Mechanical Type Stirring Means Patents (Class 422/225)
  • Publication number: 20110189059
    Abstract: A mixer for mixing a dental composition comprises a mixer housing with a wall of the mixer housing forming a light filter. The light filter provides for substantially blocking light of certain wavelengths, whereas it transmits light of at least some other wavelengths. The invention may help to prevent dental compositions from degrading.
    Type: Application
    Filed: May 14, 2009
    Publication date: August 4, 2011
    Inventors: Andreas Johannes Boehm, Marc Peuker, Alexander Walter, Bruce R. Broyles, Joel D. Oxman, John W. Dubbe, Martin G. Hartung, Sebastian Guggenmos
  • Patent number: 7985388
    Abstract: There is disclosed a process of making nano-sized or micro-sized precipitate particles. The process comprising the steps of mixing, in a reaction zone, a metal salt solution with a precipitant solution to form a precipitate, said precipitate being at least one of a metal chalcogenide, metal hydroxide and metal oxide; and applying a shear force to said mixing solutions in said reaction zone during said mixing step, wherein said shear force and the conditions within said reaction zone form said nano-sized or micro-sized precipitate particles.
    Type: Grant
    Filed: October 2, 2007
    Date of Patent: July 26, 2011
    Assignee: NanoMaterials Technology Pte Ltd
    Inventors: Zhigang Shen, Jiyao Zhang, Giawen Sim, Jimmy Sung Lai Yun, Jianfeng Chen
  • Publication number: 20110171101
    Abstract: The present invention relates to a reactor (1) for preparing hydrogen cyanide by the Andrussow process, comprising a reactor vessel (2), at least one gas inlet (3) which opens into a gas inlet region (4), an outlet for the reaction products (5) and a catalyst (6), wherein at least one mixing element (7) and at least one gas-permeable intermediate layer (8) are provided within the reactor vessel (2) between the gas inlet region (4) and the catalyst (6), the mixing element (7) being arranged between the gas inlet region (4) and the gas-permeable intermediate layer (8). The present invention further relates to a process for preparing HCN, in which an inventive reactor is used.
    Type: Application
    Filed: May 9, 2008
    Publication date: July 14, 2011
    Applicant: Evonik Roehm GmbH
    Inventors: Thomas Schaefer, Robert Weber, Udo Gropp, Thomas Mertz
  • Patent number: 7976788
    Abstract: A reductant decomposition reactor for use in exhaust systems is provided that includes a middle tube portion formed with a reductant injector mount, an inlet tube, an outlet tube and a mixer. The inlet tube is formed at a first end of the middle tube portion and the outlet tube is formed at a second end of the middle tube portion and both are configured to create a sealed connection to different portions of the exhaust system. The mixer fits between the middle tube portion and the outlet tube and is configured to decompose the reductant in an exhaust stream. The injector mount comprises a tube like section that connects at a first end to the middle tube portion and at a second end to an injector port of the injector mount, and is configured to reduce recirculation flow patterns in the reactor, create a high velocity flow at an inner surface of the injector mount and thereby reduce the formation of reductant deposits.
    Type: Grant
    Filed: October 16, 2008
    Date of Patent: July 12, 2011
    Assignee: Cummins Filtration IP, Inc.
    Inventors: Jason Drost, Diane Boose, Robert Schellin, Achuth Munnannur, Mihai Chiruta
  • Patent number: 7964059
    Abstract: The large volume reactor or a thin film evaporator including a housing enclosing a reactor chamber . A reactor rotor driven about an axis of rotation is located in the reactor chamber. The housing comprises a reactor chamber inlet opening and a product outlet. A premixing unit is located adjacent the reactor chamber inlet opening, which is configured to mix a starting material fed through one or more product inlet openings to form a prepared substance which is fed directly to the reactor chamber.
    Type: Grant
    Filed: October 5, 2006
    Date of Patent: June 21, 2011
    Assignee: Buss-SMS-Canzler GmbH
    Inventors: Hans Peters, Rainer Naef
  • Patent number: 7964026
    Abstract: A gasification system having a combustor vessel, an optional scrubber vessel, an optional fixer vessel, an optional cyclone vessel and an optional demister vessel. A wide variety of possibly moist solid or semi-solid carbonaceous fuels may be partially combusted in the combustor to generate a combustible gas and a mineral ash. An improved ash support and removal subsystem reduces clogging and other problems. The combustible gas is conveyed by optional heavy-duty blowers through the optional vessels to remove liquids and particulates and to undergo catalytic chemical reactions to provide a relatively clean, dry, highly-combustible hydrocarbon gas that captures a relatively high fraction of the potential heating value of the fuel. Internal gases, liquids and particulates from the vessels may be recycled inside the system to improve efficiency and prevent liquid waste. A portion of the internal liquids may also be extracted for other uses.
    Type: Grant
    Filed: July 17, 2006
    Date of Patent: June 21, 2011
    Assignee: Power Reclamation, Inc.
