Specific Pressure Or Lack Or Pressure Recited Patents (Class 419/39)
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Patent number: 5561827Abstract: A nickel-base superalloy article has a coating having a composition, in weight percent, of from about 10 to about 20 percent cobalt, from about 14 to about 25 percent chromium, from about 2 to about 12 percent aluminum, from 0 to about 0.2 percent yttrium, from about 0.001 to about 3 percent boron, from about 1 to about 10 percent silicon, balance nickel and incidental impurities. The coating is preferably applied by mixing together two powders, one with a higher solidus temperature and one with a lower solidus temperature, whose net composition is that of the coating. The powder mixture is compacted with a binder, applied to a surface of the article, and heated to a temperature above the lower solidus temperature.Type: GrantFiled: December 28, 1994Date of Patent: October 1, 1996Assignee: General Electric CompanyInventors: Jim D. Reeves, David E. Budinger, Robert A. Anderson
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Patent number: 5561830Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 325 weight-% binder phase with extremely good properties at extremely fine machining with high cutting speeds and low feeds. The method relates to the use of a raw material comprising a complex cubic carbonitride containing the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.87.ltoreq.X.sub.IV .ltoreq.0.990.66.ltoreq.X.sub.C .ltoreq.0.76where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: October 1, 1996Assignee: Sandvik ABInventors: Gerold Weinl, Rolf Oskarsson
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Patent number: 5552109Abstract: This invention relates to a process of forming a sintered article of powder metal comprising blending graphite and lubricant with a pre-alloyed iron based powder, pressing said blended mixture to shape in a single compaction stage sintering said article, and then high temperature sintering said article in a reducing atmosphere to produce a sintered article having a density greater than 7.4 g/cc.Type: GrantFiled: June 29, 1995Date of Patent: September 3, 1996Inventors: Rohith Shivanath, Peter Jones, Danny T. D. Thieu
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Patent number: 5552108Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 3-25 weight-% binder phase with extremely good properties at extreme fine machining when turning with high cutting rates. The method relates to the use of a raw material comprising a complex cubic carbonitride containing the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.86.ltoreq.X.sub.IV .ltoreq.0.990.74.ltoreq.X.sub.C .ltoreq.0.83where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: September 3, 1996Assignee: Sandvik ABInventors: Gerold Weini, Rolf Oskarsson
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Patent number: 5529746Abstract: The invention relates to a process for pressing electrically conductive powders to high-density compacts in dimensionally stable pressing molds, whereby the achievable compression density is greater than 96% and, in many cases, amounts to almost 100% of the theoretical density of suitable materials. For said purpose, static pressing of the powders according to conventional methods is superimposed by a second process step, in which from 1 to 3 electric current pulses of from 5.times.10.sup.-5 to 5.times.10.sup.-2 s duration and high electric power are applied to the punches of the press. As opposed to known methods, no notable sintering of powder of particles occurs in such process. The process is especially suitable for the manufacture of high-density and high-strength, sintered mass-produced components, where compacts are produced on automatic presses with high cycle frequencies.Type: GrantFiled: March 8, 1995Date of Patent: June 25, 1996Inventors: Walter Knoss, Manfred Schlemmer
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Patent number: 5529745Abstract: By compacting in a magnetic field a mixture containing powder raw material A having a composition represented by (Tb.sub.x Dy.sub.1-x)T.sub.y wherein T is at least one metal of Fe, Co, and Ni and 0.30<x.ltoreq.x 0.50 and 1.70.ltoreq.y.ltoreq.2.00, powder raw material B having a composition represented by (Dy.sub.1-t Tb.sub.t).sub.z T.sub.1-z wherein 0.ltoreq.t.ltoreq.0.30 and 0.40.ltoreq.z.ltoreq.0.80 and optionally, powder raw material C consisting essentially of element T, and sintering the compact, there is prepared a magnetostrictive material having a composition represented by (Tb.sub.v Dy.sub.1-v)T.sub.w wherein 0.27.ltoreq.v<0.50 and 1.70.ltoreq.w.ltoreq.2.00, with grains oriented along [111] axis. The material having minimal crystalline magnetic anisotropy at room temperature and large magnetostrains is obtained at low cost by powder metallurgy.Type: GrantFiled: April 18, 1995Date of Patent: June 25, 1996Assignee: TDK CorporationInventors: Teruo Mori, Tomoko Nakamura
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Patent number: 5527504Abstract: To a fine R-Fe-B alloy powder comprised predominantly of 10-30 atomic % of R (wherein R stands for at least one elements selected from rare earth elements including yttrium), 2-28 atomic % of B, and 65-82 atomic % of Fe in which up to 50 atomic % of Fe may be replaced by Co, at least one boric acid ester compound such as tributyl borate is added as a lubricant in a proportion of 0.01%-2% by weight and mixed uniformly before, during, or after fine grinding of the alloy powder. The resulting powder mixture is compacted by compression molding in a magnetic field and the green compacts are sintered and aged. Compression molding can be performed continuously without need of mold lubrication, and the resulting magnets have improved magnet properties with respect to residual flux density, maximum energy product, and intrinsic coercive force.Type: GrantFiled: May 9, 1995Date of Patent: June 18, 1996Assignees: Sumitomo Metal Industries, Ltd., Sumitomo Special Metals Co. Ltd.Inventors: Yoshihisa Kishimoto, Nobushige Hiraishi, Wataru Takahashi, Masakazu Ohkita, Naoyuki Ishigaki, Yutaka Matsuura
