And Alkali Metal Or Alkaline Earth Metal Containing Patents (Class 423/594.2)
  • Publication number: 20130122372
    Abstract: Provided is spinel-type lithium transition metal oxide (LMO) used as a positive electrode active material for lithium battery, said LMO being capable of simultaneously achieving all output characteristics (rate characteristics), high temperature cycle life characteristics, and rapid charging characteristics. The disclosed is spinel-type lithium transition metal oxide including, besides Li and Mn, one or more elements selected from a group consisting of Mg, Ti, Ni, Co, and Fe, and having crystallite size of between 200 nm and 1000 nm and strain of 0.0900 or less. Because the crystallite size is markedly large, oxygen deficiency is markedly little, and the structure is strong, when the LMO is used as a positive electrode active material for lithium secondary batteries, all output characteristics (rate characteristics), high temperature cycle life characteristics, and rapid charging characteristics can be achieved simultaneously.
    Type: Application
    Filed: July 13, 2011
    Publication date: May 16, 2013
    Applicant: Mitsui Mining & Smelting Co., Ltd.
    Inventors: Shinya Kagei, Keisuke Miyanohara, Yoshimi Hata, Yasuhiro Ochi, Tetsuya Mitsumoto
  • Publication number: 20130115160
    Abstract: Processing techniques for forming a textured hexagonal ferrite materials such as Z-phase barium cobalt ferrite Ba3Co2Fe24O41 (Co2Z) to enhance the resonant frequency and other magnetic properties of the material for high frequency applications are provided. The processing techniques include magnetic texturing by using fine grain particles and sintering the material at a lower temperature than conventional firing temperatures to inhibit reduction of iron. The processing techniques also may include aligning M-phase (BaFe12O19 uniaxial magnetization) with non-magnetic additives in a static magnetic field and reacting with BaO source and CoO to form Z-phase (Ba3Me2Fe24O42). In some implementations, processing techniques includes aligning Co2Z phase (planar magnetization) with magnetic texturing occurring in a rotating magnetic field.
    Type: Application
    Filed: December 7, 2011
    Publication date: May 9, 2013
    Applicant: SKYWORKS SOLUTIONS, INC.
    Inventor: Michael D. Hill
  • Patent number: 8425679
    Abstract: It is the object of the invention to provide a cement admixture, and a cement composition that can impart good enough rustproofness to reinforcing bars in hardened cement concrete, and can have resistance to penetration of chloride ions entering from the outside, prevent the hardened cement concrete from getting porous due to reduced leaching of Ca ions and have a self-recovery capability. The invention provides a cement admixture characterized by containing a calcium ferroaluminate compound comprising a CaO—Al2O3—Fe2O3 system, and having a Fe2O3 content of 0.5 to 15% by mass and a CaO.2Al2O3 structure with a CaO/Al2O3 molar ratio ranging from 0.15 to 0.7.
    Type: Grant
    Filed: November 25, 2010
    Date of Patent: April 23, 2013
    Assignee: Denki Kagaku Kogyo Kabushiki Kaisha
    Inventors: Taiichiro Mori, Kazuto Tabara, Kenji Yamamoto, Minoru Morioka, Takayuki Higuchi
  • Patent number: 8419967
    Abstract: A perovskite oxide represented by a general expression, (Aa, Bb)(Cc, Dd, Xx)O3. (where, A: an A-site element, A=Bi, 0<a, B: one or more types of A-site elements, 0?b<1.0, C: an B-site element, C=Fe, 0 <c<1.0, D: one or more types of B-site elements, 0?d<1.0, 0<b+d, X: one or more types of B-site elements, the average valence of which is greater than the average valence of C and D in chemical formula, 0<x<1.0, (average valence of A-site in chemical formula) +(average valence of B-site in chemical formula)>6.0, O: oxygen, and standard molar ratio among A-site elements, B-site elements, and oxygen is 1:1:3, but it may deviate from the standard within a range in which a perovskite structure is possible.
    Type: Grant
    Filed: July 16, 2009
    Date of Patent: April 16, 2013
    Assignee: FUJIFILM Corporation
    Inventors: Tsutomu Sasaki, Yukio Sakashita, Hiroyuki Kobayashi
  • Patent number: 8394299
    Abstract: Provided is a transition metal precursor comprising a composite transition metal compound represented by Formula I, as a transition metal precursor used in the preparation of a lithium-transition metal composite oxide: M(OH1?x)2??(1) wherein M is two or more selected from the group consisting of Ni, Co, Mn, Al, Cu, Fe, Mg, B, Cr and transition metals of period 2 in the Periodic Table of the Elements; and 0<x<0.5.
    Type: Grant
    Filed: April 2, 2009
    Date of Patent: March 12, 2013
    Assignee: LG Chem, Ltd.
    Inventors: Ho Suk Shin, Sung Kyun Chang, Hong-Kyu Park, Seung Tae Hong, Sinyoung Park, Youngsun Choi
  • Patent number: 8383077
    Abstract: A method of stabilizing a metal oxide or lithium-metal-oxide electrode comprises contacting a surface of the electrode, prior to cell assembly, with an aqueous or a non-aqueous acid solution having a pH greater than 4 but less than 7 and containing a stabilizing salt, for a time and at a temperature sufficient to etch the surface of the electrode and introduce stabilizing anions and cations from the salt into said surface. The structure of the bulk of the electrode remains unchanged during the acid treatment. The stabilizing salt comprises fluoride and at least one cationic material selected from the group consisting of ammonium, phosphorus, titanium, silicon, zirconium, aluminum, and boron.
