Tin, Lead, Or Germanium Containing (e.g., Stannate, Plumbate, Etc.) Patents (Class 423/594.9)
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Patent number: 7901657Abstract: The invention relates to amphiphilic, nanoscalar particles comprising lipophilic hydrolyzable groups on their surface. The invention also relates to methods for producing amphiphilic, nanoscalar particles and to compositions containing said particles.Type: GrantFiled: February 25, 2005Date of Patent: March 8, 2011Assignee: Leibniz-Institut Fuer Neue Materialien Gemeinnuetzige GmbHInventors: Ertugrul Arpac, Helmut Schmidt, Murat Akarsu
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Publication number: 20110042712Abstract: The present disclosure provides a new type of gapless semiconductor material having electronic properties that can be characterized by an electronic band structure which comprises valence and conduction band portions VB1 and CB1, respectively, for a first electron spin polarisation, and valence and conducting band portions VB2 and CB2, respectively, for a second electron spin polarisation. The valence band portion VB1 has a first energy level and one of CB1 and CB2 have a second energy level that are positioned so that gapless electronic transitions are possible between VB1 and the one of CB1 and CB2, and wherein the gapless semiconductor material is arranged so that an energy bandgap is defined between VB2 and the other one of CB1 and CB2.Type: ApplicationFiled: March 12, 2009Publication date: February 24, 2011Inventor: Xiaolin Wang
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Publication number: 20110036269Abstract: Surface-modified agglomerate of indium tin oxohydrate with a proportion of indium of 80 to 98.9% by weight, of tin of 2 to 20% by weight and of carbon of 0.01 to 1% by weight. Process for preparing a surface-modified agglomerate of indium tin oxide, in which the surface-modified agglomerate of indium tin oxohydrate is dried under air at temperatures of more than 150° C. and less than 310° C., and is then calcined under reducing conditions. Surface-modified agglomerate of indium tin oxide obtainable by this process. Process for preparing a surface-modified powder of indium tin oxide and a dispersion thereof, in which the surface-modified agglomerate and one or more solvents are combined to give a mixture, the mixture is converted to a dispersion by means of a dispersing unit and liquid constituents are optionally removed from the dispersion in order to obtain a powder.Type: ApplicationFiled: April 16, 2009Publication date: February 17, 2011Applicant: EVONIK DEGUSSA GmbHInventors: Sven Hill, Willibald Wombacher, Katharina Dauth
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Publication number: 20110015325Abstract: A polymer additive for improving the reheat characteristics of a polymer or polymeric composition comprises an inorganic material which is such that a 2.5 mm thick polyethylene terephthalate plaque incorporating the inorganic material has, when tested, an absorption ratio of less than 0.9, wherein the absorption ratio is either the ratio of A1/A2 or the ratio A1/A3, wherein: A1 is the maximum absorption between 400 nm and 550 nm; A2 is the maximum absorption between 700 to 1100 nm; A3 is the maximum absorption between 700 to 1600 nm. Preferred inorganic materials are titanium nitride, indium tin oxide and lanthanum hexaboride.Type: ApplicationFiled: September 22, 2010Publication date: January 20, 2011Inventors: Anthony Jarvis, Mark Frost, Mark Rule
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Patent number: 7867472Abstract: An insulating target material for obtaining a conductive complex oxide film represented by a general formula ABO3. The insulating target material includes: an oxide of an element A; an oxide of an element B; an oxide of an element X; and at least one of an Si compound and a Ge compound, the element A being at least one element selected from La, Ca, Sr, Mn, Ba, and Re, the element B being at least one element selected from Ti, V, Sr, Cr, Fe, Co, Ni, Cu, Ru, Ir, Pb, and Nd, and the element X being at least one element selected from Nb, Ta, and V.Type: GrantFiled: January 19, 2007Date of Patent: January 11, 2011Assignee: Seiko Epson CorporationInventors: Koji Ohashi, Takeshi Kijima, Setsuya Iwashita
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Patent number: 7867471Abstract: A process of producing a ceramic powder including providing a plurality of precursor materials in solution, wherein each of the plurality of precursor materials in solution further comprises at least one constituent ionic species of a ceramic powder, combining the plurality of precursor materials in solution with an onium dicarboxylate precipitant solution to cause co-precipitation of the ceramic powder precursor in a combined solution; and separating the ceramic powder precursor from the combined solution. The process may further include calcining the ceramic powder precursor.Type: GrantFiled: April 3, 2009Date of Patent: January 11, 2011Assignee: SACHEM, Inc.Inventor: Wilfred Wayne Wilson