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Patent number: 5522976Abstract: The target element (2) is formed from an inorganic compound layer (16) with a melting point above 300.degree. C. deposited on a foam or metallic felt support layer such that the layer of inorganic compound sinks to part of its depth into the support layer to define a composite layer (17). In order to form the target element, a precursor system of the inorganic compound is applied to the support layer, the assembly so formed is subjected to a pressure of between 0.1 MPa and 15 MPa, the resulting assembly is maintained at between 300.degree. C. and 1600.degree. C. and below the melting temperature of the support in order to obtain a sintered assembly. Said assembly is than cooled to an ambient temperature avoiding any sudden cooling. In order to produce the target, the element (2) is glued to a metallic substrate (4) using a conductive adhesive.Type: GrantFiled: June 14, 1994Date of Patent: June 4, 1996Assignee: Societe Nationale Elf AquitaineInventors: Guy Campet, Jean-Michel Chabagno, Claude Delmas, Joseph Portier, Jean Salardenne
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Patent number: 5516483Abstract: A process of forming a sintered article for powder metal comprising blending carbon and ferro alloys and lubricant with compressible elemental iron powder, pressing said blended mixture to form sintering said article, and then high temperature sintering said article in a reducing atmosphere to produce a sintered article having a high density from a single compression.Type: GrantFiled: February 8, 1994Date of Patent: May 14, 1996Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones, Danny T. D. Thieu
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Patent number: 5514327Abstract: Apparatus for use in cooling an integrated circuit structure. The apparatus includes a heat sink having a first portion configured for thermal engagement with an integrated circuit device and a second portion configured for the dissipation of heat into an ambient fluid, such as air. The heat sink is made from a powdered metal which, in one preferred embodiment, includes copper. The heat sink may be formed from the plurality of discrete layers, each layer having a button projecting from one surface, and a depression formed in an opposing surface. The depression is configured to receive a projecting button portion from another layer. In an alternative embodiment the heat sink includes a plurality of plugs projecting from the generally flat surface.Type: GrantFiled: December 14, 1993Date of Patent: May 7, 1996Assignee: LSI Logic CorporationInventor: Mark R. Schneider
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Patent number: 5512236Abstract: A process of coining sintered articles of powder metal comprising: blending carbon, ferro manganese, and lubricant with compressible elemental iron powder, pressing the blended mixture to form the articles, high temperature sintering of the articles in a reducing atmosphere and then coining the sintered articles to final shape so as to narrow the tolerance variability of coined articles and substantially eliminate secondary operations.Type: GrantFiled: August 25, 1994Date of Patent: April 30, 1996Assignee: Stackpole LimitedInventors: Peter Jones, Roger Lawcock
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Patent number: 5503926Abstract: A glass embedded, sintered ceramic comprising a total sintering aid concentration of between about 1 and about 5 w/o, said ceramic having a reaction layer of less than about 750 microns, where the reaction layer is defined as the depth at which the sintering aid concentration is 80% of that of the bulk of the ceramic, and the ceramic is selected from the group consisting of silicon nitride, silicon carbide, boron carbide, titanium diboride, and aluminum nitride.Type: GrantFiled: January 11, 1995Date of Patent: April 2, 1996Assignee: Saint-Gobain/Norton Industrial Ceramics CorporationInventors: Glenn Sundberg, Russell Yeckley
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Patent number: 5487771Abstract: A high-porosity metallic membrane element comprising a sintered element having at least about 55% porosity, the sintered element comprising a matrix of substantially interconnected pores, each of the pores being defined by a plurality of dendtritic metallic particles. A preferred form is made from pure nickel, preferably filamentous nickel powder. The high-porosity metallic membrane element, comprising the aforementioned sintered element having at least about 55% porosity, can be sealed within a filter housing to produce a highly porous filter device with a filtered fluid flow path through the metal membrane element. Also disclosed is a method of making the high-porosity metallic membrane element which includes depositing by air-laying techniques a substantially uniform low-density bed of a sinterable dendritic material into a mold suitable for applying compressive force thereto, compressing the low-density bed of sinterable dendritic material to form a green form, and sintering the green form.Type: GrantFiled: July 27, 1994Date of Patent: January 30, 1996Assignee: Millipore CorporationInventor: Robert S. Zeller
