Including Means Separating Reaction Chamber Into Plural Reactant-containing Compartments And Means Moving Reactant Therebetween Patents (Class 422/236)
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Patent number: 8235361Abstract: A structured packing for a reactor is formed from a metal sheet to promote heat and mass transfer near the wall of the reactor. The structured packing causes lateral flow of fluids flowing through the packing such that jet impingement of at least one reactor wall is promoted. The packing may be used in a cylindrical, annular or plate-type reactor, e.g., a catalytic reactor, or a heat exchanger.Type: GrantFiled: January 18, 2010Date of Patent: August 7, 2012Assignee: Tribute Creations, LLCInventor: Jonathan Jay Feinstein
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Publication number: 20120141335Abstract: A hydrogen generating device is adapted for a fuel cell. The hydrogen generating device includes a casing, a button, a solid reactant, a bag-shaped body, and at least one flexible element. The casing has a containing space and an opening. The button is integrally formed and connected to the casing to seal the opening. The solid reactant is disposed in the casing. The bag-shaped body is disposed in the casing and contains a liquid reactant. The flexible element is connected to the casing and is located in the containing space. The flexible element includes a bending end, wherein the flexible element is aligned to the button and is located between the button and the bag-shaped body. When the button is pressed, the button pushes the flexible element so the bending end pierces the bag-shaped body, and the liquid reactant flows out and reacts with the solid reactant to generate hydrogen.Type: ApplicationFiled: July 21, 2011Publication date: June 7, 2012Applicant: YOUNG GREEN ENERGY CO.Inventors: Yu-Hsiang Lin, Hsuan-Yi Lu
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Patent number: 8152873Abstract: A system is disclosed to generate hydrogen. The system includes a fuel cartridge, a cartridge interface, and a fuel cartridge receiver. The fuel cartridge includes a liquid permeable material with one or more cavities that encloses a solid anhydrous chemical hydride. The fuel cartridge also includes a housing that is heat and pressure resistant that houses the liquid permeable material, and a liquid. The fuel cartridge also includes one or more liquid sources that introduce the liquid into the housing such that the liquid contacts at least a portion of the liquid permeable material.Type: GrantFiled: December 22, 2009Date of Patent: April 10, 2012Assignee: Trulite, IncInventors: Kevin Shurtleff, Eric Ladd, John Patton, Chris Brydon, Ken Pearson
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Patent number: 8118893Abstract: A gas-generating apparatus includes a reaction chamber having a first reactant, a reservoir having an optional second reactant, and a self-regulated flow control device. The self-regulated flow control device stops the flow of reactant from the reservoir to the reaction chamber when the pressure of the reaction chamber reaches a predetermined level. Methods of operating the gas-generated apparatus and the self-regulated flow control device, including the cycling of a shut-off valve of the gas-generated apparatus and the cycling of the self-regulated flow control device are also described.Type: GrantFiled: January 26, 2009Date of Patent: February 21, 2012Assignee: Societe BicInventors: Alain Rosenzweig, Paul Adams, Andrew J. Curello, Floyd Fairbanks, Anthony Sgroi, Jr., Constance R. Stepan
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Patent number: 8071820Abstract: A method and apparatus for converting glycerol into propylene glycol by directing a basic glycerol containing feed and a hydrogen containing gas into a reaction zone including a fixed bed of catalyst that is operating at glycerol conversion conditions where the reactor includes and at least one quench zone and directing a quench material into the quench zone.Type: GrantFiled: December 23, 2008Date of Patent: December 6, 2011Assignee: UOP LLCInventors: Maureen L. Bricker, Laura E. Leonard
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Publication number: 20110262342Abstract: An on-demand portable chlorine dioxide generator has a reagent bound medium in a first enclosed volume; a complementary reagent solution in a second enclosed volume, and a structure for selecting between a first position where the complementary reagent solution is forced through the reagent bound medium and a second position where said complementary reagent solution remains isolated from the reagent bound ion exchange medium, where a ClO2 solution is generated only during periods when the structure for forcing is actuated. The ClO2 solution can be discharged for use as a portable sprayer that can be used to treat surfaces infected by anthrax or other biological contaminants. When the bound reagent is chlorite, the complementary reagent is an acid or an oxidant. When the bound reagent is an acid or an oxidant, the complementary reagent solution is a chlorite solution.Type: ApplicationFiled: May 11, 2011Publication date: October 27, 2011Applicant: UNIVERSITY OF FLORIDA RESEARCH FOUNDATION INC.Inventors: DAVID E. RICHARDSON, Daniel Denevan, Dwight C. Ramdon