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Publication number: 20110002831Abstract: A sol-gel process for preparing a mixture of metal-oxide-metal compounds wherein at least one metal oxide precursor is subjected to a hydrolysis treatment to obtain one or more corresponding metal oxide hydroxides, the metal oxide hydroxides so obtained are subjected to a condensation treatment to form the metal-oxide-metal compounds, which process is carried out in the presence of an encapsulated catalyst, whereby the catalytically active species is released from the encapsulating unit by exposure to an external stimulus, and wherein the catalytically active species released after exposure to such external stimulus is capable of catalyzing the condensation of the metal-hydroxide groups that are present in the metal oxide hydroxides so obtained.Type: ApplicationFiled: December 15, 2008Publication date: January 6, 2011Inventors: Nanning Joerg Arfsten, Pascal Jozef Paul Buskens, Jens Christoph Thies
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Patent number: 7837781Abstract: A pigment of empirical composition (TiO2)a(ZnO)b(SnO)c(SnO2)d(RExOy)e(AEO)f(MuOv)g wherein RE is a metal from transition group 3 or a rare earth metal, AE is an alkaline earth metal, and M is any other metal, where a=0.8-3; b=0.5-1.3; c=0.5-1.3; d=0-0.5; e=0-0.3; f=0-0.3; and g=0-0.1, and e+f?0.01. Preferably RE is selected from the elements Y, La, Ce, and Pr. The pigments are used as colorants for coloring paints, inks, plastics, and rubber.Type: GrantFiled: December 17, 2007Date of Patent: November 23, 2010Assignee: BASF SEInventors: Norbert Mronga, Kirill Bramnik
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Patent number: 7820138Abstract: At least one basic precipitant selected from the group consisting of NaOH, KOH, NH4OH, NH3, NH4HCO3 and (NH4)2CO3 is added to an indium salt solution, which contains 0.1 to 3 M of indium, in an adding time of not longer than 24 hours, while the solution is maintained at a temperature of 5 to 95° C. until the equivalent of the basic precipitant reaches an equivalent of 0.5 to 3. Then, a precipitate obtained from the solution by a solid-liquid separation is dried and calcined at a temperature of 570 to 780° C. in an non-oxidizing atmosphere which contains ammonia gas and water vapor.Type: GrantFiled: March 15, 2006Date of Patent: October 26, 2010Assignee: Dowa Mining Co., Ltd.Inventors: Makoto Watanabe, Tatsumi Inamura, Yoshio Moteki
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Publication number: 20100266787Abstract: An oxide material including indium (In), tin (Sn), and metal element M, and including an ilmenite structure compound; a sputtering target composed thereof; a transparent conductive film formed by using such a sputtering target; and a transparent electrode composed of such a transparent conductive film.Type: ApplicationFiled: September 15, 2006Publication date: October 21, 2010Inventors: Koki Yano, Kazuyoshi Inoue, Nobuo Tanaka, Tokie Tanaka
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Publication number: 20100266485Abstract: A process comprises (a) combining (1) at least one base and (2) at least one metal carboxylate salt comprising (i) a metal cation selected from metal cations that form amphoteric metal oxides or oxyhydroxides and (ii) a lactate or thiolactate anion, or metal carboxylate salt precursors comprising (i) at least one metal salt comprising the metal cation and a non-interfering anion and (ii) lactic or thiolactic acid, a lactate or thiolactate salt of a non-interfering, non-metal cation, or a mixture thereof; and (b) allowing the base and the metal carboxylate salt or metal carboxylate salt precursors to react.Type: ApplicationFiled: December 16, 2008Publication date: October 21, 2010Inventor: Timothy D. Dunbar
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Patent number: 7799312Abstract: A method for manufacturing an indium tin oxide (ITO) target and methods for preparing indium oxide powder (In2O3) and tin oxide powder (SnO2). The method for manufacturing an ITO (indium tin oxide) target includes preparing an In2O3 powder having a surface area of about 10-18 m2/g and an average particle diameter of between about 40 to 80 nm; preparing a SnO2 powder having a surface area of about 8-15 m2/g and an average particle diameter of about 60-100 nm; molding a mixture of the In2O3 powder and the SnO2 powder; and sintering the mixture at atmospheric pressure under oxidation atmosphere. The ITO target is applicable for a high-quality, transparent electrode for a display, such as a liquid crystal display, electroluminescent display, or field emission display.Type: GrantFiled: May 29, 2007Date of Patent: September 21, 2010Assignee: Samsung Corning Precision Glass Co., Ltd.Inventors: Kyong-hwa Song, Sang-cheol Park, Jung-gyu Nam
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Patent number: 7781491Abstract: A process of doping zero-valance double metals into a cationic exchange resin to increase reactive activity of zero-valance metals includes providing a cationic exchange resin to contact a first metal in the form of ions to reduce the first metal which then attaches to the cationic exchange resin; providing a second metal in the form of ions to contact and attach to the first metal; and reducing the second metal to zero valance and forming a carrier containing double metals. The cationic exchange resin is selected from a strong acidic ion exchange resin of which the ion exchange functional group is SO3Na and SO3H. The first metal is selected from the noble metal group: palladium, platinum and copper. The second metal is selected from the normal metals group, such as tin. The first metal and the second metal respectively have particle diameters ranging from 20 to 100 nm.Type: GrantFiled: October 18, 2007Date of Patent: August 24, 2010Inventors: Ya-Hsuan Liou, Shang-Lien Lo, Chin-Jung Lin