    Inventor: Michael W. Rogers
  • Patent number: 7947803
    Abstract: The present invention provides an apparatus for recovering a polymer from polymer solution, and a method of recovering a polymer using the apparatus. The apparatus includes a polymer solution-storage tank for storing a polymer solution; a polymer solution feeding pump for pumping the polymer solution from the polymer solution storage tank; an antisolvent storage tank for storing an antisolvent; an antisolvent feeding pump for pumping the antisolvent from the antisolvent storage tank; a reaction chamber to which the polymer solution pumped by the polymer solution feeding pump and the antisolvent pumped by the antisolvent feeding pump are supplied; a high-speed mixer that is rotated in the reaction chamber at a speed range of 1000 to 30000 rpm, mixes the polymer solution with the antisolvent under a shearing force corresponding to a tip speed of 5 to 30 m/sec, and precipitates a polymer; and a precipitate storage tank for storing the precipitation mixture of the polymer and the solvent/antisolvent.
    Type: Grant
    Filed: December 5, 2007
    Date of Patent: May 24, 2011
    Assignee: LG Chem, Ltd.
    Inventors: Sung-Don Hong, In-Su Lee, Jong-Ku Lee, Sung-Ho Chun, Seung-Young Park, Sung-Cheol Yoon
  • Publication number: 20110110831
    Abstract: A crystallizer system for forming solid crystals includes a vessel defining a cylindrical sidewall, a sparge device located at a bottom of the vessel, a plurality of impellers attached to a shaft, and a plurality of redistribution funnel assemblies vertically spaced apart. Each funnel assembly may be positioned underneath a respective impeller of the plurality of impellers. Each funnel assembly may include a funnel, a disc attached to the shaft such that the disc rotates with the impellers, and a channel extending radially inward from a location near the sidewall. The channel may be adapted to direct gas bubbles from the sidewall to a location near blade outer edges of the respective impeller A lower edge of the funnel and the disc may define a lower gap therebetween, such that solid particles falling from within the funnel are directed out of the lower gap when the disc is rotated.
    Type: Application
    Filed: November 6, 2009
    Publication date: May 12, 2011
    Inventors: Wojciech Wyczalkowski, Robert W. Higbee, Chris Hibshman, Kevin Smith, Robert Peter Dowd, Carl P. Laird
  • Publication number: 20110105719
    Abstract: Reactors, reactor systems and methods for producing particles in a precipitation process are provided. The reactor includes a housing defining a reaction chamber, a stator assembly including two or more stators, a rotor assembly including two or more rotors, the rotor assembly configured for rotation about an axis of rotation relative to the stator assembly, a first inlet to supply a first reactant material to the reaction chamber at a first radial location, a second inlet to supply a second reactant material to the reaction chamber at a second radial location different from the first radial location, wherein the first and second reactant materials react to produce precipitation of particles in the reaction chamber, and an outlet to supply the particles formed in the reaction chamber.
    Type: Application
    Filed: November 2, 2010
    Publication date: May 5, 2011
    Applicant: MannKind Corporation
    Inventors: Sanket Gandhi, Karen Moraleda, Jadwiga Jachowicz, Michael Zupon
  • Publication number: 20110105629
    Abstract: A method of producing an emulsion includes preparing a droplet solution comprising first and second molecular species, the droplet solution being in a fluid phase, wherein the first molecular species is soluble in the second molecular species; forming a plurality of droplets from the droplet solution in a bulk fluid to create a first emulsion, the plurality of droplets having a first ensemble average radius in the bulk fluid, wherein the first molecular species of the droplet solution is at least partially soluble in the bulk fluid and the droplet solution is at least partially immiscible in the bulk fluid; and allowing molecules of the first molecular species to migrate from the plurality of fluid droplets to the bulk fluid due to a higher concentration of the first molecular species in the droplet solution than the bulk fluid to result in the plurality of droplets having a second ensemble average radius that is smaller than the first ensemble average radius.
    Type: Application
    Filed: June 17, 2009
    Publication date: May 5, 2011
    Applicant: The Regents of the University of California
    Inventors: Thomas G. Mason, Michael M. Fryd
  • Patent number: 7931876
    Abstract: The invention provides a method and an apparatus for manufacturing a developer, which can manufacture a developer having a uniform and fine particle shape in a narrow particle size distribution and having a coloring agent highly dispersed therein at the primary particle level, the method and apparatus at the same time enabling continuous and efficient production without opening and closing a reactor. The method comprises the steps of: dissolving a binding resin component in a supercritical or subcritical fluid so that the binding resin component is blended with a coloring agent component; and reducing the solubility of the binding resin component in the supercritical or subcritical fluid so that the binding resin component is precipitated in the form of particles with the coloring agent component dispersed in the interior thereof.
    Type: Grant
    Filed: December 17, 2008
    Date of Patent: April 26, 2011
    Assignee: Sharp Kabushiki Kaisha
    Inventors: Shinichi Nakano, Yasuhiro Shibai, Keiichi Kikawa
  • Publication number: 20110085945
    Abstract: A mixing unit, a mixing device, an agitation impeller and a pump mixer can mix a large amount of fluid while having significant mixing effects in a small space. There are also provided a mixing system that uses the pump mixer and achieves a continuous operation and a reaction device that uses the mixing unit and achieves an efficient operation. The mixing unit (1) includes: a stacked member (2) in which a plurality of mixing elements (21) are stacked; and a first plate (3) and a second plate (4) between which the stacked member (2) is sandwiched and which are arranged opposite each other.