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Patent number: 8043579Abstract: A gas hydrate production apparatus capable of reacting a raw gas with a raw water to thereby form a slurry gas hydrate and capable of removing water from the slurry gas hydrate by means of a gravitational dewatering unit. This gravitational dewatering unit is one including a cylindrical first tower body; a cylindrical dewatering part disposed on top of the first tower body; a water receiving part disposed outside the dewatering part; and a cylindrical second tower body disposed on top of the dewatering part, wherein the cross-sectional area of the second tower body is continuously or intermittently increased upward from the bottom.Type: GrantFiled: April 5, 2006Date of Patent: October 25, 2011Assignee: Mitsui Engineering & Shipbuilding Co., Ltd.Inventors: Yuichi Katoh, Shigeru Nagamori, Toru Iwasaki, Takashi Arai, Kiyoshi Horiguchi, Tetsuro Murayama, Akira Tokinosu, Masahiro Takahashi, Toshio Yamaki
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Patent number: 8017099Abstract: A method for producing polycrystalline silicon, including: reacting trichlorosilane and hydrogen to produce silicon and a remainder including monosilanes (formula: SiHnCl4-n, wherein n is 0 to 4) containing silicon tetrachloride, and a polymer including at least trisilanes or tetrasilanes; and supplying the remainder and hydrogen to a conversion reactor and heating at a temperature within the range of 600 to 1,400° C. to convert silicon tetrachloride into trichlorosilane and the polymer into monosilanes.Type: GrantFiled: October 26, 2007Date of Patent: September 13, 2011Assignee: Mitsubishi Materials CorporationInventor: Masayuki Tebakari
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Publication number: 20110214982Abstract: Technologies are generally described for a levitation microreactor adapted to facilitate a chemical reaction. The levitation microreactor may comprise one or more levitation zones arranged in spatial communication with one another, each levitation zone including a levitator that is effective to levitate a reactant droplet. In some examples, a first levitation zone may include a first levitator effective to levitate a first reactant droplet, while a second levitation zone may include a second levitator effective to levitate a second reactant droplet. The second reactant droplet may be distinct from the first reactant droplet. Some example microreactors may further include a third levitation zone that is arranged in spatial communication with the first and second levitation zones. The third levitation zone may be effective to facilitate a chemical reaction on the first and second reactant droplets while the first and second reactant droplets are levitated to produce a product.Type: ApplicationFiled: March 8, 2010Publication date: September 8, 2011Inventor: Jeffrey John Hagen
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Publication number: 20110203995Abstract: A device is provided for performing chemical transformation in a fluid, with a flow distributor having at least one fluid medium inlet, at least one fluid medium outlet, and at least one confinement wherein the chemical transformation is performed; and a means for rotating, rocking, wagging, or oscillating the device. At least one confinement may be equipped with a provision for providing heat, cooling, sound, light or other types of radiation, such provision being contacted to an external source through an actuator shaft. The flow distributor may be provided with sectors connected with the centrally located fluid medium inlet and a designated peripheral fluid medium outlet. The means for rotating, rocking, wagging, or oscillating the device may be an element producing magnetic fields or a shaft mechanically connected to an external actuating device.Type: ApplicationFiled: February 11, 2011Publication date: August 25, 2011Inventors: Jonas Persson, Kjell Öberg, Fredrik Almqvist, Knut Irgum
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Patent number: 7967879Abstract: The present invention provides a cartridge for the generation of hydrogen. The cartridge includes a case, an igniter, and a structural component. The case defines an interior cavity and the igniter is positioned within the cavity. The structural component is also positioned within the cavity and is formed of a particulate embedded in a matrix and the particulate includes a metallic material. An oxidizing agent is positioned within the cavity. The structural component is configured such that the metallic material and the oxidizing agent react together to generate hydrogen after the igniter generates sufficient heat to remove the matrix from the structural component and to initiate the reaction between the metallic material and the oxidizing agent.Type: GrantFiled: March 11, 2009Date of Patent: June 28, 2011Assignee: Advanced Hydrogen Technologies CorporationInventor: Peter James Lohr, Sr.