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Patent number: 5476632Abstract: A process of forming a sintered article of powder metal comprising: selecting elemental iron powder; determining the desired properties of said sintered article and selecting, a quantity of carbon, and ferro alloy from the group of ferro manganese, ferro chromium, ferro molybdenum, ferro vanadium, ferro silicon and ferro boron; grinding said ferro alloy to a mean particle size of approximately 8 to 12 microns; introducing a lubricant while blending the carbon, ferro alloy, with said elemental iron powder; pressing the mixture to form the article; and then high temperature sintering the article at a temperature between 1,250.degree. C. and 1,350.degree. C. in a neutral or reducing atmosphere; so as to produce the sintered article of powdered metal; and includes the product formed thereby.Type: GrantFiled: January 14, 1994Date of Patent: December 19, 1995Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones
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Patent number: 5476631Abstract: An automatic adaptive fill cavity adjust system for a powder metal press to control trend variations in the weight of multi-level parts as the result of the flowability and apparent density characteristics of the powder metal. The system comprises a monitoring component to monitor compacting load or tonnage changes, or part weight changes. A computer control is provided to receive the monitor signals, to keep a running average of a small sample of parts, to execute the proper logic to determine when a fill adjustment is needed, and to calculate the new fill position for each moveable platen bearing a tooling member to assure that the percent change in powder column height is the same for all columns. The system further includes a motor drive component responsive to the control computer output to position the up stop of each moveable platen bearing a tooling member and the core rod mechanism (if used), to achieve proportionally correct adjustments to the fill cavity.Type: GrantFiled: June 9, 1992Date of Patent: December 19, 1995Assignee: Cincinnati IncorporatedInventors: Richard S. Brown, William J. Molleran
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Patent number: 5472662Abstract: A method for manufacturing a stator for an ultrasonic motor, wherein the stator includes a circular land portion, a plurality of teeth secured to the land portion by a plurality of radial slits, the method comprising the steps of: compressing fine metal particle to form a pre-compression body having a predetermined shape, whereby said pre-compression body is provided with a plurality of projections for forming a plurality of teeth of the stator; baking said pre-compression body, for producing a sintered body; applying a densification process on the teeth of said sintered body produced in said baking step, whereby each of said teeth is provided with a high dense portion having a density ratio of at least 90%; and applying a sizing process to said sintered body produced in said baking step.Type: GrantFiled: May 17, 1994Date of Patent: December 5, 1995Assignee: Asmo Co., Ltd.Inventors: Motoyasu Yano, Yoshinori Takemura, Takao Suzuki
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Patent number: 5470525Abstract: Tantalum anode pellets or tantalum powders are treated to remove carbon content (mostly attributable to binders used in pressing the powders to pellet form and/or sintering of the pellets) by an aqueous leach at 50.degree.-200.degree. F. in lieu of the conventional complex distillation/decomposition methods.Type: GrantFiled: July 1, 1994Date of Patent: November 28, 1995Assignee: H. C. Starck, Inc.Inventors: Terrance B. Tripp, Malcolm Shaw
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Patent number: 5466277Abstract: A sintered Al-alloy, which has a composition of 0.2 to 2.0% of Mg, 10.0 to 35.0% of Si, from 0.2 to 4.0% of Cu, and Al and unavoidable impurities in balance, is produced by using a mixture of the main powder (10.0-35.0% of Si, 0.2-2.0% of Cu, and Al and unavoidable impurities in balance) and at least one metal or mother-alloy powder selected from (a)-(i): (a) Mg powder; (b) Al--Mg powder; (c) Al--Cu powder; (d) Al--Mg--Si powder; (e) Al--Cu--Si powder; (f) Al--Mg--Cu powder; (g) Al--Mg--Cu--Si powder; (h) Mg--Cu powder; and, (i) Mg--Cu--Si powder.Type: GrantFiled: March 30, 1994Date of Patent: November 14, 1995Assignee: Showa Denko K.K.Inventors: Shin Miura, Youichi Hirose, Mitsuaki Sato
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Patent number: 5466414Abstract: A process for fabrication of sintered metal components having improved mechanical, physical and wear-resistent properties.Type: GrantFiled: September 1, 1994Date of Patent: November 14, 1995Assignee: TecSyn, Inc.Inventor: Bjorn O. A. Pettersson
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Patent number: 5460776Abstract: The invention relates to a method of producing connected sintered articles obtained by breaking a unitary preform.It is characterized in that:a) a preform is pressed from powdered metals while imprinting in it a superficial groove (3) located in a plane for the purpose of subsequent breakage,b) this preform is presintered in order to consolidate it mechanically, the preform however remaining brittle,c) it is optionally compacted by recompression,d) recesses for the members for the mechanical connection of the final parts are optionally machined in this preform,e) this preform is broken into at least two parts,f) final sintering is carried out,g) the articles are cooled.The invention is applicable in particular to the production of connecting rods and connecting rod covers or of annular articles with or without an undercut (broken in the axial plane).Type: GrantFiled: October 26, 1994Date of Patent: October 24, 1995Assignee: SintertechInventors: Luc Ackermann, Henri Gueydan
