Abstract: A microencapsulation and electrostatic processing (MEP) device is provided for forming microcapsules. In one embodiment, the device comprises a chamber having a filter which separates a first region in the chamber from a second region in the chamber. An aqueous solution is introduced into the first region through an inlet port, and a hydrocarbon/polymer solution is introduced into the second region through another inlet port. The filter acts to stabilize the interface and suppress mixing between the two immiscible solutions as they are being introduced into their respective regions. After the solutions have been introduced and have become quiescent, the interface is gently separated from the filter. At this point, spontaneous formation of microcapsules at the interface may begin to occur, or some fluid motion may be provided to induce microcapsule formation. In any case, the fluid shear force at the interface is limited to less than 100 dynes/cm2.

Abstract: Nestable canisters for use in a dispersal valve that normally holds only a single canister with the nestable canisters suitable for replacing single canisters to enable a fluid mixing stream to be bifurcated and simultaneously but separately treat the water with different materials. The fluid mixing stream which normally flows through the set of ports that are used for dispensing only one solid chemical into the liquid stream flowing through the dispersal valve is bifurcated to provide for both dispersant type bacteria killing as well as in situ bacteria killing. In addition the nestable canisters are provided with an improved bactericide and algaecide for killing algae in the water and absorbing acids that might be generated by use of chlorine in the dispersal valve.

Abstract: The present invention relates to a process for the production of methanol from a hydrocarbon feedstock comprising: contacting a vaporous mixture comprising the feedstock and steam in a steam reforming zone with a catalyst effective for catalysis of at least one reforming reaction; recovering from the reforming zone a synthesis gas mixture comprising carbon oxides, hydrogen and methane; supplying material of the synthesis gas mixture to a methanol synthesis zone charged with a methanol synthesis catalyst and maintained under methanol synthesis conditions; recovering from the methanol synthesis zone a product gas mixture comprising methanol and unreacted material of the synthesis gas mixture; supplying material of the product gas mixture to a methanol recovery zone maintained under methanol recovery conditions; recovering from the methanol recovery zone a crude methanol product stream and a vaporous steam comprising unreacted material of the synthesis gas mixture; separating material of the synthesis gas mixtur

Abstract: A process and apparatus for indirectly heating an endothermic reaction by combustion of reactants or products from the endothermic reaction using a plate heat exchange arrangement in a highly efficient manner. This invention is particularly suited for processes such as the production of styrene or synthesis gas. When producing synthesis gas, oxidizing reactants in a secondary reforming step generates heat for a primary reforming step and the process improves selectivity and yield with a highly efficient heat exchange step that uses narrow channel for indirect heat exchange. The narrow channels are preferably defined by corrugated plates. The primary reaction channels will contain a catalyst for the promotion of the primary reaction such as steam reforming or ethylbenzene dehydrogenation.

Abstract: An improved reactor for generating water from hydrogen and oxygen which allows production of moisture at a high conversion rate exceeding 99 percent with the temperature kept under some 400° C. inside the reactor shell (1) and with the water vapor production being more than 1,000 sccm. One form of the reactor (FIG. 1) according to the invention is constructed with a closed cylinder divided into two compartments by an interior partition, a first reactor structural component (2) and a second reactor structural component (3), united to define a sealed interior space (1a). The sealed interior space (1a) of the reactor shell (1) is partitioned by a diffusion filter (10) into a first chamber (1b) provided with an inlet reflector unit (9) and a second chamber (1c) provided with an outlet reflector-diffuser unit (11). On the inside surface of the second reactor structural component (1c) is formed a platinum coated catalyst layer (13).

Abstract: A method is provided for removing hydrogen sulfide and hydrogen polysulfide compounds out of liquid sulfur by stripping with a gas, such as air. The method is conducted in an apparatus equipped with at least two degassing compartments and a sulfur collection pit wherein the degassing compartments are separated from each other by a first partition wall, the last degassing compartment is separated from the sulfur collection pit by a second partion wall and each degassing compartment contains at least first and second subcompartments which are separated from each other by a third partion wall and are open to each other at the top and the bottom. At least one first subcompartment in each said degassing compartment is provided, at the bottom thereof, with a plurality of stripping gas inlet nozzles and at least one second subcompartment in each said degassing compartment is not provided with stripping gas inlet nozzles.