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Patent number: 7964059Abstract: The large volume reactor or a thin film evaporator including a housing enclosing a reactor chamber . A reactor rotor driven about an axis of rotation is located in the reactor chamber. The housing comprises a reactor chamber inlet opening and a product outlet. A premixing unit is located adjacent the reactor chamber inlet opening, which is configured to mix a starting material fed through one or more product inlet openings to form a prepared substance which is fed directly to the reactor chamber.Type: GrantFiled: October 5, 2006Date of Patent: June 21, 2011Assignee: Buss-SMS-Canzler GmbHInventors: Hans Peters, Rainer Naef
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Patent number: 7964138Abstract: An on-demand portable chlorine dioxide generator has a reagent bound medium in a first enclosed volume; a complementary reagent solution in a second enclosed volume, and a structure for selecting between a first position where the complementary reagent solution is forced through the reagent bound medium and a second position where said complementary reagent solution remains isolated from the reagent bound ion exchange medium, where a ClO2 solution is generated only during periods when the structure for forcing is actuated. The ClO2 solution can be discharged for use as a portable sprayer that can be used to treat surfaces infected by anthrax or other biological contaminants. When the bound reagent is chlorite, the complementary reagent is an acid or an oxidant. When the bound reagent is an acid or an oxidant, the complementary reagent solution is a chlorite solution.Type: GrantFiled: November 29, 2006Date of Patent: June 21, 2011Assignee: University of Florida Research Foundation, Inc.Inventors: David E. Richardson, Daniel Denevan, Dwight C. Ramdon
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Publication number: 20110144384Abstract: A liquid-gas phase reactor system including a slinger located in an upper section (headspace region) of a reaction vessel. The slinger comprises an upper horizontal surface including a plurality of vertically raised vanes extending radially outward along a curved path which effectively distribute liquid about the reactor vessel. A method for conducting an oxidation reaction using a liquid-gas phase reactor system is also disclosed. The disclosed reactor system and method have a broad range of applications but are particularly suited for the production of terephthalic acid.Type: ApplicationFiled: September 20, 2007Publication date: June 16, 2011Inventors: Luciano Piras, Marzio Monagheddu, Andrea Gnagnetti, Kishore K. Kar
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Publication number: 20110129390Abstract: The instant application provides apparatus and methods for the generation of gas, preferably chlorine dioxide. The methods and apparatus of the invention use a removable reaction chamber for the reaction of precursor chemicals, e.g., chlorite salt and an acid. The methods and compositions of the invention provide gas for a number of personal and commercial applications.Type: ApplicationFiled: July 1, 2010Publication date: June 2, 2011Applicant: TBS TECHNOLOGIES, LLCInventors: Thomas J. Dee, Paul Sabin, Douglas Sabin
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Patent number: 7938868Abstract: The inventive stage system for producing hydrogen consists of at least two upstream/downstream stages, respectively, each of which comprises, optionally, a catalytic reactor (C1 to C5) followed by a separator comprising a space (E1 to E4) for circulation of a gaseous mixture contacting at least one oxygen extracting membrane and a hydrogen collecting space, wherein the reactor (C1) of the upstream stage is connected to a reaction gaseous mixture source, the circulation stage (E1) of the upstream stage separator is connected to the reactor (C2) of the downstream stage and the spaces for extracting/collecting oxygen from two separators are connected to a hydrogen collecting circuit (TC, 8) which is common for two stages.Type: GrantFiled: July 28, 2005Date of Patent: May 10, 2011Assignee: Compagnie Européenne des Technologies de l'Hydrogène (C.E.T.H.)Inventors: Eric Gernot, Arnaud Deschamps
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Patent number: 7935316Abstract: Disclosed is a chemical reaction cartridge including an elastic body with which at least a portion of the chemical reaction cartridge is formed and a plurality of chambers and a flow path to connect the plurality of chambers, which contain solution inside, and the solution is moved or blocked in the chambers and the flow path by applying external force to the elastic body from outside, the elastic body is structured in at least two elastic body layers which are layered vertically and the plurality of chambers and the flow path are provided between an upper elastic body layer and a lower elastic body layer, and the elastic body is attached to a surface of a substrate made of hard material.Type: GrantFiled: January 11, 2008Date of Patent: May 3, 2011Assignee: Yokogawa Electric CorporationInventors: Katsumori Gyonouchi, Nobuyuki Takeuchi, Takeo Tanaami, Hisao Katakura
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Publication number: 20110089377Abstract: A molten metal reactor for converting a carbon material and steam into a gas comprising hydrogen, carbon monoxide, and carbon dioxide is disclosed. The reactor includes an interior crucible having a portion contained within an exterior crucible. The interior crucible includes an inlet and an outlet; the outlet leads to the exterior crucible and may comprise a diffuser. The exterior crucible may contain a molten alkaline metal compound. Contained between the exterior crucible and the interior crucible is at least one baffle.Type: ApplicationFiled: October 19, 2009Publication date: April 21, 2011Applicant: BATTELLE ENERGY ALLIANCE, LLCInventors: Dennis N. Bingham, Kerry M. Klingler, Terry D. Turner, Bruce M. Wilding