    Type: Grant
    Filed: February 14, 2012
    Date of Patent: February 26, 2013
    Assignee: UChicago Argonne, LLC
    Inventors: Michael M. Thackeray, Sun-Ho Kang, Christopher S. Johnson
  • Patent number: 8372441
    Abstract: The subject invention concerns methods for preparing alkaline earth ferrates and the preparation of hemostatic compositions from alkaline earth ferrates. In one embodiment, the alkaline earth ferrate is strontium ferrate. In one embodiment, methods of the invention comprise heat treating mixtures of alkaline earth oxides and/or peroxides with iron oxides, such as hematite or magnetite. The subject invention also concerns hemostatic compositions produced using metallic oxides that are reacted with alkaline earth oxides and/or peroxides and the methods used to produce the hemostatic compositions.
    Type: Grant
    Filed: November 30, 2009
    Date of Patent: February 12, 2013
    Assignee: Biolife, LLC
    Inventors: John Alfred Thompson, John Hen
  • Patent number: 8357309
    Abstract: Single crystal and polycrystal oxoruthenates having the generalized compositions (Baz,Sr1?z)FexCoyRu6?(x+y)O11 (1?(x+y)?5; 0?z?1) and (Ba,Sr)M2±xRu4?xO11 (M=Fe,Co) belong to a novel class of ferromagnetic semiconductors with applications in spin-based field effect transistors, spin-based light emitting diodes, and magnetic random access memories.
    Type: Grant
    Filed: April 3, 2008
    Date of Patent: January 22, 2013
    Assignee: University of Kentucky Research Foundation
    Inventors: Larysa Shlyk, Sergly Alexandrovich Kryukov, Lance Eric De Long, Barbara Schüpp-Niewa, Rainer Niewa
  • Patent number: 8323612
    Abstract: The present invention relates to lithium manganate particles having a primary particle diameter of 1 to 8 ?m and forming substantially single-phase particles, which have a composition represented by the following chemical formula: Li1+xMn2-x-yY1yO4+Y2 in which Y1 is at least one element selected from the group consisting of Ni, Co, Mg, Fe, Al, Cr and Ti; Y2 is P and is present in an amount of 0.01 to 0.6 mol % based on Mn; and x and y satisfy 0.03?x?0.15 and 0.05?y?0.20, respectively, and which lithium manganate particles have a specific surface area of the lithium manganate particles of 0.3 to 0.9 m2/g (as measured by BET method); and have an average particle diameter (D50) of the lithium manganate particles of 3 to 10 ?m. A positive electrode active substance of a lithium ion secondary battery using the lithium manganate particles of the present invention has a high output and is excellent in high-temperature stability.
    Type: Grant
    Filed: December 26, 2008
    Date of Patent: December 4, 2012
    Assignee: Toda Kogyo Corporation
    Inventors: Kazumichi Koga, Masayuki Uegami, Kazutoshi Ishizaki, Hideaki Sadamura
  • Publication number: 20120301390
    Abstract: A method for producing a lithium mixed metal oxide, which includes mixing a lithium compound, metallic Ni or a compound thereof, and one or more transition metals selected from the group consisting of Mn, Co, Ti, Cr and Fe or a compound thereof; and calcining the obtained raw material mixture under an atmosphere of the concentration of carbon dioxide of from 1% by volume to 15% by volume at 630° C. or higher.
    Type: Application
    Filed: December 24, 2010
    Publication date: November 29, 2012
    Applicant: SUMITOMO CHEMICAL COMPANY, LIMITED
    Inventors: Yoshihiro Kawakami, Ryuji Matsushita, Satoshi Shimano
  • Publication number: 20120196130
    Abstract: Spherical ferrite nanoparticles produced by a method that includes the steps of: preparing a first aqueous solution containing a disaccharide, an alkaline, an oxidation agent, seed particles and divalent iron ions; and conducting particle growth in the first aqueous solution to produce the spherical ferrite nanoparticles.
    Type: Application
    Filed: April 2, 2012
    Publication date: August 2, 2012
    Applicants: TAMAGAWA SEIKI KABUSHIKI KAISHA, Tokyo Institute of Technology
    Inventors: Masanori ABE, Hiroshi Handa, Takashi Nakagawa, Masaru Tada, Ryuichi Shimazu, Toshiyuki Tanaka
  • Patent number: 8158071
    Abstract: A unit for use within a furnace which is absent a controlled atmosphere, for carrying out a synthesizing process for synthesizing precursors to form a synthesized product at elevated temperatures. The unit consists of a vessel, having at least one opening, for containing materials of the synthesizing process, and a solid reductive material. The materials of the synthesizing process are separated from the atmosphere of the furnace by either the vessel or the reductive material. The unit is especially suited for synthesizing LiFePO4 from Fe2O3, Li2CO3, carbon black, and phosphoric acid precursors.