Abstract: An arrangement for the controlled production of an essentially linear array of hydrocarbon feed injection jets reduces required clearances and elevation while facilitating modification of the contacting locating a feed distributor containing a linear array of jets at a standpipe junction point to provide choke point for particle flow control. The flow properties of the extended particle layer are controlled by adjusting the density of the particles above the choke point created by the upper part of the standpipe inside diameter and the top of the distributor. Steam or another fluidization medium may be added to the particles directly above the distributor for this purpose. This invention can also modify the particle or feed injection characteristics by changing the projection of the distributor into the standpipe to adjust the flow area over the choke point and by the use of bottom slides or baffles to change the flow area size and configuration.

Abstract: A compact combination blood cell count and immunoassay apparatus for measuring drawn whole blood specimen includes a load station for receiving the whole blood specimen and a nozzle member that can selectively withdraw whole blood from the blood specimen. A blood cell count section and an immunoassay section are mounted along a unitary path of movement of the nozzle member so that a single nozzle member may be used for transporting the whole blood to the respective blood cell count section and immunoassay section. A controller can automatically direct a transport mechanism to use only the whole blood and to perform various steps of adding dilution liquid and reagents, along with appropriate washing of the nozzle and sample cells to insure an automatic operation. A hematozorit value can be determined from the blood cell count signal and used to correct the immunoassay signal when whole blood is used.

Abstract: An automatic immunoassay method and apparatus which not only permit automatic operations of supplying and discarding reaction tubes, washing for B/F separation, dispensation of reagents, and measurement, but also permit the reaction time to be varied arbitrarily and can cope with any of the assay techniques including one-step and two-step noncompetitive sandwich techniques and competitive techniques.

Abstract: An ultrasonic energy source is used to provide a variable force for measuring the binding forces between molecular entities and for sensing the presence of an analyte in a test sample. The device includes a surface that has a first binding member attached thereto and one or more particles that have a second binding member attached thereto. A reaction vessel is provided for exposing the surface to the particles whereby, if the first binding member has a binding affinity for the second binding member, a complex is formed between individual first binding members and individual second binding members and the particles thereby become immobilized with respect to the surface. The ultrasonic energy source is positioned for applying a variable ultrasonic force onto the surface, and the position of the particles is monitored as the intensity of the ultrasonic force is varied.

Abstract: The preparation of finely-divided, homodisperse dispersions from a liquid medium having sparingly soluble particles contained therein, the particles being produced in a tubular reactor by the reaction of reactants dissolved in the medium, is carried out by introducing the solutions of the reactants, at least at the reaction temperature, into the tubular reactor separately from one another, as coaxial, laminar, parallel flows, and by shielding them from the reactor wall.

Abstract: An integrated micro-ceramic chemical plant having a unitary ceramic body formed from multiple ceramic layers in the green state which are sintered together includes a reaction chamber and a first passage for providing communication with the reaction chamber so that two or more fluids may be delivered to such reaction chamber for reaction, and the unitary ceramic body defining a catalytic bed in the reaction chamber, such catalytic bed being formed of micro-porous ceramic impregnated with at least one catalyst for promoting the reaction in the reaction chamber to produce reaction products; and the unitary ceramic body defining a filtration channel connected to the reaction chamber including filters disposed in such filtration channel for separating the reaction products so as to retrieve desired reaction products.

Abstract: An apparatus is provided for conducting solid phase oligomer synthesis. The apparatus includes a reaction vessel in which a solid phase support is contained. The reaction vessel has a top opening through which gases and solvents can be delivered by way of a series of conduits and valves. The reaction vessel is interconnected through a bottom opening therein and through a series of conduits and valves with a vessel or series of vessels containing a reagent or series of reagents, respectively, required for the synthetic reaction. The reagent vessel serves a both a source of reagent delivered to the reaction vessel and as a repository for unused reagent returned thereto from the reaction vessel. Reagent delivery and mixing is gas-driven using an associated source of an inert gas.