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Patent number: 7896934Abstract: A gas-generating apparatus (10) includes a reaction chamber (18) containing a solid fuel component (24) and a liquid fuel component (22) that is introduced into the reaction chamber by a fluid path, such as a tube, nozzle, or valve. The flow of the liquid fuel to the solid fuel is self-regulated. Other embodiments of the gas-generating apparatus are also disclosed.Type: GrantFiled: June 12, 2006Date of Patent: March 1, 2011Assignee: Societe BicInventors: Andrew J. Curello, Floyd Fairbanks, Constance R. Stepan, Anthony Sgroi, Jr., Michael Curello
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Patent number: 7879296Abstract: A reactor system for gas phase reacting of at least two fluid feed streams, where the reactor system has an injectively-mixed backmixing reaction chamber in fluid communication with a tubular-flow reactor. The injectively-mixed backmixing reaction chamber has a bulkhead that slides during real-time operation to either diminish or expand the internal volume of the backmixing reaction chamber. In one embodiment, the effective passageway space through the bulkhead is also variably adjustable. In another embodiment, the tubular-flow reactor shares the bulkhead so that axial bulkhead movement commensurately expands one reaction space while diminishing the other reaction space. Input gas streams enter the backmixing reaction chamber with sufficient velocity to turbulently agitate the contents of the injectively-mixed backmixing reaction chamber by injective intermixing of the alkane-containing gas feed stream and the oxygen-containing gas feed stream.Type: GrantFiled: March 14, 2007Date of Patent: February 1, 2011Assignee: Gas Technologies LLCInventors: Nathan A. Pawlak, Robert W. Carr, Roger J Grunch
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Patent number: 7879298Abstract: A microreactor (1) comprises a vacuum casing (2), a microreactor proper (4) located in a vacuum-tight cavity (3) in the vacuum casing (2), and a getter heat-generation substrate (6) positioned on at least one surface of the microreactor proper (4). The microreactor proper (4) has a feed inlet (19a) connected to outside the vacuum casing (2) by way of a feed supply pipe (5A) and a gas outlet (19b) connected to outside the vacuum casing (2) by way of a gas discharge pipe (5B). The getter heat-generation substrate (6) comprises a substrate (7), and a heat generator (9) and a getter material layer (10) that are located on the substrate (7) alternately in mutual non-contact fashion.Type: GrantFiled: November 20, 2007Date of Patent: February 1, 2011Assignee: Dai Nippon Printing Co., Ltd.Inventors: Takeshi Kihara, Hiroshi Yagi, Akihiko Takeuchi
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Publication number: 20100329949Abstract: This specification discloses a radial flow continuous reaction/regeneration apparatus. Through employing a rotary device to individually and annularly distributing process fluid and regeneration fluid into a stationary segmented reaction/regeneration box and receiving effluents individually and annularly from the same stationary reaction/regeneration box, the mentioned radial flow continuous reaction/regeneration apparatus can be operated continuously and efficiently without the need for shutting down for regeneration. This radial flow continuous reaction/regeneration apparatus is not only used to separate components by adsorption, such as dehumidification, but also is used in chemical processes to carry out catalytic reaction, regenerate catalyst and used as filtration device to trap particles by changing the filler in the stationary reaction/regeneration box.Type: ApplicationFiled: May 31, 2010Publication date: December 30, 2010Inventor: Leon Yuan
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Patent number: 7833353Abstract: A liquid material vaporization apparatus for a semiconductor processing apparatus includes: a vaporization tank; an inner partition wall disposed in the tank for dividing the interior of the tank into a charging compartment and a vaporization compartment which are liquid-communicatable with each other over an upper edge of the inner partition wall. A liquid material charged in the charging compartment overflows over the upper edge of the inner partition wall toward the vaporization compartment to store and vaporize the liquid material in the vaporization compartment.Type: GrantFiled: January 24, 2007Date of Patent: November 16, 2010Assignee: ASM Japan K.K.Inventors: Kazunori Furukawahara, Hideaki Fukuda
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Patent number: 7824614Abstract: In a cartridge for chemical reaction, there are provided an inner part in which a chemical reaction is caused by feeding a liquid in accordance with a deformation when an external force is applied, and a plurality of passages that are connected with each other, and the passages can be switched between an opened state and a closed state by the external force. Since the plurality of passages are connected together in the cartridge, the cartridge can be applied to various uses. The plurality of passages may be connected together in the form of a network. Wells may be provided at the junctions of the passages. When the external force is applied on the well, the liquid may be pushed out of the well through the passages connected to the well. A passage may be provided for introducing a sample into the cartridge from an external part of the cartridge.Type: GrantFiled: July 17, 2006Date of Patent: November 2, 2010Assignee: Yokogawa Electric CorporationInventor: Takeo Tanaami