    Type: Grant
    Filed: April 29, 2006
    Date of Patent: April 17, 2012
    Inventors: Chun-Chieh Chang, Tsun-Yu Chang
  • Patent number: 8153097
    Abstract: A method for manufacturing ferrite powder comprises a step (a) of causing a precursor, obtained by a liquid-phase reaction method, to pass through a sieve with openings of 2 mm or less, and a step (b) of causing free fall, through the interior of a furnace tube heated to the range 750 to 1250° C. by a heater, of the precursor which has passed through the sieve. In the process of causing free fall through the interior of the furnace tube heated by the heater, ferrite powder, which is a single phase of hexagonal ferrite, is obtained by heating the precursor to a prescribed temperature and holding the precursor at the prescribed temperature.
    Type: Grant
    Filed: September 25, 2008
    Date of Patent: April 10, 2012
    Assignee: TDK Corporation
    Inventor: Mamoru Satoh
  • Publication number: 20120080638
    Abstract: An aspect of the present invention relates to a magnetic recording medium comprising a magnetic layer comprising ferromagnetic powder and a binder, wherein the ferromagnetic powder is magnetic powder comprised of gathering magnetic particles, the magnetic particles are a reduction product of hexagonal ferrite magnetic particles wherein a ratio Dc/Dtem of a crystallite size Dc obtained from a diffraction peak of a (220) plane to a particle diameter Dtem in a direction perpendicular to a (220) plane as determined by a transmission electron microscope ranges from 0.90 to 0.75.
    Type: Application
    Filed: September 23, 2011
    Publication date: April 5, 2012
    Applicant: FUJIFILM CORPORATION
    Inventor: Yasushi HATTORI
  • Patent number: 8137844
    Abstract: A method for manufacturing a cathode active material for a lithium rechargeable battery, including: selecting a first metal compound from a group consisting of a halide, a phosphate, a hydrogen phosphate and a sulfate of Mg or Al; selecting a second metal compound from a group consisting of an oxide, a hydroxide and a carbonate of Mg or Al; combining the first metal compound and the second metal compound to obtain a metal compound, the metal compound containing either Mg or Al atoms; mixing a lithium compound, a transition metal compound and the metal compound to obtain a mixture; and sintering the mixture.
    Type: Grant
    Filed: November 16, 2007
    Date of Patent: March 20, 2012
    Assignee: Nippon Chemical Industrial Co., Ltd.
    Inventors: Hidekazu Awano, Minoru Fukuchi, Yuuki Anbe
  • Patent number: 8123973
    Abstract: A method of manufacturing magnetic material is described hereinafter. Firstly, Fe(NO3)3.9H2O and other metal nitrate compounds are dissolved in an alcohol solvent to form a mixed solution. Secondly, the mixed solution is heated to 60˜100 degrees Centigrade. Next, citric acid is added into the mixed solution for being reacted with each other under the temperature of 60˜100 degrees Centigrade so that can make the alcohol solvent volatilized and further obtain brown solid powder. Lastly, the solid powder is further heated for a period of time so as to obtain the magnetic material having a fluffy powdery form.
    Type: Grant
    Filed: December 10, 2008
    Date of Patent: February 28, 2012
    Assignee: Cheng Uei Precision Industry Co.
    Inventor: Chih-Hao Huang
  • Publication number: 20120015189
    Abstract: A bonded magnet is required to have a large energy product, which is the product of magnetization Br and coercive force Hc. However, in a ferrite powder for a bonded magnet, when the particle diameter is reduced to improve the coercive force, the packing properties are impaired, and the Br is lowered. When the particle diameter is increased to improve the magnetization, the coercive force is lowered. Therefore, to increase the energy product, both the Br and Hc must be increased. A ferrite powder that has a large particle size, is composed of smooth crystals, and suffers only a small reduction in coercive force even after pressurization is obtained by mixing a fine ferrite powder having a small particle size with a ferrite powder calcined at a temperature of 1050° C. to 1300° C. in the presence of a chloride at its saturated vapor pressure and then annealing the mixture at 800° C. to 1100° C. A bonded magnet produced using the powder has an energy product of 2.0 MGOe or more.
    Type: Application
    Filed: April 9, 2010
    Publication date: January 19, 2012
    Applicant: DOWA Electronics Materials Co., Ltd.
    Inventors: Shinichi Suenaga, Kouji Hirata, Satoru Tsuboi, Keisuke Ayabe, Kazuyosi Horii
  • Patent number: 8088349
    Abstract: Disclosed is a clean method for preparing layered double hydroxides (LDHs), in which hydroxides of different metals are used as starting materials for production of LDHs by atom-economical reactions. The atom efficiency of the reaction is 100% in each case because all the atoms of the reactants are converted into the target product since only M2+(OH)2, M3+(OH)3, and CO2 or HnAn? are used, without any NaOH or other materials. Since there is no by-product, filtration or washing process is unnecessary. The consequent reduction in water consumption is also beneficial to the environment.
    Type: Grant
    Filed: September 11, 2007
    Date of Patent: January 3, 2012
    Assignee: Beijing University of Chemical Technology
    Inventors: Xue Duan, Dianqing Li, Zhi Lv, Yanjun Lin, Xiangyu Xu
  • Publication number: 20110303869
    Abstract: The present invention relates to cubic or octahedral ferrite nanoparticles and a method for preparing the same. In particular, the present invention is directed to a ferrite nanocube which is superparamagnetic or ferromagnetic, and a method for preparing a ferrite nanocube, comprising heating a mixture of a metal precursor, a surfactant and a solvent.