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Publication number: 20100189636Abstract: Provided is an amorphous film comprised substantially of indium, tin, magnesium and oxygen, and containing tin at a ratio of 5 to 15% based on an atomicity ratio of Sn/(In+Sn+Mg) and magnesium at a ratio of 0.1 to 2.0% based on an atomicity ratio of Mg/(In+Sn+Mg) with remnant being indium and oxygen, and having a film resistivity of 0.4 m?cm or less as a result of crystallizing the film by annealing the film at a temperature of 260° C. or lower. An amorphous ITO thin film for use as a display electrode and the like in flat panel displays is obtained by way of sputter deposition without heating the substrate and without the need of adding water during the deposition. This amorphous ITO film has the property of being crystallized by annealing at 260° C. or lower, which is not such a high temperature, and having low resistivity after crystallization. Also provided are a method of producing the film and a sintered compact for producing the film.Type: ApplicationFiled: June 13, 2008Publication date: July 29, 2010Applicant: NIPPON MINING & METALS CO., LTD.Inventors: Masakatsu Ikisawa, Masataka Yahagi
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Patent number: 7759006Abstract: Disclosed is a compound represented by the following formula 1. A lithium secondary battery using the same compound as electrode active material, preferably as cathode active material, is also disclosed. LiMP1-xAxO4??[Formula 1] wherein M is a transition metal, A is an element having an oxidation number of +4 or less and 0<x<1. The electrode active material comprising a compound represented by the formula of LiMP1-xAxO4 shows excellent conductivity and charge/discharge capacity compared to LiMPO4.Type: GrantFiled: July 14, 2005Date of Patent: July 20, 2010Assignee: LG Chem, Ltd.Inventors: Sung Kyun Chang, Jeong Ju Cho
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Publication number: 20100135937Abstract: Nanocrystalline forms of metal oxides, including binary metal oxide, perovskite type metal oxides, and complex metal oxides, including doped metal oxides, are provided. Methods of preparation of the nanocrystals are also provided. The nanocrystals, including uncapped and uncoated metal oxide nanocrystals, can be dispersed in a liquid to provide dispersions that are stable and do not precipitate over a period of time ranging from hours to months. Methods of preparation of the dispersions, and methods of use of the dispersions in forming films, are likewise provided. The films can include an organic, inorganic, or mixed organic/inorganic matrix. The films can be substantially free of all organic materials. The films can be used as coatings, or can be used as dielectric layers in a variety of electronics applications, for example as a dielectric material for an ultracapacitor, which can include a mesoporous material. Or the films can be used as a high-K dielectric in organic field-effect transistors.Type: ApplicationFiled: September 24, 2009Publication date: June 3, 2010Applicant: The Trustees of Columbia University in the City of New YorkInventors: Stephen O'Brien, Limin Huang, Zhuoying Chen, Ioannis Kymissis, Zhang Jia
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Publication number: 20100111803Abstract: Disclosed herein is a spinel article. The article comprises a spinel material, wherein the spinel material has a monomodal grain size distribution with average grain sizes of less than or equal to about 15 micrometers, and a biaxial flexural strength of greater than or equal to about 300 megapascals when measured by a ring-on-ring flexural test as per ASTM Standard C1499-08. Disclosed herein too is a spinel article manufactured by a method comprising calcining a spinel powder; milling the powder in a milling medium; granulating the powder; screening the powder to a mesh size of about 40 to about 200 mesh; pressing the powder to form an article; burning out organics from the article; sintering the article; and hot isostatically pressing the article.Type: ApplicationFiled: November 6, 2008Publication date: May 6, 2010Applicant: GENERAL ELECTRIC COMPANYInventors: Milivoj Konstantin Brun, Anteneh Kebbede, Sean Michael Sweeney, Timothy James Yosenick
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Patent number: 7700067Abstract: A crystallographically-oriented ceramic including first regions, in which crystal nuclei remain and which contain a specific element in a predetermined concentration range and extend at least partially in a layered shape along a crystal plane, and second regions, which contain the specific element in a different concentration range from the first regions and extend at least partially in a layered shape along the crystal plane. The regions are alternately repeated, and a compositional distribution exists in a direction orthogonal to the crystal plane. In the first region, the concentration of Na is higher, the concentration of K is lower, the concentration of Nb is lower, and the concentration of Ta is higher than the second region, and in the second region, the concentration of Na is lower, the concentration of K is higher, the concentration of Nb is higher, and the concentration of Ta is lower than the first region.Type: GrantFiled: February 22, 2008Date of Patent: April 20, 2010Assignee: NGK Insulators, Ltd.Inventors: Shohei Yokoyama, Nobuyuki Kobayashi, Tsutomu Nanataki