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Patent number: 5456740Abstract: A getter-filter composite membrane element, comprising a sinterable getter material and a sinterable metal filter material, the composite element defining a matrix of substantially interconnected pores. Membrane elements may be comprised of at least three alternating layers of a first sinterable getter material layer and a second sinterable metal filter material layer, the first getter layer being located between the second filter layers, the second layers acting to hold the getter layer, and to retain the getter particles. Also disclosed is a method of making the getter-filter element.Type: GrantFiled: June 22, 1994Date of Patent: October 10, 1995Assignee: Millipore CorporationInventors: James T. Snow, Walter Plante, Robert S. Zeller
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Patent number: 5451244Abstract: A process for preparing a consolidated nickel-base superalloy compact suitable for tensile force inducing high strain rate deformation. It includes the steps of: preparing a melt of a nickel-base superalloy in a vacuum; atomizing the melt into powder in a protective atmosphere; collecting the powder; screening the powder to proper size; introducing the powder into a container; evacuating and sealing the container in a vacuum; and consolidating the powder under pressure at a temperature below the solidus temperature of the alloy and at a temperature at which grain boundaries grow past prior particle boundaries.Type: GrantFiled: April 6, 1994Date of Patent: September 19, 1995Assignee: Special Metals CorporationInventor: B. Wayne Castledine
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Patent number: 5451365Abstract: A ceramic composite may be densified, strengthened and toughened by the present transient plastic phase processing method. The ceramic composite comprises a transient plastic phase and a reactant phase. The transient plastic phase includes a metallic component and may also include a non-metallic component. The transient plastic phase has a yield strength which is a function of the stoichiometric concentration of the metallic component therein. In the present method, heat and pressure are applied to the ceramic composite to plastically deform the transient plastic phase of the composite and densify the composite. The densified composite is heated to react the transient plastic phase and the reactant phase in the solid state at a reaction temperature lower than the melting temperature of either of the transient plastic phase or the reactant phase.Type: GrantFiled: May 24, 1993Date of Patent: September 19, 1995Assignee: Drexel UniversityInventor: Michel Barsoum
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Patent number: 5447681Abstract: A method for manufacturing a metal graphite brush comprises steps of preparing natural graphite powders of 60-70 wt %, electrolytic copper powders of 30-40 wt %, molybdenum disulfide and lead of 2.5 wt % and the mixed resin of novolak phenol resin and furfural resin powders of 1-15 wt % which are adhesives, wet-mixing graphite powders with adhesives, pulverizing mixed powders to diameters of less than 200 .mu.m, press-molding all the powders under a pressure of 2-3 ton/cm.sup.2 and heating at a temperature 700.degree. C., and attaching a lead wire thereto, simultaneously, wherein the average particle distribution of the powders is 27 .mu.m. The compound ratio of graphite powders: copper powders: molybdenum disulfide: lead is 62.5 wt %: 35 wt %: 1.5 wt %: 1.0 wt %, the adhesives comprising the mixed resin of novolak phenol resin and furfural resin by 50:50 is added by a weight ratio of 7.5 wt % to the graphite powders.Type: GrantFiled: December 27, 1993Date of Patent: September 5, 1995Assignee: Mando CorporationInventors: Chung Tai Seung, Kim Seong Soo, Lee Jae Sung
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Patent number: 5445787Abstract: The process of forming an extruded product of tantalum or niobium requires a cold isostatic pressing of a charge of the powder to a density sufficient to form a green compact which is then placed in a capsule. The capsule is then sealed and heated to a temperature and for a time sufficient to anneal the green compact. Thereafter, the capsule and encapsulated compact are subjected to a cold isostatic pressing to achieve a density of from 70% to 85%. This is followed by subsequent heating and extrusion of the heated capsule and encapsulated compact to form the extruded product. The outer layer on the capsule which has been formed by the capsule material can be removed, as by pickling, in the case of the capsule being a carbon steel.Type: GrantFiled: November 2, 1993Date of Patent: August 29, 1995Inventors: Ira Friedman, Christer Aslund
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Patent number: 5445788Abstract: Complex-shaped parts can be produced from powders, for example metal-matrix composites, by injection molding using a mixture of the powders with a suitable binder. The binder must be removed from the powder mixture before the final thermal treatment of the so-called green part. The present invention proposes to remove the binder by surrounding a cast part with a layer of a particulate material and to subject the cast part to isostatic pressure through the surrounding layer which can thus act as an absorbent. The surrounding layer is removed after the isostatic pressing and the part can be subjected to sintering. The method is suitable for example for aluminum-ceramic powder mixtures.Type: GrantFiled: December 1, 1993Date of Patent: August 29, 1995Assignee: National Research Council of CanadaInventors: Sylvain Turenne, Paul-Emile Mongeon