    Type: Application
    Filed: September 25, 2009
    Publication date: December 15, 2011
    Applicant: SNU R&DB FOUNDATION
    Inventors: Taeghwan Hyeon, Dokyoon Kim
  • Patent number: 8048398
    Abstract: Process for preparing a mixed metal oxide powder, in which oxidizable starting materials are evaporated and oxidized, the reaction mixture is cooled after the reaction and the pulverulent solids are removed from gaseous substances, wherein as starting materials, at least one pulverulent metal and at least one metal compound, the metal and the metal component of the metal compound being different and the proportion of metal being at least 80% by weight based on the sum of metal and metal component from metal compound, together with one or more combustion gases, are fed to an evaporation zone of a reactor, where metal and metal compound are evaporated completely under nonoxidizing conditions, subsequently, the mixture flowing out of the evaporation zone is reacted in the oxidation zone of this reactor with a stream of a supplied oxygen-containing gas whose oxygen content is at least sufficient to oxidize the starting materials and combustion gases completely.
    Type: Grant
    Filed: May 9, 2007
    Date of Patent: November 1, 2011
    Assignee: Evonik Degussa GmbH
    Inventors: Stipan Katusic, Guido Zimmermann, Michael Kraemer, Peter Kress, Horst Miess
  • Patent number: 8034319
    Abstract: A process for producing a complex oxide containing the valuable metal and an alkali (earth) metal salt, which comprising co-milling a mixture of the valuable metal oxide and/or a precursor thereof, or a mixture of a substance containing the valuable metal oxide and/or a precursor thereof, with an alkali (earth) metal salt to a particle size of the valuable metal oxide or a substance containing the oxide, of 10 ?m or less, and heating the co-milled product to a temperature of at least 200° C. so as to induce a solid-phase reaction of the valuable metal oxide with an alkali (earth) metal salt.
    Type: Grant
    Filed: May 28, 2004
    Date of Patent: October 11, 2011
    Assignee: JFE Mineral Co., Ltd.
    Inventor: Hidetaka Suginobe
  • Publication number: 20110151283
    Abstract: Thin-film lithium-based batteries and electrochromic devices (10) are fabricated with positive electrodes (12) comprising a nanocomposite material composed of lithiated metal oxide nanoparticles (40) dispersed in a matrix composed of lithium tungsten oxide.
    Type: Application
    Filed: August 31, 2007
    Publication date: June 23, 2011
    Applicant: ALLIANCE FOR SUSTAINABLE ENERGY, LLC.
    Inventors: Dane T. Gillaspie, Se-Hee Lee, C. Edwin Tracy, John Roland Pitts
  • Patent number: 7964175
    Abstract: A procedure for obtaining mixed multimetallic oxides derived from hydrotalcite type compounds, characterized in that the laminar metallic hydroxides obtained are constituted by three or four metallic cations, forming part of the sheets of the hydrotalcite type material represented by the formula: [M(II)1?x?y?zM(II)?xM(III)yM(III)?z(OH)2](An?y+z/n).mH2O. by a process comprising: (1) preparing an aqueous or organic solution containing three or more cations; (2) preparing an alkaline solution; (3) slowly combining solutions (1) and (2) to cause the co-precipitation of the cations in the form of hydroxides; (4) washing the precipitate containing the hydrotalcites with water, until removal of the non-precipitated ions; (5) drying; and (6) calcining the hydrotalcites.
    Type: Grant
    Filed: January 6, 2006
    Date of Patent: June 21, 2011
    Assignee: Instituto Mexico del Petroleo
    Inventors: Jaime Sánchez Valente, Esteban López Salinas, Manuel Sánchez Cantú, Francisco Hernández Beltrán
  • Patent number: 7935270
    Abstract: Provided is a cathode active material having a layered-spinel composite structure lithium metal oxide represented by Formula 1: xLi2MO3-yLiMeO2-zLi1+dM?2?dO4??(1) where x+y+z=1 where 0<x<1, 0<y<1 and 0<z<1; 0?d?0.33; M includes at least one metal selected from the group consisting of Mn, Ti, and Zn; Me includes at least one metal selected from the group consisting of Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Al, Mg, Zr, and B; and M? includes at least one metal selected from the group consisting of Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Al, Mg, Zr, and B. The cathode active material has a layered-spinel composite structure in which lithium can be intercalated and deintercalated so that a lithium battery including the cathode active material shows high initial coulombic efficiency and a high capacity retention ratio.
    Type: Grant
    Filed: August 17, 2007
    Date of Patent: May 3, 2011
    Assignee: Samsung SDI Co., Ltd
    Inventor: Kyu-sung Park
  • Patent number: 7927506
    Abstract: Cathode active materials including lithium composite metal oxides having layered-spine composite structures are provided. The lithium metal oxide may be represented by the formula xLi2MO3-yLiMeO2-zLi1+dM?2?dO4, in which 0?d?0.33, 0<x<1, 0<y<1, 0<z<1 and x+y+z=1. In the formula M is selected from Mn, Ti, Zn, and combinations thereof. Me is selected from Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Al, Mg, Zr, B and combinations thereof. M? is selected from Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Al, Mg, Zr, B, and combinations thereof. The cathode active materials have layered-spinel composite structures in which lithium can be intercalated and deintercalated. Lithium batteries including the cathode active materials show high initial coulombic efficiencies and high capacity retention ratios.