    Type: Application
    Filed: June 16, 2009
    Publication date: April 14, 2011
    Applicant: ISEL CO., LTD.
    Inventor: Noboru Mochizuki
  • Patent number: 7914750
    Abstract: A continuous process and related system for producing high purity silica are disclosed. The process and system utilize a unique high temperature rotary reactor which excludes oxygen. The use of one or more anoxic gases is described, that upon administration into the system promote the exclusion of oxygen.
    Type: Grant
    Filed: October 7, 2009
    Date of Patent: March 29, 2011
    Assignee: Unimin Corporation
    Inventors: Scott D. Goldblatt, Chris Capobianco, Thomas A. Gallo
  • Publication number: 20110067466
    Abstract: An apparatus for the treatment of faeces, includes a tank (200) for housing faeces that has been subjected to treatment. There is a process vessel (202) in which the faeces is treated and which is located inside the tank (200) having an inlet (204) for feeding faeces into the process vessel (202). A rotary device (300) is provided for stirring the faeces in the process vessel (202) and for introducing oxygen into the faeces, which is operable in two modes of operation at different speeds of rotation. A partitioning member (212) separates the interior of the process vessel in a lower (216) and an upper (218) portion, while at the same time allowing communication between the lower and upper portions. The rotary device (300) is arranged to at least cause a suction of material mainly from the lower compartment in a first mode of operation and into the rotary device.
    Type: Application
    Filed: April 29, 2009
    Publication date: March 24, 2011
    Inventor: Rolf Ahlstrom
  • Patent number: 7910758
    Abstract: Hydrogenated vegetable oil exhibiting superior thermal stability and containing reduced levels of saturates and trans fatty acids are produced using an activated hydrogenation catalyst and/or an improved hydrogenation process incorporating high shear. The use of a high shear mechanical device incorporated into the hydrogenation process as a reactor device is shown to be capable of enabling reactions that would normally not be feasible under a given set of reaction pressure and temperature conditions. For example, the hydrogenation process described herein enables a reduction of hydrogenation time, and operation at lower temperatures than current processes. The resulting hydrogenated vegetable oil is particularly useful in frying, confectionery baking, and other applications where a product with a low trans fat content or higher thermal stability is desirable. The hydrogenated oil produced may comprise less than 10 weight % of trans fatty acids with less than 5 weight % of linolenic acid (C18:3).
    Type: Grant
    Filed: December 20, 2007
    Date of Patent: March 22, 2011
    Inventors: Abbas Hassan, Ebrahim Bagherzadeh, Rayford G. Anthony, Gregory Borsinger, Aziz Hassan
  • Patent number: 7906581
    Abstract: Methods, apparatuses, and systems for manufacturing a hot melt adhesive containing an adhesion promoter in a continuous mode include supplying a melted, hot melt adhesive to a mixing device at a first predetermined rate while simultaneously supplying an adhesion promoter to the same mixing device at a second predetermined rate to form a homogeneous admixture containing the hot melt adhesive and adhesion promoter. The hot melt adhesive/adhesion promoter mixture is subsequently reacted in at least one tubular reactor at a predetermined temperature for a predetermined residence time to allow the adhesion promoter to chemically bond with the hot melt adhesive and form an adhesive-promoter-treated hot melt adhesive. The adhesion-promoter-treated hot melt adhesive is collected in a product receiver and may be further processed.
    Type: Grant
    Filed: September 5, 2007
    Date of Patent: March 15, 2011
    Assignee: Xerox Corporation
    Inventors: Frank Ping-Hay Lee, Tie Hwee Ng, Sheau Van Kao, Guiqin Song
  • Publication number: 20110040049
    Abstract: In the present invention, a tubular flow reactor can maintain a plug flow property even though the tubular flow reactor is downsized, and provided is the tubular flow reactor with which uniform resin fine particles exhibiting a narrow particle size distribution and a narrow molecular weight distribution can be prepared when the tubular flow reactor is used for preparation of the resin fine particle via emulsion polymerization or the like. Disclosed is a tubular flow reactor possessing a stirring blade and a cylindrical channel, wherein a ratio d/D is 0.3-0.9 when a diameter of the stirring blade is represented by d and an inner diameter of the cylindrical channel is represented by D, and a ratio Lb/La is 0.80-0.99 when a length of the stirring blade is represented by Lb and a length of the cylindrical channel is represented by La.
    Type: Application
    Filed: March 2, 2009
    Publication date: February 17, 2011
    Applicant: KONICA MINOLTA BUSINESS TECHNOLOGIES, INC.
    Inventors: Yasuharu Saita, Masashi Mamino
  • Patent number: 7887765
    Abstract: A method and apparatus for the conversion of aromatic alkyls to aromatic carboxylic acids in a reactor are provided, wherein the location of the feeding of the reaction mixture into the reactor significantly increases the conversion efficiency of the precursor materials.
    Type: Grant
    Filed: June 21, 2007
    Date of Patent: February 15, 2011
    Assignee: Tereftalatos Mexicanos, S.A. de C.V.
