukundan, Eric L. Brosha, Fernando Garzon
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Publication number: 20030218268Abstract: A method of synthesizing negative-thermal-expansion ceramics of synthesizing Zr(1−x)XxW2O8 in which X represents a substituent element for zirconium Zr, and 0≦x <<1, having a negative thermal expansion coefficient, the method comprising mixing two mols of tungsten trioxide WO3 and one mol of the sum of zirconium oxide ZrO2 and a substituent element X in accordance with substitution amount x at a stoichiometrical ratio, further mixing the thus obtained starting material in a powdery form having a particle size distribution including two groups of particles comprising smaller diameter particles with a particle size of 0.Type: ApplicationFiled: May 22, 2003Publication date: November 27, 2003Applicant: Moritex CorporationInventors: Yuhkoh Morito, Kouji Takahashi, Takuya Hashimoto
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Patent number: 6641776Abstract: X-ray imageable articles, for instance surgical implements or parts therefore which are used in minimally invasive surgical procedures, may be prepared by a process including the steps of: (a) preparing a mixture composition comprising: i) radiolucent particulate material selected from ceramic materials, metallurgic materials, and combinations thereof and having a particulate size of no more than 40 microns, ii) radiopaque particulate material selected from ceramic materials, metallurgic materials, and combinations thereof and having a particulate size of no more than 40 microns, and (iii) at least one polymeric binder material; (b) injection molding the mixture composition into a preform; (c) optionally removing the binder material from the preform; and (d) sintering the preform.Type: GrantFiled: November 15, 2000Date of Patent: November 4, 2003Assignee: SciMed Life Systems, Inc.Inventors: Timothy J. Weaver, Dion Mraz
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Publication number: 20030183990Abstract: A method for manufacturing a ceramic heater includes mixing a conductive ceramic powder, an insulating ceramic powder, a sintering aid powder, and a solvent so as to obtain a slurry, drying the slurry so as to obtain a heating-element material powder, forming a green resistance-heating element from the heating-element material powder, embedding the green resistance-heating element in a ceramic substrate, and firing a resultant assembly. Water is used as the solvent. Drying of the slurry is performed by use of a fluidized-bed drying apparatus, a rotary drying apparatus, or a vibratory drying apparatus and, the apparatus being employed in combination with a medium for pulverization.Type: ApplicationFiled: February 25, 2003Publication date: October 2, 2003Applicant: NGK SPARK PLUG CO., LTD.Inventor: Shindou Watanabe
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Patent number: 6627019Abstract: A ceramic matrix composite part having elongated cooling channels within the wall thereof is manufactured by inserting decomposable inserts within a woven ceramic fiber preform. The inserts are tows of continuous carbon fibers surrounded by a carbonaceous filler, and are inserted where the channels are desired. The preform, with the inserts in place, is disposed within a mold. A ceramic matrix material is added and the fiber preform is consolidated with the ceramic matrix material. The consolidated part is then heated to thermally decompose the inserts to create the elongated channels within the part. The inserts may be flexible and woven into the preform using an automated weaving loom, or they may have limited flexibility and be inserted by machine or by hand.Type: GrantFiled: December 18, 2000Date of Patent: September 30, 2003Inventors: David C. Jarmon, Xiaolan Hu, Steven Wayne Burd, Christopher Dale Jones, Stephen K. Kramer, Christopher L. Kogstrom, Nikolaos Napoli, Bruce Bond
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Patent number: 6620370Abstract: Plasma addressed liquid crystal display ribs are formed by a method which includes forming a temporary mask on portions of a surface of a substrate, depositing a layer of a glass paste having a curable medium and at least one pigment blended therein over the substrate and temporary mask, micro-molding rib structures from the glass paste on the substrate surface in areas between the masked sections, removing any residual layer of paste material present on the temporary mask, removing the temporary mask from the substrate, and firing the substrate with micro-molded rib structures thereon.Type: GrantFiled: June 27, 2002Date of Patent: September 16, 2003Assignee: Corning IncorporatedInventor: Jean-Pierre Themont