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Publication number: 20100274034Abstract: The present invention provides a method of producing a fatty acid alkyl ester and/or glycerin by bringing an oil and an alcohol into contact with each other, the method including: reacting the oil and alcohol with each other; performing solid-liquid separation for removing a solid sterol from a reaction liquid obtained in the step of reacting; and performing phase separation for separating the reaction liquid into a hydrophobic phase and a hydrophilic phase after the reaction liquid is subjected to the step of performing the solid-liquid separation, the hydrophobic phase containing the fatty acid alkyl ester, and the hydrophilic phase containing glycerin. Thereby, the present invention provides a method allowing stable continuous operation for a long time period for production of a fatty acid alkyl ester and/or glycerin.Type: ApplicationFiled: December 18, 2008Publication date: October 28, 2010Applicants: NIPPON SHOKUBAI CO., LTD, RESEARCH INSTITUTE OF INNOVATIVE TECHNOLOGY FOR THInventors: Izuho Okada, Tomoharu Oku, Hironori Horie, Masanori Nonoguchi, Atsushi Tachibana
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Patent number: 7811529Abstract: A compact hydrogen generator for use with fuel cells and other applications includes a hydrogen membrane reactor having a combustion chamber and a reaction chamber. The two chambers are have a fluid connection and a heat exchange relationship with one another. The hydrogen generation apparatus also includes a fuel supply, a fuel supply line for transporting fuel from the fuel supply to the reaction chamber, an oxygen supply, an oxygen supply line for transporting oxygen form the oxygen supply to the combustion chamber, as well as a tail gas supply line for transporting tail gas supply line for transporting tail gases form the reaction chamber, a combustion by-product line for transporting combustion by-products for the combustion chamber, and a reaction product line for transporting hydrogen from the reaction chamber.Type: GrantFiled: April 23, 2002Date of Patent: October 12, 2010Assignee: Intelligent Energy, Inc.Inventors: Michael Powell, Charles J. Call
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Patent number: 7807114Abstract: The present invention provides a reactor system having: (1) a plurality of reactors connected in fluid flow communication and having at least one pair of reactors separated by an interstage position; (2) a line for supplying a reactant feed stream separately to an inlet of more than one of the plurality of reactors; and (3) a diverter in fluid communication with the interstage position and capable of directing a first portion of a product stream exiting one reactor in said pair of reactors to a first location and a second portion of the product flow stream to an inlet of another reactor in said pair of reactors.Type: GrantFiled: July 27, 2009Date of Patent: October 5, 2010Assignee: UOP LLCInventors: Andrea G. Bozzano, Tom N. Kalnes, Carl J. Stevens, Steven M. Poklop
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Patent number: 7785548Abstract: Disclosed is a fuel filter for removing sulfur containing compounds from an internal combustion fuel stream. In one embodiment, the fuel filter comprises at least one column comprising an adsorbent. In one exemplary embodiment the adsorbent is capable of removing sulfur containing compounds, especially sulfur containing aromatic compounds, from fuels used in internal combustion engines, especially diesel fuels. Also disclosed is an apparatus for extending the life cycle of a post combustion emission control device. In one exemplary embodiment, the apparatus comprises a fuel filter for removing sulfur containing compounds from an internal combustion fuel stream and an emission control device. Finally, a method for removing sulfur containing compounds from an internal combustion fuel stream is disclosed.Type: GrantFiled: July 22, 2008Date of Patent: August 31, 2010Assignee: Honeywell International Inc.Inventors: Ronald P. Rohrbach, Peter D. Unger, Gary B. Zulauf, Daniel E. Bause, Russ Johnson, David R. Rockwell
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Patent number: 7776290Abstract: The invention relates to a container (10) for a multi-component reaction, having at least two chemical chambers (20) and at least one mixing space, the container (10) being formed from a base film (40) provided with recesses (30) and an upper film (50), which is optionally structured, the upper film (50) being joined, especially sealed, to the base film (40), at least over sections. The invention relates also to a method of filling such a container.Type: GrantFiled: April 14, 2005Date of Patent: August 17, 2010Assignee: Huhtamaki Ronsberg Zweigniederlassung der Huhtamaki Deutschland GmbH & Co. KGInventors: Andreas Michalsky, Raphael Cholodewicz
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Publication number: 20100182868Abstract: A microfluidic device (10) for performing chemical or biological reactions comprises a chamber (20) for use as a self-sustaining oscillating jet mixing chamber and two or more separate feed channels (22, 24, 40) separated by one or more inter-channel walls (25), the two or more channels (22,24,40) terminating at a common side (18) of the chamber (20), the two or more channels (22,24,40) having a total channel width (28) comprising the widths of the two or more channels (22,24,40) and all inter-channel walls (25) taken together, the chamber (20) having a width (26) in a direction perpendicular to the channels (22,24,40) and a length (32) in a direction parallel to the channels, the width (26) being at least two times the total channel width (28), the chamber (20) having two opposing major surfaces (56) defining a height (30) thereof, the chamber (20) having a major-surface-area to volume ratio of at least 10 cm2/cm3.Type: ApplicationFiled: May 15, 2008Publication date: July 22, 2010Applicant: CORNING INCORPORATEDInventor: Pierre Woehl