    Inventors: Fernando Varela-Fuentes, Arturo Bulbarela-Croda, Guillermo Ramirez-Aguilar, Bertha Moran-Delgado
  • Patent number: 7887763
    Abstract: The present invention relates to an apparatus for use in conducting chemical or biological reactions requiring the input of at least one fluid reagent and/or the output of at least one fluid product, the apparatus comprising a reaction chamber having an inlet for the supply of at least one reactant and an outlet for the recovery of at least one product, the reaction chamber being provided with a regulator comprising a propeller mounted in the reaction chamber in the region of the inlet for dispersing the at least one reactant in the reaction chamber.
    Type: Grant
    Filed: December 23, 2004
    Date of Patent: February 15, 2011
    Inventor: Roger Kennedy
  • Patent number: 7887764
    Abstract: A mixer and mixer assembly for turbulent mixing and enhancing a chemical reaction is provided. A method for using a mixer and mixer assembly for treatment of fluids is also provided. The mixer generally includes a first and second end, a surface configured for turbulent mixing, a catalyst supported thereon, and surface structure configured to increase interaction of catalyst and reactant. The mixer assembly generally includes a mixer inserted inside a fluid container or a tube and may also include a catalytic sleeve for enhancing interaction between catalyst and reactant.
    Type: Grant
    Filed: September 18, 2007
    Date of Patent: February 15, 2011
    Inventor: Gary R. Jernberg
  • Patent number: 7883671
    Abstract: Process and apparatus for the (co) polymerization of styrene. The process is carried out by employing a liquid polymerization reaction mixture that includes styrene, in a mechanically stirred reactor in the form of a vessel comprising a side wall having the shape of a cylinder of revolution with a vertical axis (A), a bottom head and a top head that are joined to the side wall. The vessel is provided with a mechanical stirring device comprising (i) a central shaft of vertical axis coincident with the axis (A), connected to a drive system comprising a motor for rotating the central shaft, (ii) at least one baffle attached to the vessel. The baffle is away from the side wall of the vessel and takes the form of a cylinder of vertical axis and of rhomboidal cross section.
    Type: Grant
    Filed: November 10, 2005
    Date of Patent: February 8, 2011
    Assignee: Ineos Europe Limited
    Inventor: Jean-Marc Galewski
  • Publication number: 20110028663
    Abstract: The invention relates to a stirred-tank reactor and to a method for carrying out a polymerisation reaction of unsaturated monomers using a stirred-tank reactor. According to the invention, said stirred-tank reactor is characterised in that the product discharge point is designed as the central base outlet that is at least partially traversed by the agitator shaft. Said polymerisation is performed continuously under positive pressure, so that the stirred-tank reactor is operated hydrodynamically.
    Type: Application
    Filed: November 28, 2008
    Publication date: February 3, 2011
    Applicant: Evonik Roehm GmbH
    Inventors: Ruediger Carloff, Joachim Heid, Olaf Pickenaecker
  • Publication number: 20110027147
    Abstract: A method for producing toluene diisocyanate is disclosed which comprises forming a dispersion comprising phosgene gas bubbles dispersed in toluene diamine liquid phase, wherein said gas bubbles have a mean diameter less than 1 micron; and subjecting the dispersion to phosgenation reaction conditions, whereby at least a portion of the toluene diamine is phosgenated to form toluene diisocyanate. A system for carrying out the phosgenation of toluene diamine is also disclosed.
    Type: Application
    Filed: October 11, 2010
    Publication date: February 3, 2011
    Applicant: H R D CORPORATION
    Inventors: Abbas HASSAN, Ebrahim BAGHERZADEH, Rayford G. ANTHONY, Gregory BORSINGER, Aziz HASSAN
  • Publication number: 20100329948
    Abstract: The present invention provides an apparatus comprising a vessel having a conduit extending therefrom, and a stirrer, a section of which is adapted to be located within the conduit and a section of which is adapted to be located within the vessel, said stirrer being adapted such that, in use, material within the conduit is conveyed in a direction towards the vessel and/or in a direction away from the vessel.
    Type: Application
    Filed: July 6, 2010
    Publication date: December 30, 2010
    Applicant: Ineos Europe Limited
    Inventor: Stephen Roy Partington
  • Publication number: 20100331488
    Abstract: Provided is a tubular flow reactor containing: a cylindrical channel; a mixing shaft which is concentric with the cylindrical channel; and a mixing blade attached to the mixing shaft, wherein the tubular flow reactor satisfy the following requirements: t<2C and t/2C<A/C?1, provided that C is a radius of the mixing shaft, t is a thickness of the mixing blade; A is a distance between a mixing blade plane B located at a forward position in a rotating direction of the mixing blade and a plane S passing through the center of the mixing shaft in a shaft direction, when plane B and plane S are parallel; and the mixing blade plane B is located at a more forward position in the rotating direction than the plane S.
    Type: Application
    Filed: June 16, 2010
    Publication date: December 30, 2010
    Applicant: KONICA MINOLTA BUSINESS TECHNOLOGIES, INC.