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Patent number: 6616890Abstract: A method for fabricating electrically conductive silicon carbide articles by doping and sintering submicron silicon carbide particles using sub-micron alumina as the dopant source. Submicron alumina particles are made by milling aluminum powder. Despite the ductility of metallic aluminum, it is successfully ball milled in an aqueous medium through the creation and abrasion of successive layers of an alumina skin to yield alumina particles as small as 0.01 &mgr;m across. When suitably composed mixtures of the silicon carbide and alumina are molded into a green body and heated sufficiently in a non-oxidizing furnace atmosphere, the alumina breaks down to metallic aluminum which diffuses into the silicon carbide. The small particle sizes and the presence of a sintering aid enable rapid processing kinetics which favor saturation of the silicon carbide by the aluminum and inhibit grain growth.Type: GrantFiled: June 15, 2001Date of Patent: September 9, 2003Assignee: Harvest Precision Components, Inc.Inventor: Richard B. McPhillips
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Patent number: 6609294Abstract: A novel process for fabricating metal clad laminates used in the manufacture of printed wiring boards. The process which eliminates multiple use separator plates within laminate books during buildup and pressing, utilizes a sacrificial separator sheet between copper sheets and wherein the separator sheet remains intact throughout the pressing and cutting steps and is finally removed after the laminates have been sized to the desired dimensions. This process provides time and cost savings, as well as a significant increase in quality and quantity of the laminates produced.Type: GrantFiled: September 27, 2000Date of Patent: August 26, 2003Assignee: Polyclad Laminates, Inc.Inventors: Christopher Vernon Smith, Richard Allen Correia, Ed Carignan
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Patent number: 6596168Abstract: The invention relates to a filter element and its manufacture to be used in removal of liquid from solids containing material to be dried in a capillary suction dryer which filter element contains a ceramic microporous layer having the pore size under 5 micrometer and supported by a ceramic internal layer having recess areas for liquid flowing. The internal layer is made of at least one substrate which continuously surrounds at least one recess area and which ceramic internal layer is surrounded by at least one essentially continuous microporous surface layer.Type: GrantFiled: January 16, 2001Date of Patent: July 22, 2003Assignee: Outokumpu OyjInventors: Kerry Johnson, Olli Högnabba, Bjarne Ekberg
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Patent number: 6596224Abstract: A powder bed (32) is built up by repeated deposition of a slurry that contains powder. Layers are made by depositing a liquid dispersion of the desired powdered material, which then slip-casts into the forming powder bed to make a new layer (34). The slurry may be deposited in any suitable manner, such as by raster or vector scanning, or by a plurality of simultaneous jets that coalesce before the liquid slip-casts into the bed, or by individual drops, the deposits of which are individually controlled, thereby generating a regular surface for each layer.Type: GrantFiled: March 1, 2000Date of Patent: July 22, 2003Assignee: Massachusetts Institute of TechnologyInventors: Emanuel M. Sachs, Michael J. Cima, Michael A. Caradonna, Jason Grau, James G. Serdy, Patrick C. Saxton, Scott A. Uhland, Jooho Moon
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Patent number: 6576173Abstract: An improved method for manufacturing a porcelain object in a desired shape, from a mixture of at least clay, feldspar and quartz. According to the method, an aqueous dispersion of vinyl acetate and ethylene based copolymer is added to the mixture, and the mixture transformed into an aqueous mass in the shape of a foil with a thickness of 50 &mgr;m to 3 mm and dried. The dried foil is then formed into a desired object shape, and permanently hardened by a ceramic firing process. The dried foil may be brought into the desired object shape by known processes such as rolling, laminating, calendering, cutting, punching, paper folding methods and deep drawing. Once brought into the desired object shape, no drying is required before ceramic firing.Type: GrantFiled: August 22, 2000Date of Patent: June 10, 2003Inventors: Franz Koppe, Gerald Weber
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Patent number: 6565797Abstract: A method for the production of a silicon nitride filter includes heat treating in nitrogen a green body containing from 40 to 90% of metal silicon particles having an average particle size of from 1 to 200 &mgr;m and from 10 to 60% of a pore forming agent. The green body contains at least 90% of the metal silicon particles and the pore forming agent and forms a porous product. The filter is excellent in heat resistance, corrosion resistance, acid resistance and mechanical strength and suitable for dust arresting or dust removing and is particularly suitable as a filter for particulates. The porosity of the silicon nitride filter is from 40 to 70% and the cumulative pore volume of pores with diameters of at most 1 &mgr;m is from 1 to 15 vol % of the total pore volume.Type: GrantFiled: August 24, 2001Date of Patent: May 20, 2003Assignee: Asahi Glass Company, LimitedInventors: Naomichi Miyakawa, Nobuhiro Shinohara, Kanji Arai, Hideo Takahashi