Abstract: A quench zone mixing apparatus that occupies a low vertical height and has an improved mixing efficiency and fluid distribution across the catalyst surface includes a swirl chamber, a rough distribution network, and a distribution apparatus. In the swirl chamber, reactant fluid from a catalyst bed above is thoroughly mixed with a quench fluid by a swirling action. The mixed fluids exit the swirl chamber through an aperture to the rough distribution system where the fluids are radially distributed outward across the vessel to the distribution apparatus. The distribution apparatus includes a plate with a number of bubble caps and associated drip trays that multiply the liquid drip stream from the bubble caps to further symmetrically distribute the fluids across the catalyst surface. The distribution apparatus can be used in the reaction vessel without the swirl chamber and rough distribution system, e.g., at the top of a vessel.

Abstract: This method and apparatus for detecting target molecules in a liquid phase. The apparatus monitors whether the target molecule has selectively bound to recognition agents on the surface of a magnetic field sensor by monitoring the output of the sensor. The recognition agents which selectively bind target molecules are covalently bound to microfabricated magnetic field sensors. These sensors are then exposed to a sample suspected of containing the target molecules, whereupon the recognition agents bind to and immobilize any target molecules present. Depending on the embodiment, recognition agents that selectively bind the target molecule, or recognition agents that selectively bind the sensor-bound recognition agents, are covalently bound to magnetizable particles. These particles are then added to the sensors and, again depending on the embodiment, attach either to any immobilized target molecules or to sensor-bound recognition agents.

Abstract: The present invention relates to devices for conducting, simultaneously, exothermic and endothermic chemical conversions with transfer of heat therebetween. More particularly, this invention relates to autothermic modules using oxygen ion-conducting dense ceramic membranes to separate, selectively, oxygen from an oxygen-containing gas and supply it directly to partial combustion of gaseous organic compounds. Processes using autothermic modules in accordance with this invention are, advantageously, used for production of synthesis gas comprising carbon monoxide and molecular hydrogen which synthesis gas is substantially free of deleterious and/or inert gaseous diluents such as nitrogen. In particular, for conversions, within the integral autothermic module, of natural gas or other forms of gaseous lower alkanes to synthesis gas by means of partial combustion followed by reforming.

Abstract: An integrated micro-ceramic chemical plant having a unitary ceramic body formed from multiple ceramic layers in the green state which are sintered together includes a unitary ceramic body defining a reaction chamber and first passages are provided for communication with the reaction chamber so that two or more fluids may be delivered to such reaction chamber, a permeable partition wall being provided within the reaction chamber to permit the mixing of fluids during a reaction process. The integrated micro-ceramic chemical plant further includes a filtering chamber including filters disposed in such chamber for separating the solid reaction products from the fluid and for retrieving desired solid reaction products; and other passages for directing the desired solid reaction products to exit from the unitary ceramic body and other passages for directing the desired liquid reaction products to exit from the unitary ceramic body.

Abstract: A method and apparatus for dynamically controlling the crystallization of proteins including a crystallization chamber or chambers for holding a protein in a salt solution, one or more salt solution chambers, two communication passages respectively coupling the crystallization chamber with each of the salt solution chambers, and transfer mechanisms configured to respectively transfer salt solution between each of the salt solution chambers and the crystallization chamber. The transfer mechanisms are interlocked to maintain the volume of salt solution in the crystallization chamber substantially constant. Salt solution of different concentrations is transferred into and out of the crystallization chamber to adjust the salt concentration in the crystallization chamber to achieve precise control of the crystallization process.

Abstract: The invention relates to a device for depolymerizing used and waste plastics, comprising a closed reactor and a circulation system the mildly heating of the reactor contents connected to the reactor, as well as to a process for depolymerizing used and waste plastics. To protect the circulation system from erosion by solid particles contained in the reactor contents, the reactor is designed so that the reactor contents drawn off into the circulation system traverse a riser section integrated into the reactor for removing fairly coarse solid particles having correspondingly high settling rate before entry into the take-off line.