    Type: Grant
    Filed: September 21, 2007
    Date of Patent: April 19, 2011
    Assignee: Samsung SDI Co., Ltd.
    Inventor: Kyu-sung Park
  • Publication number: 20110076212
    Abstract: An after-treatment system architecture and method for oxidizing the nitric oxide component of a gas stream.
    Type: Application
    Filed: November 30, 2010
    Publication date: March 31, 2011
    Applicant: GM GLOBAL TECHNOLOGY OPERATIONS, INC.
    Inventors: Steven J. Schmieg, Chang H. Kim, Gongshin Qi, Wei Li, David B. Brown
  • Patent number: 7910084
    Abstract: A compound oxide manufacturing method includes: dispersing micelles, in each of which an aqueous phase is formed, in an oil phase; producing primary particles of a precursor of compound oxide in the aqueous phases in the micelles; synthesizing secondary particles by causing the primary particles to aggregate; and causing the secondary particles to aggregate by breaking the dispersion state of the micelles, or by causing the micelles to coalesce. In particular, polarization is produced in each of the micelles with the use of a cation having an ionic radius larger than that of a metal ion at least when the secondary particles are synthesized in the micelles.
    Type: Grant
    Filed: August 29, 2007
    Date of Patent: March 22, 2011
    Assignee: Toyota Jidoshi Kabushiki Kaisha
    Inventors: Shinichi Takeshima, Akio Koyama
  • Patent number: 7897128
    Abstract: The present invention provides a process for making a complex metal oxide comprising the formula AxByOz. The process comprises the steps of: (a) reacting in solution at a temperature of between about 75° C. to about 100° C. at least one water-soluble salt of A, at least one water-soluble salt of B and a stoichiometric amount of a carbonate salt or a bicarbonate salt required to form a mole of a carbonate precipitate represented by the formula AxBy(CO3)n, wherein the reacting is conducted in a substantial absence of carbon dioxide to form the carbonate precipitate and wherein the molar amount of carbonate salt or bicarbonate salt is at least three times the stoichiometric amount of carbonate or bicarbonate salt required to form a mole of the carbonate precipitate; and (b) reacting the carbonate precipitate with an oxygen containing fluid under conditions to form the complex metal oxide.
    Type: Grant
    Filed: April 20, 2007
    Date of Patent: March 1, 2011
    Assignee: Air Products and Chemicals, Inc.
    Inventors: Robert Quinn, Diwakar Garg, Frederick Carl Wilhelm, Terry Lee Slager
  • Publication number: 20110044876
    Abstract: A method for the decomposition of one or more metal oxide precursor compounds, at least one of which is a metal carboxylate salt, to a metal oxide or mixed metal oxide by contacting the metal oxide precursor compound or compounds with an aqueous reaction mixture at a pH, pressure and temperature effective to decompose all metal oxide precursor compounds, wherein the temperature is between about room temperature and about 350° C. and the contact duration is effective to decompose all metal oxide precursor compounds to form an essentially pure metal oxide or mixed metal oxide.
    Type: Application
    Filed: November 26, 2008
    Publication date: February 24, 2011
    Applicant: Rutgers University
    Inventors: Richard E. Riman, Vahit Atakan
  • Publication number: 20110033368
    Abstract: Methods of forming a nanocrystal are provided. The nanocrystal may be a binary nanocrystal of general formula M1A or of general formula M1O, a ternary nanocrystal of general formula M1M2A, of general formula M1AB or of general formula M1M2O or a quaternary nanocrystal of general formula M1M2AB. M1 is a metal of Groups II-IV, Group VII or Group VIII of the PSE. A is an element of Group VI or Group V of the PSE. O is oxygen. A homogenous reaction mixture in a non-polar solvent of low boiling point is formed, that includes a metal precursor containing the metal M1 and, where applicable M2. For an oxygen containing nanocrystal the metal precursor contains an oxygen donor. Where applicable, A is also included in the homogenous reaction mixture. The homogenous reaction mixture is under elevated pressure brought to an elevated temperature that is suitable for forming a nanocrystal.
    Type: Application
    Filed: October 3, 2008
    Publication date: February 10, 2011
    Applicant: AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH
    Inventors: Enyi Ye, Yin Win Khin, Mingyong Han
  • Publication number: 20110014301
    Abstract: A mixed metal compound for pharmaceutical use is free from aluminium and has a phosphate binding capacity of at least 30%, by weight of the total weight of phosphate present, over a pH range of from 2-8. The compound is especially useful for treatment of hyperphosphataemia. The metals are preferably iron (III) and at least one of calcium, magnesium, lanthanum and cerium. A metal sulphate for pharmaceutical use is selected from at least one of calcium, lanthanum and cerium sulphate compounds and has a phosphate binding capacity of at least 30% by weight of the total phosphate present, over a pH range from 2-8.
    Type: Application
    Filed: July 1, 2010
    Publication date: January 20, 2011
    Applicant: INEOS HEALTHCARE LIMITED
    Inventors: Norman B. Roberts, Maurice Webb, Benjamin J. Rankin
  • Patent number: 7867472
    Abstract: An insulating target material for obtaining a conductive complex oxide film represented by a general formula ABO3. The insulating target material includes: an oxide of an element A; an oxide of an element B; an oxide of an element X; and at least one of an Si compound and a Ge compound, the element A being at least one element selected from La, Ca, Sr, Mn, Ba, and Re, the element B being at least one element selected from Ti, V, Sr, Cr, Fe, Co, Ni, Cu, Ru, Ir, Pb, and Nd, and the element X being at least one element selected from Nb, Ta, and V.