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Patent number: 7691352Abstract: A new set of additives to be sued in the preparation of inorganic materials; especially of perovskite nature is proposed. The chemical compositions of the perovskites prepared in the presence of the mentioned additives are found to be more homogenous, leading to better catalytic behavior, including higher selectivity and yields as compared to catalysts of identical formulations prepared through the conventional method of using EDTA/citrate (or other organic additive) method.Type: GrantFiled: April 2, 2009Date of Patent: April 6, 2010Assignee: Research Institute of Petroleum Industry (RIPI)Inventors: Khodadad Nazari, Zahra Taheri, Naser Seyed Matin, Reza Ahmadi, Saeed Zarrinpashneh, Morteza Rezapour
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Patent number: 7670585Abstract: Provided is a method for preparing an electroconductive mayenite type compound with good properties readily and stably at low cost without need for expensive facilities, a reaction at high temperature and for a long period of time, or complicated control of reaction. A method for preparing an electroconductive mayenite type compound comprises a step of subjecting a precursor to heat treatment, wherein the precursor contains Ca and/or Sr, and Al, a molar ratio of (a total of CaO and SrO:Al2O3) is from (12.6:6.4) to (11.7:7.3) as calculated as oxides, a total content of CaO, SrO and Al2O3 in the precursor is at least 50 mol %, and the precursor is a vitreous or crystalline material; and the method comprises a step of mixing the precursor with a reducing agent and performing the heat treatment of holding the mixture at 600-1,415° C. in an inert gas or vacuum atmosphere with an oxygen partial pressure of at most 10 Pa.Type: GrantFiled: November 30, 2007Date of Patent: March 2, 2010Assignees: Asahi Glass Company, Limited, Tokyo Institute of TechnologyInventors: Hideo Hosono, Katsuro Hayashi, Sung Wng Kim, Masahiro Hirano, Satoru Narushima, Setsuro Ito
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Patent number: 7632477Abstract: This invention relates to a process for preparing zirconium oxide, in its various forms, including zirconium-based mixed oxides. There is described a process for preparing a zirconium oxide in the absence of a cerium salt which comprises precipitating a zirconium hydroxide from an aqueous solution of a zirconium salt by reaction with an alkali in the presence of a controlled amount of sulphate anions at a temperature not greater than 50° C. and then calcining the hydroxide to form an oxide, wherein the oxide thus formed is essentially sulphate free. Catalysts and ceramics can be produced from the product oxides having improved thermal stability and improved sinterability, respectively. A particular use of the product oxide is as a promoter or catalyst support in automobile exhaust systems.Type: GrantFiled: April 29, 2004Date of Patent: December 15, 2009Assignee: Magnesium Elektron, Ltd.Inventors: Yasuhide Takao, Colin Norman, Gavin Edwards, Ian Chisem, Clare Jones
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Publication number: 20090272437Abstract: A photovoltaic cell can include a transparent conductive layer including cadmium stannate.Type: ApplicationFiled: May 1, 2009Publication date: November 5, 2009Applicant: First Solar, Inc.Inventors: Dale Roberts, John German, Keith J. Burrows, Benyamin Buller, Boil Pashmakov
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Patent number: 7601661Abstract: The invention provides an indium oxide-tin oxide powder which can be produced at low cost and which can provide a high-density sputtering target having a prolonged target life, and a sputtering target employing the powder. The indium oxide-tin oxide powder containing an In—Sn oxide as a predominant component is characterized in that the oxide powder contains no compound oxide (In4Sn3O12) detectable through X-ray diffraction and has a SnO2 solid solution amount in In2O3 of 2.3 mass % or more, the SnO2 solid solution amount being calculated from the precipitated SnO2 content (mass %) obtained from the ratio between integral diffraction intensity attributed to In2O3 (222) and integral diffraction intensity attributed to SnO2 (110).Type: GrantFiled: December 24, 2004Date of Patent: October 13, 2009Assignee: Mitsui Mining & Smelting Co., Ltd.Inventors: Seiichiro Takahashi, Hiroshi Watanabe
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Patent number: 7582276Abstract: The invention relates to nanoscale rutile or oxide powder that is obtained by producing amorphous TiO2 by mixing an alcoholic solution with a titanium alcoholate and with an aluminum alcohalate and adding water and acid. The amorphous, aluminum-containing TiO2 is isolated by removing the solvent, and is redispersed in water in the presence of a tin salt. Thermal or hydrothermal post-processing yields rutile or oxide that can be redispersed to primary particle size. The n-rutile or the obtained oxide having a primary particle size ranging between 5 and 20 nm can be incorporated into all organic matrices so that they remain transparent. Photocatalytic activity is suppressed by lattice doping with trivalent ions. If the amorphous precursor is redispersed in alcohol, or not isolated, but immediately crystallized, an anatase is obtained that can be redispersed to primary particle size.Type: GrantFiled: August 30, 2002Date of Patent: September 1, 2009Assignee: ITN Nanovation AGInventor: Ralph Nonninger