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Publication number: 20100178221Abstract: It is aimed to promote further integration of channels in a reactor. A channel forming body of a reactor is provided with a base plate, a first sealing member bonded to one surface of the base plate while covering the one surface, and a second sealing member bonded to the other surface of the base plate while covering the other surface. A plurality of first inlet grooves for forming the first inlet paths are formed in parallel and side by side and a plurality of reaction grooves for forming the reaction grooves are formed in parallel and side by side in the one surface of the base plate. On the other hand, a plurality of second inlet grooves for forming the second inlet paths are formed in parallel and side by side in the other surface of the base plate.Type: ApplicationFiled: June 12, 2009Publication date: July 15, 2010Applicant: Kabushiki Kaisha Kobe Seiko Sho (Kobe Steel, Ltd.)Inventors: Tatsuo YOSHIDA, Koji NOISHIKI
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Publication number: 20100174124Abstract: This invention relates to a process for conducting a hydrocracking or a hydrotreating process in a microchannel reactor. This invention also relates to a process and apparatus for flowing a vapor and liquid into a plurality of microchannels in a microchannel processing unit.Type: ApplicationFiled: October 9, 2009Publication date: July 8, 2010Inventors: Anna Lee Tonkovich, Ravi Arora, John Brophy, Francis P. Daly, Soumitra Deshmukh, Maddalena Fanelli, Kai Tod Paul Jarosch, Timothy J. LaPlante, Richard Q. Long, Terry Mazanec, Daniel Francis Ryan, Laura J. Silva, Wayne W. Simmons, Bruce Stangeland, Yong Wang, Thomas Yuschak, Steven T. Perry, Jeffrey Dale Marco, Michael Alan Marchiando, Robert Dwayne Litt
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Publication number: 20100158756Abstract: Fluidic devices and methods including those that provide storage and/or facilitate fluid handling of reagents are provided. Fluidic devices described herein may include channel segments positioned on two sides of an article, optionally connected by an intervening channel passing through the article. The channel segments may be used to store reagents in the device prior to first use by an end user. The stored reagents may include fluid plugs positioned in linear order so that during use, as fluids flow to a reaction site, they are delivered in a predetermined sequence. The specific geometries of the channel segments and the positions of the channel segments within the fluidic devices described herein may allow fluid reagents to be stored for extended periods of time without mixing, even during routine handling of the devices such as during shipping of the devices, and when the devices are subjected to physical shock or vibration.Type: ApplicationFiled: December 17, 2009Publication date: June 24, 2010Applicant: Claros Diagnostics, Inc.Inventors: Jason Taylor, Vincent Linder
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Patent number: 7731919Abstract: A fixed bed reactor for gas-phase catalytic oxidation, the fixed bed reactor, comprising a reaction tube filled with a gas-phase oxidation catalyst, wherein a solid acid is placed in an end portion(s) of the reaction tube or between catalyst layers of the catalyst, or mixed in the catalyst; the solid acid is an oxide or a complex oxide containing at least one kind of element selected from the group consisting of aluminum (Al), silicon (Si), titanium (Ti) and zirconium (Zr), and has a shape of sphere, cylindrical column, cylindrical tube, star, ring, tablet or pellet; the catalyst is a complex oxide containing molybdenum (Mo) and bismuth (Bi) or a complex oxide containing molybdenum (Mo) and vanadium (V); and acid strength(H0) of the solid acid meets an inequality: ?5.6?H0?1.5.Type: GrantFiled: April 18, 2006Date of Patent: June 8, 2010Assignee: Nippon Shokubai Co., Ltd.Inventor: Naohiro Fukumoto
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Publication number: 20100137634Abstract: The present invention relates to a hole-jetting type reactor and its applications, in particular to a process for the production of isocyanates by the phosgenation of aliphatic or aromatic diamines or triamines in the gas phase using this reactor. The present invention achieves a good mixing and reacting result of the gas-phase phosgenation reaction at a high temperature by improving the mixing of reactants in the reactor to reduce the possibility of forming swirls and eliminate negative pressure produced at a local jet area, which can finally reduce back-mixing and formation of solid by-products.Type: ApplicationFiled: August 21, 2007Publication date: June 3, 2010Inventors: Jiansheng Ding, Yong hua Shang, Deqiang Ma, Jingquan Hao, Peicheng Luo, Shuang Hu
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Publication number: 20100137654Abstract: A method and apparatus for converting glycerol into propylene glycol by directing a basic glycerol containing feed and a hydrogen containing gas into a reaction zone including a fixed bed of catalyst that is operating at glycerol conversion conditions where the reactor includes and at least one quench zone and directing a quench material into the quench zone.Type: ApplicationFiled: December 23, 2008Publication date: June 3, 2010Applicant: EUDYNA DEBICES INC.Inventors: Maureen Bricker, Laura E. Leonard