    Type: Grant
    Filed: January 19, 2007
    Date of Patent: January 11, 2011
    Assignee: Seiko Epson Corporation
    Inventors: Koji Ohashi, Takeshi Kijima, Setsuya Iwashita
  • Publication number: 20100310935
    Abstract: The invention relates to materials for use as electrodes in an alkali-ion secondary (rechargeable) battery, particularly a lithium-ion battery. The invention provides transition-metal compounds having the ordered-olivine, a modified olivine, or the rhombohedral NASICON structure and the polyanion (PO4)3? as at least one constituent for use as electrode material for alkali-ion rechargeable batteries.
    Type: Application
    Filed: August 20, 2010
    Publication date: December 9, 2010
    Inventors: Michel B. Armand, John B. Goodenough, Akshaya K. Padhi, Kirakadu S. Nanjundaswamy, Christian Masquelier
  • Patent number: 7846416
    Abstract: Anitrate-nitrogen-reducing agent for a farm product, comprising as an active ingredient a hydroxide solid solution represented by the formula (1), [(M12+)1-x(M22+)x]1-z(M3+)z(OH)2(An?)z/n·mH2O??(1) wherein M12+ represents Ca and/or Mg, M22+ represents at least one essential mineral selected from Fe, Mn, Zn, Cu, Ni and Co, M3+ represents at least one trivalent metal, An? represents an anion having a valence of n, x is a positive number in the range of 0<x<0.5, m is 0 or a positive number in the range of 0?m<10, z is a positive number in the range of 0<z<0.4, and n is a positive number in the range of 1?n?10, and/or the formula (2), (M12+)1-x(M22+)x(OH)2??(2) wherein M12+, x and M22+ are as defined in the formula (1).
    Type: Grant
    Filed: November 2, 2005
    Date of Patent: December 7, 2010
    Assignee: Kabushiki Kaisha Kaisui Kagaku Kenkyujo
    Inventor: Shigeo Miyata
  • Patent number: 7815888
    Abstract: Disclosed is a process for producing a secondary battery cathode material by calcining raw materials. The process is characterized by calcining the raw materials together with one or more substances, which are selected from the group consisting of hydrogen, water and water vapor, and conductive carbon and/or a substance, which can form conductive carbon by pyrolysis, added thereto. As crystals of the secondary battery cathode material obtained by this process have been controlled fine sizes, the secondary battery cathode material promotes movements of ions of an alkali metal led by lithium between the interiors of grains of the cathode material and an electrolyte to suppress polarization in an electrode reaction, and further, increases an area of contact between the positive material and a conductivity-imparting material to provide improved conductivity so that improvements are assured in voltage efficiency and specific battery capacity.
    Type: Grant
    Filed: July 31, 2002
    Date of Patent: October 19, 2010
    Assignees: Mitsui Engineering & Shipbuilding Co., Ltd.
    Inventors: Naoki Hatta, Shigeto Okada, Jun-Ichi Yamaki
  • Patent number: 7811501
    Abstract: A mold which is processed by ion beam irradiation or electron beam irradiation and in which a throughput of the mold is high and a decrease in the throughput or electrostatic discharge due to charging does not occur, a method of producing the mold, and a method of producing a molded article produced using the mold. When molding a plastic resin, at least one of a cavity and a core is provided on the surface of a conductive glass substrate. A method of producing a mold for molding a plastic resin or the like includes forming at least one of a cavity and a core by irradiating an ion beam on the surface of a conductive vanadate glass substrate that contains vanadium pentoxide (V2O5) as a main component and that has an electric conductivity in the range of 1.0×10?1 to 1.0×10?8 S/cm.
    Type: Grant
    Filed: September 5, 2005
    Date of Patent: October 12, 2010
    Assignee: Kitakyushu Foundation for the Advancement of Industry, Science and Technology
    Inventors: Tetsuaki Nishida, Ken-ichi Kobayashi, Akira Morishige
  • Patent number: 7807128
    Abstract: Multimetallic anionic clays (MACs) are prepared using economical raw materials or reactants and a procedure for obtaining a series of multimetallic mixed oxides derived from the thermal decomposition of the MACs which comprises: (1) dissolving water-soluble bimetallic and/or trimetallic sources in water, (2) dispersing and homogenizing separate water-insoluble divalent and/or trivalent metal precursors with a high-speed stirrer in order to obtain small and reactive particles; depending on the nature of the water-insoluble divalent and/or trivalent metal precursors, this process can be adjusted to a desired pH, (3) adding the suspension obtained in (2) to solution (1) with the reaction medium still dispersed to facilitate solid particle's reduction/dissociation, and (4) afterwards the slurry is aged for several hours and finally dried. This process enables raw materials or reactants to be easily handled, and eliminates unit operations involving product washing and/or purification steps.