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Patent number: 5439500Abstract: A magneto-optical sputter target having a composition comprising at least one rare earth element and at least one transition metal, with a structure which includes a transition metal constituent and a finely mixed alloy constituent of a rare earth phase and a rare earth/transition metal intermetallic compound. The structure of the present target contains a minimum of the intermetallic compound. A method of producing the present sputter target includes mixing particles of the transition metal constituent (preferably only alloyed transition metals) with particles of the finely mixed alloy to produce a powder blend and subjecting the powder blend to a pressing operation in an oxidizing inhibiting environment for a time and at a temperature and pressure which minimizes the rare earth/transition metal intermetallic compound content of the target.Type: GrantFiled: December 2, 1993Date of Patent: August 8, 1995Assignee: Materials Research CorporationInventor: Daniel R. Marx
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Patent number: 5439499Abstract: A cermet useful in the fabrication of metal cutting, rockdrilling and mineral tools, as well as wear parts. The cermet comprises (i) a hard phase of a simple boride of a transition metal, a mixture of simple borides of transition metals, or a mixed boride of transition metals; (ii) a binder phase of Fe, Ni, Co, Cr, or alloys thereof; (iii) a dispersion of particles of oxides of transition metals in which the oxygen can be replaced by nitrogen and/or carbon; and (iv) a dispersion of oxides of metals chosen from aluminum and Group IIA and IIIA metals.Type: GrantFiled: February 26, 1993Date of Patent: August 8, 1995Assignee: Sandvik ABInventors: Henri Pastor, Colette Allibert, Laurent Ottavi, Manuel Albajar, Francisco Castro-Fernandez
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Patent number: 5427734Abstract: The object of the invention is to provide a manufacturing method of a complex shaped R--Fe--B type sintered anisotropic magnet improved the moldability of injection molding and preventing the reaction between R ingredients and binder and controlled the degradation of magnetic characteristics due to residual carbon and oxygen. Utilizing the R--Fe--B type alloy powder or the resin coated said alloy powder, and methylcellulose and/or agar and water, instead of the usual thermoplastic binder, it is mixed and injection molded. The molded body is dehydrated by the freeze vacuum dry method to control the reaction between R ingredients and of the R--Fe--B alloy powder and water; furthermore, by administering the de-binder treatment in the hydrogen atmosphere, and sintering it after the dehydrogen treatment, residual oxygen and carbon in the R--Fe--B sintered body is drastically reduced, improving the moldability during the injection molding to obtain a three dimensionally complex shape sintered magnet.Type: GrantFiled: June 24, 1993Date of Patent: June 27, 1995Assignee: Sumitomo Special Metals Co., Ltd.Inventors: Osamu Yamashita, Masahiro Asano, Tsunekazu Saigo
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Patent number: 5413751Abstract: High density heatsinks for microcircuit packages are formed by first mold-pressing a composite powder of free-flowing spray-dried particles of copper and at least one other denser material such as tungsten and/or molybdenum, the proportions of which are adjusted to match the thermal expansion characteristics of the microcircuit material. The pressed compacts are then heated in a sintering furnace at 1,200.degree. C. to 1,350.degree. C. in order to effect an homogeneous distribution of the melting copper throughout the structure. The process results in a readily usable component having good thermal conductivity and matched thermal expansion that requires no further machining.Type: GrantFiled: May 20, 1993Date of Patent: May 9, 1995
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Patent number: 5403542Abstract: Method of manufacturing a sintered carbonitride alloy comprising wet milling powders of forming binder phase containing Co, Ni and mixture thereof and powder forming hard constituents of nitrides and carbonitrides with Ti as the main component to a mixture with desired composition; compacting said mixture to form compact; heating the compact at 100-300 C. in oxygen or air and subjecting said compact in multiple heating steps to effect sintering.Type: GrantFiled: February 10, 1994Date of Patent: April 4, 1995Assignee: Sandvik ABInventors: Gerold Weinl, Rolf G. Oskarsson, Per Gustafsson
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Patent number: 5395464Abstract: A method for obtaining a product from pre-alloyed powders in which the powders are subjected to compaction treatment. The powders are first subjected to pre-treatment under low pressure (or without pressure) at a temperature such that segregating materials precipitate out in stable phases.Type: GrantFiled: April 7, 1994Date of Patent: March 7, 1995Assignee: TECPHYInventor: James Davidson
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Patent number: 5376329Abstract: A method of making a composite orifice having a tungsten core which is diffusion bonded to a molybdenum shell. Tungsten and molybdenum powders in contact with each other in a mold are isostatically pressed to form a pressed bonded composite part. The pressed, unsintered tungsten core portion of the part is then machined to the desired dimensions. The pressed composite part is then sintered to form a diffusion bonded composite orifice. The pressed and sintered molybdenum shell portion of the orifice may then be machined to the desired dimensions.Type: GrantFiled: November 16, 1992Date of Patent: December 27, 1994Assignee: GTE Products CorporationInventors: Ricky D. Morgan, James A. Giffen, Jr.