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Patent number: 7722835Abstract: A closed and yet flexible and easily adaptable reaction vessel system for performing liquid handling operations, such as sampling, incubating, homogenizing and/or metering fluids, can be constructed in a modular fashion, comprising a first container, to which at least two second containers are connected, wherein the contents of said second containers can be transferred from one of said second containers into said first container and back, or into another second container.Type: GrantFiled: April 29, 2005Date of Patent: May 25, 2010Inventor: Mats Malmqvist
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Publication number: 20100119412Abstract: The present invention relates generally to chemical and biological decontamination solutions and methods of using them. The invention is useful for decontaminating and/or disinfecting a wide range of compounds and organisms. In particular, the systems, methods, solutions, and formulations of the invention can be used to remove and/or neutralize organophosphates, mustard agents, and other toxic chemicals, bacteria, bacterial spores, fungi, molds and viruses.Type: ApplicationFiled: December 4, 2009Publication date: May 13, 2010Applicant: Aries Associates, Inc.Inventor: Michael J. Conrad
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Patent number: 7713479Abstract: A liquid analyser has a reactor portion and an associated measurement portion. A sample pump is operable to deliver a liquid sample to a reactor vessel. A base pump supplies a base solution to the reactor vessel. An ozone generator supplies ozone to the reactor vessel. The liquid sample is oxidised in the reactor vessel by means of hydroxyl radicals which are generated using the base solution and ozone to reduce complex components of the liquid sample to their lowest state in solution. The oxidised sample solution is delivered to an optical detector in the measurement portion to determine the concentration of one or more selected materials such as nitrogen, phosphorous or a heavy metal in the oxidised sample solution.Type: GrantFiled: February 24, 2009Date of Patent: May 11, 2010Assignee: Analytical Developments LimitedInventors: Martin Horan, Seamus O'Mahony
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Publication number: 20100104481Abstract: Disclosed herein are multiple embodiments of a hydrogen generator (10) that measures, transports or stores a single dose of a viscous fuel component from first fuel chamber (12) in storage area (38) when the internal hydrogen pressure (44, 44?) of the hydrogen generator is high, and transports this single dose to a metal hydride fuel component in second fuel chamber (14) when the internal pressure is low, so that the viscous liquid and metal hydride fuel components react together to generate more hydrogen and to restart the cycle. The viscous fuel component can be water or alcohol, such as methanol, in liquid or gel form, and the metal hydride fuel component can be sodium borohydride or other metal hydride that chemically reacts with the viscous fuel to produce hydrogen. The metal hydride fuel component can be in solid or viscous form, e.g., aqueous form.Type: ApplicationFiled: February 1, 2008Publication date: April 29, 2010Applicant: Societe BICInventors: Andrew J. Curello, Constance R. Stepan, Anthony Sgroi, Paul Spahr, Michael Curello, Alain Rosenzweig, Kurt Rath
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Publication number: 20100074815Abstract: Mold releasability of a molding die from a master is improved. The master is a mother body of the molding die. The master has a groove corresponding to a flow channel of a resin molded product, and the cross-section of the bottom surface portion of the groove is in the form of a curved surface.Type: ApplicationFiled: October 19, 2007Publication date: March 25, 2010Inventors: Kanji Sekihara, Masayoshi Uehira
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Publication number: 20100074813Abstract: The instant application provides apparatus and methods for the generation of chlorine dioxide. The methods and apparatus of the invention use a water dissolvable membrane to allow the reaction of precursor chemicals, e.g., chlorite salt and an acid. The methods and compositions of the invention provide chlorine dioxide for a number of personal and commercial applications.Type: ApplicationFiled: April 17, 2009Publication date: March 25, 2010Inventor: Thomas J. Dee
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Publication number: 20100068107Abstract: A method of making a microfluidic device by providing first and second substrates and forming a first frit structure on the first substrate and a second frit structure on the second substrate and consolidating the first and second substrates together, with frit structures facing, so as to form a consolidated-frit-defined and consolidated-frit-surrounded recess between said first and second substrates, where the second substrate has at least one pre-formed through-hole therein, and where forming a second frit structure includes forming a frit layer within said through-hole covering the interior surface of the through-hole to a thickness sufficiently thin to produce, on consolidating the substrates and the first and second frit structures together, a through-hole having an interior surface of consolidated frit continuous with the consolidated frit surrounding the recess.Type: ApplicationFiled: November 26, 2007Publication date: March 18, 2010Inventor: Ronan Tanguy