Abstract: A reactor for the production or formulation of flowable viscous products is equipped with an internal piston which assists in the removal of product from the reactor interior.

Abstract: A fluid bed reactor is provided having a grid baffle structure to provide increased theoretical stages within the reactor to enable the reactor to be used for time/temperature dependent reactions requiring a number of mixing stages and/or an increased particle residence time. The preferred baffle structure comprises a plurality of staggered first and second vertical members extending partly across the reactor from opposed sides of the reactor which form a path for the feed to travel therethrough from the inlet to the outlet of the reactor with the vertical members having vertical cross-members, preferably shorter than the vertical members, extending completely between adjacent vertical members and/or partly in the space between the members to form reaction stage sections whereby feed entering the reactor moves in a serpentine path and/or a sequential underflow and/or overflow path through the reaction stage sections of the baffle from the inlet of the reactor to the reactor outlet.

Abstract: A method for reducing the viscosity of a liquid heavy hydrocarbon feedstock comprising the steps of bringing said feedstock to a temperature capable of cracking of at least a portion of the hydrocarbons present in said feedstock and introducing said feedstock into a bottom portion of a maturation device (i.e. a "soaker"), where the feedstock is displaced from the bottom upwards, to get evacuated from a top portion of the soaker towards a fractioning unit. The invention also relates to an apparatus comprising a soaker in which are located, transversely to the direction of displacement of the feedstock to be treated, a plurality of annular discs spaced apart from one another, each disc comprising a circular central passage substantially coaxial to the soaker, the treated feedstock circulating from the bottom portion upwards in the soaker through the central passages of the various annular discs.

Abstract: A plate-type chemical reactor and method of using same to react two or more mutually separated fluid component streams are disclosed, wherein the reactor contains one or more reactor plates including at least one reaction-chamber reactor plate; at least one reaction chamber formed on a front facial surface of the reaction-chamber reactor plate(s); and at least one heat exchange channel passing through the reaction-chamber reactor plate(s) such that at least one section of heat exchange channel(s) is disposed in a heat exchange relationship with the reaction chamber(s); the reaction chamber containing: a plurality of inlet means for receiving and directing a plurality of mutually separated fluid component streams, a first mixing zone for mixing the separated fluid component streams to form a single at least partially reacted multicomponent fluid stream thereof, and at least one outlet means.

Abstract: The invention relates to a device for dissolving smelt chemicals from recovery boilers, a so-called soda smelt dissolver, and to a process for such dissolution using the device. The device is characterized in that it consists of at least two separate dissolving tanks (I, II), which are connected to each other near the bottom, via a connecting pipe (3), to allow free flow of liquid between them, and of devices for the separate supply to each tank of dissolving liquid and smelt chemicals in dependence on the measured and established chemical concentration in the solution in each of the tanks (I, II), wherein the outlets from the tanks (I, II) can be separately shut off and regulated. The process according to the invention involves using the device and switching over the functions of the different tanks.

Abstract: A high throughput chemical synthesis system utilizing cylindrical reaction vessels is disclosed. Reaction vessels are utilized which include a tubular member adapted for placement of electronically readable identifying indicia thereon. The identifying indicia are representative of reaction conditions within the tubular member and of one or more reagents utilized in a reaction within the tubular members. A method of performing chemical synthesis on solid phase reactive material within a plurality of reaction vessels using a plurality of reaction stages resulting in final products and employing identifying indicia representing the reaction stages is also disclosed. The method includes reading the identifying indicia located on the reaction vessels, reacting one or more reagents within the reaction vessels under particular reaction conditions which may be determined by reading the identifying indicia, thereby synthesizing chemical compounds within the reaction vessels.

Abstract: An improved catalyst assembly for vapor/liquid contact towers. Catalyst media used to promote chemical reactions is secured substantially in the liquid phase of the tower, such as in the lower portion thereof for improving mass transfer efficiency. Unlike previous process tower assemblies, wherein distillation in conjunction with chemical reaction occurs in the vapor phase or in a mixed phase, the present invention substantially confines the reaction step to the liquid phase. In this manner, the reaction is less obstructive to vapor flow within the tower, promoting better mixing and diffusion of the feed components.