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Patent number: 5372776Abstract: A density element (12) for use in ruminal delivery devices (10) which is manufactured by partial sintering in such a manner as to fragment upon contact with the many parts in rendering machinery without damage to the blades. The density element (12) has density of at least about 1.5 gm/cm.sup.3 and a transverse rupture strength greater than about 3000 psi no greater than about 30,000 psi. The part is sintered under conditions which do not permit full weld bond strength to be obtained and may thereafter be heat treated or impregnated with an inert hydrophobic material to increase corrosion resistance.Type: GrantFiled: March 2, 1994Date of Patent: December 13, 1994Assignee: Alza CorporationInventors: John R. Peery, James B. Eckenhoff
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Patent number: 5368629Abstract: The rapidly solidified aluminum alloy powder is preformed in a cold or warm environment to form a powder compact having a relative density of 75-93%. Then, the preformed compact is heated and degassed in the atmosphere of an inert gas at temperature of 300.degree. C. to 560.degree. C. for 0.25-3 hours. Immediately thereafter, the compact is subjected to hot coining at 300.degree.-560.degree. C. to obtain a solidified compact having pores at a rate of 2-5%. The solidified compact is then subjected to sizing. Since the inorganic gas prevents reaction between the evaporated water and aluminum while preheating the compact, the hot coining can be carried out in a state where solid state diffusion easily occurs. Thus, the powder particles can be bonded together strongly with a single forging. Also, at the end of hot coining, pores remain in the solidified compact at the rate of 2-5%. Utilizing these pores, the compact can be subjected to sizing to improve its dimensional accuracy.Type: GrantFiled: December 3, 1992Date of Patent: November 29, 1994Assignee: Sumitomo Electric Industries, Ltd.Inventors: Katsuyoshi Kondo, Yoshinobu Takeda
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Patent number: 5364586Abstract: A filter membrane and a process for making the filter membrane are provided. The filter membrane comprises a metal substrate having a filtering layer thereon comprising sintered ultra-fine particles of metal or ceramic compounds. The filtering layer preferably has an average pore size of from about 30 nanometers to about 200 nanometers. The filter membranes can withstand pressure drops of up to about 0.6 MPa and are useful for a variety of filtering applications.Type: GrantFiled: August 17, 1993Date of Patent: November 15, 1994Assignee: Ultram International L.L.C.Inventors: Lev I. Trusov, Vladimir N. Lapovok, Victor I. Novikov
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Patent number: 5342571Abstract: Dual phase sputter targets consisting essentially of TiN and Al, methods of manufacture thereof, and cathodic sputtering methods using such targets are disclosed. The targets are prepared by blending TiN and Al powders followed by compaction to full density. The thus compacted materials are optionally sintered and are then formed into the desired target shape. The targets are used in cathodic sputtering processes to form opaque, dark colored decorative and wear resistant coatings.Type: GrantFiled: February 19, 1992Date of Patent: August 30, 1994Assignee: Tosoh SMD, Inc.Inventors: Mark B. Dittmar, Paul E. Scheiderer
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Patent number: 5338332Abstract: The present invention is an isothermal current shunt device with excellent temperature coefficient of resistivity characteristics stability for use in a power measuring circuit having a wide temperature and dynamic range and particularly for customers of electric utility companies, and it includes a first arm having a first flange portion, a second arm having a second flange portion, and a bridge means coupling the first arm to the second arm wherein the bridge means is a monolithic sintered powdered-metal piece having a block portion and a loop portion. The block portion has a first face juxtaposed to and electrically coupled to the first flange portion of the first arm and a second opposing face juxtaposed to and electrically coupled to the second flange portion of the second arm. This configuration allows a majority of electrical current to conduct between the first arm and the second arm.Type: GrantFiled: June 15, 1992Date of Patent: August 16, 1994Assignee: Metricom, Inc.Inventors: Paul Baran, Ronald S. Palmer
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Patent number: 5330704Abstract: Powder composed of particles of a rapidly solidified dispersion strengthened aluminum base alloy is compacted into billet form. The billet is vacuum autoclaved at a temperature ranging from 350.degree. C. to the alloy's incipient melting temperature and formed into a substantially fully dense wrought product. Gas content of the alloy is decreased and powder degassing steps are eliminated. The dispersion strengthened aluminum wrought product is produced in an economical and efficient manner.Type: GrantFiled: February 4, 1991Date of Patent: July 19, 1994Assignee: AlliedSignal Inc.Inventor: Paul S. Gilman