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Patent number: 7582222Abstract: An oxide semiconductor doped with a transition metal and exhibiting room-temperature ferromagnetism is disclosed. The transition metal-doped oxide semiconductor is preferably manufactured in powder form, and the transition metal is preferably evenly distributed throughout the oxide semiconductor. The preferred embodiments are iron-doped tin dioxide and cobalt-doped tin dioxide. Gases may be detected by passing them across a material and measuring the change in magnetic properties of the material; the preferred material is iron-doped tin dioxide.Type: GrantFiled: August 1, 2005Date of Patent: September 1, 2009Assignee: Boise State UniversityInventor: Alex Punnoose
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Patent number: 7578455Abstract: A particulate material is ground more efficiently using a mixture of at least two different sizes of yttrium-stabilized zirconia balls. The method facilitates preparation of photocatalysts with high activity.Type: GrantFiled: August 9, 2004Date of Patent: August 25, 2009Assignee: General Motors CorporationInventors: Jin D. Kim, Wei Li, Se H. Oh
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Publication number: 20090208404Abstract: An alloy generating hydrogen easily and safely for a long time is obtained. The alloy is obtained by melting in a blast furnace a first metal composed of one or more metals of Al, Zn and Mg and a second metal composed of one or more metals of Ga, Cd, In, Sn, Sb, Hg, Pb and Bi; and then placing the alloy in a molten state in water to cool the alloy.Type: ApplicationFiled: June 15, 2007Publication date: August 20, 2009Applicants: CENTRAL GLASS COMPANY, LIMITEDInventor: Isao Itoh
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Publication number: 20090185971Abstract: A crystallographically-oriented ceramic including first regions, in which crystal nuclei remain and which contain a specific element in a predetermined concentration range and extend at least partially in a layered shape along a crystal plane, and second regions, which contain the specific element in a different concentration range from the first regions and extend at least partially in a layered shape along the crystal plane. The regions are alternately repeated, and a compositional distribution exists in a direction orthogonal to the crystal plane. In the first region, the concentration of Na is higher, the concentration of K is lower, the concentration of Nb is lower, and the concentration of Ta is higher than the second region, and in the second region, the concentration of Na is lower, the concentration of K is higher, the concentration of Nb is higher, and the concentration of Ta is lower than the first region.Type: ApplicationFiled: February 22, 2008Publication date: July 23, 2009Applicant: NGK Insulators, Ltd.Inventors: Shohei Yokoyama, Nobuyuki Kobayashi, Tsutomu Nanataki
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Publication number: 20090185412Abstract: A phase-change material and a memory unit using the phase-change material are provided. The phase-change material is in a single crystalline state and includes a compound of a metal oxide or nitroxide, wherein the metal is at least one selected from a group consisting of indium, gallium and germanium. The memory unit includes a substrate; at least a first contact electrode formed on the substrate; a dielectric layer disposed on the substrate and formed with an opening for a layer of the phase-change material to be formed therein; and at least a second contact electrode disposed on the dielectric layer. As the phase-change material is in a single crystalline state and of a great discrepancy between high and low resistance states, the memory unit using the phase-changed material can achieve a phase-change characteristic rapidly by pulse voltage and avert any incomplete reset while with a low critical power.Type: ApplicationFiled: July 30, 2008Publication date: July 23, 2009Applicant: NATIONAL TAIWAN UNIVERSITYInventors: Lung-Han Peng, Sung-Li Wang, Meng-Kuei Hsieh, Chien-Yu Chen
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Publication number: 20090136757Abstract: A method of fractionating a dispersion of oxidic nanoparticles wherein at least one step of the method is a membrane crossflow filtration step, the flow of the dispersion over the membrane being brought about by means of driven rotating parts; and dispersions of oxidic nanoparticles that are obtainable by the method.Type: ApplicationFiled: November 14, 2008Publication date: May 28, 2009Applicant: EVONIK DEGUSSA GmbHInventors: Roland WURSCHE, Goetz Baumgarten, Wolfgang Lortz, Michael Kroell