Abstract: Apparatus and method for performing a nucleic acid amplification reaction and preferably a polymerase chain reaction (PCR) in a reaction mixture in at least one capillary tube. Several different embodiments are disclosed. One embodiment cycles a sample through a capillary tube loop passing through two thermostatted fluid baths. Another embodiment has the capillary tube routed alternatingly between two heat exchangers to that the sample makes only one pass through the tube. Other embodiments maintain the heat exchangers stationary and translate the samples between them. Still further embodiments maintain the samples stationary and either automatically translate or rotate the heat exchangers past the samples contained within the capillary tubes to perform the thermal cycles necessary for the amplification reaction.

Abstract: A device for the catalytic dehydrogenation of a C.sub.2+ paraffinic hydrocarbon charge is applicable to the synthesis of methyl tert-butyl ether. Effluent coming from the dehydrogenation reactor and containing olefins and water is cooled in at least one heat exchanger (41), saturated with water in a column (3) and sent to a stripping column (10) where it is at least partly put in contact with a recycled aqueous liquid phase containing a solvent, preferably methanol. The compressed gaseous effluent in which the water is thereby inhibited from freezing by the methanol is cooled in a heat exchanger (13) then separated in separator (8) into olefins and into hydrogen. An aqueous liquid phase with methanol is decanted at (8) and recycled in column (10).

Abstract: A device for catalytic dehydrogenation of a C.sub.2+ paraffinic cut with an improved system for cooling the effluent is applicable, for example, to the synthesis of methyl tert-butyl ether. Liquid charge 12 is evaporated in the calandria of a heat exchanger 13 in the optional presence of at least one part recycled hydrogen 15, then optionally compressed in a compressor 14 before being pre-heated in an exchanger 41 by effluent 1 and introduced into a dehydrogenation reactor 40. The effluent cooled in the tubes of exchanger 13 can be mixed with a cryogenic phase 17 resulting from the isentropic expansion of a hydrogen-rich phase separated in a separator 8, the hydrogen optionally being recycled to the calandria of the heat exchanger. The olefins recovered with the unconverted paraffins are stabilized in a column 20.

Abstract: A toy is disclosed for producing a simulated eruption. The toy comprises a container having a first chamber for holding a predetermined quantity of a first reagent and a second chamber for holding a predetermined quantity of a second reagent. The second chamber communicates with an upstanding convergent nozzle terminating at its upper end in an orifice opening to the exterior of the container. When the sidewalls defining the first chamber are squeezed, a portion of the first reagent held therein is forced through a connecting tube into the second chamber, where the first regent reacts with the second reagent to produce gaseous products. The elevated pressure thereby created within the second chamber causes the reagent mixture to be ejected from the nozzle orifice at high velocity. The toy may additionally comprise a simulated volcano landscape having a eruption tube depending from the volcano crater which receives at its lower end the tip of the nozzle.

Abstract: A plate-type chemical reactor and method of using same to react two or more mutually separated fluid component streams are disclosed, wherein the reactor contains one or more reactor plates including at least one reaction-chamber reactor plate; at least one reaction chamber formed on a front facial surface of the reaction-chamber reactor plate(s); and at least one heat exchange channel passing through the reaction-chamber reactor plate(s) such that at least one section of heat exchange channel(s) is disposed in a heat exchange relationship with the reaction chamber(s); the reaction chamber containing: a plurality of inlet means for receiving and directing a plurality of mutually separated fluid component streams, a first mixing zone for mixing the separated fluid component streams to form a single at least partially reacted multicomponent fluid stream thereof, and at least one outlet means.

Abstract: Apparatuses for treating gas streams containing variations in VOC concentration whereby the VOC's are destroyed in a combination non-catalytic/catalytic oxidation system are disclosed. A non-catalytic destruction matrix composed of inert ceramic materials that enhance process mixing and provide thermal inertia for process stability is used when VOC concentrations are high and a catalytic oxidizer is principally used when VOC concentrations are low. The exhaust from the non-catalytic destruction matrix is passed through the catalytic oxidizer to maintain proper catalytic oxidizer operating temperatures. Supplemental fuel and air are added as appropriate upstream or downstream of the non-catalytic oxidizer to maintain proper heat values in each portion of the system.