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Patent number: 5316718Abstract: A composite electrode for electrochemical processing having improved high temperature properties, and a process for making the electrode by combustion synthesis. A composition from which the electrode is made by combustion synthesis comprises from about 40% to about 90% by weight of a particulate or fibrous combustible mixture which, when ignited, is capable of forming an interconnected network of a ceramic or metal-ceramic composite, and from about 10% to about 60% by weight of a particulate or fibrous filler material capable of providing the electrode with improved oxidation resistance and maintenance of adequate electrical conductivity at temperatures above 1000.degree. C. The filler material is molybdenum silicide, silicon carbide, titanium carbide, boron carbide, boron nitride, zirconium boride, cerium oxide, cerium oxyfluoride, or mixtures thereof.Type: GrantFiled: June 14, 1991Date of Patent: May 31, 1994Assignee: Moltech Invent S.A.Inventor: Jainagesh A. Sekhar
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Patent number: 5310520Abstract: Discrete powder particles of copper 14 and INVAR 12 are mixed together in a container 16 and packed into a powder metal article. This article is hot vacuum degassed and vacuum sealed and then heated to temperature well below the sintering temperature of copper or INVAR. Immediately after heating the article, it is subjected to a high pressure, high strain force such as extrusion through a die thereby yielding a fully dense, strong composite material 10 with excellent combined thermal expansion and conductivity properties.Type: GrantFiled: January 29, 1993Date of Patent: May 10, 1994Assignee: Texas Instruments IncorporatedInventors: Sunil C. Jha, James A. Forster, Henry F. Breit
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Aluminum-alloy powder, sintered aluminum-alloy, and method for producing the sintered aluminum-alloy
Patent number: 5304343Abstract: An aluminum-alloy main-starting powder for producing a sintered aluminum-alloy consists of from 0.1 to 3.0% of Cu, the balance being Al and unavoidable impurities. Mother alloy powder consists of from 4 to 20% of Mg, from 12 to 30% of Si, and Al and unavoidable impurities in balance.Type: GrantFiled: October 19, 1992Date of Patent: April 19, 1994Assignee: Showa Denko K.K.Inventors: Shin Miura, Youichi Hirose, Yoshio Machida, Mitsuaki Sato -
Patent number: 5288454Abstract: A method for controlling the remanance of a sintered magnet by varying the time when the orienting field is applied during cold compression. The method comprises obtaining powders of an appropriate particle size, compressing the powders in an oriented field, sintering, heat treating, machining and magnetizing to technical saturation. The cold compressing in an orienting field takes place at a precompression rate of more than 15% before the orienting field is applied. The method applies to magnets of all shapes which must have magnetic induction well defined in modulus and in direction, particularly annular magnets for traveling wave tubes.Type: GrantFiled: January 6, 1993Date of Patent: February 22, 1994Assignee: Aimants Ugimag S.A.Inventors: Jean-Marc Lang, Robert Tissot
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Patent number: 5284615Abstract: The present invention presents a method of processing ferrous powder materials to produce small component parts exhibiting excellent soft magnetic properties, in particular, residual magnetic flux density. The processing steps involve, in part, mixing with a binder, dewaxing or presintering at a temperature higher than in the conventional dewaxing process, followed by final sintering and a further conversion sintering, at a temperature lower than in the conventional sintering process, to produce parts having density values of over 96% theoretical density and excellent soft magnetic properties. The invented method is suitable for producing small component parts having sufficient strength and excellent soft magnetic properties to make them suitable for miniaturized electrical and electronic equipment.Type: GrantFiled: July 15, 1992Date of Patent: February 8, 1994Assignee: Mitsubishi Materials CorporationInventors: Koshiro Ueda, Mutsumi Moribayashi, Tohru Kohno