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Patent number: 7534528Abstract: An electrode material for an anode of a rechargeable lithium battery, containing a particulate comprising an amorphous Sn.A.X alloy with a substantially non-stoichiometric ratio composition. For said formula Sn.A.X , A indicates at least one kind of an element selected from a group consisting of transition metal elements, X indicates at least one kind of an element selected from a group consisting of O, F, N, Mg, Ba, Sr, Ca, La, Ce, Si, Ge, C, P, B, Pb, Bi, Sb, Al, Ga, In, Tl, Zn, Be, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, As, Se, Te, Li and S, where the element X is not always necessary to be contained. The content of the constituent element Sn of the amorphous Sn.A.X alloy is Sn/(Sn+A+X)=20 to 80 atomic %.Type: GrantFiled: October 10, 2006Date of Patent: May 19, 2009Assignee: Canon Kabushiki KaishaInventors: Soichiro Kawakami, Masaya Asao
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Patent number: 7510693Abstract: Process for the production of a metal oxide powder having a BET surface area of at least 20 m2/g by reacting an aerosol with oxygen in a reaction space at a reaction temperature of more than 700° C. and then separating the resulting powder from gaseous substances in the reaction space, wherein the aerosol is obtained by atomisation using a multi-component nozzle of at least one starting material, as such in liquid form or in solution, and at least one atomising gas, the volume-related mean drop diameter D30 of the aerosol is from 30 to 100 ?m and the number of aerosol drops larger than 100 ?m is up to 10%, based on the total number of drops, and metal oxide powder obtainable by this process.Type: GrantFiled: January 30, 2006Date of Patent: March 31, 2009Assignee: Degussa AGInventors: Stipan Katusic, Michael Kraemer, Michael Kroell, Peter Kress, Edwin Staab
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Patent number: 7504351Abstract: Provided are an ITO sputtering target wherein the number of particles having a grain diameter of 100 nm or greater exposed in the ITO sputtering target as a result of royal water etching or sputter etching is 1 particle/?m2, and an ITO sputtering target having a density of 7.12 g/cm3 or greater capable of improving the sputtering performance, in particular inhibiting the generation of arcing, suppressing the generation of defects in the ITO film caused by such arcing, and thereby effectively inhibiting the deterioration of the ITO film.Type: GrantFiled: August 4, 2004Date of Patent: March 17, 2009Assignee: Nippon Mining & Metals Co., Ltd.Inventor: Toshiya Kurihara
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Publication number: 20080299035Abstract: A method for recycling a used sputtering target is provided, including the steps of: (1) cleaning, (2) pulverization, (3) dissolution, (4) filtering, (5) peptization, (6) neutralization and precipitation, (7) rinsing and filtering, (8) drying, and (9) calcination; through the steps above, which can then be recycling used sputtering target to recover the constituent components of the ITO targets.Type: ApplicationFiled: May 30, 2007Publication date: December 4, 2008Inventors: Hsin-Chun Lu, Chih-Ming Hsieh, Yi-Chieh Chen, Cherng-Yuan Shiao, Kuo-Shu Hsu, Nai-Sheng Syu
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Patent number: 7449235Abstract: An aqueous alkaline solution containing a tin salt dissolved therein is mixed with a zinc compound, and an aqueous solution of an indium salt is added to the mixture. The resultant hydroxide or hydrate containing tin, indium and zinc is treated by heating at a temperature of 110 to 300° C. in the present of water. Then, the resultant product is filtered, dried and treated by heating at a temperature of 300 to 1,000° C. in an air and further reduced at a temperature of 150 to 400° C. under a reducing atmosphere to obtain composite indium oxide particles of zinc oxide and tin-containing indium oxide, which have an average particle size of 5 to 100 nm. The resultant composite particles of zinc oxide and tin-containing indium oxide are suitably used to form a transparent conductive coating film having a UV-shielding effect.Type: GrantFiled: March 31, 2004Date of Patent: November 11, 2008Assignee: Hitachi Maxell, Ltd.Inventors: Yuko Sawaki, Mikio Kishimoto
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Publication number: 20080272682Abstract: The invention relates to a discharge lamp having a thin film indium oxide coating on the interior lamp envelope surface that effectively reflects UV, near IR and microwave radiation while transmitting light in the visible spectrum, the lamp being a high temperature operating lamp.Type: ApplicationFiled: May 1, 2007Publication date: November 6, 2008Inventors: Deeder Aurongzeb, Philip Ellis
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Patent number: 7442668Abstract: An object is to provide a sulfated tin oxide catalyst with strong catalytic activity, and a method for preparation thereof. It was discovered that in the preparation of a solid acid catalyst containing tin, stronger solid acid properties than before could be achieved by preparing a support comprising a crystalline tin oxide, preferably metastannic acid, bringing this support into contact with organic acid ions, then bringing it into contact with a sulfate group-containing compound, and then calcining it. The solid acid catalyst of the present invention has a tin content of 30% or more by weight as metal in the catalyst, a sulfate group supported thereon and an argon adsorption heat of more than 30 kJ/mol, and is used in acid-catalytic reactions.Type: GrantFiled: April 21, 2004Date of Patent: October 28, 2008Assignee: Japan Energy CorporationInventor: Satoshi Furuta