Abstract: An apparatus for purifying pollutant-containing waste or exhaust air from industrial plants by means of regenerative afterburning includes a heat exchanger in the form of a heat exchanger fill. The material for the heat exchanger fill is a sponge-like foamed ceramic material having open pores. In accordance with another embodiment, the material of the heat exchanger fill may be constituted by ceramic grate plates or grate bodies.

Abstract: An apparatus enabling reaction and post-reaction processing in a single assembly including a reaction chamber and a filtration and/or drying chamber adjacent to one another, the chambers being selectively isolated or in communication. A shaft common to both chambers is capable of rotation and axial movement. An agitator arm is fitted to the shaft in the reaction chamber while a smoothing and pressing arm is fitted to the shaft in the filtration and/or drying chamber. The chambers may be formed in a single cylindrical vessel with an intermediate cross wall providing isolation between the chambers. A U-shaped conduit extends between the chambers and by-passes the cross wall to enable communication between the chambers. The conduit may incorporate a valve/pump to facilitate transfer between the chambers. The shaft is journalled through the cross wall and has a bellows apparatus to protect the bearing from the respective chambers.

Abstract: An apparatus for photochemically oxidizing gaseous volatile or semi-volatile organic compounds includes: a) a reactor vessel having a plurality of reaction chambers provided therein, the reaction chambers having respective chamber lining sidewalls; b) a source of ultraviolet light provided within and along the reaction chambers to oxidize gaseous volatile or semi-volatile organic compounds fed to the reaction chambers into gaseous oxidation products; c) the sidewalls of the reaction chambers comprising a dry porous cementitious and chemically sorbent material, the sorbent material being chemically reactive with the gaseous oxidation products to produce solid reaction products incorporated in the reaction chamber sidewalls; and e) the sidewalls of the reaction chambers comprising a series of baffles mounted relative to the reactor vessel, the baffles defining a serpentine gas flow path within the reactor vessel between a gas inlet and a gas outlet.

Abstract: A reactor arrangement and process for indirectly contacting a reactant stream with a heat exchange stream uses multiple passes of the heat exchange stream in a transverse flow arrangement to control temperature conditions over the width and length of channels through which the reactant passes. The heat transfer coefficient may be varied by changing the number and/or the arrangement of the corrugations along the plates or adding a heat adjustment plate to a channel containing the heat exchange fluid. The reactor arrangement and process of this invention may be used to operate a reactor under isothermal or other controlled temperature conditions. The variation in corrugation arrangements within a single heat exchange section is highly useful in maintaining a desired temperature profile in an arrangement having a cross-flow of heat exchange medium relative to reactants. The corrugations arrangement eliminates or minimizes the typical step-wise approach to isothermal conditions.

Abstract: A device for controlling a liquid flow in a vertically extending pipe is disclosed which includes a plate member horizontally disposed in the pipe for receiving the liquid flow thereon and having an opening to permit the liquid received on the plate member to pass therethrough, a tubular guide downwardly inwardly extending from the periphery of the opening and terminating to form a liquid outlet, and a plurality of partition plates disposed on the tubular guide. Each partition plate has an upper end upwardly protruding from the periphery of the opening and a lower end obliquely downwardly extending from the periphery of the opening along the wall of the tubular guide member, so that a plurality of discrete passages are defined on the tubular guide. A cover plate is provided to cover the passages so that the liquid received on the plate member flows through the passages and is discharged from the liquid outlet of the tubular guide to form a vortex flow.

Abstract: The present invention provides assay methods for performing binding assays, wherein the detectable label is a magnetically responsive material. Direct and indirect, competitive and sandwich assay formats are used to partition the magnetically attractable label between a solid phase and a fluid phase in proportion to the presence or amount of analyte in the test sample. The magnetic responsiveness of the magnetically attractable label in one or both phases results in the exertion of a force upon the label. By determining the extent of the force or influence of the force exerted upon the label, the amount of the analyte in the test sample is determined.