    Inventors: Yasuharu SAITA, Ryuji KITANI, Masashi MAMINO
  • Publication number: 20100324308
    Abstract: Herein disclosed is a method, comprising: forming a dispersion under high shear comprising gas bubbles of an oxidant dispersed in a liquid phase, wherein the bubbles have a mean diameter of less than 1.5 micron; and contacting the dispersion with an oxidation catalyst to produce a product stream, wherein the product stream comprises a substance selected from the group consisting of dicarboxylic acid, benzoic acid, 2-methylbenzoic acid, 3-methylbenzoic acid, 4-methylbenzoic acid, and phthalic anhydride. In some cases, forming the dispersion under high shear comprises introducing the oxidant and the liquid phase into a high shear device comprising at least one rotor and at least one complementarily-shaped stator. Herein also disclosed is a system for producing a substance selected from the group consisting of dicarboxylic acid, benzoic acid, 2-methylbenzoic acid, 3-methylbenzoic acid, 4-methylbenzoic acid, and phthalic anhydride.
    Type: Application
    Filed: August 12, 2010
    Publication date: December 23, 2010
    Applicant: H R D CORPORATION
    Inventors: Abbas HASSAN, Aziz HASSAN, Rayford G. Anthony, Gregory G. BORSINGER
  • Patent number: 7850926
    Abstract: A process for the discontinuous production of granules from polycondensation polymers by precondensation of an oligomer at 5 to 400 mbar and subsequent polycondensation in a stirring reactor and subsequent granulation. In the vicinity of the outlet port, the density of the entraining surfaces lies between 1 and 8 m2 per m3 reactor space and constantly increases with increasing distance from the discharge region. Inside the reactor, there is a viscosity gradient between the region most remote from the discharge port and the zone of the discharge port. The thermal decomposition of the polymer melt flowing out of the reactor is compensated during granulation. The stirring reactor with horizontal longitudinal axis approximately has the shape of a single or double truncated cone. The reactor has rotatable, vertical product entraining surfaces and stationary scrapers between the same.
    Type: Grant
    Filed: January 8, 2001
    Date of Patent: December 14, 2010
    Assignee: Lurgi Zimmer GmbH
    Inventors: Fritz Wilhelm, Ferdinand Finkeldei
  • Publication number: 20100296982
    Abstract: Disclosed is a crystallizer comprising: a reaction bath having an inlet for feeding a reactant, an outlet for discharging a reaction product, and an inner reaction space in which a crystallization reaction is proceeded; and an agitation bar placed in the inner reaction space of the reaction bath, one cross-section of which is smaller than the other cross-section of the bar in a direction of flowing the reactant.
    Type: Application
    Filed: June 10, 2008
    Publication date: November 25, 2010
    Applicant: KNDT&I CO., LTD
    Inventors: Jongpal Hong, Hyeryeon Kang, Dayoung Kim, Changhoon Lee, Woosik Kim
  • Patent number: 7837955
    Abstract: A continuous process and related system for producing high purity silica are disclosed. The process and system utilize a unique high temperature rotary reactor which excludes oxygen. The use of one or more anoxic gases is described, that upon administration into the system promote the exclusion of oxygen.
    Type: Grant
    Filed: October 1, 2009
    Date of Patent: November 23, 2010
    Assignee: Unimin Corporation
    Inventors: Scott D. Goldblatt, Chris Capobianco, Thomas A. Gallo
  • Patent number: 7820119
    Abstract: The present invention involves a system and method of making ferric chloride with reduced amounts of hydrochloric acid for water treatment. The method comprises preparing a reactant batch comprising ferric oxide and hydrochloric acid at a predetermined molar ratio. The method further includes mixing the reactant batch with an impeller rotating between about 60 and 150 revolutions per minute. The method further includes maintaining the reactant batch at a temperature between about 70° Fahrenheit and 180° Fahrenheit. The method forms a reaction product including ferric chloride and a reduced amount of hydrochloric acid.
    Type: Grant
    Filed: March 7, 2005
    Date of Patent: October 26, 2010
    Assignee: PVS Technologies, Inc.
    Inventors: Dennis E. Rutkowski, Andy M. Yaksic
  • Patent number: 7803324
    Abstract: A catalyst slurry for a polymerization reactor can be prepared in a mixing tank and the catalyst slurry fed to one or more storage tanks. The storage tanks can include agitators so that the catalyst slurry is maintained at an essentially homogeneous solids-to-liquid ratio. From the storage tank(s), the catalyst slurry can be pumped to the polymerization reactor along a fluid passage having a flow meter. The flow of the catalyst slurry can be continuous and/or adjusted based on a measured parameter. The catalyst slurry may be continuously and reliability fed to the polymerization reactor.
    Type: Grant
    Filed: April 18, 2005
    Date of Patent: September 28, 2010
    Assignee: Chevron Phillips Chemical Company LP
    Inventors: David H. Burns, Donald W. Verser
  • Patent number: 7794837
    Abstract: A stationary phase for a liquid chromatograph and process for making is provided. The stationary phase material may have a modified base substrate and a fluorinated carboxylic acid covalently bonded thereto through an amide or ester bond. The stationary phase may have a substantially consistent shape selectivity characteristic with an ?TBN/BaP of less than 1 within a temperature range of at least 10-70° C. Advantageously, a fluorinated stationary phase has a shape selectivity characteristic exhibited with an ?TBN/BaP of less than 1 with a mobile phase having up to at least 30% water. A process for making the stationary involves mixing a substrate material or fluorinated carboxylic acid with a reactive alkylsilane linker and at least one organic solvent to form a first solution. The other of the substrate material or fluorinated carboxylic acid is then added to the first solution, or to a product separated from the first solution, to form a second solution.