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Publication number: 20080260622Abstract: A method of preparing indium tin oxide (ITO) and such an oxide per se are described. The method utilises a cryogenic process wherein an aqueous formulation of indium sulphate, ammonium sulphate and a tin compound, optionally in the presence of an organic polymer, are frozen to produce a solid; the solid is conditioned by heating it to cause crystallisation of water in the solid; the water is removed for example by freeze drying; and the solid is then calcined. The ITO produced may have a surface tin concentration of less than 2 and other desirable properties.Type: ApplicationFiled: May 24, 2005Publication date: October 23, 2008Applicant: Imperial Chemical Industries PicInventor: Derek A. Graham
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Publication number: 20080233033Abstract: This invention relates to a Polyoxometalate (POM) represented by the formula: (An)m+[HqM16X8W48O184(OH)32]m? or solvates thereof, wherein: A represents a cation, n is the number of the cations A, m is the charge of the polyoxoanion, q is the number of protons and varies from 0 to 12, M represents a transition metal, and X represents a heteroatom selected from P, As and mixtures thereof. This invention also relates to a process to produce such POMs and to a process for the homogeneous or heterogeneous oxidation of organic substrates comprising contacting the organic substrate with such POMs.Type: ApplicationFiled: March 23, 2007Publication date: September 25, 2008Inventors: Ulrich Kortz, Sib Sankar Mal
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Publication number: 20080226528Abstract: The product of a molten alkali metal metalate phase separation can be processed into a purified metal from a metal source. Metal sources include native ores, recycled metal, metal alloys, impure metal stock, recycle materials, etc. The method uses a molten alkali metal metalate as a process medium or solvent in purifying or extracting high value metal or metal oxides from metal sources. Vitrification methods using the silicate glass separation phase can be prepared as is or can be prepared with a particulate phase distributed throughout the silica glass phase and encapsulated and fixed within the continuous glass phase. Tungsten metal can be obtained from an alkali metal tungstate. A typically finely divided tungsten metal powder can be obtained from a variety of tungsten sources including recycled tungsten scrap, tungsten carbide scrap, low grade tungsten ore typically comprising tungsten oxide or other form of tungsten in a variety of oxidation states.Type: ApplicationFiled: December 7, 2007Publication date: September 18, 2008Inventor: RODNEY KIETH WILLIAMS
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Publication number: 20080210902Abstract: Lattice doped stoichiometric-nanostructured materials having a plurality of discrete nanocrystalline particles, which are at least 95% crystalline, and a dopant either substituted in at least one nanocrystalline particle crystal lattice or interstitially located between crystal lattices or crystal planes of the nanocrystalline particles.Type: ApplicationFiled: July 12, 2007Publication date: September 4, 2008Applicant: NANOPHASE TECHNOLOGIES CORPORATIONInventors: Dan Coy, Harry Sarkas, Robert Haines
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Publication number: 20080163994Abstract: The present invention relates to a security feature for security papers, value documents and the like having an acid-labile feature substance as the core and a shell consisting substantially of metal oxide, the security feature exhibiting greater stability against the action of acids compared with the acid-labile feature substance.Type: ApplicationFiled: December 15, 2005Publication date: July 10, 2008Inventors: Rainer Hoppe, Thomas Giering
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Publication number: 20080166289Abstract: Surface-modified indium-tin oxides are produced by mixing the oxides with the surface-modifying agent in liquid or vapour form and heat treating the mixture. They can be used to produce coating systems.Type: ApplicationFiled: October 29, 2005Publication date: July 10, 2008Applicant: DEGUSSA AGInventors: Jürgen Meyer, Günther Michael
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Publication number: 20080124265Abstract: An anode in a Direct Carbon Fuel Cell (DCFC) operating in a temperature range between 500 and 1200 degrees Celsius is provided. The anode material has high catalytic activity and selectivity for carbon oxidation, sufficient oxygen non-stoichiometry, rapid oxygen chemical diffusion, wide thermodynamic stability window to withstand reducing environment, sufficient electronic conductivity and tolerance to sulfur and CO2 environments. The anode has doped ruthenate compositions A1?xA?xRuO3, AB1?yRuyO3, or A1?xA?xB1?yRuyO3. A and A? may be divalent, trivalent, or tetravalent cation, and B is a multivalent cation. A is among lanthanide series elements La, Ce, Pr, Nd, Sm, Eu, Gd, Dy, Er or Yb, and dopant A? is from Group IIA, IIIB, or IVB elements. The doped ruthenates can also be a (AB1?yRuyO3) structure or an ordered Ruddlesden-Popper series ((A1?xAx?)n+1(B1?yRuy)nO3n+1) structure where n=1 or 2. The dopant B is among Group IVB, VB, VIB, VIII, IB, and IIB elements.Type: ApplicationFiled: October 16, 2007Publication date: May 29, 2008Inventor: Turgut M. Gur