    Type: Grant
    Filed: October 29, 2007
    Date of Patent: October 5, 2010
    Assignee: Instituto Mexicano del Petroleo
    Inventors: Jaime Sanchez-Valente, Esteban Lopez-Salinas, Manuel Sanchez-Cantu
  • Publication number: 20100248032
    Abstract: A lithium mixed metal oxide comprising Ni, Mn and Fe and having a BET specific surface area of 2 m2/g or more and 30 m2/g or less. A method of producing a lithium mixed metal oxide, comprising bringing an aqueous solution containing Ni, Mn, Fe and Cl into contact with an alkali to obtain a coprecipitate, and calcining a mixture of the coprecipitate and a lithium compound by maintaining the mixture at a temperature of lower than 900° C. A positive electrode active material for nonaqueous electrolyte secondary battery, comprising the lithium mixed metal oxide described above or the lithium mixed metal oxide obtained by the method of producing a lithium mixed metal oxide described above as a main ingredient. A positive electrode for nonaqueous electrolyte secondary battery having the positive electrode active material for nonaqueous electrolyte secondary battery described above. A nonaqueous electrolyte secondary battery having the positive electrode for nonaqueous electrolyte secondary battery described above.
    Type: Application
    Filed: September 26, 2008
    Publication date: September 30, 2010
    Inventors: Cedric Pitteloud, Yuichiro Imanari, Kenji Nakane
  • Publication number: 20100246063
    Abstract: An aspect of the present invention relates to a method of manufacturing a hexagonal ferrite magnetic powder comprising preparing a melt by melting a starting material mixture comprising a hexagonal ferrite-forming component and a glass-forming component; rapidly cooling the melt to obtain an amorphous material comprising 0.3 to 2.0 weight percent of carbon atoms; heating the amorphous material to a temperature range of 580 to 700° C. and maintaining the amorphous material within the temperature range to precipitate hexagonal ferrite magnetic particles; and collecting the hexagonal ferrite magnetic particles precipitated.
    Type: Application
    Filed: March 30, 2010
    Publication date: September 30, 2010
    Applicant: FUJIFILM CORPORATION
    Inventors: Shiho KAMISAWA, Toshio TADA, Nobuo YAMAZAKI
  • Patent number: 7803348
    Abstract: Oxygen is reduced in the presence of a catalyst at the cathode of an alkaline-electrolyte fuel cell. Catalysts of the formula Sr3?xA1+xCo4?yByO10.5?z wherein ?0.6?x?1.0; 0?y?3; and ?1.5?z?0.5; wherein A represents Eu, Gd, Tb, Dy, Ho, or Y; and wherein B represents Fe, Ga, Cu, Ni, Mn, and Cr, demonstrate high catalytic activity and high chemical stability when used as the oxygen-reduction catalyst in alkaline fuel cells.
    Type: Grant
    Filed: February 10, 2006
    Date of Patent: September 28, 2010
    Assignee: Horizon Fuel Cells, LLC
    Inventors: Evgeny V. Antipov, Galina A. Tsirlina, Sergey Y. Istomin, Oleg A. Drozhzhin, Eduard E. Levin
  • Patent number: 7799351
    Abstract: A mixed metal compound for pharmaceutical use is free from aluminium and has a phosphate binding capacity of at least 30%, by weight of the total weight of phosphate present, over a pH range of from 2-8. The compound is especially useful for treatment of hyperphosphataemia. The metals are preferably iron (III) and at least one of calcium, magnesium, lanthanum and cerium. A metal sulphate for pharmaceutical use is selected from at least one of calcium, lanthanum and cerium sulphate compounds and has a phosphate binding capacity of at least 30% by weight of the total phosphate present, over a pH range from 2-8.
    Type: Grant
    Filed: July 10, 2003
    Date of Patent: September 21, 2010
    Assignee: INEOS Healthcare Limited
    Inventors: Norman B. Roberts, Maurice Webb, Benjamin J. Rankin
  • Patent number: 7799459
    Abstract: A compound for use as active material of a positive electrode of a lithium-ion cell. This compound has an average discharge voltage above 4.5V in relation to the Li+/Li couple of approximately 4.7V. The compound includes: a) a spinel-type crystalline phase of formula LiaNiII0.5?xMnIII2xMnIV1.5?x?yMyO4 in which elements Ti and Al, or a mixture of these; 0.8<a<1.3; 0<x?0.15; 0<y?0.15; b) a cubic crystalline phase of formula Li1?tNi1+tO in which 0?t?1; and c) a rhomboedric crystalline phase of formula Li1?ZNi1+zO2 in which 0?z?1.
    Type: Grant
    Filed: May 24, 2007
    Date of Patent: September 21, 2010
    Assignee: Saft Groupe SA
    Inventors: Jean-Paul Peres, Stephane Gillot, Frederic Chouquais, Claudette Audry, Andre Lecerf
  • Patent number: 7759006
    Abstract: Disclosed is a compound represented by the following formula 1. A lithium secondary battery using the same compound as electrode active material, preferably as cathode active material, is also disclosed. LiMP1-xAxO4??[Formula 1] wherein M is a transition metal, A is an element having an oxidation number of +4 or less and 0<x<1. The electrode active material comprising a compound represented by the formula of LiMP1-xAxO4 shows excellent conductivity and charge/discharge capacity compared to LiMPO4.
    Type: Grant
    Filed: July 14, 2005
    Date of Patent: July 20, 2010
    Assignee: LG Chem, Ltd.