    Type: Grant
    Filed: August 6, 2008
    Date of Patent: September 14, 2010
    Assignee: The United States of America as represented by the Secretary of Commerce, The National Institute of Standards and Technology
    Inventors: Katrice A. Lippa, Catherine A. Rimmer, Lane C. Sander
  • Publication number: 20100218574
    Abstract: An improved process of treating sludge to provide a stable product for use as a beneficial soil or fertilizer for agricultural lands which includes the steps (a) mixing the sludge with at least a first alkaline material and a second alkaline material in an amount sufficient to (i) raise the solids content of the mixed material to at least 50% W/W; (ii) raise the pH to at least 12; and (iii) raise the temperature to at least 70° C. by exothermic reaction of the alkaline materials with the water in the sludge; and (b) pasteurizing the mixed material at (i) at least 70° C. for at least 30 mins. and at least pH12 for at least 2 hrs.; and (ii) at least pH 11.5 for an additional 22 hrs., to provide the stable pasteurized product. The process and apparatus is readily adapted for mobility on suitable transportation.
    Type: Application
    Filed: February 16, 2010
    Publication date: September 2, 2010
    Applicant: N-VIRO SYSTEMS CANADA LP
    Inventors: Grant H. Mills, Robert Sampson, Rae E. Wallin
  • Patent number: 7780750
    Abstract: An integrated biomass converter system capable of converting gasifiable material into a combustible fuel (fuel gas). The system includes elements to convert raw gasifiable material into unprocessed fuel and by a single chamber, down-draft gasifier furnace convert) process) the unprocessed fuel to yield fuel gas. The system includes means to incorporate additional gasifiable materials into the gasifier furnace, or optionally to incorporate material into the unprocessed fuel. The gasifier furnace includes a top closure unit with means to uniformly distribute unprocessed fuel in the furnace and surface treatment means to ensure uniformity of air distribution in the gasification layer and provide means to introduce supplemental gasifiable materials directly into the gasification zone.
    Type: Grant
    Filed: February 28, 2007
    Date of Patent: August 24, 2010
    Inventor: Brent Carman
  • Patent number: 7780927
    Abstract: A spinning tube in tube reactor has the usual elongated transverse annular cross section reaction passage through which reactants pass to force reaction between them; the passage being between the rotor tube exterior surface and the stator tube interior surface. The radial dimension of the annual passage should be keep as uniform as possible so as not to cause unwanted variations in the reaction. This has proven difficult in prior constructions owing to the small radial dimension (e.g. 50-300 micrometers) and inevitable manufacturing tolerances in the bearings supporting the rotor. In apparatus of the invention the rotor is suspended within the stator passage by a flexible connection between the drive motor shaft and the rotor and uniformity is maintained by the so-called hydrodynamic effect which will become operative in such a narrow passage.
    Type: Grant
    Filed: February 20, 2008
    Date of Patent: August 24, 2010
    Inventor: Richard A Holl
  • Publication number: 20100196227
    Abstract: A device for pyrolysing biomass comprises: a reactor space; a first feed for biomass material connecting to the upper zone thereof; a second feed for heated heat carrier material connecting to the upper side of the reactor space; a first discharge for pyrolysis gas connecting to the upper zone of the reactor space at a distance from the first feed; and a second discharge for solid material, for instance carbon and heat carrier material, connecting to the underside of the reactor space. A substantial separation between the discharge flows of pyrolysis gas and solid material takes place predominantly under the influence of gravitational force, without interposing of a cyclone. The reactor space is modeled such that the direct flow from the first feed and the second feed to the first discharge is blocked. A mechanical mixer is present in the reactor space for the purpose of mixing the flow of biomass material with the flow of preheated heat carrier material.
    Type: Application
    Filed: July 19, 2008
    Publication date: August 5, 2010
    Applicant: BTG BIOLIQUIDS B.V.
    Inventors: Robertus Hendrikus Venderbosch, Lambertus Van De Beld, Daan Assink, Elwin Gansekoele
  • Publication number: 20100183486
    Abstract: Use of a high shear mechanical device incorporated into a process for the production of chlorobenzene is capable of decreasing mass transfer limitations, thereby enhancing the chlorobenzene production process.
    Type: Application
    Filed: March 31, 2010
    Publication date: July 22, 2010
    Applicant: H R D CORPORATION
    Inventors: Abbas Hassan, Ebrahim Bagherzadeh, Rayford G. Anthony, Gregory Borsinger, Aziz Hassan
  • Publication number: 20100178220
    Abstract: Compounds, synthesis of, and methods for synthesizing metal alkoxide derivatives; and metal alkoxide derivatives for use as flame retardants are described. Group 13 metal alkoxides having flame retardant properties may be prepared by reacting the group 13 metal trihydroxide with an alcohol.