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Patent number: 7357910Abstract: Method for producing metal oxide nanoparticles. The method includes generating an aerosol of solid metallic microparticles, generating plasma with a plasma hot zone at a temperature sufficiently high to vaporize the microparticles into metal vapor, and directing the aerosol into the hot zone of the plasma. The microparticles vaporize in the hot zone into metal vapor. The metal vapor is directed away from the hot zone and into the cooler plasma afterglow where it oxidizes, cools and condenses to form solid metal oxide nanoparticles.Type: GrantFiled: July 15, 2002Date of Patent: April 15, 2008Assignee: Los Alamos National Security, LLCInventors: Jonathan Phillips, Daniel Mendoza, Chun-Ku Chen
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Patent number: 7354565Abstract: The present invention discloses a relaxor material lead iron tungstate which has been synthesized in doped and undoped conditions by single and two step heat treatment. The relaxor material is seen to exhibit almost negligible hysteresis and a transducer made thereby shows pressure measurement capability over a wide range from 0.5 MPa to 415 MPa with accuracy of ±0.05%.Type: GrantFiled: December 16, 2002Date of Patent: April 8, 2008Assignees: Council of Scientific & Industrial Research, Indian Institute of Technology - DelhiInventors: Kamlesh Kumar Jain, Vinay Kumar, Subhash Chand Kashyap
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Patent number: 7338647Abstract: The present invention relates to a method for preparing an electroactive metal polyanion or a mixed metal polyanion comprising forming a slurry comprising a polymeric material, a solvent, a polyanion source or alkali metal polyanion source and at least one metal ion source; heating said slurry at a temperature and for a time sufficient to remove the solvent and form an essentially dried mixture; and heating said mixture at a temperature and for a time sufficient to produce an electroactive metal polyanion or electroactive mixed metal polyanion.Type: GrantFiled: May 20, 2004Date of Patent: March 4, 2008Assignee: Valence Technology, Inc.Inventors: Biying Huang, Jeffrey Swoyer, M. Yazid Saidi, Haitao Huang
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Publication number: 20080020236Abstract: Provided are an alkaline earth metal silicate-based phosphor which is a compound represented by Formula 1 below, and a white light-emitting device (LED) including the same. (M11-x-yAxBy)aMgbM2cOdZeFormula 1 wherein, M1 is one selected from the group consisting of Ba, Ca, and Sr; M2 is at least one selected from Si or Ge; A and B are each independently one selected from the group consisting of Eu, Ce, Mn, Pr, Nd, Sm, Gd, Tb, Dy, Ho, Er, Tm, Yb, Bi, Sn, and Sb; Z is at least one selected from the group consisting of a monovalent or divalent element, H, and N; and 0<x<1, 0?y?1, 6.3<a<7.7, 0.9<b<1.1, 3.6<c<4.4, 14.4<d<17.6, 14.4<d+e<17.6, and 0?e?0.18. The alkaline earth metal silicate-based phosphor has a broad excitation wavelength range, and thus, both a UV-LED and a blue LED can be used as excitation sources for white LEDs.Type: ApplicationFiled: March 19, 2007Publication date: January 24, 2008Applicant: SAMSUNG ELECTRONICS CO., LTD.Inventors: Kubota Shunichi, Young-sic KIM, Seoung-jae IM
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Publication number: 20080003161Abstract: A method of manufacturing a complex metal oxide powder, the method including: preparing a raw material composition for forming a complex metal oxide; mixing an oxidizing solution including an oxidizing substance into the raw material composition to produce complex metal oxide particles to obtain a liquid dispersion of the particles; and separating the particles from the liquid dispersion to obtain a complex metal oxide powder. The complex metal oxide is shown by a general formula AB1-xCxO3, an element A including at least Pb, an element B including at least one of Zr, Ti, V, W, and Hf, and an element C including at least one of Nb and Ta.Type: ApplicationFiled: June 26, 2007Publication date: January 3, 2008Inventors: Takeshi Kijima, Hidemichi Furihata, Setsuya Iwashita, Satoshi Kimura, Toshihiko Kaneda
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Patent number: 7297322Abstract: A process for producing powders of metal compound containing oxygen including the steps of: feeding at least one material selected from a liquid material and a solution material obtained by dissolving solid ingredient in organic solvent via a liquid flow controller into a vaporizer; vaporizing the materials in the vaporizer; adding oxygen; heating; cooling; and crystallizing. Also disclosed is the product formed by this process, and apparatus used in performing the process. The process and the apparatus enable easily mass-producing fine powders of metal compound containing oxygen used as materials for optical crystals, nonlinear crystals or magneto-optical crystals with reasonable production cost.Type: GrantFiled: March 11, 2005Date of Patent: November 20, 2007Assignee: Japan Pionics Co., Ltd.Inventors: Yukichi Takamatsu, Koji Kiriyama, Akira Asano, Takafumi Ishii