    Inventors: Sung Kyun Chang, Jeong Ju Cho
  • Patent number: 7749321
    Abstract: The present invention is directed to pigment compositions, thick film black pigment compositions, conductive single layer thick film compositions, black electrodes made from such black conductive compositions and methods of forming such electrodes, and to the uses of such compositions, electrodes, and methods in flat panel display applications, including alternating-current plasma display panel devices (AC PDP).
    Type: Grant
    Filed: June 28, 2007
    Date of Patent: July 6, 2010
    Assignee: E. I. du Pont de Nemours and Company
    Inventors: Jerome D. Smith, Pedro A. Jimenez, Tony Jackson
  • Publication number: 20100167078
    Abstract: Disclosed are a method for fabricating nanopowders, nano ink containing the nanopowders and micro rods, and nanopowders containing nanoparticles, nano clusters or mixture thereof, milled from nano fiber composed of at least one kind of nanoparticles selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, nano ink containing the nanopowders and microrods, the method comprising spinning a spinning solution containing at least one kind of precursor capable of composing at least one kind selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, crystallizing or amorphizing the spun precursor to produce nano fiber containing at least one kind of nanoparticles selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, and milling the nano fiber to fabricate nanopowders containing nanoparticles, nano clusters or
    Type: Application
    Filed: December 23, 2009
    Publication date: July 1, 2010
    Inventors: Il Doo KIM, Seung hun CHOI
  • Publication number: 20100151049
    Abstract: The subject invention concerns methods for preparing alkaline earth ferrates and the preparation of hemostatic compositions from alkaline earth ferrates. In one embodiment, the alkaline earth ferrate is strontium ferrate. In one embodiment, methods of the invention comprise heat treating mixtures of alkaline earth oxides and/or peroxides with iron oxides, such as hematite or magnetite. The subject invention also concerns hemostatic compositions produced using metallic oxides that are reacted with alkaline earth oxides and/or peroxides and the methods used to produce the hemostatic compositions.
    Type: Application
    Filed: November 30, 2009
    Publication date: June 17, 2010
    Applicant: Biolife, LLC
    Inventors: John Alfred Thompson, John Hen
  • Patent number: 7722848
    Abstract: Lithium iron phosphate cathode materials for lithium secondary batteries and methods of preparation thereof are disclosed. Better cathode materials may be produced by multiple annealing and/or heating steps. The annealing step can be carried out before and/or after the heating steps to provide cathode materials, which exhibit superior electrical properties. In some instances, divalent iron compounds are incorporated as starting materials.
    Type: Grant
    Filed: May 27, 2008
    Date of Patent: May 25, 2010
    Assignee: BYD Company Limited
    Inventors: Quan Dai, Julin Shen
  • Patent number: 7722846
    Abstract: Provided is a method for preparing an electroconductive mayenite type compound with good properties readily and stably at low cost. A production method of an electroconductive mayenite type compound comprising a step of subjecting a precursor to heat treatment, is a method for preparing an electroconductive mayenite type compound, comprising a step of subjecting a precursor to heat treatment; wherein the precursor is a vitreous or crystalline material, which contains Ca and Al, in which a molar ratio of (CaO:Al2O3) is from (12.6:6.4) to (11.7:7.3) as calculated as oxides, and in which a total amount of CaO and Al2O3 is at least 50 mol %, and wherein the heat treatment is heat treatment comprising holding the precursor at a heat treatment temperature T of from 600 to 1415° C. and in an inert gas or vacuum atmosphere with an oxygen partial pressure PO2 in a range of PO2?105×exp [{?7.9×l04/(T+273)}+14.4] in the unit of Pa.
    Type: Grant
    Filed: November 30, 2007
    Date of Patent: May 25, 2010
    Assignees: Asahi Glass Company, Limited, Tokyo Institute of Technology
    Inventors: Hideo Hosono, Katsuro Hayashi, Sung Wng Kim, Masahiro Hirano, Satoru Narushima, Setsuro Ito
  • Publication number: 20100119429
    Abstract: Methods of preparing metal oxide nanoparticles are described. The methods involve the thermal decomposition of a metal-carboxylate complex within a continuous, flow-through, tubular reactor. The resulting metal oxide nanoparticles contain iron and can be magnetic, non-agglomerated, crystalline or a combination thereof.
    Type: Application
    Filed: February 28, 2007
    Publication date: May 13, 2010
    Inventors: Sarah M. Mullins, Grant F. Tiefenbruck, Danny B. Anderson
  • Publication number: 20100084269
    Abstract: A NOX sensor material includes a composition of Ba(1-X)AXFe(12-Y)BYO19. Constituent A and constituent B are doping elements. Constituent A is selected from the group consisting of Bi, La and Pb and X is a real number where 0?X<1. Constituent B is selected from the group consisting of Al, B, Bi, Ca, Co, Cr, Cu, Er, Ga, In, Mg, Mn, Ni, Nb, Rh, Pb, Si, Sr, Ti, Ta, Zn and Zr and Y is a real number where 0?Y<12. The NOX sensor material may be used in a sensor element of a NOX sensor.
    Type: Application
    Filed: October 3, 2008
    Publication date: April 8, 2010
    Applicant: Delphi Technologies, Inc.
    Inventors: Da Yu Wang, Sheng Yao, Thomas M. Brunette, Elizabeth Briggs, Raymond L. Bloink, David D. Cabush