    Type: Application
    Filed: March 25, 2010
    Publication date: July 15, 2010
    Applicant: AUTERRA, INC.
    Inventors: Partha S. Dutta, Sarah L. Lewis, Kyle E. Litz, Mark N. Rossetti, Tracey M. Jordan, Jennifer L. Vreeland
  • Publication number: 20100125157
    Abstract: A method and system for producing dispersed waxes, including a high shear mechanical device. In one embodiment, the method comprises forming a dispersion of wax globules in a carrier liquid in a high shear device prior to implementation in a waxy product. In another instance the system for producing waxy products comprises a high shear device for dispersing wax in a carrier liquid.
    Type: Application
    Filed: November 6, 2009
    Publication date: May 20, 2010
    Applicant: H R D CORPORATION
    Inventors: Abbas Hassan, Aziz Hassan
  • Publication number: 20100111786
    Abstract: Use of a high shear mechanical device in a process for production of starch by hydration and disruption of corn kernel particles in the presence of sulfur dioxide or bisulfite ions makes possible a decrease in mass transfer limitations, thereby enhancing starch production. A system for production of starch is also provided in which a high shear mixing device is configured to receive an aqueous corn slurry from a pump that is disposed between the reactor and a gaseous sulfur dioxide inlet of the high shear mixing device. The high shear mixing device is also configured to generate a fine dispersion of sulfur dioxide bubbles and small corn particles in the slurry. A reactor is configured to receive the output from the high shear mixing device and to provide for starch production.
    Type: Application
    Filed: July 31, 2009
    Publication date: May 6, 2010
    Applicant: H R D CORPORATION
    Inventors: Abbas Hassan, Ebrahim Bagherzadeh, Rayford G. Anthony, Gregory Borsinger, Aziz Hassan
  • Publication number: 20100112094
    Abstract: The invention provides a method for producing a peroxymonosulfuric acid solution with high stability, including the steps of mixing 35 mass % or more of hydrogen peroxide and 70 mass % or more of sulfuric acid to react them, cooling the reaction solution to 80° C. or lower within five minutes after initiation of the mixing step, and diluting the reaction solution with water four times or more as much as the reaction solution by mass.
    Type: Application
    Filed: October 18, 2007
    Publication date: May 6, 2010
    Inventors: Kiyoshi Yoshida, Tetsuo Koshitsuka, Kaoru Tsuyuki, Wakana Uesugi
  • Publication number: 20100102282
    Abstract: The present invention relates to pulverulent compounds of the formula NibM1cM2d(O)x(OH)y(SO4)z, a process for the preparation thereof and the use thereof as precursors for the preparation of active materials for lithium secondary batteries.
    Type: Application
    Filed: October 11, 2007
    Publication date: April 29, 2010
    Inventors: Stefan Malcus, Armin Olbrich, Juliane Messe-Marktscheffel, Matthias Jahn
  • Patent number: 7704465
    Abstract: Aluminum hydroxide aggregated particles which have an average particle diameter of not less than 40 ?m, an average particle diameter as determined after pressing at 1,000 kg/cm2 of not more than 35 ?m, and an L value of slurry obtained by mixing 20 ml of glycerol and 10 g of the aluminum hydroxide aggregated particles of not more than 69, are obtained by a process comprising the steps of: (a) feeding a supersaturated aqueous sodium aluminate solution to a vessel, (b) adding aluminum hydroxide seeds to the supersaturated aqueous sodium aluminate solution, (c) stirring the seed-added solution in the vessel while continuously feeding an additional supersaturated aqueous sodium aluminate solution into the vessel to hydrolyze the supersaturated aqueous sodium aluminate solution, (d) separating the aluminum hydroxide aggregated particles from the aqueous sodium aluminate solution, and (e) continuously discharging the aqueous sodium aluminate solution out of the vessel.
    Type: Grant
    Filed: November 7, 2002
    Date of Patent: April 27, 2010
    Assignee: Sumitomo Chemical Company, Limited
    Inventors: Hisakatsu Kato, Masashi Wada, Naoyuki Eguchi, Hirofumi Sasaki
  • Publication number: 20100098604
    Abstract: A reductant decomposition reactor for use in exhaust systems is provided that includes a middle tube portion formed with a reductant injector mount, an inlet tube, an outlet tube and a mixer. The inlet tube is formed at a first end of the middle tube portion and the outlet tube is formed at a second end of the middle tube portion and both are configured to create a sealed connection to different portions of the exhaust system. The mixer fits between the middle tube portion and the outlet tube and is configured to decompose the reductant in an exhaust stream. The injector mount comprises a tube like section that connects at a first end to the middle tube portion and at a second end to an injector port of the injector mount, and is configured to reduce recirculation flow patterns in the reactor, create a high velocity flow at an inner surface of the injector mount and thereby reduce the formation of reductant deposits.
    Type: Application
    Filed: October 16, 2008
    Publication date: April 22, 2010
    Applicant: CUMMINS FILTRATION IP INC.