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Publication number: 20100006478Abstract: A process for the on-stream decoking of a steam cracking furnace, the steam cracking furnace including multiple tube banks positioned between a hydrocarbon feedstock inlet and a convection section to radiant section crossover, each tube bank including a plurality of tubes arranged within the tube bank, the process comprising the steps of terminating the flow of hydrocarbon feed to a portion of the plurality of tubes of less than all of the multiple tube banks, and supplying a decoking feed comprising steam to the portion of the plurality of tubes of less than all of the multiple tube banks in sufficient amount to effect removal of coke accumulated on the interior of the radiant coils and quench system components fed by such tubes while maintaining a temperature at the convection section to radiant section crossover of below about 788° C. A furnace for the production of ethylene is also provided.Type: ApplicationFiled: July 11, 2008Publication date: January 14, 2010Inventor: David B. Spicer
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Patent number: 7632473Abstract: Processes and apparatus for the alkylation of aromatic compound with mono-olefin aliphatic compound in the presence of solid alkylation catalyst use a lights distillation for obtaining desired selectivities to arylalkane in a energy efficient manner. The processes and apparatus offer the potential for debottlenecking existing arylalkane production facilities and reducing the size and energy requirements for a new arylalkane production facility.Type: GrantFiled: January 29, 2008Date of Patent: December 15, 2009Assignee: UOP LLCInventors: Stephen W. Sohn, Michael R. Smith, Lance A. Baird
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Publication number: 20090304554Abstract: The apparatus includes a liquid permeable pouch that defines a cavity for maintaining an anhydrous hydride reactant, wherein the cavity comprises a cross-section such that a point within the cross-section is separated from a perimeter of the liquid permeable pouch by no more than double the permeation distance, and a cartridge configured to receive the liquid permeable pouch and a liquid reactant such that at least a portion of the liquid permeable pouch is submerged in the liquid reactant. The system includes a plurality of pouches formed from two rectangular sheets of liquid permeable material, and each pouch has a width selected such that each point within a cross-section is separated from the sheets by no more than double the permeation distance. The method includes joining the sheets, forming one or more seals to define a cavity, disposing anhydrous hydride within the cavity, and sealing the opening.Type: ApplicationFiled: June 3, 2009Publication date: December 10, 2009Inventors: James Kevin Shurtleff, John Madison Patton, Eric J. Ladd
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Patent number: 7622086Abstract: A selectively permeable membrane type reactor including a catalyst for promoting a chemical reaction, a selectively permeable membrane which selectively allows a specific component to pass therethrough, and a carrier for disposing the catalyst and the selectively permeable membrane the carrier being a tubular body having two or more gas passage cells partitioned and formed by a partition wall formed of a porous body, the catalyst being individually disposed in some of the cells of the carrier, the selectively permeable membrane being individually disposed in the remainder of the cells, and the cell in which the catalyst is disposed and the cell in which the selectively permeable membrane is disposed being adjacently disposed with the partition wall positioned therebetween.Type: GrantFiled: January 17, 2005Date of Patent: November 24, 2009Assignee: NGK Insulators, Ltd.Inventors: Akira Takahashi, Nobuhiko Mori
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Publication number: 20090280043Abstract: A device for activating a two component reaction system where the two reaction component are in separate containers with one container inside the other. The containers are sealed from each other and the inner container includes an activation element for opening a part of the seal. A pressure differential between the pressure in the inner and outer containers is made so the inner container has the higher pressure. Opening a part of the seal in the inner container drives the second component to react with the first reaction component. The seal is opened by cutting the inner container.Type: ApplicationFiled: May 12, 2008Publication date: November 12, 2009Inventor: Tobi W. Ferguson
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Multi-zone moving-bed reaction device with an addition of regenerated or fresh catalyst in each zone
Patent number: 7611678Abstract: A reaction device includes staged zones making it possible to implement strongly endothermic or exothermic reactions. The device reduces the differences in catalytic activity between these zones using an addition of fresh or regenerated catalyst at the inlet of each reaction zone and provides an integrated heat exchanger. A process of chemical conversion employs the device for gas-phase and/or liquid-phase exothermic or endothermic reactions, and in particular for the oligomerization reaction of C2 to C12 fractions for the purpose of producing a diesel fraction.Type: GrantFiled: November 9, 2005Date of Patent: November 3, 2009Assignee: Institut Francais du PetroleInventors: Sylvain Louret, Patrice Font, Sylvie Lacombe, Eric Sancheż, Laurent Simon -
Patent number: 7604781Abstract: Multiphasic reactions, especially those reactions using a phase transfer catalyst, are conducted in microchannel apparatus. Advantageously, these reactions can be conducted with two, planar microlayers of reactants in adjacent laminar flow streams. Microchannel apparatus and methods for conducting unit operations such as reactions and separations in microchannel apparatus is also described. Microchannel apparatus can provide advantages for controlling reactions and separating products, solvents or reactants in multiphase reactions.Type: GrantFiled: July 26, 2006Date of Patent: October 20, 2009Assignee: Battelle Memorial InstituteInventors: John H. Brophy, Bruce F. Monzyk