Abstract: The present invention provides devices for performing binding assays. Such devices comprise (i) a reaction vessel where unbound and immobilized magnetically-labeled reagent are produced in relation to the amount of said analyte in said test sample; (ii) a separation means for partitioning said immobilized magnetically-labeled reagent and said bound magnetically-labeled reagent; (iii) a magnetic field generator means for the application of a magnetic field to said magnetically-labeled reagent; and (iv) a measurement means to assess the effect of said magnetic field on said magnetically-labeled reagent as a measure of the presence or amount of said analyte in said test sample. The device provided by the instant invention can run, for example, direct indirect, competitive, inhibition and sandwich assay formats.

Abstract: An acid gas removal process employing a regenerator with an internal flash section is described. The regenerator uses gravitational flow to feed the flash section, eliminating the need for an external flash tank, and charge pump even without vacuum. The internal flash section has a first pressure side, a second pressure side having a lower pressure than the first pressure side during gas flow and a pressure reduction zone disposed therebetween. The pressure drop in the pressure reduction zone is due to liquid flow pressure losses occurring as liquid flows from said first pressure side to said second pressure side. A liquid seal between the first pressure and second pressure sides eliminates the need for a pressure let down valve. Vacuum control is provided by the first pressure side liquid level.

Abstract: Hydrogen sulfide or other gaseous component is removed from a gas stream containing the same by distribution of the gas stream in the form of fine bubbles by a rotary impeller and stationary shroud arrangement at a submerged location in an aqueous iron or other transition metal chelate solution, or other suitable catalyst, contained in an enclosed reaction vessel. Sulfur particles, or other insoluble phase product, of narrow particle size range formed in the reaction are floated off from the iron chelate solution. An oxygen-containing gas stream also is distributed in the form of fine bubbles by a separate rotary impeller and stationary shroud arrangement at a separate submerged location in the iron chelate solution. The second submerged location generally is separated from the first by a baffle extending downwardly in the reaction vessel from a top closure towards a bottom closure.

Abstract: In the manufacture of chemical products, foods, pharmaceuticals and the like, a movable tank (201) mounted on a conveying vehicle (100) movable along conveyance courses (1, 1') between a plurality of stations (11-16) for unit processes such as mixing and reaction is transferred between relative stations by a transferring device provided on the conveying vehicle, to thereby successively perform necessary processes, thus meeting the needs of a multi-product/small-lot production. An automatic connection device is provided for supplying electric power and fluid to the movable tank. Furthermore, when necessary, a traverser device (2) for transferring the movable tank is provided between one conveyance course (1) and another conveyance course (1'). Further, a washing device is provided for washing the movable tank after the completion of the processes.

Abstract: The present invention discloses a method for the enzymatic synthesis of a peptide. A protected peptide having a C-terminal carboxylate group or a protected, N-acyl amino acid having an alpha carboxylate group is reacted with a protected peptide having an N-terminal ammonium group or a protected amino acid having an alpha ammonium group in the presence of a condensation enzyme under conditions in which the carboxylate group and the ammonium group condense to form a protected, uncharged, peptide product. This peptide product is transported across a water-immiscible hydrophobic phase into an aqueous product phase and prevented from back diffusing across the water-immiscible hydrophobic phase. The peptide product can be converted, chemically or enzymatically, to a charged species that cannot back diffuse across the water-immiscible phase into the aqueous reaction phase.

Abstract: A process for turbulently flowing together reactants in uniform proportions in a reactor vessel. A process for producing ethylbenzene by reacting ethylene and benzene in the presence of a catalyst in a reactor vessel from which useful heat generated by the reaction is transferred to a heat transfer medium flowing through the reactor and in which the reaction occurs in a relatively short time period. In one embodiment, polyethylbenzenes produced in the reactor vessel are not recycled into the vessel. A reactor for a reaction of reactant materials that are uniformly and turbulently mixed together.