    Inventors: Jason Drost, Diane Boose, Robert Schellin, Achuth Munnannur, Mihai Chiruta
  • Publication number: 20100074814
    Abstract: A reductant decomposition mixer for use in exhaust systems is provided The mixer includes a plurality of mixer bars, a plurality of cross bars and an outer ring. The mixer bars have a plurality of blades and are arranged in parallel to extend in a single direction. The cross bars interlock with the mixer bars from opposing directions and are arranged in parallel to extend in a single direction that is perpendicular to the direction of the mixer bars. The outer ring is connected to the ends of each of the mixer bars and the ends of each of the cross bars.
    Type: Application
    Filed: September 25, 2008
    Publication date: March 25, 2010
    Applicant: CUMMINS FILTRATION IP INC.
    Inventor: Jason Drost
  • Publication number: 20100065512
    Abstract: A reactor is described for conversion of chemical reactants comprising an oscillator with a number of perforated discs. The reactor is also suited to continuous conversion of reactants, and a method for such conversion is also described.
    Type: Application
    Filed: November 17, 2006
    Publication date: March 18, 2010
    Applicant: FLUENS SYNTHESIS AS
    Inventor: Hans Rene Bjorsvik
  • Publication number: 20100063323
    Abstract: The invention relates to a plant for carrying out chemical reactions, having a reactor (1), the reaction space of which contains hydrogen peroxide (H2O2) and titanium silicalite (TS-1). The object of the invention is to improve such a plant such that continuous separation and recycling of the active catalyst to the reaction space is possible with a long filter service life. This is achieved in that the reaction space contains a solid silicon source, in that the plant comprises a water takeoff line (3) which is set up for drawing off water in addition to components which are dissolved and/or dispersed therein from the reaction space, in that the water takeoff line (3) leads to a filter (4) which separates off the components which are dissolved and/or dispersed in the water, and in that the plant has a return line (5) which is set up for recirculating to the reaction space components which are separated off by means of the filter (4).
    Type: Application
    Filed: September 9, 2008
    Publication date: March 11, 2010
    Applicant: EVONIK DEGUSSA GmbH
    Inventors: Goetz BAUMGARTEN, Martin ROOS, Stephan SCHAEFLEIN, Rolf AUGENSTEIN
  • Patent number: 7651670
    Abstract: A Taylor reactor (1) according to FIG. 1, comprising 1. an annular reaction volume (2) which widens in the flow direction and is defined by an outer reactor wall (3), a rotor (4) which is mounted rotatably at the end (4.1) in the reactor floor (5) and at its other end (4.2) is unmounted, and a reactor floor (5) having a seal (6) for the drive shaft (7), 2. an inlet region (8) above the reactor floor (5), having at least one side feed (8.1) and/or at least one feed (8.1) through the reactor floor (5) for the reactants and/or the process media, 3. an outlet region (9) which is disposed above the annular reaction volume (2), widens further beyond the annular reaction volume (2) in the flow direction, and subsequently tapers toward a product offtake (10), 4. a product offtake (10) which at its greatest diameter opens toward the outlet region (9) and tapers in the other direction, and 5. a pressure maintenance valve (11); and its use for continuous bulk polymerization.
    Type: Grant
    Filed: October 2, 2002
    Date of Patent: January 26, 2010
    Assignee: BASF Coatings AG
    Inventors: Werner-Alfons Jung, Heinz-Peter Rink, Heinrich Meinecke, Josef Krull
  • Publication number: 20100015019
    Abstract: A method for producing aniline or toluenediamine is disclosed which comprises forming a dispersion comprising hydrogen gas bubbles dispersed in a liquid medium comprising either nitrobenzene or dinitrotoluene, wherein the hydrogen gas bubbles have a mean diameter less than 1 micron; and subjecting the dispersion to hydrogenation reaction promoting conditions comprising pressure less than about 600 kPa and temperature less than about 200° C., whereby at least a portion of the nitrobenzene or dinitrotoluene is hydrogenated to form aniline or toluenediamine, respectively. A system for carrying out the method is also disclosed.
    Type: Application
    Filed: September 28, 2009
    Publication date: January 21, 2010
    Applicant: H R D CORPORATION
    Inventors: Abbas Hassan, Ebrahim Bagherzadeh, Rayford G. Anthony, Gregory Borsinger, Aziz Hassan
  • Patent number: RE42099
    Abstract: Elastomer masterbatch is processed in a continuous compounder having multiple parallel elongate rotors axially oriented in an elongate processing chamber. Optionally, additional materials are compounded into the masterbatch, e.g., additives, other elastomeric compositions, etc. Preferably, the masterbatch then is further processed in an open mill. Excellent control of Mooney Viscosity is achieved. In certain preferred embodiments, elastomer composites are produced by novel continuous flow methods and apparatus in which fluid streams of particulate filler and elastomer latex are fed to the mixing zone of a coagulum reactor to form a coagulated mixture in semi-confined flow continuously from the mixing zone through a coagulum zone to a discharge end of the reactor.
    Type: Grant
    Filed: November 24, 2009
    Date of Patent: February 1, 2011
    Assignee: Cabot Corporation
    Inventors: Bin Chung, Susan W. Green, Ivan Z. Podobnik, Joseph Cianciolo