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Patent number: 5269830Abstract: A process for synthesizing intermetallic compounds from elemental powders. The elemental powders are initially combined in a ratio which approximates the stoichiometric composition of the intermetallic compound. The mixed powders are then formed into a compact which is heat treated at a controlled rate of heating such that an exothermic reaction between the elements is initiated. The heat treatment may be performed under controlled conditions ranging from a vacuum (pressureless sintering) to compression (hot pressing) to produce a desired densification of the intermetallic compound. In a preferred form of the invention, elemental powders of Fe and Al are combined to form aluminide compounds of Fe.sub.3 Al and FeAl.Type: GrantFiled: October 26, 1990Date of Patent: December 14, 1993Assignee: The United States of America as represented by the United States Department of EnergyInventors: Barry H. Rabin, Richard N. Wright
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Patent number: 5260018Abstract: The finished metallic material of this invention is constituted by an agglomerate of finely divided metallic powder, the grains of which are bonded together by means of an organic substance, the volume of such substance being comprised between 0.5 and 7% of the total volume of the material. In order to obtain said material, the metallic powder is mixed with the organic substance, the mixture is moulded under high pressure and after removal from the mould, the material is heated in order to harden the organic substance. The material is employed to advantage for elements constituting horological articles.Type: GrantFiled: October 3, 1991Date of Patent: November 9, 1993Assignee: Eta SA Fabriques d'EbauchesInventors: Rudolf Dinger, Robert Soder, Albert Willemin
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Patent number: 5256368Abstract: A pressure-reaction synthesis process for producing increased stiffness and improved strength-to-weight ratio titanium metal matrix composite materials comprising exothermically reacting a titanium powder or titanium powder alloys with non-metal powders or gas selected from the group consisting of C, B, N, BN, B.sub.4 C, SiC and Si.sub.3 N.sub.4 at temperatures from about 900.degree. to about 1300.degree. C., for about 5 to about 30 minutes in a forming die under pressures of from about 1000 to 5000 psi.Type: GrantFiled: July 31, 1992Date of Patent: October 26, 1993Assignee: The United States of America as represented by the Secretary of the InteriorInventors: Laurance L. Oden, Thomas L. Ochs, Paul C. Turner
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Patent number: 5250255Abstract: Green compacts for sintered ceramic bodies and for sintered permanent magnets are produced by first preparing outside a die press machine a mold which contains a rubber portion in at least a side portion. The mold cavity is then filled with the fine powder which is to form the compact to a density which is at least 1.2 times the natural filling density of the powder. The filled rubber mold is then placed in the die press machine and compacted in the die press machine to produce the green compact. The natural filling density is obtained by allowing the powder to fall from a powder pan into the rubber mold until the powder reaches the top of the rubber mold, where the distance from the powder pan to the bottom of the rubber mold is 3.7 times the depth of the cavity of the rubber mold.Type: GrantFiled: December 2, 1991Date of Patent: October 5, 1993Assignee: Intermetallics Co., Ltd.Inventors: Masato Sagawa, Hiroshi Nagata, Hiroo Shirai
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Patent number: 5234487Abstract: Tungsten-titanium sputter targets of at least 95% theoretical density are provided with little or no .beta.(Ti, W) phase constituent. Such targets will minimize troublesome particulate emissions during sputter coating conditions.Type: GrantFiled: April 15, 1991Date of Patent: August 10, 1993Assignee: Tosoh SMD, Inc.Inventors: Charles E. Wickersham, Jr., John J. Mueller
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Patent number: 5226947Abstract: Superconductors formed by powder metallurgy have a matrix of niobium-titanium alloy with discrete pinning centers distributed therein which are formed of a compatible metal. The artificial pinning centers in the Nb-Ti matrix are reduced in size by processing steps to sizes on the order of the coherence length, typically in the range of 1 to 10 nm. To produce the superconductor, powders of body centered cubic Nb-Ti alloy and the second phase flux pinning material, such as Nb, are mixed in the desired percentages. The mixture is then isostatically pressed, sintered at a selected temperature and selected time to produce a cohesive structure having desired characteristics without undue chemical reaction, the sintered billet is reduced in size by deformation, such as by swaging, the swaged sample receives heat treatment and recrystallization and additional swaging, if necessary, and is then sheathed in a normal conducting sheath, and the sheathed material is drawn into a wire.Type: GrantFiled: February 17, 1992Date of Patent: July 13, 1993Assignee: Wisconsin Alumni Research FoundationInventors: Paul D. Jablonski, David C. Larbalestier