Abstract: A filter for the separation of impurities or contaminants from a fluid or gaseous medium, especially of harmful components from the exhaust fumes of an internal combustion engine, with a filter body having a plurality of inlet and outlet channels, whereby the inlet channels are separated from the outlet channels by filter walls forming reaction spaces. The filter bodies consist of a plurality of compression molded, high-temperature-resistant filter plates which, arranged one above the other, form a plurality of flow channels between themselves. For the formation of inlet and outlet openings, the channels are each open on one filter body end face and closed on the opposite end face. The channel closure and the connection of adjacent filter plates takes place alternately on each end face by two adjacent filter plates being pushed into and tightly surrounded by stirrup parts which extend over and grip the entire width of the filter plate adjacent end edges.

Abstract: A CO.sub.2 gas generator for a utilization device is located in a housing and chemically generates CO.sub.2 from a chemical reaction between two reagents contained within a common container. The reagents are located in different chambers of the container with a CO.sub.2 accumulation region being included in one of the chambers. A reference pressure source of a predetermined pressure forces the two reagents into contact with each other when the pressure of gas in the CO.sub.2 accumulation region is less than the predetermined pressure whereupon CO.sub.2 is generated in one of the chambers. An output conduit in fluid communication with the CO.sub.2 accumulation region is provided to withdraw the generated gas from the generator. As the CO.sub.2 is withdrawn, the gas pressure drops permitting more mixing of the reagents. When the CO.sub.2 pressure becomes equal to or higher than the predetermined pressure applied by the reference pressure source, the reagents become separate again and gas generation ceases.

Abstract: A process and apparatus for the manufacture of high purity, ultra-fine aluminum nitride powder by the carbo-nitridization of alumina. In the method, agglomerates uniform in both size, chemical composition and porosity are formed containing a stoichiometric mixture of alumina and carbon, and a small amount of catalyst, and furnaced in a controlled manner in a well-mixed two chamber reaction vessel having optional top or bottom fluidizing gas feed to achieve a uniform and consistent level of conversion. Milling of the as-reacted agglomerates under a controlled atmosphere will produce high purity, micron sized aluminum nitride powder. The reactor is an automatically controlled fluid bed reactor for treatment of refractory materials with a hot fluidizing gas having a two chamber design in which the lower furnace chamber and reactor bed are removable from the bottom of the reactor. With unique reactor, unusually high reaction temperatures of up to 2000.degree. C. are obtainable.

Abstract: A disposable CO.sub.2 gas generator cartridge of cylindrical construction and including inner and outer coaxial reagent chambers which are interconnected when installed in a cylindrical pressure vessel and having a top cover assembly including a pusher type activating mechanism which is operated by a cam surface located on a handwheel. The cover assembly connects to a carbonated drink dispenser by means of a quick disconnect coupling activated by the operation of a manually operated pull down lever assembly including the handwheel. Operation of the handwheel acts to start gas generation and also vent the cartridge to atmosphere when spent.

Abstract: A unit in the form of a bubble pack for creating an anaerobic gaseous atmosphere in an upright container and for indicating the presence of the anaerobic atmosphere in the container. One bubble of the pack houses acid-containing ampoules while another bubble houses a tablet which generates hydrogen and carbon dioxide when activated by squeezing the first bubble to crush the ampoules and release the acid. Gas flows from the second bubble, through the first bubble and then into the container and enters still another bubble which houses an ampoule containing a redox color indicating liquid. When the latter ampoule is crushed, the liquid moistens an absorbent pad which changes colors as the atmosphere of the container changes from aerobic to anaerobic. The pack also carries catalyst pellets to promote a reaction between the generated hydrogen and the oxygen in the container.

Abstract: A chemical type CO.sub.2 gas generator for a carbonated drink dispenser, which while embodied in several different implementations, commonly includes a first and a second liquid reagent container with the second reagent container including a reaction chamber for generating a carbonating gas when the two reagents are mixed. The containers are coupled so that the first reagent transfers from the first container to the reaction chamber of the second container when the pressure of the generated gas falls below a predetermined value.