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Patent number: 6562745Abstract: This invention relates to an aging resistant SiC igniter having a second layer of recrystallized SiC within the body.Type: GrantFiled: July 24, 2001Date of Patent: May 13, 2003Assignee: Saint-Gobain Ceramics and Plastics, Inc.Inventors: Craig A. Willkens, Normand P. Arsenault, James Olson, Roger Lin
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Publication number: 20030078156Abstract: A creep-resistant and chemical-resistant ceramic refractory composition includes a mixed oxide of the general formula R3Al5O12 where R is at least one of Dy, Ho, Y, Er, Tm, Yb, and Lu, the mixed oxide having a garnet structure and comprising in solid solution at least one dopant of a transition metal element and a rare-earth element, which effects in the composition enhanced optical emission in at least one spectral range.Type: ApplicationFiled: August 23, 2001Publication date: April 24, 2003Inventors: Richard A. Lowden, Robert J. Lauf, Frederick C. Montgomery, Claudia J. Rawn
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Patent number: 6544090Abstract: A method for chemically etching of a foam glass layer to provide at least one cavity pattern in the foam glass layer. The method utilizes a substrate with at least one major surface suitable for receiving a glass layer. At least one layer of a glass paste composition in then applied onto the major surface of the substrate. The substrate and glass paste composition are then heated to a temperature sufficient enough to obtain a foam glass layer bonded to the major surface of the substrate. At least a portion of the foam glass layer is chemically etched to obtain at least one cavity pattern in the foam glass layer. The chemical etching of the foam glass layer results in an anisotropic etching rate.Type: GrantFiled: June 16, 2000Date of Patent: April 8, 2003Assignee: E. I. du Pont de Nemours and CompanyInventors: Paul R. Anderson, Charles J. Barnhart, Randall J. Cutcher, Jill M. Wyse
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Patent number: 6533969Abstract: Process for the manufacture of dental restorations using high strength ceramic components. A wax pattern is built around a high strength ceramic component on a die. The wax pattern with the high strength ceramic component is surrounded with investment material. The wax is burned out, leaving a mold with the high strength ceramic component. The mold is filled with a ceramic material, covering the high strength ceramic component, creating a dental restoration.Type: GrantFiled: September 26, 2000Date of Patent: March 18, 2003Assignee: Jeneric/Pentron, Inc.Inventors: Gregg Daskalon, Dmitri Brodkin, Ajit Karmaker, Elie Zammarieh, Martin L. Schulman, Arun Prasad, Carlino Panzera, Paul Panzera
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Patent number: 6503441Abstract: A method for producing shaped articles of ceramic composites provides a high degree of dimensional tolerance to these articles. A fiber preform is disposed on a surface of a stable formed support, a surface of which is formed with a plurality of indentations, such as grooves, slots, or channels. Precursors of ceramic matrix materials are provided to the fiber preform to infiltrate from both sides of the fiber preform. The infiltration is conducted under vacuum at a temperature not much greater than a melting point of the precursors. The melt-infiltrated composite article substantially retains its dimension and shape throughout the fabrication process.Type: GrantFiled: May 30, 2001Date of Patent: January 7, 2003Assignee: General Electric CompanyInventors: Gregory Scot Corman, Milivoj Konstantin Brun, Henry Charles McGuigan
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Publication number: 20020195750Abstract: A ceramic powder of grains having a shape-anisotropy is mixed with a calcined or uncalcined (or both) powder of a ceramic raw material. A ceramic slurry containing the produced mixed powder, a solvent and a binder is prepared and the ceramic slurry is formed into a sheet. A laminate comprising a plurality of the sheets laminated to each other is uniaxially pressed to form an oriented product in such a manner that the length of the laminate in the direction parallel to the pressing axis becomes larger than that before the pressing, and the area of a plane perpendicular to the pressing axis of the laminate becomes larger than that before the pressing. The oriented formed product is fired and sintered.Type: ApplicationFiled: May 7, 2002Publication date: December 26, 2002Inventors: Hirozumi Ogawa, Masahiko Kimura, Akira Ando
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Patent number: 6497776Abstract: A method of manufacturing a ceramic matrix composite comprises forming a slurry comprising a ceramic sol, filler particles and a solvent and forming laminates of fibres (12). The laminates of fibres (12) are impregnated with the slurry and are stacked (14) on a mould (10). The stack (14) of laminates of fibres (12) is covered by a porous membrane (16), a breather fabric (18) and a vacuum bag (20). The vacuum bag (20) is evacuated and is heated to a temperature of 60° C. for 10 hours to produce a ceramic matrix composite. The ceramic matrix composite is then heated to a temperature of 1200° C. at atmospheric pressure to sinter the ceramic matrix composite.Type: GrantFiled: December 15, 1999Date of Patent: December 24, 2002Assignee: Rolls-Royce plcInventors: Edwin G. Butler, Anthony G. Razzell, John Dominy, Paul A. Doleman, Ihsan AI-I Al-Dawery
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Patent number: 6488885Abstract: A health support device having a lamination of a semiconductor film on a surface of a partially-reduced sintered material of titanium oxide. The semiconductor film is preferably a p-type semiconductor film of silicon or germanium. The partially-reduced sintered material is preferably represented by TiO2−x, where 0<×<0.5. The thickness of the semiconductor film is preferably from 1 nm to 500 nm. In production, a mixture of a titanium oxide powder and a binder is press-molded, and the molded material is sintered at a temperature of from 500° C. to 1100° C. in a vacuum, inert or reducing atmosphere. A p-type semiconductor film is formed on a surface of the resulting partially-reduced sintered material of titanium oxide.Type: GrantFiled: September 19, 2000Date of Patent: December 3, 2002Assignee: Furukawa Co., Ltd.Inventors: Saburo Ishiguro, Yoshitsugu Fujita, Tetsuhiro Iwata
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Publication number: 20020171182Abstract: A high density ceramic thick film is fabricated by providing vehicle comprising an organic binder and solvent, dispersing ceramic powders into the vehicle to be paste, forming the paste to thick film by screen printing, removing the organic binder from the film, applying sol or sol-like solution to the surface of the film so that the sol or sol-like solution can infiltrate into the film, removing remaining sol or sol-like solution from the surface of the film, drying and preheating the film, and sintering the film.Type: ApplicationFiled: April 4, 2002Publication date: November 21, 2002Inventors: Tae-Song Kim, Yong-Bum Kim, Hyung-Jin Jung
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Patent number: 6467137Abstract: A method of manufacturing an ink jet recording head. On one and the other surfaces of an ink supply plate, formed with a plurality of discrete ink supply ports and a corresponding number of discrete nozzle ports, a green sheet for a pressure chamber plate and a green sheet for an ink pool plate are laminated, respectively. The resulting lamination is then sintered. A vibration plate is subsequently adhered to the pressure chamber plate formed by the sintering step and a nozzle plate is adhered to the sintered pool plate.Type: GrantFiled: September 14, 1999Date of Patent: October 22, 2002Assignee: NEC CorporationInventors: Torahiko Kanda, Yasuhiro Otsuka, Kazuhiro Ikuina, Takaharu Kondo, Katsuhiro Notsu
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Publication number: 20020140135Abstract: A green sheet stack having a cavity is produced, and a shrinkage-reducing sheet containing inorganic powder material, which is not fired in a step of firing the green sheet stack, is prepared. The shrinkage-reducing sheet is placed so as to close an aperture of the cavity and to cover an end face in the sheet-stacking direction of the green sheet stack. The green sheet stack is pressed via an elastic member in the sheet-stacking direction so that the shrinkage-reducing sheet is cut and a shrinkage-reducing sheet piece formed of a cut portion of the shrinkage-reducing sheet is placed on a bottom surface of the cavity. The green sheet stack is fired in such a state in which the shrinkage-reducing sheet piece is placed on the bottom surface of the cavity.Type: ApplicationFiled: March 8, 2002Publication date: October 3, 2002Inventor: Hideyuki Harada
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Publication number: 20020142611Abstract: A corrosion resistant component of semiconductor processing equipment such as a plasma chamber comprises a cerium oxide containing ceramic material as an outermost surface of the component. The cerium oxide containing ceramic material comprises one or more cerium oxides as the single largest constituent thereof. The component can be made entirely of the cerium oxide containing ceramic material or, alternatively, the cerium oxide containing ceramic can be provided as a layer on a substrate such as aluminum or an aluminum alloy, a ceramic material, stainless steel, or a refractory metal. The cerium oxide containing ceramic layer can be provided as a coating by a technique such as plasma spraying. One or more intermediate layers may be provided between the component and the cerium oxide containing ceramic coating.Type: ApplicationFiled: March 30, 2001Publication date: October 3, 2002Inventors: Robert J. O'Donnell, John E. Daugherty